View Document Here - Hanford Site

Quanterra Incorporated 

13715 Rider Trail North 

Earth Citv, Missouri 63045 

314 298-8566 Telephone 

314 298-8757 Fax 

Bechtel Hanford Incorporated 

3350 George Washington Way 

Richland, Washington 99352 

April 21, 1998 

Attention: Joan Kessner 

Project Number 

Date Received by Lab 

Number of Samples 

Sample Type 

SDG Number 

Data Deliverable 

I. Introduction 

CASE NARRATIVE 

^$9501112 >b 

do, 

ti 

Environmental 

Services 

0(14.`332 

^' R ^ ^^ ^ p 

PR 1993 ^ 

RECEIVED i 

550.260"—^ 

March 09, 10, 11, 12, 13 and 16, 1998 

Fifteen (15) 

Other Solid 

W02275 

Summary 

le Ab 

" OL 6 19 L95^ 

Between March 9 and 16, 1998, a total of fifteen (15) other solid samples were received by 

Quanterra, Richland and was transferred to Quanterra, St. Louis for chemical analyses. Upon 

receipt, the samples were given the following laborato ry ID numbers to correspond with the 

specific client IDs: 

The samples were filtered to separate the liquid phase from the solid phase. The solid phase 

sample IDs are listed below: 

St. Louis ID BHI ID Richland ID Matrix Date Receipt of 

17199-001 

BON680 80316001 Solid 09-MAR-98 

17199-002 BON681 80316002 Solid 09-MAR-98 

17200-001 BON685 80320501 Solid 11-MAR-98 

17200-002 BON686 80320502 Solid 11-MAR-98 

17200-003 BON687 80320503 Solid 11-MAR-98 

17202-001 BON682 80318301 Solid 10-MAR-98 

17202-002 BON683 80318302 Solid 10-MAR-98 

17202-003 BON684 80318303 Solid 10-MAR-98 

17203-001 BON688 80322101 Solid 12-MAR-98 

17203-002 BON689 80322102 Solid 12-MAR-98 

17221-001 BON690 80324301 Solid 13-MAR-98 

17221-002 BON691 80324302 Solid 13-MAR-98 

17224-001 BON692 80327101 Solid 16-MAR-98 

17224-002 BON693 80327102 Solid 16-MAR-98 

17224-003 BON694 80327103 Solid 16-MAR-98 

o0006'L


April 21, 1998 

Project Number: 550.260 

SDG: W02275 

Page 2 

imbanterra 

Emironmental 

Services 

The liquid phase of the samples were placed in containers and put on hold for the following 

sample IDs: 

St. LouisID BHI ID Richland ID Matrix Date of Receipt 

17199-003 BON681 FILTRATE 80316002 Liquid 09-MAR-98 





1I. Analytical Results/ Methodology 

The analytical results for this report are presented by analytical test. Each set of data includes 

sample identification information, analytical results and the appropriate detection limits. 

Analyses requested 

PCBs (Aroelor-1254) by EPA 8080. ICP-Trace Metals (Lead) by EPA Method 6010. Mercury 

by EPA Method 7471. 

III. Quality Control 

A Laboratory Control Sample and Method Blank were analyzed with each preparation batch 

MatrixSpike and Matrix Spike Duplicate analyses were performed per the protocol for each 

analyte in this SDG. 

IV. Definitions 

The following codes were used to denote laboratory quality control samples and can he found in 

the data summary secti-)n of this report: 

QCBLK- Quality Control Blank, Method Blank 

QCLCS- Quality Control Laborator y Control Sample. Blank Spike 

V. Comments 

0 000 63


April 21. 1998 

Project Number: 550.260 

SDG: W02275 

Page 3 

f,mbanterra 

Environmental 

Som, e, 

Shipping and Receiving 

There are no comments or nonconformances associated with the shipping and receivin g of these 

samples. 

Wet Chemistry 

Percent Moisture analyses for the solid phase samples were requested after the priority results 

were reported. A Percent Moisture report was transmitted by facsimile on April 13, 1998. 

PCBs 

There are no comments or nonconformances associated with this analysis. 

Metals 

Percent solids was not determined for the samples in SDG W02275. Due to software 

configuration, the CLP forms list solid sample result units as " dry weight" and `7 solids as " 

100 ". The results on the forms are actually mg/Kg as is and are not corrected for percent 

solids. The figure of 100 was used as percent solids for calculation purposes only and does not 

represent measured solids content of the samples. 

The percent difference for the Lead serial dilution (12.9) was greater than 10. therefore all 

associated data was flagged with a "E". 

I certify that this data package is in compliance %vith the SOW. hoth technically and for 

completeness, for other than the conditions detailed above. Release of the data contained in this 

hard copy data package has been authorized by the Laboratory Manager or a designee. as 

verified by the following signature. 

Reviewed and approved: 

Robert E. White 

Project Manager 

000-00y

Control #: B98-043 

Sample Disposition Record Revisionu: O 

Section 1 - BACKGROUND 

SAF#: B98-061 

OU: N/A 

Project ID: 105-C Reactor 

Task ID: 9 

Sampling Event: 105-C Phase I & Phase If 

Laboratory: Quanterra Incorporated 

Project Coordinator: WEISS, RL 

Task Manager: ARMATROUT. JF 

Section 2 - SAMPLE INFORMATION 

Number of Samples: 15 

Date Initiated: 3/17/98 

ID Numbers: BON680, BON681, BON683, BON684, BON686, BON687, BON688. BON691, BON692, BON693. BON694, 

BON682, BON685, BON689, BON690 

MATRIX: 

Collection Date: 

Section 3 - ISSUE 

N/A 

Class: Lab Direction 

NCR Number: N/A 

Type: Multiple Phase Sample 

Description: Concrete samples were wet ground in the field. The procedure resulted in too much liquid for analysis of the 

samples as a single phase 

NCR Validation (Print/Sign) Date 

Section 4 - DISPOSITION 

Type: Use As Is 

Description: For all samples, separate liquid from solid phase and analvze liquid for CrVI. For the following, assign new 

sample numbers as shown to liquids and analvze liquid for all other consitituents identified for solid. 

BON680(solid) to BON894 (liquid), BON683(solid) to BON895(liquid ). BON686(solid) to BON896(liquid), 

BON68 (solid) 

to BON897(liquid), BON692(solid) to BON898(liquid) 

ol L ' 

Project Coordinator (^^PnL""Sign) Date 

ARMATROUT, JF 

Task Manager (Print/Sign Date 

N/A 

QA (Print/Sign) Date 

Section 5 - INSPECTION (Issue Class: Nonconformance Onlvl 

N/A 

Inspection Number: N/A 

Inspection Results: N/A 

Inspector (Print/Sign) Date

Ouanterra April 13, 1998 10:47 am 

Account: 10722 Project: 550.260 Ouanterra-Richland OAS No. 550.26 Rev. 

Master Sample Login: 17199 

Project Manager: N. Price 

Draft: final: Entered and Reviewed by: 

{,M^ 

L^J ^{-^ PM Review: 

Sample Header Template: 

WO 22 75IAJC 2P,6 

y 

2 ,^^fy 

Sample No. Client ID C-Matrix Date: Collected Received Due Shipper Rad Category Red Semple ND. 

Comments 

# Container Type Analysis Class Preservative AnaL. Due Date Hold Date Site (Container Numbers:% Filled) 

Data: 

17199-001 BON680 Solid 09- 14AR-98 10:30 09-MAR-98 13:42 27-MAR-98 AIRBORNE 3 

RICHLAND I.D. 80316001///ICAPT = PS ONLY. 

1 PH - Plastic-250m1 HG/7471/04 S COLD 23-MAR-98 06-APR-98 R58 

1 ICAPT/6010/04 S COLD 23-MAR-98 05-SEP-98 R5 11 

1 PCB/8080/04 S COLD 23-MAR-98 23-MAR-98 R58 

1 PM/17/04 S COLD 23-MAR-98 05-SEP-98 R58 

17199-002 DON681 Solid 09-MAR-98 13:45 09-MAR-98 15:15 27-MAR-98 AIRBORNE 1 

RICHLAND I.D. 80316002///ICAPT = PB ONLY. 

1 PN - Ptastic-250mL HG/7471/04 S COLD 23-MAR-9B 06-APR-98 R5B 

1 ICAPT/6010/04 S COLD 23-MAR-98 05-SEP-98 R5B 

2 PCB/8080/04 S COLD 23-MAR-98 23-MAR-98 R5 1; 

1 PM 1 IT/04 S COLD 23-MAR-98 05-SEP-98 R56 

17199-003 SON681 FILTRATE Liquid 09-MAR-98 13:45 09-MAR-98 15:15 27-MAR-98 AIRBORNE 1 

RICHLAND I.D. 80316002///ICAPT = PB ONLY. 

1 PM - PlastiC-1 1- HOLD//04 S COLD 23-MAR-98 19-MAR-98 R5B 

17199-004 SON894 Liquid 09-MAR-98 10:30 09-MAR-98 12:15 27-MAR-98 AIRBORNE 1 

RICHLAND I.D. 80321501///ICAPT = PB ONLYWUSE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17199-001. 

1 PH - Plastic-1 1- HG/7470/04 S COLD 23-MAR-98 06-APR-98 EMPTY 

1 ICAPT/6010/04 S COLD 23-MAR-98 05-SEP-98 EMPTY 

1 PCB/8080/04 S COLD 23-MAR-98 16-MAR-98 EMPTY 

O C 

3- =Sample has not been rad screened. 

R7045-001 tv 8 -2 2 -7` 

(364122:20) J 

Page 1 

(364122:20) 

(364123:21) 

(364122:20) 

Screening not Required 

(364312:2D) 

(364312:20) 

(364313:21 364323:22) 

(364312:20) 

(364316:99) 


Screening not Required- 

(364317;99) (J 

(364317:99) 

(364317:99) 

'fJ

Chain of 

Custody Record 

QUA 4124 0797 

Client 

gS^ 7 e p^ °^ ^C ^t K 

IYU^S! 


Dale 

C#^l,^Q 

1 ^^'C^ 

,^ SIG ^ R 

Address Telephone Number (Area Code) ax Number Lab Number 

City Slate Zip Code S ite Contact Lab Contact Analysis 

s p (A ttach list if 

ace ce is needed 

Project Name( /^ ^ 0G 

Con(rac t/PUrchasJrderlQu u 00lee No. 

S 

(4//,(^(I 

Sample I.D. No. and Description 

(Containers for each sample may be combined on one line) 

GO 

CarnerANaybdi Number 

Matrix 

Containers & 

Preservatives 

Date Time = a ° o o 

Posslele na2ara ltlenbhCatlenJ npre ursposar 

U 

^. 

- 

Q'banterra 

Chain of Custody Numbe 

Page of 

Special ions ru ec 

Conditions of Receipt 

(A lee may be assessed i/samples are retained 

El Non -Hazard q Flammable El Skin le-dan( El Poison B Unknown Relurn To Chen l q Disposal By Lab q Archive For Months longer than 3 months) 

Turn Around Time Required OC Requirements (Speci fy) 

l /^ ) ^"J 

q 24 Hours J [1 48 Hours q 7 Days q 14 Days V21 Days q Other 

^ReMrqu a y' I 1 I^ r - lane 1. ecerved D e Time 

— 

If 

Relinquished By Date Time . Received By Date Time 

G elrnquished By Dale Time 3. Received By Date Time 

DISTRIBUTION. WHITE - Slays with the Sample, CANARY - Returned to Cleat with Report, PINK - Field Copy 

I 

I` 

I

I 

Chain of 


S I CDJa'D 

QUA 4124 0797 

Client Project Manager 1 

1 Q^^^ 

of 

Address Telephone Number (Area Code)/F Number Lab Number 

C it 

y State Zrp Code Site Contact Lab Contact 

Project Name J ]\ ! Carner/Waybill Number 

Contract/Purchase Order/Quote No. 

Sample 1. 0. No. and Description 

(Containers for each sample maybe combined on one line) 

Matrix 

Containers & 

Preservatives 

Date Time o _ "e n el `^ o = 0 a s 0 

N i 

Analysis 

more space 

^3 -1ZS1 

(Att 

ach list if 

is needed 

îivanterra 


Page o1 

Special Instructions/ 


9L 8 g --- 

ra v 3 v q C^ ^/ v l^ 8 

L1 Non -Hazard q Flammable El Inifant El Poison B 

I p 

Unknown 

rpie lapVSa1 

7 Realm Io Client q Disposal By Lab q Archive For Months 

(A lee maybe assessed it samples are retained 

longer than 3 months) 

Turn Around Time Required\^ / 

-/ 

--D o! hlours El Hours El 7Days El 14 Days ^J 21 Days 

'Alh fy 

l 

q I Ulher f I ^ I IJ Kn 

J 

QC Requirements (Speci fy) 

I 5 n( /.k:r 1 

LO 

..- .. .............. ..r 3are 

1. l (/Ll^'V 

elinquisheOBy Date Time 2 Received By Data Time 

Relinquished By Date Time 3. Receiver) By I Date I Time 

DISTRIBUTION: WHITE - Stays with the Sample; CANARY - Returned to Client with Repo"; PINK - Field Copy

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-01 page I of 

Collector Company Contact 'Telephone No. Project Coordinator Data Turnaround 

R. Fahlberg Steve Marske 373-4316 WEISS, RI. 

Project Designation 

105C Phase I k Phase If -Conc 

Sampling Location AF No. 

21 Days 

re te Samples 100 A re a B98-061 

fee Chest No. Field Logbook No. Melbod of Shipment 

_ 3 [land deliver 

Shipped To 

Quanteria Incorporated 

POSSIBLE SAMPLE HAZARDSIREMARKS 

0.adiasetive 

Special Handling exciter Storage 

31 LD 

SAMPLE ANALYSIS 

T . to I 

U^V 

Bslte Property No. 

N /.^ 

Preservation 

Type of Container 

No. of( onlainer(s) 2 

^ 

21 

Volume 

l^ 

IL 

See item(I)in 

Sp«ial 

Waiom 

SOI[^ 

Î 

Bill of fading/Air illll No. 

Ali /!,J 

Sample No. Metric • Sample Dale Samplc'1lme *,5^ e 

ON680 D I Other Solid -^ y-^ e 10 3 J LCC44 0N k 4 0 1 

rI b 

x^So r, l- /+ Ce, Fws^ 7wbo 

SPECIAL INSTRUCTIONS / _- / Malris- 

CHAIN OF POSSESSION Sign/Print Names s 

s.,,i 

(1)ICP Metals- 6010A(Sigxi 1race) l l-eadl, Mvauy-7471- ( CV) , Chmmiom 11, 7196. '1 t..i.^,ra 

ehnquisbedB DalNrime ei By 1^ I Time PCB, X080 JArocl°r-1254 J, Gamma SpecnoscopY ((^"noo 117,C, ,hA60,Furapiuo M, 5p - c°hd 

3^ 'a l Aril ^'-7 ( Europium-154, Europium-1551: Amencium- 2 41, Iso topic Plutonium, Isotopic Uranium: Sele sl. - o"J" 

9 ^P.^CRIw I-.-t -l9 

e q Mime R edBY 1 f Datc/T^me 

NI alff -^03 Sf^ 1,9 - j7j/za 5 o wl• 

teJ — a I'9( T^t^ 

y9 mot, ô I l¢ Av; S^ IJ, 111 opt lnlida 

in wished By Daleffime Recei ed By Dalc/linen ] n1 u . 1 .pinr 

Nl Wipe 

inquished By Dale/rime Received By Date/rim, I I " z 

-J 

^.eeiau„ 

nme, 

LABORATORY Received By 

SECTION 

—'lisle 

-__ _.. Uatu lime 

FINAI.SMIPLE 

DISPOSITION 

IXsptnal Method - U sposed Bs -------- 

_ 

Uatclllme 

__ 

-- 

1 

1

Y 

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUES T 1198-061-02 

Collector Company Contact 'I elephant No. Project Coordinator DATA "I urnaround 

R. Fahlbcrg Steve Manske 3734316 WEISS, RL 

21 Days 

Project Design ation Sampling Location AF No. 

105-C Ph as e 1 R Phase II - Concrete Samples 100 Area B99-061 

Ice Ch est No. Field Logbook No. Method or Shipment 

Iland deliver 

Shipped To Mile Property 1. Bill of Ladin A BIII No. 

Quanterra In co rporated 

POSSIBLE SAMPLE IIAZARDS/REMARKS 

Radioactive 

Special Handling And/or Storage 


903W -burin 6031(Î - ILLcr- 

Prae vAlinn 


No. of Container(s) 

Volume 

Sample No. Matrix • Sample Dale Sample Time 

ONSB1 N Other Soliq 

P 

2 

IL 

6m imm,l, in 

Specid 

ô/^ D3/, 

3 /x/ Z- ^\Ir/ ^^ /d A ^ I 

SPECIAL[ TRUC'IIONS Q tau is 

CHAIN OF POSSESSION Sign/Print Names Vd ^.,. i 

(I)ICI'Meais- 6010A ISupenrace) 1[rid), 7471 (CV) Cluumimn Ile.-7196. 

e[i 

e' 

uished 

y 

Dale/Time 

^ ^ p/ 

G 

DAINI'ime 

Reuiv 

ive 

B 

Y On 

Date/Time 

151 

- s 

PCBs-80801Atoclor 12541, Gamma Spectnosc. py(Cesium-U7. Cohxll-60, Europium-152, 

r-opium; 154, Eumpimm-1551; Amencium-241. Isotopic Plutonium; Isotopic IIranium, Sele 

SdPnl sn -^9 

r Ni[J^N (03 i Sr- $9 9a-- 7G I S^ " 

T h 9 q^, b0fl 

1 c-C7 

gl 

a 

tc 

"hat 

'^t3^. 

j 

'nquished By Date/Time Received By DaterTime !'^ 1 

ZD 

'ntonshed By Dalelfime Received By Dalerlime 

BORATORY 0.euived By 

SECTION 

Tine naie'I une 

FINAL SAMPLE 

DISPOSITION_ 

Diallo»I Mahod 

-- 

Uisrysscd -- By -- - 

- W(" (une 

1 

s• 

- 

_. 

r 

I 

^ra.,t,> 

I 

Iv i 

I 

^ ;;'-? 

l

Client Sample Screening Results 

!0-Mar-98 

CLIE14TCODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSB NETCPMB 

B M4CI /9/15981:42:00 PM 21A 7/10/199811:27:38 BOM4C1 30 16 A9^3777 e41 27.23 313 

IQUID Bk . 3/10/1998 :51 AM BKO 100 4 0.04 0 0.8 

AN Do /Ia1998 Alq: 3.00E-01 LDOEMI (DpM 3 .49E-01 (uCl/ 1.24E-05 CU 2.47E+01 ±2.3E+01 QA 0E+00 1.a0^ 

t mLt 2.1 UdU: L Bet; 3.42E+01 So):fl. 2E-03 LIL): +03 ±8.7E+OI I 2.0 

Ue 'ylaq^ 

BHI BOM4 422 

LIQUID 

3/9/1998 1:42:00 PM QUAD I 3/10/199811:23'38 AM 

7-. 3/10/19988:43:5 998 9:43 

BOM4C2 

IIK 

30 

100 

6 

3 

.17 

0.03 

202 3 937333 - 

/ 

95/ 0.95 

AdD 3/1 Tol S., Alq: 3.00E-0 Ô^ 

E401 Alp; (Dp 0 (uCU 807E-06 (p 1.6 01 ± 2. 4E4 01 AT E+00 Lob 

pt mR 2.6 

BHI BON680S 

NV: L 

3 /9/1998 1:42:00 PM QUAD24D 

Bel/Alq): /I.IIE I.1+OI 

c 

3 1 101 1998 11:23:51 AM BON690S 

Ljll): 

30 

3.01E+02 3 +01 

1130 37.6066667 

I 

124390 

Alq 

1.0E-0 

e 

4145, 4 333 

SOLID Bkg: 3/10/1998 8:43:35 AM BKO 100 6 0.06 90 0.9 

Ad Dol es 3/10/1998 To1Ee,Alq: 1.63E+02 9.81E401 Alp; (Dpm/.1.71E401 (uCU . 1.27E-02 (pCU -7.83E+01 ±9AE400 CAT 1.6E402 

Lab 

Pp/mp 88,1 / UNb: L me Bolt Alq), 9.19E+03 eo): 6. 116E+00 t4e)t 4.22E404 f 1.2E+02 

111 / 

2.48-03 Alt 

1•IL 

BHI BON681F 3 /9/19983:13:00 PM QUAD2 1 A 3/10/199811:54:54AM DON681F 30 3 0.12666667 96 2.4 

LIQUID like: 3/101 1998 8:43:51 AM BKO 100 4 0.04 8o 01 

Ad Delet 3/10/1998 Tot S., Alq: 1.80E+00 1.00E+01 Alp; (Dpm/ 3.23E-0 1 (uCU 2.62E-03 (pCU 1.45E+01 ± 2.4E+01 CAT 1.7E+00 Lab 

PptmL: 6.9 U nite: L / ml Bel; Alq): 4.79E+00 So): 3.88E-04 LIL): 2.16E+02 ±3.IE+01 I I 2.3E-ul Alq 

LIt 

BHI BON6919 3/9/I9983:I 3 :00 PM QUAD2 1 B 3/10/199811:54:54 AM BON691S 30 13 0.40333333 234 6.55 

SOLID BkL: 3/10/1998 8:43:31 AM BKO 100 3 0.03 95 0.95 

Ad Dole: 3/10/1998 Tot Se, Alq: 1.90E+02 1.15E+02 Alp; (Dpm/ 2.38E+00 (uCU 1.93E-03 (pCU 1.02E+01 +5.3E+00 CAT 49E400 L.b 

Pp/ me: 114.3 / Units: g i mg Bet; Alq): 1.35E+01 Sa): 1.16E-02 Lit): 6.08E+01 ± 4.6E+00 1 1.6E+00 Alq 

ide 

BHI BON69OF 3 /9/19981:42:00 PM QUAD24C 3/10/199911123:51 AM BON68OF 30 43 1.39333333 3426 113.39 

LIQUID Blig: 3/10/19989:43:55 AM BKG 100 4 0.04 81 0.81 

A nt Dole: 3/10/1998 Tot Se, Alq: 1.80E+00 1.00E+01 Alp; (Dpn3 4.48E-0 1 (uCU 3.64E-0 5 (pCl/ 2.02E401 + 2.2E+01 CAT L2E400 I..b 

N P t m 3.4 

P P Units; 1, ml Bet; AI 2.14E402 

9): 

n 

So : 

) 1.74E-02 L C): 9.66E+03 ± 1.7E+02 1 / 5.2E-03 Alq 

Ide 

10-Mar-98 Quan(erra Environment Se rvices, SCP V2.03 1

OateRme Received: 

FIVISM t 

SAMPLE CHECK-IN UST 

y J^/3 S start (^(/0^1^ 

o 

Work Order Number 0 ^0 ^^ SAF i J 11S - " t 

Shipping Cantainv I-l 

1f 

b fain of Custody rt 

fi ^1 

RMSOW-43 -0003 - 

1. Custody Seals oosttpp- g mr I iietibf ? Yes [pw[ I 

Z 

Custody Seals dated and signed? 

Yes.H', [ I 

3. Chain-d-Custodf rer 9 d preswe Yes [ I 

1 t GC 

4. Cooler temperature 

5. VermicufiWpaddm materials is Wet [ j 'rl 

6. Number of samples in shipping =muter. 

Revision 5 

YT'^ ^' 

7. Sample holding 5nes exceeded? Yes [ ; uo [ }^ 

8. Sampws have: 

pe hazard labels 

dy seats maple labels 

9. Sam s are_ 

__,Lim good mrdifiaon kalong 

broken _gave air bubbles 

10. Where any anomalies identified in sanpte receipt? Yes (j No 

11. Description of anoma lies (utc'.ude sample numbers): 

Sample Custcdia n/Laboatnrf.* —X. LL LIu.^ Date: 

Telephoned To: Dn^_By 

0000 11

Five* 1 

SAMPLE CWCK4N UST 

DatePrme Received:^ J 1 `J7S SGS W(),U7J 

RFSHSOW 93-4003 

Revision 5 

ak 

Work Order Number 86310 + 164 1 SAF * e9 

g 

A - 

y 

Shipping Container 10:W635 a%& of Custody * Imo( (1 - U.9 1 - 0a 

1. Custody Seals an sltippi 9 container irfart? Yes Hl c ( ] 

2 Custody Seals dated and signed? Yes ( No ( ] 

3. Chain-of-Curb* n=rd present? Yes ] 

4. Cooler temperak re 

5. Vermiculite/pacidng materials is Wet [ Dry [ Y, /-A 

6. Number of swoes in shipping ccldai er 

7. Sample holding Imes exceeded? Yes [ ] No [ 9^ 

8. 

3 ' 

have: 

tape 

custody seats 

9. Sam are 

in good con diti 

on 

broken 

hazard lab els 

?ppo¢iate sample Labels 

kaking 

Rave air bubbles 

10. Where any anoma lies identified in sample receipt? Yes [ ] No [-]------ 

11. Description of anomalies (in clude sample manbers): 

l eiepnui i^ 1 u. w by 

0 

Y 

600012

Environmental 

Contractor 

Contractor ERC Team 

Interoffice Memorandum 

M. A. St. John x.0-19 

40mm` Scc Below 

°"7e l;ebruary 27.1999 

0-o' S. L. Wiôw 

RadCun Eaginceriag 

X3411531-070, 

wuEcr. CVHlF FSTTMATE FOR S111PP1NC CONCRFTF. CORE SAMPLES 

CCN: 055088 

Job So. n1 92 

W", O.P. Xft.I w 

w 

Oil a 1«c 

MA w 

$ 

C. !LO 

The 1•olluwing calculations show that cvn: satnplawith a direct reading of equal to or less than 

400.000 dpm/100cm' will be below the de fi nitionafradimttive mate rial as defined in 49 CFR 173.40 3 

of 70 Bq/g (2F.3 pCi/g). L'ach sample will consistofcoacrcte mate rial from Ibur, two inch co re 

samples and enough wat er to make r slum consiotocy. The distrihution of radionuc lides is bussed tin 

previous concrete samples taker from the below grade Fad Storage Basin that would also he 

representative of these cuncrcte samples. 

iven: 

Cylinder Vulurrtc = ttr'h Radius ofcaocrcte core (r) = I inch 

Concrete Density = 2.35 g/cm' Height of care sample taken (h) - 0.25 inches 

27 pCi = Dq Maximum & Lt Wading on core = 40,000 dpm/ 1 UUcm' 

2?2 dpm = pCi 

Calculations: 

V - (3.14) (1 in.)'(U 25in) =0.78 in' (16.4 cm'/irrl(4 mix samples) = 51.2 cm, 

(400,000 dpm/51.2 cm') (cm'1235 g) = 3.32E3 dpdg 

3.32ED dpm/g (pCi/2.2 dpm) = 1.SE3 pCi/g or 9.4 8419 

SI.W:did 

Percent Distribution(7) Concemratina (oC: i/c) 

ACo 0.17 2.55 pCi/g 

'rrCs 82 1.2F3 pCi/g 

131 E 0.33 4.95 pCi/g 

134 E 0.05 7.5E-1 pCi/g 

'Sr 17 2.55E: pC ilg 

741 Am 0. W5 7.5F Z pCi/g 

n9 210p u 0.1 1.5 

TOTAL: 1.460 PCi/g 

C(2 j! 5E 

S. 6. Marske X5 -53 

P. A. Newman X3-41 

RadCun Enginee ring File/LB X0-23 

Document and into Se rvices 1 10-09 00001)

eo-Z/-7b 11=ZBA RAOCC" 373 an7o n - C. 

Environmental 

Restoration =RC Team 

Contractor 


To` D. A. St. John 1.0-19 da: 

ò^''`` Sec Below nmr: 

Concentration (vCi/e) 

2.55 pCi/g 

1.2F3 pCi/g 

4.95 pCi/g 

7.5E-1 pCi/g 

2.55E2 pCi/g 

7.5F.-2 pCilg 

1.5 '/ 

I.46L3 pCi/g 

February 27. 1999 

S. L. Winslow 

RadCon Engineering 

X3-41/531-0706 

suwzcr: CU141F FSTIMATE FOR SHIPPING CONCRETE CORE SAMPLES 

Job N9.22192 

DrOr,. ww 

^Y^r ww 

a^. ieec 

AA 

S w, 

ww 

ibwl CeA. 41W 

CCN: 055088 

The following calculations show that cu re samples with a direct reading or equal to or less than 

400,000 dpm/100cm = will be below the de finition ol'radivactive mate rial as de fined in 49 CFR 173.40 1 

of 70 Bq/g (2F.3 pCi/g). Each slugrle will consist of comrctc material from tiour. two inch core 

samples and enough water to make a slur ry consistency. The distri bution of radionuc lides is based tun 

previous concrete samples taken f ro m the below grade Fuel Storage B asin that would also be 

representative of these concrete samples. 

"ven: 

Cylinder Volurnc = nr'h Radius of concrete core (r) = I inch 

Concrete Density = 2.35 g/cm' l leight of core sample taken (h) = 0.25 inches 

27 pCi = Bq Maximum direct reading on core = 400.000 dpm/lOUcm1 

2.22 dpnn = pCi 

Calculations: 

V = (3.14) (1 in.)'(0.25in) = 0.79 in' (16.4 em'/in) (4 mn; samples) = 51.2 cm' 

(400.000 dpm/51.2 cm) (cm'12.35 g) = 3.32E3 dpm/g 

3.3213 dpm/g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 BWg 

S1. W AId 

"'Ca 

Percent Distribulion( 7o ) 

0.17 

[IT 

CS 82 

12Eu 0.33 

"°Eu 0.05 

°0Sr 17 

7°'Am 

ZJ 

"PU 

0.005 

0.1 

TOTAL: 

C(! ics: 

S. G. Mtuske X5-53 

P. A. Newman X3 -4 1 

RadCun Enginee ring File/LB XO-23 

Document and Info Se rv ices HO-09 

GOOOi4

Quanterra 6W V S 014488 

Effiroameattl 

Son= 

Condi ti on Upon Receipt Variance Report 

St. Louis Laboratory 

3 

Client. _ Daze:_ 

Project No: -Sz) 2- Initiated by: oz, 

f 

Shipper/No: A i r b• rrt C RFA/COC Numbers: l Q y L4 

Condition/Variance (Check all that apply): 

1. q Sample received b roken leaking. 

2. q Sample received without proper prese rv ative. 

q Cooler temperature not within 4C ± 2C 

q pH 

q other: 

Record temperature: 

3. q Sample received in improper con ta iner. 

4. q Sample received without proper paperwork. Explain: 

5. q Paperwork received without sample. 

6. q No sample ID on sample con tainer. 

7. q Custody tape disturbed broken/missing. 

q No variances were noted during sample receipt. Cooler 

/ 

Login No.: / ^7/9' 

8. q Sample ID on con tainer does not match sample ID 

on paperwork. Explain: 

9. q III coolers on airbill not received with shipment. 

10. q Other (explain below!: 

Temperature Upon Receipt: 

Notes: C^ ' /, 5 ^— CJrt ^G(/t-e..s, So /cJl-I 

Corrective Action: 

A F C 0 1 

CL I/, 

/ L( 0 Lc t >fX 

v= 

q Client's Name: Informed verbally on: By: 

q Client's Name: Informed in writing on: By: 

q Sample(s) processed "as is". 

q Sample(s) on hold unt il : If released. notify 

Sample Control Supe rvisor Review: (or desienat Date 

Project Management Review: (A— 71 G.,i^,— Date: 3 — If — ^.3 

SL-ADMIN-0004. Rev¢ed 1121;95 

SIGNED ORIGINAL xIL:ST BE RETAI N-ED IN THE PROJECT FILE 

(p 

^rC— 

î,Ji5

O 

C 

L=, 

C 

r4 

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-qb't'-0I 

Collector Company (outnel I elrphone No. Project f nnrdinalor Wim I or11Nr n11111I 

R. rahlberg Sieve Mnrske 171-411 1, WrISS, lll. 


105-0 Ph ase 1 k Phase 11 -Concrete Samples 

Sampling Lo ca tion 

100 Area ` 

'AF No. 

1198-0(I3 

Ice Ch iral No. Field Logbook No. Method of Shipment 

_ Iland deliver 

3 

fL 

Shipped To )Belie Property No. 11111 of LadInR/Al, IIIII No. 

Quenterra Incorporated N 

POSSIBLE SAMPLE IIALARDS/RE AIARKS 

Radioactive 

Special Handling and/or Storage 

8032150) G, 

g o3aicôi 

I j^ 

(S 

Preservation 


No. of Conlabrer)s) 

Volume 

N°^r I -I 

P 

2 

IL 

5

1 

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST 

Collec tor 

R. 1'ahlhera 

Project Design ation 

105-C Ph ase I R Phase 11 - Concrete Samples 

Ice Chesl No. 

Shipped To 

Quanleres Incorporaled 

POSSIBLE SAMPLE IIAZARDS/REIIIARKS 

Radioactive 

Con+pany /'u ntact '1 e""'eNo. 

Alcvc 1,10,4C:171-4716 

Sampling Location 

100 Aren 

Field Lagbooh No. 

L: -- L — l r ,. ` 

I 

Project (bnrdin ldw 

wFlxs. Ill. 

SA F No. 

I19 9 -01" 1 

Nlethad of Shipment 

(land deliver 

Offislic Properly No.. BIII of lading/Alr Bill Nn. 

il.i 

Prtacnalion 

I ype of fbnlRiner 

No. of Conlalner(s) 

Special llandlag end/or Storage 

go3a^ ^ &YPU oa 


Volume 

Q^ 

L 

BOA) 89 

%Î LL I r 1 UIL41--1 ID 11 1\-LUll 

p 

2 

IL 

a«^ Ii5 in 

063 

u9x-Iwt o4 i ' ' ye !n' ! 

DAN 'l urnnnnmd 

'n'lô'•a' + 

Sample No. Ma (rla• Semple Date Sample IIme N .. } vTe!.^. CVas , jl+^:n,tl ;]'-;a1 tf+ l! p^ ' sn-^ 

Othar6eRd- 

1) 

^- /Q " 9 cT 

IAIN OF POSSESSION SIgNPrint Names 

R npuhhed ^ 

/ ' 

S O 

aldflm^ R ived By Daleyl irne 

el uished8 By DnNllme 

ReceNed0By Dat ime -G / 

Impoished By Wicnime Received By Wlerlime 

npuished By Dalerlime Received By Dale/lime 

BORATORY 

SECTION 

FINAL SA pIP1.E 

DISPOSITION 

21 Days 

Oft ^l y y^ x.,^%.- "7 _ + 

SPECIAL INSI RUCTIONS 

O ICP McWk 60104 S.. ( Pubacel lLeaJ), Mvcuq-7471-(CVI. Chromium tic.-7196, 

PCI]s; 1100.0 254 1. Omnma Speetrnscq, ICesimn-117, COWL-60. r:uropium 157, 

L.,.pmm . 134, Ellropium-1511, Amtpcitim-24 I', Isowrie Phllnili mn, knlnplc Upnnim, 5ele 

Q n+hc/ -^ 9 /l/r-l.Kel (o3 Sf -&'9 50-- yp,^ /jr• 

fi2o1299 ' Ci rbo t ^¢ ' 4c -iVr SCaot 

/ 

Retsived By title Dam/lout 

Disposal Mtlhod UispuuJ Uy 

(^ 

_—_—___ 

Ualc/Iona 

hSAllli 

s s...l 

to o,6,1 

11 bade[ 

u - ol 

4 

Ill 

WI 

u, 

q',re 

\, \f4' r 

^ 

..

Bechtel Hanford Inc. CHAIN Ole CUSTODY/SAMPLE ANALYSIS REQUEST u^xyet^Dt ! "' -' 

olleclnr Company /'onlacl 'I elephone Nn. 

Project ('oordinalor 

R. rahlhcrg ./] Steve Mw4c 171 -4116 

N119 1" S. It 1. 

Project Designation Sampling Loca tion 

'AF No. 

105-C Phase 1 k Phase If - Concrete Samples 100 Arcn 1398-061 

Ice Cheat No.^l /I^/^^^ 

JM 15 

_ 

Field Logbook No. v 

Method of Shipment 

1lnnd deliver 

Shipped To Offdle I'ropnly Nu 11111 of Lading/Air 11111 Nu. 

Quanlena Incorporated AJ 

OSSIBLE SAMPLE IIAYAR/RERIARkS 

OS 

RWIosed.8 

pedalItandlingand/orStorage 

^ 

1 l^lf{ 


1'yuerral an 

Type of Container P 

No. of Contriner(s) _ 

Volume 

SD3^JS0e3 ^,,... gD^JC^3^ 

See 11em 1)' n 

SMW 

Sample No. Matrix • Sample Date Sample I une ) lÎ - l} y}grrGr y, +1iA l. 4j j ^,f{P S!,.. T 5 5,1 : 4 t "` r 

$ 0,(18 9 b G V('f1 

Other Becht- ^^^- ff ^^^ CD 

AIN OF PO ION Sign/Print Names 

li ish By /] ime 1 Ree y Uaro/f lne 

e 1 YI 0 1 

/ 

ellnqu ithed By J DMNrime Received By % D.Wl,.c 

eiinquished By DatdTime Received By Date/1imc 

elinquished By DodeoM a Received By WWI u, 

t"oNr""" 

G 

6 

Ditta I nrnaround 

21 Days 

-- -- 

SPECIAL INSTRUCTIONS Liavis 

(1) ICP Metals- 6010A ISupMmcel l Lead l'. Mncury -7471-(CV), Chrmnimn lln -7196, 

PCBs - R080 lAroclor-11541; Gamrna Spectroscopy (Cesium-137, Cuhah-60, Europium-157, 

N ropio n-154, EuropiumAinericimnPiuwnin,n; 

-1551, -141; Isumpic Isrnnpic thorn mn; .Sete 

/ 

^/Gl^l ( u-k'I -^9j /Ul (,^^ - r03 SV'- 8 Cf ^jQ 

l 

—tzek 99 . Carbon 4; 11C ¢,v1hJ' 

/ 

LABORATORY Received By 

_--_—_ 

role umdGmc ._ 

SECTION 

FINAL SAMPLE 

DISPOSITION 

Dispovl Method Ustwsed By - llaic lime 

5 1. 

9p S„i,4 

°, 

n, u., I,^,m 

t .. 

Nl nTr 

1

C^ 

C-3 

C) 

1"J 

Cz 


12-Mar-98 

12-Afar-98 

Quanterra Environment Se rvices, SCP V2.03 

/ ^ 

`N 

3I^ZI11^ 

CLIENTCODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSB NETCPMB 

Bill BON697 3/12/1998 QUAD2 1 A 3/12/1998 11:01:02 AM BON687 30 7 0.18 74 1.54 

LIQUID Bkg: 3/12/199812:01:04 AM BKO 600 32 0.05333333 556 0.9266667 

Ad Dole: 7/12/1998 Tot So, Atq: 1.00E+00 I.00E+00 ^ Alp; 3 

p; (Upm/ p - 8.19E-01 (uCU 3.78E-04 (pCU 3.78E+02 ±3.9E+02 CAT 6.6Ei..b 

-02 

Ppl mp 49 .6 / Units; 1 1 ml Bel; Alq): 3.27 E4 00 So): 1.48E-03 Leg): 1.48E+03 ± 2.8E+02 I 3.4E-0 2 X116

C 

U 


12-Mar-98 

v") ') 1 ^1 0 

CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM R 

POW BON0 119 3/12 1 1998 QUAD2 1 B 3/12/199811:01:02AM BON0 1-19 30 5 0.105 155 4 1733333 

LIQUID BkC: 3 1 12/1998 12:01:04 AM BKO 600 37 0.06166667 536 0.8933333 

And Date: 3 1 121 1998 Tot Sa, Alq: 1.60E+01 I.00E+OI Alp; (Dpm/ 2.08E-0 1 (uCi/ 1.50E-04 (pC'V 9.36E+00 ± 2.3E+01 CAT 2.7E+00 Lab 

Ppt mg: 7.4 i U nits: L ml Bet; Alq): 8.31E+00 Sa): 5.99E-03 LlC): 3.74E+02 ±3.7E+01 I 1.3E-01 

POW B0 1 , 1010 3/12/1998 QUAD2 1 C 3/12/199511:01:02 AM B0 1,10J0 30 7 0.18833333 148 4.0233333 

LIQUID RkC: 3/12/1998 12:01:04 A61 BKG 600 27 0.045 546 0.91 

An] Dale: 3/12/1998 Tot Sa,Adq: 1.60E+01 1.00E+01 Alp; (Dpm/ 4.81E-0 1 (uCV 3.47E-04 (pCt/ 2.17E+01 ±2.3E+01 CAT 1, 2E+00 Lab 

Ppt nil: 7.5 Units: L ! ml Bet; Alq): 7.89 E+ 00 Sa): 5.69E-03 LIC): 3.55E+02 + 3.6E+01 I 1.4E-01 

Iq 

Lit 

POW BONOJI 3/12/1998 QUAD2 1 D 3/12/199811:01:02AM BONO31 30 12 0.31166667 132 3 3 75 

LIQUID BkC: 3/ 12/199812:01:04 AAI BKO 600 53 0.08833333 615 1.025 

Ad Date: 3/12/1998 Tot Sa, Alq: 1.60E+01 / LOGE+01 Alp; (Dpm/ 9.54E-0 1 (uCV 6.88E-04 (pCi/ 4.30E+01 ± 2.7E+01 CAT 5.8E-0 1 lab 

P P1 m L 8.7 / 

Units: L ml Bet; AI9) 6.56E+00 Sal: ) 4.73E-03 L IL): 2.96E+02 + 3.4E+01 I 1.7E-01 Alq 

LIC 

POW B0 1,14 119 3/12/1998 QUAD22A 3/12 1 1998 10:40:55 Abt BON4119 10 2 0.14666667 10 0.135 

LIQUID BkC: 3/12.! 1998 12:01:14 MI BKG 600 32 0.05333333 519 0.865 

Ad Date: 3/12/1995 Tot Sa, Alq: 2.00E+00 I.00E+01 Alp; (Dpnd 4.31E-01 (uCV 3.88E-05 (pCi/ 1.94E+01 ± 3.4E+01 CAT 1.3E+00 Lab 

li ps ring: 2.7 / Units: L ml Bet; Alq): 1.65E-0 1 Sa): 1.48E-OS LAC): 7.41E+00 + 2.7E+01 I 6.7E+00 

POW BON541 3/12/1998 QUAD22B 3/12/1998 10:40:55 AM BON541 t0 2 0.15166667 22 1.2516667 

LIQUID BkC: 3. 12/199812:01:14 AM BKG 600 29 004833333 569 0.9483333 

,W Date: 3/12/1998 Tot Sa, Alq: 1.00E+00 / 1 OOF- 01 Alp; (Dpn t/ 4.34E-0 1 (uCV 1.95E-05 (pC'V 1, 95E+01 +3.6EWI UA2 13E+00 Lab 

Ppt ring: 2 / Unlls: L ml Bet; Alit): 2.30E+00 S.): 1 03E-04 LIC): 103C+02 + 4 .0E+01 

Alq 

N 

Lig 

1 Alq 

4 SE-01 

II I 

POW BON595 3/12/1998 QUAD22C 3/12/199810: 40: 55 ANI BON595 10 1 0-04333333 14 0.4783333 

LIQUID BkC: 3/12/1998 12:01:14 AM BKG 600 34 0.05666667 553 0.9216667 

0 Ant Date: 3/12/1998 Tot S&Alq: 2.00E+00 / I.00E+01 Alp; (DpnJ 1.14E-01 (uCV 1.03E-05 (p(-V 5.13E+00 +3.3E+01 CAT /4.9E+00 lab 

i 

C 

P Pt m G 2 / Units: L nil Bet, AI9h 8.68E-01 Sal: ) 7.82E-05 L IL ): 3 91E+01 + 3.2E+01 1 1.3E+00 

AIq 

1-IL 

12-Mar-98 Quanterra Environment Se rvices, SCP V2.03

K) 'ApItN 

CLIENT CODE ID MATRIXRECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B 

POW BON5 133 3 1 12/1998 QUAD22D 3/12/1998 10:40:55 AM BON5 133 10 1 0.055 22 1.2633333 

LIQUID Bkg: 3/12 1 1998 12:01:14 AM BKG 600 27 0.045 562 0.9366667 

AN Date: 3/12/1998 Tot Say Alq: 2.00E+00 1.00E+01 Alp; (DpM 1.27E-01 (uCV 1.14E-0 5 (pCV 5.71E+00 ± 3.5E+01 GAT 4.4E+00 Lab 

Ppt mg: 3.7 / units: ts: 1, ml Bet; Alq): 2.36E+00 So): 2.12E-04 Llg): 1.06E+02 ±4.OE1 

1 

4.7E-01 

AIy 

I-I[ 

POW B01, 1589 3/12/1998 QUAD23A 3/12/1998 11:01:05 AM DON5 119 30 1 1 0.33166667 51 0.81 

LIQUID Bkg: 3/ 12/199812:0 1.20 AAI BKG 600 21 0.035 534 0.89 

AN Date: 3/12/1998 Tot Sa, Alq: 2.00E+00 1.00E+01 Alp; (DpM 937E-0 1 (uCV 8.80E-05 (pCV 4.40E+01 ± 2. 2E+01 CAT 5.7E-01 Lab 

Ppt P P mL 3.3 

Units: L ml Bet; AI9): 1.34E+00 Sa ) : 1.21E-04 L I[) 6.05E+01 + 2.0E+01 

1 

8.3E-01 

AN 

POW B0 1 , 1 50 3/12/1998 QUAD23B 3/12/1998 11:01:05 AM BONK5 30 5 0.09333333 40 0.3516667 

LIQUID Bkg: 3/12/1998 12:01:20 AA1 BKG 600 44 0.07333333 589 0.9816667 

Ant Date: 3/12/1998 Tot So, Alq: 2.00E+00 / 1.00E+01 Alp; (DpM 2.79E-0I (uCV 2.51E-0 5 (pCV 1. 26E+01 ±2.1 E+01 CAT 2.0E+00 Lab 

Ppt mg: 2 ,- U nits: L ml Bet; Alq): 6.12E-01 So): 5.51E-05 Llg): 2.76E+01 + 1.9E+01 I 1.8E+00 Alq 

POW B0N5D1 3/12/1998 QUAD23C 3/12/1998 11:01:05 Abl BON5D1 30 13 0.38666667 49 0.725 

LIQUID Bkg: 3/12/1998 12:01:20 AS1 BKG 600 28 0.04666667 545 0.9083333 

AN Date: 3/12/1998 Tot Sa, Alq: 200E+00 LOOE+01 Alp; (D i n/ 1.12E+00 (net/ 1.01E-04 (pC'I/ 5.05E+01 +2.3E+01 CAT 5.0E-0 I Lab 

Ppt mg: 2 / Units: L ml Bet; Alq): 1.17E+00 Sp: 1.06E-04 L [): 5.28E+01 ± 2.0E+01 

1 

9.5E-01 

AlqIt 

POW BON6 1`9 3/12/1998 QUAD23D 3/12/1998 11:01:05 AM BON6E9 30 8 0.21333333 32 0.1533333 

LIQUID Bkg: 3/12/1998 12:01:20 AAI BKG 600 32 0.05333333 548 0.9133333 

AN Date: 3/12/1998 Tot So, Alq: 1.00E+00 1.00E+01 Alp; (DpM 6.29E-0 1 (uCV 2.83E-05 (pCV 2.83E+01 ± 2.1E+0I CAT 8.8E-01 Lab 

Ppl mg: 0 Units: L ml Bet; Alq): 1.54E-01 So): 6.94E-06 LIg): 6.94E+00 + 1.6E+01 1 7.2E+00 AIq 

Id[ 

POW BON6H0 3/12/1998 QUAD24A 3/12/199811: 00: 58 AM BON6110 30 4 0.06833333 36 0.2416667 

LIQUID Bkg: 3/12/199812:01:08 AAI BKG 600 39 0.065 575 0.9583333 

C^ Ant Dole: 3/12/1998 Tot Sa,Alq: 1.00E+00 I.00E+OI Alp; (Dpm/ 2.04E-01 (uCV 9.20E-06 (pCL/ 9.20E+00 +2.IE+01 CAT 2.7E+00 Lab 

(J 

Ppt mg: 0 Units: L ml Bet; Alq): 4.29E-01 So): 1.93E-0 5 Llg): I.93E+01 + I.BE+01 I 2.6E+00 

All "It 

12-Afar-98 Quanterra Environment Se rvices, SCP V2.03 2 

AIL 

1.1[

0uanterra March 23, 1998 03:02 pm 

Account: 10722 Project: 550.260 ouanterra-Richland OAS No. 550.26 Rev. 2 


Master Sample Login: 17200/1 

pf 

Draft: Final: Entered and Reviewed by PM Review: !/^/\— 

7^^1 

r 1 fw^ 


.^ (` 

pll f, 

A j( 1'. F 

^'^ 1 - TOU^ 7 

+aT"rT' 

M^ 

Of *007 

Sample No. 

Co 

Client ID C-Matrix Date: Collected Received Due Shipper Red Category gad SalRp(e No. 

mm ents 

N 

Data: 

Container Type Analysis Class Preservative Anal. Due Date Hold Date Site (Container Numbers:% Filled) I ,^ LZ-,^f 

L— 

17200-001 BON685 Solid 11-MAR-98 08;30 11-MAR-98 11:57 31-MAR-98 AIRBORNE 1 Screening not Required 

RICHLAND I.D. 80320501//ICAPT = PIT ONLY//PCB 1254 ONLY///THIS SAMPLE MUST BE FILTERED TO CREATE A FILTRATE SAMPLE (17200-005). 

1 PN - Plastic-1 1, HG/7471/Q4 S COLD 27-MAR-98 08-APR-98 R5B (364124:99) 

1 ICAPT/6010/04 S COLD 27-MAR-98 07-SEP-98 R5B (364124:99) 

1 PCB/8080/04 S COLD 27-MAR-98 25-MAR-98 R5B (364124:99) 

17200-OOIMS BON685 Solid 11-MAR-98 08:30 11-MAR-98 11:57 31-MAR-98 AIRBORNE 1 Screening not Required 

RICHLAND I.D. 80320501//ICAPT = P8 ONLY/(PCB 1254 ONLY. 

1 PN - Plastic-1L HO/7471/Q4 $ COLD 27-MAR-98 08-APR-90 R58 (3641Z4:99) 

1 ICAPT/6010/04 S COLD 27-MAR-98 07-SEP-98 R58 (364124:99) 

1 PCB/8080/Q4 S COLD 27-MAR-98 25-MAR-98 R5B (364124:99) 

17200-OOlMSD BON685 Solid 11-MAR-98 08:30 11-MAR-98 11:57 31-MAR-98 AIRBORNE 1 Screening not Required 

RICHLAND I.D. 80320501//ICAPT = PB ONLY//PCB 1254 ONLY. 

1 PH - Plastic-1 1. NG/7471/04 S COLD 27-MAR-98 08-APR-90 R56 (364124:99) 



17200-002 BON686 Solid 11-MAR-98 10:00 11-MAR-98 11:57 31-MAR-98 AIRBORNE 3 87042-001 

RICHLAND I.D. 80320502//THIS SAMPLE MUST BE FILTERED TO CREATE A FILTRATE SAMPLE (17200-004).ICAPT = PIT ONLY.//PCB 1254 ONLY; 

1 PH - Plastic-1L HG/7471/Q4 S COLD 27-MAR-98 08-APR-98 R5B ' (364125;:99) 

1 ICAPT/6010/04 S COLD 27-KAR-98 07-SEP-98 R5B (364125:99) 

1 PCB/8080/Q4 S COLD 27-MAR-98 25- 14AR-98 R5B (364125:99) 

17200-003 BON687 Solid 11-MAR-98 13:05 11-MAR-98 14:20 31-MAR-98 AIRBORNE 1 

RICHLAND I.D. 80320503//ICAPT = Pit ONLY//PCB 1254 ONLY///THIS SAMPLE MUST BE FILTERED TO CREATE A FILTRATE SAMPLE (17200.006) 

1 PN - Plastic-1 1.HG/7471/Q4 S COLD 27-MAR-98 08-APR-96 R5 0 

1 ICAPT/6010/Q4 S COLD 27-MAR-98 07-SEP-98 R58 

i PCB/8080/04 S COLD 27-MAR-98 25-MAR-98 R58 

,1-200-004 BON896 Liquid 11- 140 -98 10:00 11-MAR-98 11:57 31-MAR-98 AIRBORNE 

G RICHLAND I.D. 80321503//ICAPT = PS ONLY//AROCLOR 1254 ONLY///USE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17200.002. 

1 PN - Plastic-1 1.HG/7470/04 S COLD 27-MAR-98 08-APR-98 R5B 

d 1 

J i 

ICAPT/6010/04 

PCB/8080/04 

S 

S 

COLD 

COLD 

27-MAR-98 

27-MAR-98 

07-SEP-98 R5 11 

18-MAR-98 R5B 

3 - =Sample has not been rad screened. 

Page 1 

(364126:99). 

(364126:99) 

(364126:99) 


1 Screening not Required 

(364324p99) 

(364324:99) 

(364324:99) 

^ÛO2LG^


Ouanterra March [3, 199B US:UC pm 

Account: 10722 Project: 550.260 Ouanterra-Richland OAS No. 550.26 Rev. 2 


Draft: Final: Entered and Reviewed by: PM Review: 

Samp le Header Template: 

Sample No. Client ID C-Matrix Date: Collected Received Due Shipper Red Category Red Sample No, 

Comments 

p Container Type Analysis Class Preservative Anal. Due Date Hold Date Site (Container Numbers:% Filled) 

Data: 

17200-005 DON685 FILTRATE Liquid 11-MAR-98 08:30 11-MAR-98 11:57 31-MAR-98 AIRBORNE 

RICHLAND I.D. 80321501///USE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17200-001. 

1 PN - Plastic-1L HOLD//04 S COLD 27-MAR-98 21-MAR-98 R58 

17200-006 BON687 FILTRATE Liquid 11-MAR-98 13:05 11-MAR-98 14:20 31-MAR-98 AIRBORNE 

RICHLAND I.D. 80321503///USE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17200-003. 

1 PN - Plastic-1 1.HOLD//04 S COLD 27-MAR-98 21-MAR-98 R58 

r-, 

U 

C^ 

3 - = Sample has not been red screened. 

Page 2 

t screening not ..R" !red 

(365372:99) 

1 Screening not Required 

(365373:99).

^ 

Chain of 


UOA 1134 11 19 7 

Cleat 

f3f^ l,lf^ 

51 


L 6 0^S^;C^ 

t 

Dal 

I-Izr1^ 


Qty State Zip Code Site Contact Lab Contact 

Prolecl NameA ' - 

1 

Contract Purchase Order/Quo te No 

Sample 1. 13. No. and Description 

(C:onldumas for each sample may be combined on ono line) 

Date Time 

Carder/WaybIll Number 

Ma trix 

1 wh. - i a,ard munnncen m pyrnple rn 1-0 al 

^.-y I Non Hazard 

q Flam m able f] Skm hrifanf q Poison B Unknown I 

L ^XI 

f 

-Iurn Around Time Requeed 

^ 

_ 

-- 

gefurn To Glianf 

4 flours q 4 8 Hours q 7 Days q 14 Days 21 Days q ^ Iher ^^ ^^ ^_ 

„ q^ e N y 

Date ,ê 

h 

l 

^ y r ^ ^_^^^— 

I

Ilecldel Ilan ford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUES T u9a-Obi-ul 1''b` ! 

Collec for Counpauy Cnulocl 'I vlrphone No. Project l'unnlblalur I).Ia I or'us roond 

It I uhiber8 slave KSnu.ske 171-4116 VVV.1.SX, Ill. 

foujoel Designation Sampling Location 

105-4' Phase I & Phase II -Concrete samples 

100 Area ` 

AFNo. 

1.—d)73 

lu Chest No. Fi eld Logbook No. Method of Shipment 

_ Iland deliver 

hipped To ORaI(e 1'rnperty Nu. IIIII of Ladil KIA it 11111 No. 

Qumncrra Incorporated N ^f- N 3f 

POSSIBLE SAMPLE HAZARDS/REMARKS 

RWlaanva 

pedal Handling and/or Sto rage 

A03^1 Sol /1 WmI 

^D 3^1^/I ^lGl 


Preservation 


21 Days 

No. of Conlaiucr(s) 7 _. 

Volume 

IL 

Sn ium I , In 

I^^"^Ì^°^• 

"'"o, 

sample No Matrix • Sample Da te sample'l imc ^`, ^", ', {^. ' 3g{ payenn '^ k 9 d 1 

LN- 

x"689- Other 6elirY 

S -^ C^^ /[^ ,^ L^ LCK,1!1 

e)N8 N L1eJ" 1 

l—L 

CILUN OF POSSESSION Sign/Print Names 

Reliogai.hed 05 r Dwe/yLne 

J -4'-Y a 

Iq c 1 

I P 2^^_, ^5 — 

Ic/time 

I 

eel d 0y 

l., A 

I /rim. 

I -1 

R edgy 1- ` / Ua1e/I'ime10'- 

eiu niched By UaWI...m Recei ed By WWI im. // 

ioquishcJ By Dwcil ne Received By D.ICIFimc 

IAIIOIIATORV 

SECIIt1N 

FINAL. SAKIPLE 

DISPOSII ION 

SPECIAL. INS'fRIICI'IONS 

I ICP Mail. - 6010A S,, nuce Leal ' Merco 7471 - CV Chromium Ilea 7196; 

NCB. - 8080 1Aroclor-13341; Gamma Spearosoupy IC.s om-137. Coba1660, Earopiwm 153, 

liuopiwm 154. Luopiow 1351. A... oral-741; 1.°mpic Plwmmun; bolapie Unnlmn: S ol e 

SeleR,w&- -'t9^ MLtCI-63 Sr- 5 5^ • 

3ri, o -- tDrn-1 

}Ee^t7^ - G0. r{J Uvl l¢ Fl cliv, t^ s^«-., 

Received By Title Dmdfimc 

e• 

— 

f Q 

1,5 A.. 

DL u, 

T 1.: 

W I W." 

I. Ilq.i J 

V yew^°n 

x 0Lh, 

I 

1_. 

l 

1 

Manix 

1LIDI 

so - Sa6d 

SL - 5;-1, 

w"` 

Di.po..I Mahal —. .-_ 

- -- Urs 1,used o y Dale/1'imc -- 

l=11 

4 

y

Iicchlel IlBnford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST lil8•h(fioI ., 

'ulleclor 

R Pnld6c tp 

Project D es ignation 

105 C Phase I & Phase 11 - Concrete Samples 

Coulpuly Con fact 

.1 

hour Nn. 

Slew Mnrskc :171-4116 


IDO Arco 1 

Ice Ch es t No. Field Logbook No. 

Shipped To 

Quanleua Incorpo rated 

POSSIBLE SAMPLE IIAZARDS/REAIARKS 

RaJioanirc 

peclal llandiing and/or Storage 

1: - L- — / I o ^ ` 

Offrlle Proper ly No 

`Q 

Preservalion 

'Iypc of Container 

^60301^^ -m x,27 Da y 


N^^• 

No. of Conlainer(s) 1 

Volume 

IL 

P 

,..3'nW a 

Project Courdlnalur or 

WI T S$, Ill. 

•AF No. 

1198- 061 

Alelhod of Shipment 

hand deliver 

Bill of LadinWAir Bill Nn. 

iV A 

fl urnaruund 

No....Oâ 1 

21 Days 

Sample No Matrix • Sample Dare Sample ' I hoc 4y i -... 

Ilf 1Sk+x yux6^/3 eJ; 

gef^.I4I 

/5,;1'.^lfq ^' 1. 

60.1. -64 Other 6elicY ^- /o- 9v" t7 fl s'^ `^ ^ 

.. 

/ 

x.o/^. , -•" 7 Yl t 

onl8 q S 

^'^'" 

IAIN OF POSSESSION Sign/Print Nunn 

R inquirhned 'pn\1 alelfim 

1L^5°, S^^ 3 I^ ' ^3 

R ived Dy Dalell'iine 

_ r, 

du uishcd DY Uale/Time R

0 J 

d 

Î 

C)6-3 

Ilechlel Ilanforll Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B9XybrBI 

Collector ,y- 

R. ISddhcrg 13I- ./(.J 


105-C Phase I & Phase 11 -Concrete Samples 

Company Conlacl 'P

C^ 

G 

LJ 

C% 

ry 

00 


12-Afar-98 

CLIEN'1' CODE 11) AIATIUX RECEIVED DETECIOB ACQ DATE SAMPLE 

DIII I1ON687 3/12 1 1998 QUAD21A 3/12/199811:O 1:02AM BON687 

LIQUID Bkg; 3/12/199012:01:04 AM BKO 

MINUTES CNTS A NET CPAI A CNTS 8 NET CPA1 B 

n 

30 7 0.18 74 1.54 

600 32 0.05333333 556 0.9266667 

Aid Ilde: 3/12/1998 To1 So, Alq: 1.00E +00 3 IAOE400 Alp; (Dyad 8 .39E-0 1 (uCll 3 . 78E-04 (pCU 3 .78E+02 ± 3 .9E+02 CAT / 6 .6E-02 Enk 

Ppl uq: 49.6Units; 1. nil Bel; M q): 3.27E+00 Su ) : IABE-03 uv: 1.48E+03 f 2.8E+02 1 3.4E-02 M 

q 

18 

12-Afar-98 Quamerra Environment Se rvices, SCP V2.03 1


12-A far-98 

CLIENT CODE 11) MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B 

PGW BON0119 3112/1998 QUAD21B 3/12/199811:01:02AM BON0119 30 5 0.105 155 4.2733373 

I.IQIIIU BUZ: 3/12/1998 12.01:04 AM DKG 600 37 0.06166667 536 0.8933333 

Ad Dole: 3/12/1998 Tul Sy, AIq: 1.60E+01 1.00E+01 Alp; (Dpi./ 2.08E-0l (uCU 1.50E-04 (pC1/ 9.36E+00 ± 2.3E+01 CAT 2.7E+00 Lob 

1'07 me: 7.4 ! U.N.. L / ,.,1 U... el..+• v atc+nn co+. c ooc na .1-1. a an c.na - a I.,., I / , ac n 

. ALI 

l`G\V BONOJO 3/12/1998 QUAD21C 3/12/199811:01:02 AM UONOJO 30 7 0.18833333 148 4.0233333 

LIQUID 868; 3/12/1998 12:01:04 AM BKG 600 27 0.045 546 0.91 

AW hole: 3/12/1998 Tut So, Alq: 1.60E+01 1.00E+01 Alp; (Dpnd 4.81E-01 (uCV 3.47E-04 (pCY/ 2.17E+01 ±2.3E+01 CAT / 1.2E+00 Lob 

Ppl me: 7.5 Ud13: 1, / ml Bet; Alq): 7.89E+00 So): 5.69E-03 LIC): 3.55E+02 ± 3.6E+01 I 1.4E-0 I 

Alq 

LIJJ 

POW BONOJI 3/12/1998 QUAD2ID 3/12/199811:01:02 A t BONOJI 30 12 0.31166667 132 3.373 

I-lQU1U DUB: 3/12/1998 12:01:04 AM BK(J 600 53 0.08833333 615 1.025 

Ad Dote. 3/121998 Tut So, Alq: 1.60E+01 / LOGE 101 Alp; (Dpnd 9.54E-01 (uC'U 6.88E-04 (p(-'U 4.30Et0l ±2.7E+01 CAT S.SE-01 Lob 

Pptmt: 8.7 / Udta; L ml Bel; Alq): 6.56E+00 So); 4.73E-03 LIZ): 2.96E+02 f3.4E+01 I ! 1.7E-0 1 AN 

Ids 

POW BON4119 3/12/1998 QUAD22A 3/12/199810x40: 55 AM 13ON4119 10 2 0.14666667 10 0.135 

I.IQOID IIUZ: 3/12/1998 12:01.14 AEl IJKG 600 32 0.05333333 519 0.565 

AM Dole: 3/12/1998 Tut So, Alq. 200E+00 I.00E,01 Alp; (Dpnd 4.31E-01 (uC1/ 3. SSE-05 (pCU 1.94E+01 ±3.4E+01 CAT 1.3E+00 Lab 

Ppl mZ: 2.7 / IIn11o: L / ml Bel; Alq): 1.65E .01 So): 1.48E-05 LIZ): 7,41 E+00 f 2.7E+01 

I 

/ 6.7E+00 Alq 

148 

POW BON541 3/12/1998 QUAD22B 3/12/199810:40:55 AM BON541 10 2 1E 15166667 22 1.2516667 

LIQUID BUZ: 3/12/1998 12:01:14 AEI BKG 600 29 0.04833333 569 0.9483333 

Aul hole: 3/12/1998 - -- 'I'ul So, Alq. 100E+00 IO0Ei01 Alp; (Dpnd 4.34E-01 (ICY/ 1.951:05 (pCU I95E101 ±3.6Ef01 CAT 1.3E+00 I.ab 

Ppl n,Z: 2 ,/ UWte: L ml [let; Alq): 2.30E+00 So): 1.03E-04 J.IZ): 1.03E+02 ± 4.OE+01 1 4.8E-0 1 

KAV IJON585 3/12/1998 QLJAI322C 3/12/1998 10:40:55 AEI BON595 10 1 0.04333333 14 0.4783333 

(-_' LIQUID B4Z: 3/12/199812:01:14 AM BKG 600 34 0.05666667 583 0.9216667 

l 

AWnote: 3112/1998 '1'o1SO,Alq: 2.00E+00 IOOLM Alp; (Dpnd 1.14E-01 (ICU 1.03E-05 (pCY/ 513E+00 +3.3E+01 CAT 4.9E+00 Irb 

Ppl mZ: 2 / Units: I. ml Bel; Alq): 8.68E-01 So): 7.82E-05 Ilit): 3.91E+0I ± 3.2E+01 

I 

1.3E100 Mq 

Ile 

%2-Afar-98 Quanterra Environment Services, SCP V2.03 

y 

/ 

LIL

C LIEN 'f('ODE 11) MATRIX RECEIVED 

PGW BONSBS 3/12/1998 

LIQUID 

Aul Dule: 3/12/1998 Tut Sa, Alq: 2.00E100 

C =' 

U 

Ppl me: 3.7 - Unllr, 1 1 

12-.A far-9H 

DETECTOR ACQ DATE SAMPLE MINUTES CN 'I'S A NET CPM A CNTS B NET CPbt B 

QUAD22D 3/12/199810:40:55 AM BON5B3 10 1 0055 22 1.2633333 

BkB; 3/12/199812:01:14 AM BKG 600 27 0.045 562 0.9366667 

LOOEt01 Alp; (B lind 1.27E-01 (uCV 1.14E-05 (p(-'V 5.71E100 ± 3.5E-1 01 CAT 4.4E+00 IAIJ 

ml Bel; Al 2-36E-100 So : 

9Y• ) 2.12E-04 1. 1.06Ei02 

ID: 

QDanlerra Environment Se rvices, SCP V2. 0 3 

t 4.0E+01 

I / AN 

4.7E-01 

1.18 

PGW 13ON5B9 3/12/1998 QUAD23A 3/12/199811:01:05Aki BON5B9 30 11 0.33166667 51 0.81 

LIQUID BkB: 3/12/1998 12:01:20 AM BKO 600 21 0.035 534 0.89 

Ail Dole: 3/12/1998 Tut So, Alq: 200E-100 LOOEi01 

1- pt 1n8: 3.3 ! 11 11113: 11 

Alp; (Dpnd 9.77E-01 (uCV 8.80E-0 5 (pCV 4AOE101 ± 2.2E+01 CAT 5.7E-0 1 l.ab 

Bel; Al it); 1.34E-100 So): 1.21E-04 1.18): 6.05Ei01 +2.OEi01 I 8.3E-01 Alq 

PGW BON5C5 3/12/1998 QUAD23B 3/12/199811:01:05AA1 BON5 42 5 30 5 0.09333333 40 0.3516667 

LIQUID BkB: 3/12/199812:01:20 AM BKG 600 44 0.07333333 589 0.9816667 

Aul Dune: 3/12 1 1998 '1'ol Sa,Alq: 2.00Ei OO / LOOE401 

Ppt m8: 2 / Un113: 1- ml 

PGW BON5U1 31 12/1998 QUAD23C 3/12/199811:01:05 AM BON5D1 30 13 0.38666667 49 0.725 

LIQUID BkB: 3/12/199812:01:20 AM BKG 600 28 0.04666667 345 0.9083333 

And Dole: 3 1 12/1996 Tut Sr,Alq: 2.00E+00 LOOEi01 Alp; (Dpm/ 1.12E+00 (uCV 1.01E-04 (pCV 5.05E+01 ±2.3E+01 CAT 5.0E-0 1 Lob 

Ppl nq,: 2 / Units; I- -/ ml Bet; Alq): 1.17E+00 So): 1.06E-04 1.^8): 5.26E+01 ± 2.0E+01 

1-18 

1 Alq 

/ 9.5E-01 

118 

POW BON6F9 3/12/1998 QUAD23D 3/12/199811:01:05AM BON6F9 30 8 0.21333333 32 0.1533333 

LIQUID BkB: 3/12/199812:01:20 AM BKO 600 32 0.05333333 548 0.9133333 

And Dote: 3/12/1998 'Iu1Su,Alq: 100E-100 1OOL101 

Ppi nq: 0 , Anita: L nit 

Alp; (Dpn3 2.79E-01 (uCB 2.51E-05 (pCV 1.26E+01 +2AE+01 CAT 2.0E+00 Lab 

Bet; Alq): 6.12E-01 So): 5.51E-05 1.18): 2.76E+01 ± 1.9E01 I 1.8E+00 Alq 

1-18 

Alp; (Dpn3 6.2913.01 (u( 'V 2.831:05 (pCV 2.83E101 ± 2.IEf01 CAT 8.8E-01 IAIJ 

Bet; Al it): 1.54 E-01 So): 6.94E-06 L1B): 6.94E+0U + 1.6E+01 I 7.2E+00 Alq 

1-18 

PGW BON6110 3/12/1998 QUAD24A 3/12/199811:0058AAI BON6110 30 4 0.06833333 36 0.2416667 

LIQUID BkB: 3/12/1998 12:01:08 Ali] BKO 600 39 0.065 575 0.9583333 

Aid D.w 3/12 1 1998 3'u1 So, Alq- LOOS+00 1.00E+01 Alp; ( Dpnd 2 .04E-01 (uCV 9 . 20E-06 (pCV 9 . 20E+00 + 2 . IE+01 CAT 2.7E+00 Lab 

Ppt ut8: 0 Un113: I. , ml Bel; Alit): 419E -01 So); 1.93E-05 LAB): 1.93E-1 01 ± L8E+01 I 2.6E-100 All 

1-18

uuanterra March e3, Tenn ua:ul pm 


Account: 10722 Project: 550.260 Ouanterra-Richland QAS No. 550.26 Rev. 2 


1(^ 

Draft: Final: Entered and Reviewed by: c 

///{//n)/

(l7 

Chain of ^,; . Qivanterra 


OHA 41-A msr 

L c C' 

CbeN _ .^ 


C 6 a 1- ^C^ 

Dat 

7-1 Z- e-1 ^ 

AAdress Telephone Number (Area Code)/F Number Lab Number 

Ciry Stale Z1p Code See Contact Lab Contact 

Project Name . 0 / -- ` 

C...Wact Purchase Ordedouote No 

r 

^) (^ '^'^^^ 1 

Sample 1, D. No. and Description 

(Gonlainers for each sample maybe combined on one line) 

Date Time 

Carne rlWayblll Number 

Matrix 

$ m y 

tL I _ _ I t ^l .^,? 

3 

^ 

d 

`^ 

Containers s 

Preservatives 

o 

i i 

o 

2 

o 

ti i 

L, _ 

Analysis (A ttach list it 

mores ace is needed 

- 

` 


Page o! 

0131 



rossm;a rruam mennncaoon a1 7ple Disposal 

_ (A lea maybe assessed it samples a re retained 

Nun-f fazanl q Flarmnabla q SkWn I...1, - q Poison B Llnknuwn H turn 10 Clent q Disposal By l ab q Arcbrvu Tor _. _ Months longer than 3 months) 

_- 

n AO, 

u round limo Regwred `pC Regmrenênls / (SpeutyJ r 

aft q aeROUm q 0ays [71a Days z1Days 11 her ^^ ^^ ^ (-^^'> of 

i ;had 3y^ -- -f -^ 

- 

Date 1 _ Receued By Date Time 

- - -- - - - 

linq^ ^ncd Hy j -- ^ Date ^ Lrno 1. Received By -- --- - I Date I Time 

-- 

9 ...... l¢'d B V 

-- - - ^ Dal -j e 7inm - 3. nor ceivod By OBIa Time 

Conmienis 

DISTRIBUTION: WFIITE SIeVS wnh the Sample. CANARY - Retumetl to Client with Report; PINK -Field Copy

Bechtel Hanford Inc. I 

'olleclor 

Il.I ,Iilbcfg 

Yo)ttl Iletgnallon 

105-C Phase 1 A Phase II - Concrete Samples 

cc Chest No. 

CHAIN OF POSSESSION 

^&.goohcd By 

J 

T.AIIOI1.51(1111' SVC- I ION 

FINAI. SARIPI E 

DISPOS1114 ON 

Incorporated 

POSSIBLE SAMPLE IIAZAHUS/a EMAn6S 

Ndloacdva r 

fly 

CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUES'1 

Company ('nnlxrl ,'I el, phon y No. P rolerl Conr.11nxlnr 

slevc Mnrske 111 4116 wpISS. 111 ^J 

wrpling L oration -- AF NsS_ 

fT^ 

100 Arco 1195-1113 

Field Logbook No. McOlod of Shipment 

_- _ (-' Iland deliver 

Offdle Properly No. 1101 of Lading/Air 111 

N/ 1T ti /31 

Name 

`^ 

I , 

Preservation 


No. of ConlahrerlQ 2 

Special Handling and/or Slonge ^ _ ^ 

Volume 

I'^-• 

/^ i M 

srr iom 111 in 

CSN 

^ 

Il/IhLe• -, / i ^ 

sryctid 

^0^2 

f^ SANIPL E ANALYSIS ^.,.--, cam lyn `li^^ 

sample NO mairlx Sample [)are Sample 1111 I 

Other Sehd- S ^ C^ .^/ 

I1 ^^ ^,'5)I 

I 

f- l4 

ime 

(1 

i 1)alc/lime 

DaINI c // 

Dmerime 

SPECIAL INSTRUCA IONS Matrix 

( 

s s.,d 

l) ICPMdAI - 60101 IS upcnrecel lLcadl; Aicrany-7471-ICV1;Chromiom Ilex-7196; 

S[ - s^^^^^.i 

PCnr- 110801Arociur 12541. Gamma Spcmmf

Uechlel Hanford Inc. CHAIN Ole CUSTODY/SAMPLE ANALYSIS Itl:QUES'1' 

Collector Company /'oulxcl 'I c1cphune Nu. 

R I :nhlherp 

Slcve Mprskc 371-1316 

Prnlrxt Ilaignallun 

105 C Phase I & Phase 11 - Concrete Samples 

smulpling Localion 

100 Area I 

Ice Chest No. Field Logbook No. 

(,-L _ I 

Shipped I 

1)uenlun Incnrpnu (ed 

Poss l"LL SAMPLE IIAZanusntEMARKS 

RaJiwclive 

Special llandling and/or Storage 

&^kooa e 


Ondte 1'rup,rty No.. 

A i/`J 

1'reservaliun 

ra, ` 

e7 

'i ype of Container 1' 

No. of Containers) 

Volume 

IL 

,..,P. 

Sample No Matrix • Sample Date Sample 'I'6nc ° ^' 

7111 

3^'r als x,{S ee 

. -7 

'S P,? F x 5 ±•'SA 

^r 3-, 

: r 

Project Coordinator 

wFiss. RI. 

SAF No. 

1198-061 


Iland deliver 

(sill of Lading/Alr 11 111 Nn. 

w 

8m6" -Q7 Other 6eRd- ^- /Q- iJ (!t'r7 K.a 

130AJ?q 

ILUN OF POSSESSION Sign/Print Nunn 

R inquished ll} 

\,,r 

"^ S •' 

c S oi,eJRy 

L', 

am/fim q1 

R ived Ry 

^^ ^^ 305 4 

Damn'imc 

Received By 

Dalen i1ne 

Dal nine, 

Rckslnls islmJ try 

Dalc/l unc 

ReccivcJ By Ila1c/I hnc 

U 

R ish

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST ^ 

1198y 

! 

"olleclnr ,/- Company Contact 'Iclephnnt Nu. 


Data Turnaround 

H. Iahlhcrg G . ^jl'j /(ter 

.s(eve hlnlske 171-4116 

wl;I%N. It 

1•rolal Iltsignal un Sampling Location i 'AF Nu. 

105 .0 Phasc I & Phase II - Concrete Samples 100 Area 1198-061 

Ice Chest No.l yJ p /^ G/ Field Logbaok No. hiclhnd of Shipment 

J M ^ 

^1J{O _ hand deliver 

Shipped To Offsltt 

Quanlxn• Incorporated 

POSSIIILI: SAMPLE IIA7.AIInS/ItEhIAR6S 

NaJluadbe 

Special handling and/or Storage 

j 

- 

I 

pSAMPLE 

ANALYSIS 

Properly Nu 

I,^d 

1'rraerval nra 

'i'ype of Coulnbmr 

N11e 

No. of Canlalner( . ) ) 

Vulwne 

P LI 

II, 

See Oem (I I in 

Special 

I."'."i°"^ 

Sangdc No Matrix • Sample Dale Sample T rate l^ 5r , I '(rl,w 

}'I}) ^, ^r ll lr i ,;1'li ^ 

I I ,111. 

Other Selhf- ^ -/^_ ^ ^(Ô (D 

11 Î i!: p1 1 ) 1 1 

E^ ^ _I +':13 :.!>

V 

CG 

C7 

Client Sample Screening; Results 

l3-,Igor-98 

QDanlerra Envi ronment Se rv ices, SCP V2.03 

(F-ji ,Î1Î1^' 

LIEN F( ME, 11) MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPAIA CNTSU NETCP111B 

Bill 130N687 3/12/1998 QUAD2IA 3/12/199811:01:02 AM BON687 30 7 0.18 74 1.54 

uQIOD Bke: 3/12/199812x01:04 AM BKG 600 32 0.05333333 556 0.9266667 

Aid Dale: 3/12/1998 'ru(Sa,Aly; IOOE100 I.00Ei00 Alp; (Dpad 8. 39E-01 (uCV 3.78E-04 (pCl/ 3.78E)02 ±3.9Et02 CAT6.6E-02 Lab 

Ppl me: 49.6 Ihdb: L nd Bet; Alq); 3.27E400 Sa); 1.48):03 Lie): I48EiO3 ±2.SE402 I 3.4E-02 

Alq 

IAg 

1


12-A1ar-98 

(3d EN "I'CODE 11) MATRIX RECEIVED BET ECI'Olt ACQ BATE SAMPLE MINUTES CNTSA NETCPNIA CNTSB NETCPMB 

PGW BON01 1 9 3 1 12/1998 QUAD2 1 B 3/12/199811:01:02 AA1 BON0119 ---- _ 30 5 0.105 155 42733333 

LIQUID Bbe: 3/12/1998 12:01:04 AM BKO 600 37 0.06166667 536 01933333 

Aul Date: 3/12/1998 Tut Sa, Alq: 1.60E+0I I . 00Ei OI Alp; (Dpad 2.08E -0 1 (uCV 1 . 50E -04 (pCV 9 .36E+00 ± 2. 3Ei01 CAT 2 .7Ei00 Lab 

1-p1mt: 7. 4 ml Bel; Alq): 8.31E+00 Sal: 5.99E-03 1.18): 3.74 E+02 f 3.7Ef01 I ^ 1.3E -0 I 

P(iW BONOJO 3/12/1998 QUAD2IC 3/12/19981LO1.02AM BONOJO 30 7 0.18833333 148 4.0233333 

LIQUID Bbt: 3/12/1998 12:01:04 AM BKG 600 27 0.045 546 0.91 

AM Dule; 3 1 12/1998 T.1 Su, Alq: 1.60E-t01 1.00E+01 Alp; (DpnV 4.81E-0 1 (uCV 3.47E-0a (p(-'I/ 2.17E101 ±23E+01 CAT 1.2Ei00 Lab 

Ppt me: 7.5 Unk.; I- ! nO Bet;Alq): 7.89E + 00 Sa); 5.69&03 I.Ie): 3.55E +02 ± 3.6E +01 I IAE-01 AIq 

PGW BONOJI 3/12/1998 QUAD2ID 3/12/199811.01:02 AM BONOJI 30 12 0.31166667 132 3.375 

1.1Quil) B4t: 3/12/1998 12:01 04 AM 11KO 600 53 0.08833333 615 1.025 

Aul Dule: 3/12/1998 To1 Sa, Alq: 160E +0I / IOOEt01 Alp; (Dpud 9 . 54E-01 (uCV 6 . 88E-04 (pCV 4 . 30E101 ± 2.7E+O1 CAT 5 . 8E -0 1 Lab 

Ppt 1nt: 8.7 - Unit.: 1 1 111 1 11,1; Alq): 6.56E+00 SO 4.731: 03 I. le): 2.96Er02 ± 3.4E+01 I 1.7E-0I AN 

PGW BONAU 

AM DUle: 3/12/1998 

Ppl mt: 2.7 

I.IQIIID 

T.1 Sa, Alq: 

hull.: 

3/12/1998 

200E+ 00 

I. 

QUAD22A 

Ilbt: 

IDOf1 OI 

al l 

3/12/199810:40:55 A61 BON-0 1 9 

3 1 12/1998 12:01:14 AM BKG 

Alp; (OpnV 431E-01 (uCV 3.SHE-05 

BeQ AI 1.65E-01 Sa : 1.48E 05 

4)1 ) 

10 

600 

( pCV 

llel: 

2 0.14666667 

32 0.05333333 

1.94Et01 ± 3AE+01 

741E+00 S 2.7E 101 

10 

519 

CAT 

1 

0.135 

0.865 

IIC 

1•le 

1 .3E100 Lab 

Alq 

6.7E 100 

1dt 

POW BON5 4 1 3/12/1998 QUAB22 11 3/12/199810: 41055 AM BON541 10 2 0.15166667 22 1.2516667 

I.IQ(IIO Bbt: 3/12/1998 12:01:14 AM BKO boo 29 004833333 569 0.9483333 

Aull).W 3 1 12/1998 1'u 1 Sa, Alq: IO01i+00 / I.00h WI Alp; (Dpud 4.34 E-01 (u('I/ 1.95E-05 (pCV 195Ef01 ±3.6E+01 CAT 1.3Ei00 Lab 

1'pt u1t; 2 Unll.: I. all Bet; Alq): 2.30E+00 Sa): 1.03E-04 1.18): 1.03E+0] ± 4.0Et01 I 4.8E-0I 

Aiq 

Idt 

POW BON585 3/12/1998 Ql1AB22C 3/12/19981OAU:55 AM BON585 10 1 004333333 14 0.4783333 

O I.IQIIID Itbt: 3/12/199912:01:14 AM BKO 600 34 005666667 553 0.9216667 

W AalD.Ie; 3/12/1998 '1.1 Sa, Alq: 2.001:100 100E-01 Alp; (Dpn) L14E-01 (u('U 1.03E-05 (pCV 5.13EfOO ±3.3Ei01 CAT / 49E+00 Lab 

PPI mg: 2 / lJnlla: I. al l llel; AI4) :) 8.68E-OI Sa : 7.82E-(15 LIt): 391E+101 ± 7.2Er01 

I 

1.3E 100 ` Iq 

4t 

1 2-Afhr-971 Quanterra Environment Se rvices, SCI' V2.03 1

CLIEN"1' CODE IB MATRIX RECEIVED 

POW BON5153 3/12/1998 

LIQUID 

And UWe: 3/12/1998 To( So, Alq: 2.00E+00 

Ppl n, g: 3.7 (Inlly: I. 

(') •Al212N 

DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B 

QUAD22D 3/12/1998 10:40:55 AM BON5113 10 1 0.055 22 1.2633333 

Bkg: 3/12/199812:01:14 AM BKO 600 27 0.045 562 0.9366667 

1.00E+01 Alp; (DpnV 1.27E-01 (uCV 1.14E-05 (pC•V 5.71E+00 ±3.5E101 CAT 4AE+00 Lob 

nd Bel; AI43: 2.36E+00 Sr ) : 212E-04 1. Ig): 1.06E+02 t 4.0E+01 

I • i 

4.7E-01 

Alq 

1.11 

PGW 11ON589 3/121998 QUAD23A 3/12/199811:01.05 AM BON589 30 11 0.33166667 51 0.81 

LIQUID Bkg: 3/121199812:01:20 AM BKO 600 21 0,035 534 0.89 

And Dute: 3/12/1998 Tot Se, Alq: 2.00E+00 1.00E+0I Alp; (DpnJ 9.77E-01 (UCU 8.80E-05 (pCV 4440E+01 +2,2E+01 CAT 5.7E-01 Lob 

Pp1 ntg: 3.3 Ihdis: 1- nd Bel; Alq): 1.34E+00 So): 1.21E-04 Ljg): 6.05E+01 ± 2.0E+0I 1 8.3E-01 

POW BON5C5 3/12/1998 QIJAD238 3/12/199811:01:05 AM DON50 30 5 0.09333333 40 03516667 

LIQUID Bkg: 3/12/199512.01:20 AM BKG 600 44 0.07333333 589 0.9816667 

And Dule: 3112/1998 3'u1 Se, Alq: 200E+00 / I.00Et01 Alp; (DpnV 279E-01 (uCV 2.51E-05 (pCV 126E+01 ±2AE+01 CAT 2.OEi00 Lob 

PpI mg: 2 / Uld1r: L m1 Bel; Alq): 6.12E-01 So): 5.51E-05 LIg): 2.76E101 ± I.9Et0( 

1 

1.8E+00 Alq 

Is 

POW BON5D1 3/12/1998 QUAD23C 3/12/199811:01:03 AM BON5D1 30 13 0.38666667 49 0.725 

LIQUID Bkg: 3/1211998 12:01.20 AM BKG 600 28 0.04666667 345 0.9083333 

AW nwe: 3/12/1998 '1'u1 S., Alq: 200E+00 1.00E+01 Alp; (DpL/ 1.12E400 (uCV 1OIE-04 (pCV 5.05E+01 ±2.3E+01 CAT 5.0E-01 Lob 

1-pt mg; 2 / troll.: L / ml Bel; Alq): 1.17E+00 Se): 1.06E-04 LIg): 5.28E +01 12.0E+01 

1 

9.5E-01 

Alq 

1-Ig 

PGW BON6i9 3/12/1998 QUAD23D 3/12/199811:01:05 AM BON61;9 30 8 0.21333333 32 0.1533333 

LIQUID Bkg: 3/12/1998 12:01:20 AM BKG 600 32 0.05333333 548 0.9133333 

Ant Dole; 3/12/1998 'IWS.,Alq: IOOE+00 LOOE101 Alp; (I)pm/ 6.29E-01 (uCV 2.83E-05 (pCV 2.83E+01 ±2.IEt01 CAT 8.8E-01 Lob 

Pp1 m g; 0 1 Una; ll 

1- ml Bel; Alq): 1.54E-01 So): 6.94E-06 LIg): 6.94E+00 ± 1.6E+01 I 7.2E+00 

PGW BON6110 3/12/1998 

LIQUID 

Aid D.1,; 3/12/1998 1n1 S., Alq: I.VV1.100 

CJ PlIt mg: 0 Unit.; L 

G 

QUAD24A 3/12/199811:00:58 AM BON6110 30 4 0.06833333 36 03416667 

Bkg: 3/12/199812:01:08 AM BKG 600 39 0.065 575 0.9583333 

1.000+01 Alp; (Dp / 2.046:-0I (tICV 9.20E-06 (pCV 9.20EWO ±21Et01 CAT 2.7E+00 Lob 

nd Bel; Alq): 4.29E-01 So): 1.93E-05 I.Ig): 1.93E+01 ± I_SEW) 

1 

2.6E/00 Alq 

LIg 

12-A/nr-98 Quanterra Environment Services, SCP V2.03 ? 

mq 

Ids 

A19 

LIg

uuanterra march ca, ivvo uo:ur pm 

n 


11 11 

Master Sample Login: 17203 ^Q.n is r1q 

".1, 

Pr ject Manager: U. Price ^^ 

Fp4 o t 

Draft: Fine L- Entered and Reviewed by: PM Review: 


Sample No. Client ID C-Matrix Date: Collected Received Due Shipper Red Category Red Sample MD... 

Cements:. 

# Container Type Analysis Class Preservative Anal. Due Date Hold Date Site (Container Nudaers:% Filled) 1 1^ ?-I ^S 

Data: W 

17203-001 BON688 Sot id 12-MAR-98 09:15 12-MAR-98 13:53 01-APR-98 AIRBORNE Screening note. Required 

RICHLAND I.D. 80322101//ICAPT = PH ONLY///PCB r S = AROCLOR - 1254///THIS SAMPLE MUST BE FILTERED TO CREATE FILTRATE SAMPLE 17203-004. 

1 PH - Plastic-1 1 - HG/7471/g4 S COLD 26-MAR-98 09-APR-98 R108 (364154¢99) . 



17203-002 BON689 Solid 12-MAR-98 13:15 12-MAR-98 14:30 01-APR-98 AIRBORNE. 3 R7043.001 

RICHLAND I.D. 80322102//THIS SAMPLE MUST BE FILTERED TO CREATE A FILTRATE SAMPLE (17203-003).ICAPT =.PB ONLY///PCB r S = AROCLOR - 1254. 

1 PH - Plastic-1 1 - H 61 7471/g4 S COLD 26-MAR-98 09-APR-96 R108. (364155:99) 

1 ICAPT/6010/04 S COLD 26-MAR-98 08-SEP-98 R10B (364155:99) 


17203-003 BON897 Liquid 12-MAR-98 13:15 12-MAR-98 14:30 01-APR-98 AIRBORNE 1. Screening not Required 

RICHLAND I.D. 80324101//ICAPT = P8 ONLY//AROCLOR 1254 ONLY///USE THIS EMPTY BOTTLE FOR FILTRATE FROM SAMPLE 17203-002. 

1 PN - Plastic-IL HG/7470/04 S COLD 26-MAR-98 09-APR-98 RIOS (364325;99) 

1 ICAPT/6010/04 S COLD 26-MAR-98 08-SEP-98 R10B (364325:99) ^.VO L L 

_a 

b11 


17203-004 BON688 FILTRATE Liquid -. 12-MAR-98 09:15 12-MAR-98 14:30 01-APR-98 AIRBORNE 1 Screening not'; Required. 

RICHLAND I.D. 80322101///USETHIS EMPTY BOTTLE FOR ` FILTRATE FROM SAMPLE 17203.00 1. 

1 PN - Plastic- 1 1. HOLD//04 S COLD 26-MAR-98 22-MAR-98 R108: (365376:99) 

r-. 

._ l 

CG 

3 . 4$amipte has not been rad screened. 

Page 1

Chain of 


QUA 4124 0797 

S1 ^ N_^` 1) 

Client ^ ^ Project Manager ^ ^ Date _ ^ ^7 

Address Telephone Number (Area Code)/ ax Number Lab Number 

City State Zip Cotle Site Contact Lab Contact 

Pooled Name /"^ r/ /' f- ^-^ ^ ^ 

I(' 

/fi 

Contract Purchase Order/Quote No 

` Sample 1. D. No. and Description 

(Confamen for each sample maybe combined on one line) 

C/^/^//A 

Date Time 

^ I C^ ^° '7 C'^^l In ^ 

CarrienWaybill Number 

Matrix 

gg 

g 

a m y j 

y 

= 

Containers & 

Preservatives 

"o 

i = 

o 

2 

ô 

^' 

u Q L (/tl (1JC 

Analysis (A ttach list if 

mores ace is needed 

Qiûanterra 

Chain of Custody Numb 

I I 

Page 1 of 1^ 



tòss,ole Hazard lde identification I Saprple Disposal 

—t^ DC1J 

1t^l ^ Non 

lee may be assessed it samples are retamed 

q Non Hazard q Flamma ble [ImSk Initanf q Poison B Unknown 1 Be(,, Return , To Client q Disposal By Lab q Archive For Months longer than 3 months) 

Tum Around Time Required OC Requirements (Specify) 

q 4 Hnprs q 45 Hours q T Days q 14 Days W, 

..._....^ _.. _r 

C`) 

I Days q 

Olhor I 

L^ 

1. Received By 

.... ..,, .. r 

eLnquuhed By IDate 

Time 3. Received By 

DISTRIBUTION WHITE Stays with the Sample. CANARY - Returned to Client with Report; PINK - Field Copy 

0 too 

Date I Time 

^..

Bechtel HanforJ Inc. CHAIN OF CUSTODY/SAMI'Lle ANALYSIS REQUEST' 119A ^ 111 • 1•"e I d I 

Collector longsanp ('onlaC( 'Velephone Nu, Project Coordlnalor Ilala 'Fonurnund 

R. Foblbcrg 

Project D esignation 

105 .0 Phase 1 k Phase 11 - Concrete Samples 

Steve Marskc 

SamplingLocation 

100 Area 

1373-4316 

- 

WEISS, RI. 

SAF Nn. 

IIUR-11(/-g 

21 Days 

let Chest No. Field Logbou l, No. Method of Shipment 

.133 _Z (land deliver 

Mpped'i a 

Quanlerra Incorporated 

Ilfraile 1•roprrly Nu. But of L..il It1A Ir 11111 Nu. 

•OSSIIII.E SAMPLE IIA%ARDS110:141ARKS 

RWltsacllve 

1're.ervalnn 

7)penf Conbiner 

N"ne 

P 

Special Ilandling and/or Storage 

1/ 

7(03^^' ► L/1`-

^^^ tr al 

Restoration Reatoratlon 

Team 

CCN: 055088 

Jo ^ IItn 

Contractor %.0W "^^"'r 

Interoffice Memorandum aI{y W 

TP D.A. St, Jahn 1.0-19 sac February 27.19% 

Cnrua! 

Scr Below pp1t S. Lîôw 

Ra dCun Eagim coat 

)C,-41/531 -0700 

suaaacr: CURIF. FSTIMATE FOR 51i1PPLN000lWRETE CORE SAMPLES 

W r 

IIÔrr 

The rullowing calculations show that cue somplawiih a direct reading of equal to ur lesis lhaa 

400.Uou dpm/1 o0em r will be below the definitiaoafrar liu=tivc material as defined in 49 CFR 173.40 

of 70 Bq/g (2>; pCi/g). Lath sample will cunsistof cm=ctc material from ruur. two inch ton 

samples and enough water to ma4 a shiny constancy. *Me distribution of radionuclides is bar d tin 

previous concrete samples Ld= fmm the belowgrr)e Ferl Storage Basin that would also Ix: 

Nprescntative of these cuncrae samples 

iver, 

Cylinder Vulunie nth Radius of cwa= core (r) = I inch 

Concrete Density = 2.35 g/cm 116ght of mwswoc taken (h ) - U15 inches 

27 pCi = Dq 

2?2 dprn = pCi 

Mxdmtun di nt among on tort = 400.000 dpr. 3 :UUcm 

Calculations: 

V - (.-,. 1 4) (1 in.) '(U 25 in) = 0.78 m' (16.4 cm%'iu1 (4 am: samples) = 511 cm' 

(400.000 dpm/51.2 cm) (cm'2.35 g) = 3-32E3 dp dg 

3.320 dp rn/g (pCi2 2 dpm) = 1SE3 pCi/g or 514 kg 

51.W:dld 

Percent D'tstribution(V Cotmeration (VO/F.1 

,.I Cc 

0.17 255 pCV9 

137 Cs 

82 1 m pCi/g 

132 E 0.33 4.95 PU3 

"'Eu 0.05 7.5E-1 PCi/g 

"'Sr 17 2.55E2 pCi/g 

741 Ain 

' 

0.005 7.5F.-2 pCi/g 

3 91tie'Pa 0.1 1.5 .J 

(te n its: 

S. (J. Marske X5-53 


RadCun Engineering File!LB XO 23 

floeumcnt and Into Services 110-09 

TOTAL: 1.460 PCi/g

t e, 

CIO 

RFSH-SOW-93-0003 - 

rJRevision 5 

Figu re 1 

SAMPLE CHECKA LIST 

Dat&Mme Received ! `1 r) Mt .. ()Oa).29' 

Work Order Number. bU3., I v^4a SAF #- _((^ 

Shipping Cbntainer ID: w Chain atCustody I wIk-Q(^ / - /G 

1. Custody Seals on shipping contanrr intact? Yes I l 

2. Custody Seals dated and signed? Yes [ No (1 

3. Chain-d-Cuddy rec ord present? Yes No I 1 

• e ^ 

4. Cooler terrmperatore 

5. Vermicufdelpadcrg materials is Wet [ j C ry 13 

6. Number of samples in shipping cmtainer. 1 

7. Sample holding fines exceeded? Yes [ J No ( j 

F Sa leshave 

custody seals 

hazard labels 

,appropriate sample labels 

9. -e6mples are: 

in good otindi5on 

leaking 

broken have air bubbles 

10. Where any anomalies identified in sample receipt? Yes (J No 

11. Description of anoma lies (include sample numbers):


13-Mar-98 

CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPAIA CNTSB NETCPIIIB 

Bill BON688 3/13/1998 QUAD2IA 3/131199810:21:17 AM BON689 30 9 0.241428 $7 57 0.96 

LIQUID Bkp 3 1 13/1998 1:30:18 AM 13KG 7110 41 0.05857143 638 094 

An[ Dole: 3/13/1998 Tot Sa, Atilt 1.00E+00 , 1.00E+00 Alp; (Dpnd 1.21E+00 (uCV 3.43E-04 (pCl/ 5.43E402 ±4.1 E+02 CAT 4.6E-02 Lab 

Pplmp 31.3 Unitas L n11 Bell Alq): 1.98E+00 Sap 8.94E-04 Leg): 8.94E+02 12.5E+02 I / 3.6E-02 Al" 

/ Bill DON689 3/13/1998 QUAD2 1 B 3/13/199810:21:17 AM BON689 30 661 21.9790476 47333 1576.8733 

(?On I gq '7 LIQUID Bkgt 3/13/19981:30: 18 AM BKO 700 38 0.03428371 672 0.96 

Anl Datat 3/13/1998 T04 list, Algd 1.00E+00 , 1.00E+00 Alp; (Dpnt/ 2.196401 (uCV 9.84E-03 (pCl/ 9,84E+03 18.3E402 CAT 2.5E-03 Lab 

Ppt mg: 30 / Unlbt L /, ml Bet; Alg )j 3.30E403 Sap 1.49E+00 Leg): 1.49E406 ±6.8E103 

III / 

3.4E-09, 

Alq 

Ids 

BIII BON733 3/13/1998 QUAD2 1 C 3/13/199810:21:17 AM DON753 30 0 -0.0371429 84 1.9037143 

SOLID Bkg: 3 1 13/1998 1:30:18 AM BKO 700 40 0.03714286 626 0.8942837 

Asst Dates 3/13/1998 Tot So. Algt 2.50E +02 , 9.77E+01 Alp; (Dpm/ -5.47E-0 1 (uCV -6.30E-04 (pCi/ -2.52E400 ± 4.8E+00 CAT 2.3E+02 Lab 

P itt mg: 97.7 / Units: g / mg Bet; Alq): 4.30E+00 So): 4.96E-03 Leg): 1.98E+01 ± 3.2 E+00 

I 

/ 3.0E+00 Alq 

ug 

BII( DON754 3/13/1998 QUAD2 1 D 3/13/199810:21:17 AM 13ON754 30 8 0.20666667 77 1.4709524 

SOLID Bkg: 3/13/19981:30:18 AM BKO 700 42 0.06 767 1.0937143 

And Dole: 3/13/1998 Tot Sa, Alq: 2.50E+02 Alp; (Dpm/ 1.31E+00 (uCV 1.34E-03 (pCl/ 6.16E+00 ±5.6E+00 CAT SJE400 Lab 

Fist Mgt 96 Un11at g , mg Bet; Alq): 3.19E+00 So): 3.74E-03 Llg)t 1.49E+01 ±3.1 E+00 

I / 

6.7E+00 

a` 

Bill 13ON753 3/13/1998 QUAD22A 3/13/1998 10:21:21 AM BON753 30 3 0.05571429 70 1.4004762 

SOLID Bkes 3/13/1998100:26 AM BKO 700 31 0.04428371 633 0.9328571 

Aid Dates 3/13/1 Tot So, Alq: 2.50E+02 / 9.61E+01 Alp; (Blind 2.80E-0 1 (uCV 3.2SE44 (pCl/ 1.31E+00 14.3E+00 CAT^ 3.8E+01 

Ppt mgt 96.1 holds g 

mg Bet; Alq)s 2.98E+00 So): 3.50E-03 Leg): 1.40E+01 3 2.8E+00 

7.2E+00 

La Alit 

I Ig 

BIII BON736 3/13/1998 QUA1322B 3/13/1998 10:21:21 AM BON756 30 S 0.20952381 66 1.2314286 

C AN Dates 3/13/1998 

SOLID 

Tot Sa, Alq: 2.30E+02 

Bkg: 

9.73E+0( 

3/13/1998 1:30:26 AM BKO 

Alp; (Dpnd 1.32 E+00 (uCV 1.53E-0 3 

700 

(pCl/ 

40 0.05714286 

6.12E+00 ±5.OE+00 

678 

CAT 

0.9685714 

8.2E400 Lab 

G 

Nip 

P itt mg: 97.3 / Units: g / , mg Bel; Alq): 2.57E+00 So): 2.97E-0 3 144): 1.19E+01 ± 2.8E+00 

I / 

8.4E+00 

Adg 

Lle 

M 

I3-Mar-98 Quanlerra Environment Se rvices, SCP V2.03 I

Project Manager: U. Price 

wuanterra March 18, 1YYB 1(i am 



^/'^J ((^^ 

Draft: ina L Entered and Reviewed by: C5 PM Review: (y Qom_ ^ L^ 


Sample No. Client ID C-Matrix Date: Collected Received Due Shipper Red Category Red Sample No. 

Comments 

p Container Type Analysis Class Preservative Anal. Due Date Hold Date Site (Container Numbers:% Filled) 

Data: 

17221-001 BON690 Solid 13-MAR-98 08:15 13-MAR-98 10:35 OZ-APR -96 AIRBORNE 1 Screening not Required 

RICHLAND I.D. 80324301//ICAPT = P8 ONLY//AROCLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17223 .003. 

1 PN - Plastic-1L HG/7471/Q4 S COLD 27-MAR-98 10-APR-98 R10A (364654:99) 

1 ICAPT/6010/04 S COLD 27-MAR-98 09-SEP-98 R10A (364654:99) 

1 PCB/8080/04 S COLD 27-MAR-98 27-MAR-98 R10A (364654:99) 

17221-002 BON691 Solid 13-MAR-98 09:00 13-MAR-98 10:35 02-APR-98 AIRBORNE 1 Screening not Required 

RICHLAND I.D. 80324302//ICAPT = P8 ONLY//AROCLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17221.004. 

1 PH - Plastic-1 1- HG/7471/Q4 S COLD 27-MAR-98 10-APR-98 R10A (364655:99) 

1 ICAPT/6010/Q4 S COLD 27-MAR-98 09-SEP-98 R10A (364655:99) 


17221-003 BON690 FILTRATE Liquid 13-MAR-98 08:15 13-MAR-98 10:35 02-APR-98 AIRBORNE 1 Screening not Required 

RICHLAND I.D. 80324301. 

1 PN - Plastic-1 1- HOLD//04 5 COLD 27-MAR-98 23-MAR-98 R10A (364656:99) 

17221-004 BON691 FILTRATE Liquid 13-MAR-98 09:00 13-MAR-98 10:35 02-APR-98 AIRBORNE 1 Screening not Required 

RICHLAND I.D. 80324302, - 

C. 

1 PN - Plastic-1 1E HOLD//04 B COLD 27-MAR-98 23-MAR-98 R10A (364657:99) 

^ l 

G 

G7 

3 •= Sample has not been Pad screened. 

Page 1 

O 

^d 

Z ^.^

Chain of 


QUA 4124 0]9] 

/^ o —r e-r" r Y 

C^ 

iiivanterra 

Clienl Project Manager Date Chain of Custody Numb 

101143 


City 

Project Name^^ 

C 

Slate Zip Code 

/^ (399 -(X p 

Site Contact 

Carrie rrWaybill Number 

Lab Contact 

Conlrac0'Purchase Order/Quote No 

Matrix 

Containers & 

preservatives 

Sample I. D. No and Description 

(Conlaviers for each sample may be combined oil line) 

Date Time 

e vi 9i 

v 8 

2 i 2 

°° a? 

to Analysis ace 

(Attach list if 

is needed 

Page of 



Possible Hazard Identilication 

q Nom Haza rd q Flam mable q Skin Irmant q Poison B Unknown 

a ple Disposal 

Return To Chem El Disposal By Lab El Arch,,, For Months 

(A lee may be assessed if samples are retained 

longer than 3 months) 

L-Jyrm Around Time Required -- OC Requirements (Specify) - c 

VR 

urs q 48 Hours q 7 Days q 14 Days 21 Days q Other 

uisDale 

5 

ished By Date 

Time 

Time 

I- Received 

eceived B 

l // i` ^ 

D to 

9-17-99 

Date 

Time 

Time 

i -lb 1b OD O g 2-0 

3. Relmgmshed By Dale Time 3. Rererved By Date Time 

Commonly 

DISTRIBUTION: WHITE Slays with the Sa 1pir. CANARY - Relurned to Client with Repo rt ; PINK - Field Copy

Bechtel Hanford Inc. CHAIN Or CUSTODY/SAMPLE ANALYSIS, REQUEST B98-061-11 fare or 

Collector "^ 

.o _c,.. 6jh"' 

pjV Ikn+ {^gsrAl 


105-C Phase I & Phase 11 - Concrete Samples 

Campion) Contact 'Telephone No. 

Steve Merskc 077-4316 

n m pling Luution 

100 Area l OS -C 1\P 4('^d 3 

Project Courdinalnr 

WIBSS, III. 

AF No. 

B98-061 

Ice Chest No. Field Logbook No. Niched of Shipment 

" L- I3U( — U7/ 

Iland deliver 

hipped'To 

Quen lcna Incorporated 

POSSIBLE SAMPLE I IAZARDS/REIIIARKS 

Radioactive 

Special I landling and/or Storage 


1Rdte Property Na. 

w 1l 

Preservatlon 

None 


NB. of Coniainer(s) ( 

Volume 

S!X G()/ s^ 

/,-)h^l7 

d D3,;24^'2r- -C"w, 96 

Sample No. - 'mo nts etrix • Sample Date Sample Time 

I L 

Seelmmlll in 

i.e.(l 

In,smcli.n, 

hill of La li /Air Bill No. 

^ ^. 

Data 'I urnarouod 

21 Days 

BON690 01 Other Solid MA2g6 IS c 1XI / 

CIIAIN OF POSSESSION SIg ntPrint Names 

Rellnquidr D.N?hna Red Dala i 

p 

iaNgT+B /O J S ^/T A 

inquhhcJ BY Dete/rim. Received By OD emlfln^c 

lingwshcd BY UalJrime Received BY DatefTimc 

elinquith

CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-12 r•ae ! ar ! 

R ct 4 

Company Conracl 

Sieve 6lurske 

'I'cieplunm No. 

3734316 

project Coordinator 

wlgsS, Rl. 

Dols Turnaround 

'amplhlg Location 

AF No. 

Phase II - Concrete Samples 

100 Arca — I OS C. R e a e iuv 1199-061 

ke a. Field Logbook No. 

F—L-13U 


p I oL 

1 land deliver 

'hipped '1' t, 

Quanterr9 in corporated 

Offalle Property No. 

MA 

(fill of Lading/Air hill Nu. 

I,vA 

POSSIBLE SAMPLE IIAZARDSlREMARKS 

Rdiwaim 

'perial Handling and/or Storage 

SON691 

SAMPLE ANALYSIS 4_ 

So3a4 CkM 9o3^4 -r-« 

Semple No. 

01OR 

f10^ 

Preservation 

'type of Container 

a^^• 

Nu. or Containers) 2 

Volume 

P 

II- 

.See imm I q in 

Sp

cc* 

Environmental 

Job Vo.22172 

Restoration 

Contractor ERC Team u. c.. rw 

Interoffice Memwandum a' 1 91C 

TO D. A. St. John x.0-19 MTL Febmary 27,1999 

nru:tc 

See Below mc"' S. L. Winslow 

RadCun Engineering 

X.1-41/531-0700 

suarecr: CVIAIF FSTIMATEFOR SWPING CONCRF•TF. CORE SAMPLES 

.0 w 

Sw.^Cnr !fib 

The fulluwing calculations shoe that cure samples with a direct reading of equal to or less than 

400,000 dpm/l00cm' will be bdow the definition ofralivactive mate rial as defined in 49 CFR 173.403 

of 70 Bq/g (2F.3 pCi/g). Lachmmple will consistofcoacrete material from four, two inch co re 

samples and enough water to mAe a slurry consi s:cary. The distribution of radionuclides is bused an 

previous concrete samples wkm from the below grade Fuel Storage Basiu that would also be 


••von: 

Cylinder Volume - nrh Radius of cam= core (r) = 1 inch 

Concrete Density = 2.35 g/cm Ìleight of cure swrtple taken (h) — U.25 inches 

27 pCi = Dq Maximum d irect reading on core = 400,000 dpm/IUUcat' 

2.22 dpm = pCi 

Calculations: 

V — (3.14) (1 in.)'(0 25in) = 0-79 in' (16.4 cm `/irr) (4 cure samples) = 512 cm' 

(400.000 dpm/5 L2 cm`) (cm'235 g) = 3.32E3 dpm/g 

3.32L3 dpm/g (pCi/2.2 dpm) = 1.5 113 pCi/g or 55.4 E4'g 

SLW:dld 

Percent Distrtbation(%) Cong=ration (vCi/e ) 

"Co 0.17 235 pCi/g 

17Cs 82 13F3 pCilg 

WEu 0.33 4.95 pCi/g 

"°Eu 0.05 7.5E-1 pCi/g 

"ST 17 2.55E2 pCi/g 

241 

Ain 

Z3912 

'pu 

0.005 

0.1 

7.5F.-2 pCi/g 

1.5 - 

Co ies: 

S. 0.lvdarske X5-53 

P. A. Newman X 3-41 

RadCun Engineering File/LB X0-23 

Document and into Serv ices 130.09 

TUrAI-: 1.460, pCi/g 

(-U00049

9. 

Samp are: 

'Ries 

in good condition 

broken 

Figure t 

SAMPLE CHECK-IN LIST 

Date/rme Received: nn221 ^Y D 3 ^l srrr. 

FF 

Work Order Nurnber. & 42Z SaF # Ô -GYP 

Shipping Container 10: ru -0 ^ C^ Chain dQatody # 

leaking 

lave air bubbles 

RFSH-SOW-93-0003 

Revision 5 

1. Custody Seals on 9**g cont*w intact? Yes (q' o [ ] 

z Custody Seals dated and signed? Yes [^}'îo ( ] 

3. Chain-of-Custody record preset Yes . o [ J 


5. Vermiculite/packing materials is Wet [ ] Cry 4/(yL 

6. Number of samples in shipping container. 

7. Sample holding times exceeded? Yes [ ] No 

S. 

Samp have: 

tape _hazardbabeis 

wstody seals _apprgsafe sample labels 

10. Where any anomalies identified in sample receipt? Yes [ ] No [^ 

11. Descrip ti 

on of anomalies ( include sample n abers): 

Sample 

Telephoned To: 

r_=

C^ 

C-J 

CG 

L7 

Client Sample Screening Results 1, 

13-Mar-98 

1, 

0, 3, 10 

CLIENT CODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B 

Blll BON690 3 1 13/1998 QUAD24B 3/13/19981; 15:37 PM BON690 30 7 0.17619048 71 1.3838093 

LIQUID Rks: 3/13/1998 1:30:14 AM DKO 700 40 0.03714286 688 0.9829571 

And Date: 3/1311998 Tot Se, AIq; 1.00E+00 , 1.00E+00 Alp; (Dpm/ 3.84E-0 1 (uCV 2.63E-04 (pCl/ 2.63E+02 ± 2.6E+02 CAT 9.3E-02 Lab 

Ppl mp 13.5 Units: L ml Bet; AIq): 2.64E+00 So): 1.19E-03 I 48): 1.19E+03 ± 2.5E+02 I / 4.2E-02 AIq 

BHI 13ON691 3/13/1988 QUAD24C 3 1 1311998 1:15:37 PM SON691 30 2 0.00666667 30 -0.002857 

LIQUID BkSs 3 1 13/1998 1:30:14 AM BKO 700 42 0.06 702 1.0028571 

AM Dale: 3/13/1998 Tot So. Alq: I.00E+00 1.00E+00 Alp; (Dpm/ 2.02E-02 (uCV 9.12E-06 (pCV 9.12E+00 ± 2.0E+02 CAT 2.7E+00 Lab 

Pptm8: 1.5 / Uatta: L / , ml Bel; Alq); -9.36E-03 Saj: -4.21 E-06 L f8): 4.21E+00 ± 1.6E+02 I / 1.0E+00 AIq 

Lis 

13-Afar-98 Quanterra Environment Se rvices, SCP V2.O3 / 

1.18

(Ruanterra G w ^- 5L 014514 

EoAroommtar 

sermw 

Condition Upon Re ce 

ipt Variance Repo rt 


Client. rì ^}6 Date: 

Login No.: 

7 

? — 1 / " U Time: 

Project No: Initiated by: 

Shipper/No: 9 3 5 2 2- 1 1 RFA/COC Numbers: ^^^/[/ 7 

ConditionNari ce (Check all that apply): 

L q Sample received broken/leaking. S. q Sample 0) on container does not match sample ID 

3. q Sample received without proper prese rv ative. on paperwork. Explain: 

q Cooler tempera ture not within 4°C --- ?•C 

Record tempera ture: 

q pH 9. q All coolers on airbill not received with shipment. 

q other. 10. q Other (explain below) 

3. q Sample received in improper container. 

4. q Sample received without proper paperwork. Explain: 


6. q No sample ID on sample container. 

7. q Custody tape dis turbed/broken/missing. 

—@'- No variances were noted during sample receipt. Cooler Temperature Upon Receipt: yr^- 

Notes: 

Corrective .action: 

q Client's Name: Informed verbally on: By: 

q Client's Name: Informed in writin g on: BV: 

q Sample(s) processed 'as is". 

q Sample(s) on hold until: f released. noufv: 

\ 

-7 g I, 

Sample Control Supe rv isor Review: or desi gnate) I cc : 37 — [ / _ 

Project Mana gement Review: 7\ t—L— 

SL-ADMIN-0003. Revised :1!'_4/95 

q 

Date: 3 — ^ I --v 

SIGNED ORIGINAL MUST BE RETAINED IN THE PROJECT FILE

Q'Auanterra 014501 

Condition Upon Receipt Variance Report 


Client: t/GC'^ Date: 3 — 7 , `! 

Project No: 5250 -2(G 6 Initiated by: o-. A-Pi 

Shipper/No: RF VCOC Numbers: /7 0 C sL 

Condition/Variance (Check all that apply): 

'1 

Login No.: / 72-2-/ 

I. q Sample received broken/leaking. 8. q $am pie ID on container does not match sample ID 

2. q Sample received without proper preservative. onn paperwork. Explain: 

q Cooler temperature not within 4-C t 2°C 


q pH 9. q All coolers on an-bill not received with shipment. 

q other: 10. q Other (explain below) 

3. q Sample received in improper container. 

4. g/ Sample received without proper paperwork. Explain: 


6. q No sample 1D on sample container. 

7. q Custody tape disturbed/broken/missing. 

^d No variances were noted during sample receipt Cooler Temperature Upon Receipt: 

Noes: 

Corrective Act on: t 

QÎ., (" ?3) t II ! 

q Client's [me: Informed verbally on: By: 

q Client's Name: Informed in writine on: By 

q Sample(s) processed "as is". 

q Sample(s) on hold until If released. notify 

Sample Control Supervisor Review: (or desi gnate) Date: 

Project Management Review: L— " I tN^ Date: J _ (^/ 79 

SL-AD?dIN:)004. Revised I1;--1/95 

SIGNED ORIGINAL ^',IL'ST BE RETAINED IN THE PROJECT FILE 

_-7 

tme: 

(1 00 053 

lozr

— - - --- --- - -- -- WO 2?^ s Q-- - - 

' L Qanterra Q April O8, 1998 02:33 pm 

Ac count: 10722 Project: 550.260 QunterrRichland 

a a- OAS No. 550.26 Be,, 3 


Project Manager: W. Price 

222J4 

Draft: Final: Entered and Reviewed by: S^^`^Q^, n'/^'. ^ PM Review: I/C07`^//^ 


Sample No Client ID C-Matrix Date: Collected Received Due Shipper Bad Category Rad Sample No, 

Comments 

N Container Type Analysis Class Preservative Anal. Due Data Hold Date Site (Container Numbers:& Filled) 

Data 

17224-001 BON692 Solid 16-MAR-98 08:30 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required 

RICHLAND I.D. 80327101//ICAPT = PB ONLY//AROCLOR 1254 ONLY" 

' FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECO ME S SAMPLE 17224-004. 

LJ v L 2") 

PN - Plast ,ll, HG/7471/Q4 S COLD 30-MAR-96 13-APR-98 R10A (364686:99) 

1 ICAPT/6010,'24 S COLD 30-MAR-98 12-SEP-98 R10A (364686:99) 

1 PCB/8080/Q4 c COLD 30-MAR-98 30-MAR-98 R10A ( 364686:99) 

17224-002 BONG93 Solid 16-MAR-98 09:25 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required 

RICHLAND i - D. 80327102 !; ICAPT = PB ONLY//AROCLOR 1254 ONLY/ !iFlLiER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOME S SAMPLE 17224-005. 

- IN Plastic-1L HG/1471 1I Q4 S COLD 30-MAR-98 11-APR-98 R10A (364687:99) 

1 ICAPT/6010/Q4 S COLD 30-MAR-98 12-SEP-98 RIGA (364667:99) 

1 PCB/8080/Q4 S COLD 30-MAR-98 30-MAR-98 R10A (364687:99) 

17224-003 BONG94 Solid 16-MAR-98 10:25 16-MAR-98 12:15 03-APR 4d AIRBORNE 1 Screening not Required 

RICHLAND I.D. 803271031/ SOAP: = PB ONLY,'/AROCLOR 1254 ONLY///F'ILtER AND ANALYZE SOLID PORTION ONLY, ;SQUID PORTION BECOME S SAMPLE 17224-006. 

1 IN Plastic 11, NO, 7471/Q4 COLD 30 MAR-96 13 APR 98 R10A 1364688:99) 

1 ICAPT'/a010iQ4 .. COLD 30-MAR-98 b'LP 98 R10A (364688:99) 

PCB/8 '",80;Q4 5 COLD 30-MAR-98 30 MAR-98 R101. 68 

11224-004 BJPB9b Liquid 16 MAR-9 8 08:30 16-MAR-98 12:15 03 APR 0 AIRBORNE 1 Screening noL Requilad 

RICHLAND I.D. 80327801;'1/ICAPT = PB ONLY'/AROCLOR 1254 ONL Y iTH: SAMPLE IS THE FILTRATE FROM SAMPLE 17224-001- 

. FN - 2)est 1 c- :L r 147. 04 

ICAPT 6010; Q4 _ 

COLD 

(101D 

,- APR-9n 

_)i-APR 98 1Z 

.Pp,8 R10A 

- EP -98 R10A 

1364689,99) 

1364689:99) 

1 PCB/8C80/Q4 _ COLD p1-APR-98 MAF 98 R10A !364689:991 

X 229-OJS B ON,,, FILTRATL' Liquid -6 -MA.-, , 9 25 16 Mild ,8 12 :15 ciI( ':E Ai3 BORNE 1 Screen il4 1r.. krq..0 ed 

'v 1(t `.AN: 1 327102:'/lIÂnT - . -_._!:AR 1254 ONL ..^ Âh CLe i= THE FILTRATE FROM SAM; E . 7 229 u02. 

i YL 1L 1 .- ,.ti CGLD _ -AFR-9' .,r.., od RI'A ',364690:99, W O 

: 

17224 CL6 F(N 6 94 FILTRATE L q,i7 MAR 36 10 c :6 MAN 5 F _ RBOR1; _ 

RICHLrU F 2 1 1'3"-ICAPT rP.. i ARJ( LO R 2. 4 ONL^ _..__ FP^PLE 1 5 THE FILTRATE FROM SAMPLE 2 _t3. 

O 

G 

CG 

cl( 

.R. 

1 t a, JLS .. , .., ,. „ .. RIOA i364,4, 991 

/ 

1^ 

( V 

-2 

t 

t^^^ 

Sc eeci^y n t kequll^d 

L e ) S 

) 

V '/ 

7 1^ Y-0

Dr a f tM 

W. Price 

Quanterra April 13, 1998 10:36 am 

Account: 10722 Project: 550.260 Ouanterre-Richland OAS No. 550.26 Rev. 3^^^ 

Master Sample Login: 

Our" 

'îfr^ 

D ref t: Final Entered and Reviewed by: 

PM Review: ^s^fA 

Samp le Header Template: 

1722224777 

^^y^—in 

1. 

Q'"A lye r^0i^" 

Semple No. Client ID C-Matrix Date: Collected Received Due Shipper Red Category Rad Sample No. 

Comments 

N Container Type Analysis Class Preservative Anal. Due Date Hold Date Site (Container Numbers:% Filled) 

Data: 

17224-001 SON692 Solid 16-MAR-98 08:30 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required 

RICHLAND I.D. 80327101//ICAPT = PB ONLY//AROCLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17224-004. 

1 PN - Plastic-1 1. HG/7471/Q4 S COLD 30-MAR-98 13-APR-98 R10A (364686:99) 



1 PM/IT/Q4 S COLD 30-MAR-98 12-SEP-98 R10A (364686:99) 

17224-002 BON693 soLid 16-MAR-98 09:25 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required 

RICHLAND I.D. 80327102//ICAPT = PS ONLY//AROCLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17224.005. 

1 PN - Plastic- 11 HG/7471/Q4 S COLD 30-MAR-98 13-APR-98 R10A (364687:99) 


1 PCBi8080/Q4 S COLD 30-MAR-98 30-MAR-98 R10A (364687:99) 

1 PM/IT/04 S COLD 30-MAR-98 12-SEP-98 R10A (364687:99) 

17224-003 DON694 Solid 16-MAR-98 10:25 16-MAR-9812:15 03-APR-98 AIRBORNE 1 Screening not Required 

RICHLAND I.D. 80327103//ICAPT = PB ONLY//AROLLOR 1254 ONLY///FILTER AND ANALYZE SOLID PORTION ONLY, LIQUID PORTION BECOMES SAMPLE 17224.006. 

1 PN - Plastic-1L HG/7471/04 S COLD 30-MAR-98 13-APR-98 RIUA (364688:99) 


1 PCB/8080/04 S COLD 30-MAR-98 30-MAR-98 RiOA (364688:99) 

1 PM/IT/Q4 S COLD 30-MAR-98 12-SEP-98 R10A (364688:99) 

17224-004 BOB898 Liquid 16-MAR-98 DB:30 16- 14AR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required 

RICHLAND I.D. 80327801///ICAPT = P8 ONLY//AROCLOR 1254 ONLY///THIS SAMPLE I $ THE FILTRATE FROM SAMPLE 17224-001. W02281 

1 PN - Plastic-IL HG/747D/Q4 S COLD 01-APR-98 13-APR-98 R10A (364689:99) 

1 ICAPT/6010/04 S COLD 01-APR-98 12-SEP-98 R10A (364689:99) 

1 PCB/8080/04 S COLD 01-APR-98 23-MAR-98 R10A (364689:99) 

17224-005 0ON693 FILTRATE Liquid 16-MAR-98 09:25 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required 

RICHLAND J.D. 803271021//ICAPT = PB ONLY//AROCLOR 1254 ONLY///THIS SAMPLE IS THE FILTRATE FROM SAMPLE 17224-002. 

1 PN - Plastic-11. HOLD//04 S COLD 01-APR-98 26-MAR-98 R10A (364690:99) 

( .-17224-006 BON694 FILTRATE Liquid 16-MAR-98 10:25 16-MAR-98 12:15 03-APR-98 AIRBORNE 1 Screening not Required 

C-., RICHLAND I.D. 80327103///ICAPT = PB ONLY//AROCLOR 1254 ONLY///THIS SAMPLE IS THE FILTRATE FROM SAMPLE 17224-003. 

J 1 PN - Plestic-1 1. HOLD//04 S COLD 01-APR-98 26-MAR-98 R10A (364691:99) 

Ci 

LI 

UI 

3-=Sample has not been cad acreened. 

Page 1

Chain of 


QUA 4124 07 97 

S i Io 

L't LO 10"banterra 

Client 

d , _. 

'lfXn^'l n Project Manager Oaf I ^— 

C 

Address Telephone Number (Area Code) Fax Number Lab Number 

City State Zip Code Site Contact Lab Contact 

Project Name 

Contract'Purchase Order/Quote Noo - 

Sample I.D. No and Description 

(Containers for each sample may be combined i on one line) 

7 V l 1^ 

^2 3 

VI 

- 

— / n / CarrierlWaybill Number 

Date Time 

Matrix 

gg 

3 E - 3 a 

Containers 8 

Preservatives 

° 

i o 6 ô 

N i 

Analysis 

more s ce 

(Attach list if 

is needed 

Chain of Custody Numb P,t 

1 o - 

Page of 



P >a, 

(A lee may beetl if samples are retained 

El No,, Hazard q Flammable q Sbn Irnlan( L1 Poison B Vonknowi, Return To Client El Disposal By Lab q Archive For Months longer than 3 months) 

Turn Around Time Required OC Requirements (Specilyr 

q 24 tVrirs q 48 Hours q / Days q 14 Days y21 Days q Other 

in uished Date Tema 1. Re ed By s Date Time 

`-- 2. Relinquished By Dale Time 2 Received By Date Time 

- J 

R ^.^n uished q BY ^ Dale f Time — 3. Received BY 

I Dale I Time 

GominenR 

DISTRIBUTION: WHITE - Slays with the Switch,, CANARY - Returned 10 Client with Report PINK - Field Copy 

1 

4 6

Chain of 


OIIA- Al 24 n>G] 

loo [D 

Client Prolecl Manager 

c^ 

Dat 

3111- 9 

Address Telephone Number (Area Code) Number Lab Number 

City Zip Code Site Contact Lab Contact 

Project Name 

^^,y ^' (/ 

L^r I I 

C 

^" 

ContrectPurchase OrderlQuote No 

Sample 1. D. No. and Description 

Coma, ners for each sample maybe combined on one line) 

^ 

CarriegWaybill Number 

Matrix 

Date Time °m - o = 

Containers 8 

Preservatives 

ei 

OX, 

= 

0 30 m 

Analysis 

more spa 

r 

(A ttach list A 

is needed 

CO"'banterrla 

Chain or Custody NumbC( 

11 0450 

Page ^ of 



rossore nezam Idenuncanon 

q NonHaeard q Flammable El Skin Initant El Poison B nknuwn 

a' nPie "bposai 

Return To Client El Disposal By Lab El Archive For Months 

(A lee me 

longer fh n 3 

ssessed if samples are retained 

onths) 

Turn Around Time Regmree OC Requirements (Specify) /// 

q 4 Hours 

in quishe 

P.^ 

q 4 8 Hours El Days El 14 Days 21 Days q Other 

D e 

1 3 

T 

l 66 

Received By 

w ^^D / 

Date 

1 

1190quished By Date Hme 2 Hecervad fly 

C 

Âelingwshed By Date Time 3. Received By 

Commerns 

DISTRIBUTION: WHITE Slays mIh Ibo Sarnple. CANARY -Returned to 

1 

Time 

— —_ — I Date I Time

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUE'S1' B98- 061 -16 rase ! "' ! 

ollector^5/ Q4r.4 ., ,/ / 

KAIU f 

Company C'nnlecl 'I'tlrydmnr No. 

Steve Mnrskc ,171-4114 

Project Coordlnalur 

WP]SS, R1, 

Project D esignallon unpling Location 'AP Nn. 

105C Pha se I & Phase 11 - Concrete Samples 100 Area 1598-001 

Ire Cheat No. Field Logbook No. Method of Shipment 

I land deliver 

Shipped To 

Quanlcr ts Incorpo rated 

Offailc Property No. 15111 ur Ladin g/Air 0111 No. 

POSSIBLE SAMPLE IIA7ARDS/REMARKS 

Radlosclive 

Preservation 

"""• 



I y'pe of Con tamer 

Nu. o(l'0nleiner ( s) 

volume 

S06- tooa^7S 

IL 

S. in 

sr«id 

momuiom 

Data 'Turnaround 

21 D21yS 

^03a I CIS m gD3^ r1 (Zc^c< 

Sample No. Matrix • Sample Dale Sample Time 1 

I' os•...'•' j '^V 

^•^.. 

1. O 2 Other Solid 3 -/6-^8 (^ 3 -^ e, o - 

SPECIAL INS"TRIK-1 IONS 

CIIAIN OF POSSESSION Sign/Print Names 

(II ICI• MeW,-6010A (S.patmce) 11.< ad), hlercwy-7471 (CV), C1. ....mm Ilse 7196, 

di 

Q.e , 

Relinquished By 

Dats?ims 

^6 f{A ?9>3 /2 / S 

Ualdfime 

R e By 

Recei) ve Y Î 

imc 

` 

Uale imc 

I'CBs,1080(Aivd,)rr 12541, Gainu Spccouv

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST 1198- 11 61 - Id 

ollector 

Q C.hlh.r 

Project Designalian 

3 ^N 

ompany Contact 

' Steve Marske 


'Telephone No. 

373-41IG 


wl;lSS, fit- 

'AF No. 

Dalo Turnaround 

2I 

105 -C Phase 1 & Phase II - Concrete Samples 100 Area 1198-061 

fee Chest No. Field Logbook No. Method of Shipment 

I land deliver 

'hipped To Offsinr Properly No. Rill of Lading/Air Dill No. 

Qulnterra Incorporated 

POSSIBLE SAMPLE IIAZARDS/RERIARKS 

Radloacdn 

Special Ilandling and/or Storage 


1'reservalloo 

7 ype of Container 

Nn. of Container(s) 

g o3 ^1 I G^-t r -, g o3aâ P-6,d 

Sample No Matrix • Sample Date Sample Timc 

"""• 

Volume IL 

P 

2 

See item (1) In 

Speaid 

Inanu,"on. - 

ON693 Q 2 Other Solid _ 6 _ O Ja — ( /^ 

Clit OFP SSfS ON Sign/Print Names - ( 1) ICP McUk - 6010A (Supunace) 11 cadl. Mercury - 7471 -(CV), Chrommm Ilex - 7196, 

el 'uis By DaIHTime 

iengte 98 S 

R B' Uale i c 

Relinquished BY Date/filne Received BY (N,L 7ale/iinle 

(CLY 1 

Rflinquidled By Daldllnm Received By Damn nm 

^rilrf^JVi-79' /V rC(Cel-(a3 •Y= S ^1, 90- TdfLiSr' echnei,'uwt 99 Cûbo l c /` 

J h ^ ^/ / 3-,-” 

l 

Days 

. 

SPECIAL INS I'BUCI IONS Man, , 

PCBs - 8080 (Aunt., -1254 ) , Gamma 5penmscopy ICevum-137, Coha 11-60, Europium-152, 

Europium-154, Lnopwm-1551, Anmunu nr 241. Isotopic Plulounnn; Isotopic Uranium; Sete 

5 

SL 

so 

51 

- 

- 

- 

- 

Sem,„mt 

S„ im 

Sn.Jye 

'uished By DaldGne Received By 1lale 7 lint 

1. - qwa 

Bdumn 

U, X - OiAu 

L ORATORY Received By ]ide DaldTime 

SECTION 

FINALSAMPLE Mspwd Me1hm1 Disposed By -- -- Date'lbur 

DISPOSITION 

o A 

Ps 

D1. 

- oJ1el 

11,,,,ns„nJ, 

u,,,m I,ywm

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS KEQUIsS'f B98- 061-15 " vc ! "r i 

olleclorpp p 

('nm pp ny (^nslacl 'I clephmle No. 

Mp "^^ 

A4,,4 

Steve Manske 3.73 4116 

Project Designation Sampling Location 

105-C Phase 1 k Phase II - Concrete Samples 

100 Area 

Projerl ( -uordinator 

WII ISS. Hi 

'AF No. 

1198-061 

I ce Chest No. Fi eld Logbook No. Method of Shipment 

Iland deliver 

- hipped To 

Qllmnella lncurpormcd 

POSSIBLE SAMPLE IIAZARIIS /RF-hIARKS 

Radipanive 

Special Dandling and/or Storage 


ORaile Properly No. Hill of Lading/Air (till No. 

I'rcservpllnn 

'T ) pe of ( nnialner 1 

No. of ('onldner( s) 

\'ulunm 

ô3an 1 U^ L.enti go3 a ^ 

2 

IL 

Scc non I I l m 

Strcatl 

I^'r'11e"""a 

flala I ornaruund 

Sample No Matrix a Sample Dale Sample Time ,}ÎNe s^„ u s ^, - r es 'j" r ; It r:, ., 1 ~,r f " 

BON694 03 Other Solid 

CI IN OF 'OSSFS'ION 

F 

0.el ' BIY'o Dalelfime 

/6 AtA R9B ^Z ^^ 

Relin fished B Date/ 1anc 

yrr y 

Sign/Prim Nunes 

Ra U rT r 

T214 ^- 

Received B '\ Dam/tim e 

Relui4uisheJ - By UauRirne Receircd By hale/I nne 

Inthatitoshed Ua¢fflme Recdred By Ua1ell in¢ 

LABORATORY 

SF.(TI ON 

TINA S 

-SAhIPLE 

IIISP(ISIII(1N 

Y 

SPECIAL INS I' RUC" I' IONS 

11)Is- a08 01roclor 12 5upallncc111cadlAkmup-7J]I-(CVI. Clllomiwu 111%-)196. 

Ls CB -. 154, oclnr-23J1, Gn11nnn Spenrosc'+Py IC esvum 117. Cnbah-60. burnpiva+-132, 

I:mupiuurl3J. llumpuumlSS;,An¢uamm241. lsnl upic l'Lilunmin. 11 0111,1 11 ILaniunr. Selc 

^/ ^ 

5_/e111 jU"1^ -79 / / , 

/vfC / Qy ^â / ^r 

^ ^^-f[A O /, / — /O"'rtt^ 

^ 

ec / 9 ,/(h 

y^ 

^ (/&r o/ 

- l¢' ^^ ^3 S41) 

Received By lisle Daelunc 

Dn sd Mnbod -"-- ---__-'- 

1 S UIdl uu< 

21 Days 

I 

St_ 

So 

Matrix 

s,, 

5'^. 

%Id"d 

%t. 

w 

'v 

s 

- II I.nly 

scud 

tr,l 

^ 

Il, 

UL 

- I4wn 5.IW. 

leiiio l ..p,w, 

Ripe 

1. t ignW 

v - rcra+11,.,, 

% +nnr+

CCN: 055088 

Environmental 

Job No. 22192 

Restoration 

Contractor ER^ Team o. ' MO 


7O I). A. St. John LO-19 DAM I;ebruary 27.1998 

I nPI"-5! 

* 

Scc Bclow "o"r` S. L. Winslow 


X3-41/531 40706 

suuEcT. CURT F: FSTTMATE FOR S111PP1NG (-VNCRFTF. CORE SAMPLES 

r.... w^ 

OIL"IW 

IAA ww 

Liloc . !1O 

The Following calculation show that curt: samples with a direct rending of equal to ur less than 

400.000 dpm/I0(kan = wllbcbclow the definition ofratlivactive matcrialas defined in 49 CFR 173.403 

of 70 By/g (2F3 pCi/g). L•ach sample will consist of concrete mate rial from four - two inch core 

samples and enough waterto make a slurry consisxmy. The dist ri hution of radionuclides is based tin 

previous concrete samples tak«t from the below grade Fuel Slortge Basin that would also lx; 

representative of these concede samples. 

'iven: 

Cylinder Volume - nr'h Radius ofcowxte core (r) = 1 inch 

Concrete Density = 2.35 glom' Height of cmL^s_ample taken (h) - U25 inches 

27 pC:i = Dq Maximum ilkeet reading on core = 400,000 dpm/1 UUcm' 


Calculations: 

V - (3. 14) (1 in.)'(0 25in) = 0.78 in' (16.4 cm J/irrj (4 cure samples) = 511 cm' 

(400.000 dpm/51 2 cm) (='2.35 g) = 3. 3 2E3 d;m/g 

3.32L I dpm/g (pCi2.2 dpm) = 1.5E3 pCi/g or 55.4 By/g 

SI.W:dld 

'OCo 

Percent Disr ributionMo 

0.17 

IJ7cS 82 

'uEu 

033 0 

I"Eu 0.05 

o'Sr 17 

'°'Ain 0.005 

'J91'"pu 0.1 

TOTAI-: 

Cn ics: 

S. (J. Nlarskc X5-53 

P. A, Newman X3-4 1 

RadCun Engineering File LB XO-23 

Doeumen: and Info Services 110-09 

Coetrntration (oC:i/e) 

2.55 pCi/g 

1.2F3 pCi/g 

4.95 pCi/g 

7.5E-1 pCi/g 

2.55E2 pCi/g 

7.5F.-2 pCi/g 

1.5 nCi/e 

1.4603 pCi/g

Figure 1 

SAMPLE CCK-IN LIST 

DateMme Received: l^ ^0^^^ SG#: &ZQQ7,-^ 

RFSH-SOW-93 -0003 

Revision 5 

Work Order Number. 0 ^3c^^ 0^ SAF #: - 

ShippingContainerID: -0 ChainofCustody# ' gW^J^^v 

1. Custody Seals on shipping container intact? - 

Yes [ 1 

2. Custody Seats dated and signed? Yes No [ ) 

f t^^ 

3. Chain-of-Custody record present? Yes Cij /No [ ) 


Ô 

5. Vermiculitefpaci ing mate ri 

als is Wet [ ] Dr/—{ ^^^^ 


( 

r' 

7. Sample ho&q times exceeded? Yes [ ] No (^ 

8. Samples have: 

--^Zape 

custody seals 

9. Same are: 

in good condition 

brdm 

hazard labels 

appropriate sample labels 

leaking 

have air bubbles 

10. Where any anoma lies identified in sample receipt? Yes [ I No Cl/ 

11. Descrip tion of anomalies (include sample numbers): 

Sample CustodiargUbo 

Telephoned To: 

7 

o^ 

/ 

Date: Ô/C)


17-Mar-98 


B ill BOIU10 3/17/1998 QUAD2IB 3/17/19989:38:04AM 0011110 30 11 0.32 107 16266667 

SOLID Bbg: 3/17/199812:19:30 AM BKO 600 28 0.04666667 364 0.94 

AN Dale: 3/17/1998 Tot Sa, All: 3.00E+02 , 1.02E+02 Alp; (DpM 2.10E+00 (uCV 4.66E-03 (pCU 9.33E+00 f 5. 311+00 CAT 3.4E+00 I.b 

Ppl mgs 101.6 Unita: O / , mg Bel; All): 3.73E+00 So): 1.27E-0 2 LIE): 2.34E+01 ± 3.4 11 +00 

1 ", 

3.9E+00 

All 

Bill BOHJII 3/17/1998 QUADZIC 3/17/19989:38:04AM B011111 30 13 0. 37333333 308 9.2816667 

SOLID Bbg: 3/17/199812:19:30 AM BKO 600 36 0.06 391 0.983 

Ad Dote: 3/17/1998 Tot So, Alls 3.00E+02 , 9.93E+01 Alp; (DpM 1.90E+00 (uCV 4.31E-03 (pCU 8.62E+00 f 3.4E+00 CAT 3.8E400 Lab 

PPlmgt 99.8 Unite: 8 mg Dell Alq)i 2.068+01 5.): 4.668-02 1,11)1 9.338+01 S f.98+00 1 " 1.18i U0 All 

• 1.18 

Bill B0H112 3/17/1998 QUAD2 1 D 3/17/19989:38:04AM B011112 30 12 0.34666667 212 6.1383333 

SOLID mist 3/17/1998 12:19:30 AM BKO 600 32 0.03333333 557 0.9283333 

Ad Dalai 3/17/1998 Tot Ba, Atli 3.00E+02 , 9.91E+01 Alp; (DpnJ 1.98E+00 (uCV 4.30E-03 (pCU 8.99E+00 13.4E+00 CAT 3.6E+00 Lab 

Ppl mp 99.1 i - Udb: g ^'- mg Bet; All): 1.36E+01 Sa): 3.10E-02 LIE): 6.20E+01 f 4.9E+00 1 / 1.6E+00 All 

4E 

Bill BOIU13 3/17/1998 QUAD22A 3/17/19989:38:08 AM BOIIJI3 30 1 -0.0183333 346 10.638333 

SOLID Bbg: 3/17/1998 12:19:41 A61 BKO 600 31 0.05166667 337 0493 

AM Dalai 3/17/1998 Tot So, Atilt 3.00E+02 9.87E+01 Alp; (DpM 4.95E-01 (uCV -1.81E-03 (pCU -3.63E+00 ± 4.6E+00 CAT 3.0E+02 Lab 

Ppt mg: 98.7 - U nitas g , mg Bel; Alq): 2.30E+01 So): 5.25E-02 LIE): I.03E+02 ± 6.1E+00 I 9.3E-01 

Bill 80}1114 3/17/1998 QUAD22B 3/17/19989:38:OSAb/ 0011114 30 20 0.39666667 670 21.383 

SOLID Bbg: 3/17/1998 12:19:41 AM BKO 600 42 0.07 569 0.9483333 

Ad Dotes 3/17/1998 Tod Sa, All: 3.00E+02 , 1.08E+02 Alp; (Blind 2.83E+00 (uCV 3.91E-0 3 (pCU 118E+01 f5.1E+00 CAT 4.2 E+00 Lab 

Ppt mgt 107.8 i Unites g / , mg Bell Alq): 4.74E+01 50), 9.90E-02 1-10 1.9 11 E+02 S t.0E+00 1 / 

Bill BON692 3/17/1998 QUAD22C 3/17/19989:38:08 AJ.1 BON692 30 7 0.19166667 310 9.375 

LIQUID Bbg: 3/17/1998 12:19:41 AM BKO 600 23 0.04166667 373 0.9383333 

i Ani Dote; 3/17/1998 Tot Sa, All: 1.00E+00 , 1.00E+00 Alp; (Dpnd 2.40&01 (uCV 1.08E-04 (p(V 1.08E+ 02± 1.9E+0I CAT 2.7E-0I Lob 

Ppt mg: OA Ulnas L ml Bet; All): 1.73E+01 So): 7.8,E-03 LIE); 7.81E+03 ±4.9E+02 

1 

/6AE-03 

All 

17-Mar-98 Quanlerra Environment Se rvices, SCP V2.03 / 

^3 

3.1E-0I 

All 

All 

tat

C ^' 

U :7) 

.A 

CLIENT CODE ID MATRIX RECEIVED DETECTOR % ACQ DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B 

Bill BON693 3/17/1998 QUAD22D 3/ 17/19989:38:08AM BON693 30 7 0.16166667 117 296 

LIQUID BLS: 3/17/199812:19:41 AM UKO 600 43 0.07166667 564 0.94 

AM Date: 3 1 17/1998 Tot Se, Alq: 1.00E+00 , 1.00E+00 Alp; (Dpm/ 6.55E-0I (uCV 2.95E-04 (pCl/ 2.95E+02 ±3.7E+02 CAT 8.5E-02 lab 

Ppt m8: 53.2 / Units: L ! ml Bet; Alq): 6.09E+00 Sa): 2.74E-03 40): 2.74E+0l ± 3.4E+02 I LBE-03 Alq 

LI S 

Bill BON694 3/17/1998 QUAD23A 3/17/19989:38:12 AM DON694 30 6 0.11166667 57 0.6816667 

LI 

QUID Bkg: 3/17/1998 12:19:48 AM BKO 600 53 0.08833333 611 1.0183333 

AM Date: 3/17/1998 Tot Sa, Adq: 1.00E+00 , 1.00E+00 Alp; (Dpm/ 5.45E-0 1 (uCV 2.45E-04 (pCV 2.45E+02 ± 3.8E+02 CAT LOE-0 1 Lab 

Pplmp 55.1 ./ Units: L ml Bel; Alq): 1.78E+0O Sa): 

I 

/ q 

8,02E-04 48): 9.02E402 4 2.4E+02 

6.2E-0 2 

Ill[ 

BBf BONSM6 3 1 17/1996 QUAD23B 3/17/1998 93 8:12 AM BONSM6 30 119 3.92 5799 192.32333 

LIQUID Blq: 3/171 1998 12:19:48 AM BKO 600 28 0.04666667 586 0.9766667 

Aal Dal es 3/17/1998 Tel Se, Allis 6.00E+00 , 1.006101 Alp: (Upm/ 7.45E+00 O,CV 7.01 H4A (pCV 1.376+07 14 09 401 CAT 7.3E-07 14,16 

Pplmp 3.5 ,/ UNta, L ml Bell Alq), 3.66E+02 Sa); 9.88E-0 2 14 8): 1.65E+04 3: 2,2E+02 I 3 .0E-0 3 Alq 

,^ 

L18 

Bill BONSM7 3/17/1998 QUAD23C 3/17/19989:38: 12 AM 130NIN17 30 23 0.71833333 107 2.6683333 

LIQUID 848: 3/17/1998 12:19:48 AAI BKO 600 29 0.04833333 539 0.8983333 

And Dale, 3/17/1998 Tot Sa, Alq: 6.00E+00 / 1.00E+01 Alp; (Dpm/ 2.18E+00 (u (-V 5.89E-0 4 (pCV 9.81E+01 ±2.7 E+01 CAT 2.5E-0 1 Lab 

Ppl mp 5.9 i Unlla, L , ml Bel; Alq): 4.79E+00 Sa); 1.29E-03 40 2,16E+02 ± 3.0E+01 I - ^- 2.3E-01 

Bill B0N8M8 3/17/1995 QUAD23D 3/17/19959:38:12AM BONSMS 30 36 1.13666667 114 2.89 

LIQUID 848: 3/17/1998 12:19:48 AA1 BKO 600 38 0.06333333 346 0.91 

Anl Dale: 3/17/1998 Tot Sa, Mq: 6.00E+00 1.00E+01 Alp; (Dpnd 3.46E+00 (uCV 9.36E-04 (p(-'V 1.56E+02 + 3.0E+01 CAT 1.6E-0 1 Lab 

Piss mg: 3.5 / Units: L ml Bel; Mq): 4.83E+00 Sa): 1.31E-03 LIZ) : .18E+02 ± 2.9E+01 

I 

2.3E-01 Alq 

1.15 

17-Mar-98 Quanlerra Environment Se rvices, SCP V2.03 2 

Lis LIB

A,, -i/I fIY6 

—1 ` c,ir3 

Beclael llRnforfl Inc. CHAIN Ol e CUS'I'ODWSAMPLE ANALYSIS ItEQOES'I' I 1j9NjIM-L6 

'a1lrslnf f Cuwpni y CoMmirl lrlrphnue Nu. 1'rulrrl f'enrdln^lur Ibb - 1 car n[. uand 

R Rr.4 1 2Aidt 

SlcvcMarske 171-4716 WIIY1.Irl. 

2I I)i 

Project Designation Sasnph"It Lo ca tion tiAF No. ,(j^^J11 Ins 

105C Phase I R Phase II • Concrete Samples 100 A,ca ' Will. 3 1 fl.J(I(/r''Î 

Ice Cheal No. Held Logbook No, Method of Shipment 

Ilend deliver 

Shipped To Uffrllr 1'rmpaly Nu. 11111 of Lullnµ/Air 11111 Nu. 

Quanlerrs Incorporated 

POSSIBLE SARIPLE IIAZARnS/REMARKS — "M• 

1 1rnrrrallon i r i 

Rrdioaclive 

Special llandling and/or Storage 

S03a 79 - ►^ g o3a^ - / 


I y'pe of Coulainer 

No. of Contalnerls) 

Volume 

P 

-_... 

7 

— 

—^ ^.. _.. I 

IL - ^- 

Srrihrmll,ha 

sp«i.1 

ImWmom . 

/ 

3 `6 y` 5F-)6— to oa3î 

sample 140 Matti. Sample [talc Songdc lime ♦.bl fr^ 5 '.:IÎ j alYhi, "'.k: .i'^ ,1 (I'j j)lp rl',YF4':)ia': hr •f 1 ,h rll, o'I I,m,Ct 1 j •i s;C+ n •II' _. 

N 898 

.01ha, So 

w TL 

CIIAIN OF POSSESSION S ign/Prin t Nunes 

Rdr ) 1)aterfime Be [ a Bj I /lime/ 

R f' /e Hq?9B /I i $ G 


l7-Mar-98 

CLIENT CODE ID MATRIX RECEIVED DETECTOR AC'Q DATE SAMPLE MINUTES CNTS A NET CPM A CNTS B NET CPM B 

BIII B0H110 3/17/1996 QUAD2 1 B 3117/19999:38:04AM 8011110 30 II 0.32 107 2.6266667 

SOLID Bkg1 3/17/1991112A9:30 AM BKO 600 28 0.04666667 564 0.94 

Ad Dole, 3/17/1998 Tot Se, AIq, 3.00E+02 , 1.02E+02 Alp; (Dpm/ 2.10E+00 (uCU 4.66E-03 (pCU 9.33E+00 ± 5.3E+00 CAT 5AE+00 Lob 

Ppt mip 101.6 Udb, 0 j mg Bel; Alq): 5.73E+00 Sep 1.27E-02 LIg): 2.54E+01 3 3.4E+00 

i ' 

3.9E+00 Alq 

1•le 

BIII 8011111 3/171 1998 QUAD2 1 C 3/17/19989:38:04AM 8011111 30 13 0.37333333 308 9.2816667 

SOLID Bkp 3/17/1998 12:19:30 AM BKO 600 36 0.06 391 0.983 

Ad Dates 3/17/1998 Tot Sa,Algl 5.00E+02 , 9.95E+01 Alp; (Dpn,/ 1.90E+00 (uCl/ 4.31E-03 

Pplmg: 99.5 Udla: g mg Bel; Alq): 2.06E+01 So): 4.66E-0 2 

Bill 6011112 3/171 1998 QUAD2 1 D 3/17/19989:38:04AM B011J 1 2 

SOLID Bkgt 3/171 1998 12:19:30 AM BKG 

Ad D ole: 3 1 17/1998 Tot Se, Mq: 5 .00E+02 9.91E,01 Alp; (1)p,N 1.981:+00 (.Cl/ 4.301:03 

Ppe mg: 99.1 i - Units: g / mg Bel; Alq): 1.36E+01 So): 3.10E-02 

(pCU 8.62 E+00 ± 5.4E+00 CAT 5.8E400 Lob 

I.Ig): 9.32E+01 ± 5.9E400 1 1.1 E+00 Alq 

: IdL 

30 12 0.34666667 212 6.1383333 

600 32 0.05333333 557 0.9283333 

(pCU 8.99E+00 ± 5.4E+100 CAT 5.6E:00 Lob 

I,Ig): 6.20E+01± 4.9E+00 I j - 1.6E+00 Alq 

IAZ 

BIII 8011113 3/17/1998 QUAD22A 3/17/19989:38:OBAM B01IJ13 30 1 -0.0183333 346 10.638333 

SOLID Bkg, 3/17/1998 12:19:41 AM BKO 600 31 0.05166667 537 0.895 

Ad Dates 3/171 1998 Tot So, Alq, 5.00E+02 , 9. 117E+01 Alp; (Dpm/ •7.93E-0 1 (uCU . 1.81E-03 (pCV -3.63E+00 +4.6E+00 CAT 5.0E+02 Less 

Ppt mg: 98.7 Units: g mg Bel; Alq): 2.30E+01 So): 5.25E-02 Leg): 1.03E+02 j6.1 E+00 

1 

j" 9.5E-01 Alq 

1•le 

Bill BOIIJ 1 4 

3/17/1998 QUAD22B 3/17/19989:38:08AK1 B011114 

30 20 0.59666667 670 21 3 85 

SOLID 

Bkg; 3/171 1998 12:19:41 AKf BKO 

600 42 0.07 369 0.9483333 

Ad Dol e,3/17/1998 Tot Se, Alq: 3.00E+02 1.011E+02 Alp; (Dpm/ 2.83E+00 (UCU 3.91E-0 3 (pCU I.I&E101 ± 3.1E400 CAT 4.2E+00 Lob 

P iss mg: 107.8 . Udb: g^ , mg Bel; Alq): 4. 74E+01 Se): 9.90E-0 2 Ljg): 1.98E+02 ±B.OE too 1 / S.IE-01 AIq 

1•IL 

Bill BON692 3/17/1998 QUAD22C 3/17/1998 9:38:08 AK1 BON692 30 7 0.19166667 310 9.375 

LIQUID Bkg: 3/17/1998 12:19:41 AKI 13KO 600 25 0.04166667 375 0.9383333 

Ad Date: 3 1 17/1998 Tot Se, Alq: 1.00 V,+00 1.00E+00 Alp; (Dpn3 2.40E-01 - (uC'U 1.08E-04 -- (pCU -- 1.08E+02 -- -_ 

± 1.9E+02 CAT 2.3E-0 1 Lab 

Piss mg: 0.4 Udb: L , ml Bel; Alq): 1.73E 101 So): 7.81E-03 

i 

LIg): 7.8IE403 ±4.9E)02 

i 

Alq 

6.4E-03 

IdL 

17-Afar-98 Ouanterra Environment Se rvices, SCP V2.03 J

Qyrhianterra 

;ter 

Sty 

orrecti Action 

(o 

Client's Name: G 

C Client ' s Name: 

Condition Upon Receipt Variance Report 


,tva Atot7lr.^.a.F.c, 

Informed verbally on: Bv: 

Informed in writin g on: By: 

014501 

Login No.: / 721-¢ 

Client. Due: _ 7- `T,f Ime: 0 Y o 

Project No: S-50. 2G D Initiated by: o -A J—kh 

Shipper/No : -7 

ConditionNariance (Check all that apply): y): 

RFA/COC Numbers: /7 D C 

.. q Sample received b roken/leaking. 8. q Sample ID on container does not match sample ID 

2. q Sample received without proper preserva tive. on paperwork. Explain: 

• 

q Cooler tempera ture not within 4"C _ 2C 


q pH 9. q All coolers on airbiil not received with shipment. 

q other: 10. q Other (expla in below): 

.. q Sample received in improper container. 

j Sample received without proper paperwork. Explain: 


6. q No sample ID on sample con tainer. 

-. q Custody tape dis turbed/brokervmissing. 

C No variances were noted 

Notes: ,3 -r- ^,l b ^ Z 

I^^^ 610 

Sample(s) processed "as is". 

\ 

sample receipt Cooler Tempera ture upon Receipt. 

7 ?o3i^Pdi 

,P.ch/.2.0• t 

ll 

/-A CT e^ —/ ^^Q 4 / [Y rl Ss^^î 3t ^^, 

C Sample(s) on hold unt il : If released. no tify 

Sample Control Supe rvisor Review: (or designate) Date: ?" ^ 7 — 

Project Management Review: ^ Date: 7 —/P -1Y 

SL.ADMIN-0004. Reviseo :! '24/95 

SIGNED ORIGINAL NR;ST BE RETALNED IN THE PROJECT FILE 

L

Category: PCB's 

Method: EPA 8080 

Matrix: SOLID 

Client ID: BON680 

OUanterra-Richlanci 


Richland, WA 99352-1613 

Project: 550.260 

Sample Date 03/09/98 

Receipt Date 03/09/98 

Report Date 04/08/98 

cuanterra ID 17199-001 

Blank Sample Prep. Analyses Detection 

Analyte CAS Number Name Date Date Result Unit Oual. Limit Dilution 

Aroclor-12 4 11097-69-1 QCRLK167668-1 03/18/98 0 / 0/98 63 UG/KG 33 .2 

DCS 2051-24-3 QCBLK167668-1 03/18/98 03/30/98 88 %REC .2 

TCM% 877-09-8 OCBLK167668-1 03/18/98 03/30/98 80 7.REC .2 

"11^^5



Matrix: SOLID 


Analyte 

Duanterra- Ri chI and 





Receipt Date 03109/98 


Duanterra ID : 17199-002 


CAS Number Name Date Date Result Unit Dual. Limit Dilution 

Aroclor-1 54 11097-69-1 DCBLK167668-1 03/18/98 03/30/98 UG/KG U 33 .2 

DC8 2051-24-3 QCBLK167668-1 03/18/98 03/30/98 101 %REC .2 

TCMX 877-09-8 QCBLK167668-1 03/18/98 03/30/98 105 %REC .2 

"1 0



Matrix: SOLID 

Client ID: SON685 

Anal yte 

DCB 

TCMX 

Blank Sample 

CAS Number Name 

11097-69-1 OCBLK1681 3-1 

2051-24-3 QCBLK168133-1 

877-09-8 QCBLK168133-1 

Ouanterra-Richland 

3350 George Washington way 



Semple Date 03/11/98 



Duanterra ID 17200-001 

Prep. Analyses Detection 

Date Date Result Unit Dual- Limit Dilution 

03/24/98 0 /2 /98 33 UG/KG U 

03/24/98 03/25/98 90 %REC 1 

03/24/98 03/25/98 103 %REC 1 

, 7.s



Matrix: SOLID 


Guanterra-Richland 

3350 George Washington Nay 

Richland, NA 99352-1613 





Guanterra ID 17200-001MS 


Analyte CAS Number Name Date Date Result Unit Qua(. Limit Dilution 

Aroclor-1016 12674-11-2 QCSLK16813 -1 03/24/98 0 /25/98 a6 %REC 

Aroclor-1260 11096-82-5 QCBLK168133-1 03/24/98 03/25/98 77 %REC 5 

DCB 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 90 %REC 5 

TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 106 %REC 5 

V _i"074



Matrix: SOLID 

Client 10: 80X685 

Analyte 

Aroclor-1016 

Aroclor-1260 

DCB 

TCM% 

Blank Sample 

CAS Number Name 

12674-11-2 OCBLK168133-1 

11096-82-5 QCBLK168133-1 

2051-24-3 QCBLK168133-1 

877-09-8 QCBLK168133-1 

Duanterra-Richland 




Prep. Analyses 

Date Date 

03/24/98 03/25/98 

03/24/98 03/25/98 

03/24/98 03/25/98 

03/24/98 03/25/98 




Duanterra ID 17200-OOIMS 

Detection 

Result Unit dual. Limit Dilution 

%REC 5 

%REC - - 5 

90 %REC 5 

106 %REC .5 

J 7'



Matrix: SOLID 






sample Date 03/11/98 



Duanterra ID : 17200-GOIMSD 


Analyte CAS Nunber Name Date Date Result Unit DuaL. Limit Dilution 

Aroclor-1016 12674-11-2 QCSLK168133-1 03/24/98 03/25/98 84 %REC .5 

Aroclor-1260 11096-82-5 QCBLK168133-1 03/24/98 03/25/98 81 %REC .5 

DC8 2051-24-3 QCSLK168133-1 03/24/98 03/25/98 91 %REC .5 

TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 104 %REC .5 

.,0076



Matrix: SOLID 


AnaLyte 

DC8 

rCMx 

Blank SampLe 

CAS NLEber Name 

11097-69-1 QCBLK168133-1 

2051-24-3 QCBLK168133-1 

877-09-8 QC8LK168133-1 

Quanterra-Rich Land 







Quanterra ID 17200-002 

Prep. Analyses Detection 

Date Date Result Unit Qua L. Limit Dilution 

03/25/98 84 %REC 

03/25/98 89 %REC 9 

A077



Matrix: SOLID 


Analyte 

ouanterra-Richlana 




Sample Date 03/11198 



0uanterra ID : 17200-003 


CAS Number Name Date Date Result Unit Dual. Limit Dilute on 

Aroclor-1254 11097-69-1 OC8LK168133-1 03/24/98 03/25/98 33 UG/KG U 33 

Oc8 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 90 %REC 

TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 105 %REC



Matrix: SOLID 









Duanterra ID 17202-001 


Analyte CAS Number Name Date Date Result Unit Oual. Limit Dilution 

Aroclor-12 4 11097-69-1 QCBLK168133-1 03/24/98 03/25/98 33 UG/KG U 33 1 

DCB 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 91 %REC 1 

TCMK 877-09-8 QCBLK168133-1 03/24/98 03/25/98 100 %REC t 

x,00079



Matrix: SOLID 


Analyte 











Aroclor-12 4 11097-69-1 DCBLK16 133-1 03/24/98 03/25/9 33 UG/KG U 33 1 

DCB 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 91 %REC 1 

TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 86 %REC 1



Matrix: SOLID 









Ouanterra ID : 17202-003 


Analyte CAS Number Name Date Date Result Unit Dual. Limit Dilution 

Aroclor-12 4 1 " 

07-69-1 QCBLK168133-1 03/24/98 03/ /98 33 UG/KG U 33 1 

DCB 2051-24-3 QCSLK168133-1 03/24/98 03/25/98 88 %REC 1 

TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 94 %REC 1



Matrix: SOLID 







Report Date 04108/98 

Client ID: BON688 Duanterra ID : 17203-001 


Analyte CAS Number Name Date Date Result Unit Dual. Limit Dilution 

Aroclor-12 4 11097-69-1 QCBLK168133-1 03/24/98 03/25/98 33 UG/KG U 33 1 

OCS 2051-24-3 QCSLK168133-1 03/24198 03/25/98 92 %REC 1 

TCMK 877-09-8 QCBLK168133-1 03/24/98 03/25/98 105 %REC 1 

(J00S^:



Matrix: SOLID 


Analyte 

Blank Sample 

LAS Number Nam 





Prep. Analyses 

Date Date 


Receipt Date 03112/98 


Ouanterra ID : 17203-002 

Detection 

Result Unit OuaL. Limit Dilution 

p roctor-1254 11097-69-1 QCBLK168133-1 03/24/98 03/25/98 UG/KG U 33 1 

DCB 2051-24-3 QCBLK168133-1 03/24/98 03/25/98 90 %REC 1 

TCMX 877-09-8 QCBLK168133-1 03/24/98 03/25/98 65 %REC 1 

^J





Category: PCB's Sample Date 03/13/98 

Method: EPA 8080 Receipt Date 03/13/98 

Matrix: SOLID Report Date 04/08/98 

Client ID: BON690 Duanterra ID 17221-001 


Analyte CAS Number Name Date Date Result Unit DuaL. Limit Dilution 

Aroclor-1254 11097-69-1 QCBLK16825 -1 03/25/98 03/29/98 33 UG/KG U 1 

DC8 2051-24-3 QCBLK168253-1 03/25198 03/29/98 94 XREC 1 

TCMX 877-09-8 QCBLK168253-1 03/25/98 03/29/98 73 XREC 

OS 6



Matrix: SOLID 









Ouanterra ID 17221-002 


Analyte CAS Number Name Date Date Result Unit DuaL. Limit Dilution 

Aroclor-1254 11097-69-1 QCBLK168253-1 03/25/98 03/29/98 33 UG/KG U 33 1 

DCB 2051-24-3 QCBLK168253-1 03/25/98 03/29/98 108 %REC 1 

TCMX 877-09-8 QCBLK168253-1 03/25/98 03/29/98 82 %REC 1 

, 6087



Matrix: SOLID 


Analyte 











Aroclor-1254 11097-69-1 QCBLK168253-1 03/25/98 03/29/98 33 UG/KG U 33 1 

DCB 2051-24-3 QCBLK168253-1 03/25/98 03/29/98 92 %REC 1 

TCMK 877-09-8 QCBLK168253-1 03/25/98 03/29/98 74 %REC 1 

tj



Matrix: SOLID 


duanterra-Richland 







duanterra ID 17224-002 


Analyte CAS Number Name Date Date Result Unit dual. Limit Dilution 

ArocLor-1254 11097-69-1 QCBLK168253-1 03/25/98 03/29/98 33 UG/KG U 3 1 

DCB 2051-24-3 QCBLK168253-1 03/25/98 03/29/98 95 %REC 1 

TCMX 877-09-8 QCBLK168253-1 03/25/98 03/29/98 87 %REC 1 

J08 9



Matrix: SOLID 

Client 10: SON694 

Anatyte 

Aroclor- 

DCB 

TCMX 

Quanterra-Richland 




Stank Sample Prep. Analyses Detection 

CAS Number Name Date Date Result Unit Qua L. Limit Dilution 

2051-24-3 QCSLK168253-1 

877-09-8 QCBLK168253-1 

03/29/98 98 %REC 

03/29/98 93 %REC 

Saapie Date 03/16/98 



Quanterra ID 17224-003 

î.,^J0

Lab Name: OUANTERRA.MO Contract: 

Lab Code: ITMO Case No.: 

Matrix: (soil/water) SOIL 

Sample wt/vol: 6.0 (g/ml) G 

Level: (low/med) LOW 

Moisture: not dec. dec. 

Extraction: (SepF/Cont/Sonc) Sonc 

GPC Cleanup: (YIN) N pH: 

CAS NO. Compound 

1D EPA SAMPLE NO. 

PCB ORGANICS ANALYSIS DATA SHEET 

SAS No.: SDG No.: W02275 

EONG80 

Lab Sample ID: 17199-001 

Lab File ID: 

Date Sampled: 03-09-98 

Date Extracted: 03-18-98 

Date Analvzed: 03-30-98 

Dilution Factor: 0.2 

CONCENTRATION UNITS: 

(ug/L or ug/Kg) UG/KG Q 

11097-69-1 ------ Aroclor-1254 63 

U Concentration of analyte is less than the value given. 

FORM I PEST 

"j0J X93



I 

BONG81 

Lab Name: OUANTERRA.MO Contract 550.260 



Sample wt/vol: 6.0 ('g/ml) G 


% Moisture: not dec. 

Extraction: (SepF/font/Sonc) 

GPC Cleanup: (Y/N) N 


dec 

pH: 

Sonc 


Lab Sample =D: 17199-002 

Lab File ID: 



Date Analyzed: 03-30-98 

Dilution Factor: 0.2 



11097-69-1 ------ Aroclor-1254 33 U_ 

U: Concentration of analyte is less than the value given. 

FORM I PEST 

j0O94

Lab Name: OUANTERRA MO Contract: 


Matr_%: (soil/water) SOIL 


eve_: flow /med) LOW 

% Moisture: not des. dec. 

Extraction: (SepF/font/Sonc) Sonc 



11097-69-1 ------ Aroclor- 




BON685 

Lab Sample 1D: 17200-001 

Lab File ID: 


FORM I PEST 




Dilution Factor: 1 



33 1 U 

1, -J0095













BONG86 


Lab File ID: 







11097-69-1 ------ Aroclor-1254 33 U 


FORM I PEST 

"j 

I

Lab Name: OUANTERRA,M0 Contract: 





W Moisture: not dec. dec. 


GPC Cleanup: (Y/N) N PH: 


1D EPA SAMPLE NO 


550.260 

SAS No. SDG No. W02275 

BONG97 


Lab File !D: 

Date Sampled: —03----1-98 





(ug/L or ug/Kq) UG/KG 

11097-69-1 ------ Aroclor-1254 33 -U-- 

U: Concentration of analyte is less than the value given, 

FORM I PEST 

1- U009 "1

Lab Name: QUANTERRA,MO Contract: 



Sample wt/vol: 30.1 jg/ml) G 


°s Moisture: not dec. dec. 


GPC Cleanup: ,Y/N) N pH: 


ID EPA SAMPLE NC. 


iBON682 



Lab File ID: 







11097-69-1 ------ Aroclor-1254 33 ^—U_i 

U: Concentration of analvte is less than the value given. 

FORM I PEST 

00098



Matrix: (scii/water) SOIL 



% Moisture: not dec. dec. 

Extraction: (SepF/font/SOnc) Sonc 

GPC Cleanup: (Y/N) N pH: 

in EPA SAMPLE NO. 


550.260 



Lab File ID: 





BONG83 -^ 


CAS NO. Compound (ug/L or ug/Kg) UG/KG Q 

11097-69-1 ------ Aroclor-1254 33 1 U 


FORM I PEST 

(:00099

Lab Name: OUANTERRA,MO Contract 






Extraction: (Sep F/font/SOnc) 

GPC Cleanup: (YIN) N 




dec. 

pH: 

Sonc 

550.260 


SON684 

Lab Sample iD: 17202-003 

Lab File ID: 






(ug/L or ug/Kg) UG/KG 4 

11097-69-1 ------ Aroclor-1254 33 U 


FORM I PEST 

"00100







Extraction: (SepF/font/SOnc) Sonc 


ID EPA SAMPLE NO. 

PCP ORGANICS ANALYSIS DATA --HEST 

550.260 


SONG88 


Lab File ID: 



Date -nalvzed: 03-25-98 

Dilution Factor: 



11097-69-1 ------ Aroclor-1254 33 U 

i 


FORM I PEST 

:. V V i V l

Lab Name: OUANTERRA,MO Contract: 


Matrix: !Soil /water) SOIL 





GPC Cleanu p : (YIN) N pH: 


PCB ORGANICS ANALYSIS DATA SHEET. 

550.260 


BONG89 

Lab Sample =D: 17203-002 

Lab File ID: 







11097-69-1 ------ Aroclor-1254 33 U 


FORM I PEST 

100102 

—











550.260 

SAS No.: 

SDG No.: W02275 

3ON690 


Lab File ID: 







11097-69-1 ------ Aroclor-1254 1 33 1 U 

U: Concentration of analvte is less than the value given. 

FORM I PEST 

00103

Lab Name: QUANTERRA,MO Contract: 550.260 

1D EPA SAMPLE :70. 


Lab Code: ITMO Case No.: SAS No.: SDG No.: W02275 

Matrix: (soil/water) SOIL Lab Sample ID: 17221-002 

Sample wt/vol: 30.1 (g/ml) G Lab File ID: 

Level: (low/med) LOW Date Sampled: 03-13-98 

o Moisture: not dec. dec. Date Extracted: 03-25-98 

Extraction: (SepF/font/SOnc) Sonc Date Analyzed: 03-29-98 

CPC Cleanup: ;Y/N) N pH: Dilution Factor: _ 

BON691 



11097-69-1 ------ Aroclor-1254 33 U 

U: Concentration of anal; ,te is less than the value given. 

FORM I PEST 

r u0iO4

Lab Name: QUANTERRA.MO Contract: 550.260 


POE ORGANICS ANALYSIS DATA SHEET 


Matr'_x: (soil/water) SOIL Lab Sample ID: 17224-001 

Sample wt/vol: 30.0 (g/ml) G Lab File ID: 

Level: (low/med) LOW Date Sampled: 03-16-98 

o Moisture: not dec. dec. Date Extracted: 03-25-98 

Extraction: (SepF/font/Sonc) Sonc Date Analyzed: 03-29-99 

GPC Cleanup : (YIN) N pH: Dilution Factor: 

EON692 



11097-69-1 ------ Aroclor-1254 33 U 


FORM I PEST 

1 00105

Lab Name: QUANTERRA MO Contract: 






Extraction: (SepF/Cont/Sonc) Son 



11097-69-1 ------ Aroclor-1254 

ID 


EPA SAMPLE NO. 

BON693 

550.260 _! 

SAS No.: 

SDG No.: W02275 


Lab File ID: 


FORM I PEST 



Date Anal y zed: 03-29-98 

Dilution. Factor: 1 



33 I-'J

Lab Name: OUANTERRA,MO Contract: 






Extraction: (SepF/font/SOnc) 

GPC Cleanup: (YIN) N 


ID EPA SAMPLE NO. 


dec. 

pH: 

Sonc 

550.260 


SON694 


Lab File ID: 



Date Analvzed: 03-29-98 ._ 

Dilution Factor: 



11097-69-1 ------ Aroclor-1254 33 U 


FORM I PEST

Category: Mercury 


Matrix: SOLID 

ouanterra-Richland 




Semple Date 03/09/98 



Client Ouanterra Blank Saapte Prep. Anityses Detection 

ID ID Analyte CAS Number Name Date Date Result Unit Ouai. Limit Dit. 

BON680 17199-001 Mercury 7439-97-6 OCBLK168655-1 03/30/98 03/30/98 0.10 MG/KG 0.033 1 

BON681 17199-002 Mercury 7439-97-6 OCBLK168655-1 03/30/98 03/30/98 0.03 MG/KG B 0.033 1 

BON685 17200-001 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1 

BON685 17200-001M5 Mercury 7439-97-6 OCSLK168333-1 03/25/98 03/25/98 116 XREC 1 

BON685 17200-001MSD Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 111 %REC 1 

BON636 17200-002 Mercury 7439-97-6 OCBLK168333-1 03/25198 03/25/98 0.13 MG/KG 0.033 1 



BON683 17202-002 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.10 MG/KG 0.033 



BON689 17203-002 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.04 MG/KG 0.033 1 

BON690 17221-001 Mercury 7439-97-6 OCSLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1 


SON692 17224-001 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.16 MG/KG 0.033 1 

SON693 17224-002 Mercury 7439-97-6 OCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1 


NA OCLCS168655-1 Mercury 7439-97-6 OCBLK166655-1 03/30/98 03/30/98 116 %REC 10 

NA OCBLK168655-1 Mercury 7439-97-6 OCBLK166655-1 03/30/98 03/30/98 0.017 MG/KG U 0.033 1 

25

category: Mercury 


Matrix: SOLID 

QUanterra-Richland 




Sample Date NA 

Receipt Date NA 


Client Quanterra Blank Sample Prep. Analyses Detection 

ID ID Analyte CAS Number Name Date Date Result Unit Qua L. Limit Dil 

NA QCLCS168333-1 Mercury 7439-97-6 QCBLKI 33-1 03/25/98 03/25/98 107 KREC 10 

NA QCBLK168333-1 Mercury 7439-97-6 QCBLK168333-1 03/25/98 03/25/98 0.017 MG/KG U 0.033 1 

^^ 6

Category: ICAP Metals 


Matrix: SOLID 

Duanterra-RichLano 


RichLand, WA 99352-1613 


Sample Date NA 

Receipt Date NA 


CLient Duanterra Blank Sample Prep. Analyses Detection 

ID ID Analyte CAS Number Name Date Date Result unit Oual. Limit Dil 

NA OCLCS168299-1 Lead 7439-92-1 OCOLK168299-1 03/25/98 03/25/98 100 %REC 1 

NA QCBLK168009-1 Lead 7439-92-1 QCBLK168C09-1 03/23/98 03/23/98 0.21 MG/KG B 0.30 1 

NA QCBLK168299-1 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 0.16 MG/KG B 0.30 1 

BON680 17199-001 Lead 7439-92-1 QCSLK168009-1 03/23/98 03/23/98 10.9 MG/KG E 0.30 1 

BON681 17199-002 Lead 7439-92-1 QCHLK168009-1 03/23/98 03/23/98 3.7 MG/KG E 0.30 1 

BON685 17200-001 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 3.2 MG/KG E 0.30 1 

BON685 17200-OOlMS Lead 7439-92-1 QCSLK168299-1 03/25/98 03/25/98 90 XREC 1 

SON685 17200-OOlMSO Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 88 %REC 1 

BON686 17200-002 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 11.8 MG/KG E C.30 1 

SON687 17200-003 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 3.7 MG/KG E 0.30 1 

8ON682 17202-001 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 3.7 MG/KG E 0.30 1 


BON684 17202-003 Lead 7439-92-1 GCBLK168299-1 03/25/98 03/25/98 3.3 MG/KG E 0.30 1 


9ON689 17203-002 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 9.0 MG/KG E 0.30 1 


SON691 17221-002 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 2.9 MG/KG E 030 1 

BON692 17224-001 Lead 7439-92-1 QCBLK168299-1 03/25/98 03/25/98 10.6 MG/KG E 0,30 1 


BON694 17224-003 Lead 7439-92-1 OCBLK168299-1 03/25/98 03/25/98 3.6 MG/KG E 0.30 1 

NA QCLCS168009-1 Lead 7439-92-1 OCOLK168009-1 03/23/98 03/23198 102 %REC 1

U.S. EPA - CLP 

COVER PAGE INORGANIC ANALYSES DATA PACKAGE 

Lab Name: QUANTERRA MO Contract: 550.260 


SOW No.: SW846 

EPA Sample No. 

_BON692 

_2 0 11 680 

_BON681 

BON682 

_B0N683 

_BON684 

_BON685 

_BON685SD 

_BON685S 

_BON686 

_BON687 

_B0N688 

_BON689 

_BON690 

_BON691 

_BON693 

BON694 

Were ICP interelement corrections applied ? 

Were ICP background corrections applied ? 

If yes - were raw data generated before 

application of background corrections ? 

Comments: 

Lab Sample ID 

17224-001_ 

17199-001 

17199-002 

17202-001 

_17202-002 

17202-003 

17200-001 

_17200-OO1SD_ 

17200-OO1S 

17200-002 

_17200-003^ 

17203-001_ 

17203-002 

17221-001 

17221-002J 

17224-002 

17224-003 

Yes/No YES 

Yes/No YES 

Yes/No 7C 

I certify that this data package is in compliance with the terms and 

conditions of the contract, both technically and for completeness, for 

other than the conditions detailed above. Release of the data contained 

in this hardcopy data package and in the computer-readable data submitsed 

on floppy diskette has been authorized by the Laboratory Mana ger r -he 

Manag er's designee, as verified by the following signature. 

Signature: Name: 

Date Title: 

COVER PAGE - IN SW-^46 

7 A 

, - J 1

U.S. EPA - --LP 

INORGANIC ANALYSES DA '.-=ET 

^ 

BON692 

Lab Name: QUANTERRA MO 

Lab Code: - TMO Case No.: 

Matrix (soil/water): SOIL 

Level (low/med): LOW 

Solids: 100.0 

Contract: 

SAS No.: SDG No.. W02275 

Sample ID: 17224-001 

-,--e Received: 03/15/98 

Concentration Units (ug/L or mg/kg dr.; :oeight) 

CAS No. Analyte Concentrat Q 

7439-92-1 LeaT 1C._^^ E 

7439-97-6 Mercury-0.15– — - 

Color Before: Clarity Before: 

Color After: Clarity After: 

^7omments: 

- 

Î 

I 

P 

CV 

MG/KG 

=1 

- 

-I 

SW-84h

Color Before: 

Color After: 

Comments: 

I- . .EPA - = 

1 --PA :SAMPLE No. 

INORGAN_ - ANALYSES -ATA. -HEET I 

BON630 





Contract: 

SAS No.: 

5 .26G 

SDG No.: 

Lab Sample ID: 

Date Received: 

W02275 

17199-001 

03,`(J9/9 c 

% Solids: 100.0 

Concentration Units "ug/L or mg/kg dry weight): MG/KG 

CAS No. 

7439-92-1 

7439-97-6 

Analyte Concentration C Q IM 

LeadI 10.9 

Mercury_ O.lO CV 

I- 

i 

— 

I- 

. , 

. 

Clarity Before : TP_xr^:ê. 

Clarity After: Art-facts: 

_ ten,•, _ - _^^ 

i 

SW-n46

U.S. EPA CLP 

1 EPA SAMPLE NO - 

INORGANIC ANALYSES DATA SHEET 

BGN631 


Lab Code: ITMO Case `To.: SAS No.: —I SDG o.: ;102275 


Sample ID: _7199-00: 

Level (low/med) LOW Date Received: 3;09/98 

s Solids: 100.0 

Concentration Units (ug/L or mg/kg dry weight): MG/KG 

CAS No. 

7439-92-1 

7439-97-6 

Analyte 

Lem 

Mercury 

Concentration Q 

i– i 

3.7 E 

0.03 B 

Color Before: Clarity Before: Text re: 


Comments: 

i 

–i 

N 

5 

_V 

i 

SW-146 

131 

i

U.S. EPA --LP 

1 EPA SAMPLE NO. 


20N682 

Lab Name: QUANTERRA MO Contract: -750.260 

Lab Code: ITMOCase No.: SAS No.: SDG No.: W02275 

Matrix (soil/water): SOIL Lab Sample ID: 17202-001 

Level ;low/med): LOW Date Received: 03/10/98 

Solids: 100.0 


CAS No. Analyte Concentration C Q M 

7439-92-1 Lead 3.7 E P 

7439-97-6 Mercury_ 0.02 U ^CV 


- 

exture: 

Color After: Clarity After: = -facts: - 

Comments: 

I_ 

- 

SW-846 

r. 2

U.S. EPA --LP 

1 EPA SAMPLE NO 


3ON683 





% Solids: 100.0 

Contract: 

SAS No.: 

550.2 6 0 

SDG `:o.: 

Lan Sample ID: 


W02275 

17202-002 

03!10/98 

Concentration Units (ug/L or mg/kg dry weight) 

CAS No. Analyte ( Concentration C 

7439-92-1 Le —a—(l Le 7.6 

7439-97-6 Mercury_ 0.10 



Comments: 

Q 

'— I 

M 

CV 

— 

MG/KG 

^'extnre 

rt -acts. 

SW-846 

^33


1 EPA SAMPLE 70 


30N634 



Matrix (soil/water): SOIL Lab Sample 1D: !7202-20 

Level !low/med): LOW Date Received: 03/10;98 

Solids: 100.0 


CAS No. Analyte Concentration . 0 Q M 

I 

7439-92-1 Lem—3.3 E P 

7439-97-6 Mercury_ 0.02 U A 

Color Before: Clarity Before: 7extsre: 

Color After: Clarity After: Artifacts: 

Comments: 

-34 

SW-&4F

U.S. EPA _LP 

i EPA SAMPLE NO. 


BONG85 

Lab Name:QUANTERRA MO Contract: 550.250 



Lan Sample ID: 17200-001 

Level (low/med): LOW Date Received: 03/11/98 

°a Solids: 100.0 

Color Before: 

Color After: 

Ccmments: 


CAS No. 

7439-92-1 

7439-97-6 

Analyte Concentration 

Lead 3.2 

Mercury_ 0.02 

Clarity Before: 

Clarity After: 

C Q M 

E P 

U ACV 

— 

–i — 

i 

– — 

I 

Texture: 

art «acts 

" ^.i -J5 

SW-646




BON685 



Matrix !soil/waterj: SOIL Lan Sample ID: 17200-002 


Solids: 100.0 


CAS No. Analyte Concentration C Q M 

7439-92-1 Lear 11.8 _E_ P 

7439-97-6 Mercury—0.13 Cv 

Color Before: Clarity Before: Texzure: 

Color After: Clarity After: Art __àcc3: 

Comments: 

I 

SW-846 

136

U.S. EPA CLP 



BON687 


Lab erode: ITMO Case No.: SAS No.: S D G No.: W02275 

Matrix (soil/water): SOIL — Lab Samp le ID: 17200-00:' 


Solids: 100.0 

Color Sefore: 

Colcr After: 

Comments: 


CAS No. 

7439-92-1 

7439-97-6 

Analyte 

Lea^— 

Mercury_ 

Concentration C Q 



3.7 - E - 

0.02 U 

–I 

M 

P 

CV 

I — I 

I 

i 

ext. _: 

Artifacts: 

" 13 '7 

SW-946




BON688 


Lab Code: iTMO Case No.: 



Solids: 100.0 

Contract: -^_ .260 

SAS No.: SDG No.: 


Cate Received: 

W02275 

17203-001 

03/12/98 


CAS No. 

7439-92-1 

7439-97-6 

Analyte 

Leaa- 

Mercury_ 

Concentraticn.0 Q 

3.0^ E 

0.02 U 

Color Before: Clarity Before: Texture: 

Color After: Clarity After: Artifacts: 

Comments: 

FORM I - IN 

i 

—I 

M 

P 

CV 

ff. 

l) ^J i J 

SW-846

Color Before: 

Color After: 

Comments: 

CAS No. 

7439-92-1 

7439-97-6 

J.S. EPA CLP 

' 

1 


EPA SAMPLE NO. 

BON6c9 

i 



Matrix (soil/waer): t SOIL 


Solids: 100.0 

Contract: 550.260 

SAS No.: SDG No.: 

n Sample La ID: 


W02275 _ 

17203-002 

03/12/98 


Analyte Concentration Q 

Lead -9.0 _ I _E 

Mercury_ 0.04 



i 

— 

—I 

M 

P 

CV 

Texture: 

Art--àcts: 

SW-=46 

139

U.S. EPA CLP 

1 SPA SAMPLE '7j 0 


BON690 

Lab Name: QUANTERPA MO Contract: 550.250 


Matrix (soil/water): SOIL Lab Sample ID: 17221-007 

Level (low/med): LOW Date Received: 03/13;'98 

°s Solids: 100.0 


CAS No. Analyte Concentration , (- Q ^M 

7439-92-1 Lem— 3.4 E P 

7439-97-6 Mercury 0.02 U CV 

I_ 

I 

I I 

— I 

– i - 

-I — 

Color Before: Clarity Before: Texti:re: 

Color After: Clarity After: Art_-acts: 

:7 omments: 

sw---;6

U. E. EPA - CT 

1 EPP_ SAMPLE NO. 

INORGANIC ^,NALYSES DATA -HEET 


Lab Code: _TMO Case No.: 



o Solids: 100.0 

Contract: 

SAS No.: 

X20 260 

SDG No.: 


Date Rece_ved: 

BON691 

W02275 

17221-,702 

03/13/58 

Color Before: 

Color After: 

Comments: 


CAS No. 

7439-92-1 

7439-97-6 

i 

Analyte I Concentration!CI Q M I 

Lear—2 . 9 E P 

Mercury_ 0.02 U CV 

Clarity Before: exture 

Clarit y After: Artifacts: 

vO141 

SW-c}6

CAS No. Analyte 

7439-92-1 Lem 

7439-97-6 (Mercury_ 

U.S. EPA - CLF 



-N69_ 

Lab Name: QUANTERRA MO Contract: 000.260 _1 

1 

Lab Code: ITMO Case ^;o.: SAS No.: SDG No.: ::02275 

Matrix (soil/water): SOIL _L__aE Sample ID: 17224-00 


% Solids: 100.0 


Concentration C 

'3 c 

0.02 U 

_i 

– 

Q M 

Color Betcre: Clarity Before: Text r 

Color Af*_er. Clarity After: Art S: — 

Comments: 

E 

i 

P CVI 

SW- Hfir,

Color Before: 

Color After: 

Comments: 

U.S. EPA CLP 

1 -xPA ',AM P LE 0. 

INORGANIC ANALYSES DAT I SHEET 

SONG 741 



Matrix soil/water): SOIL Lab Sampie ID: 17224-003 

Level ;low/med): LOW Date Received: 03!16/98 

% Solids: 100.0 

Concentration Units (ug/L or mg/kg dry weight): MG//KG 

CAS No. Analyte 

7439-92-1 LeacT- 

7439-97-6 Mercury_ 

Concentration C Q M 

_ I 

3.6 E P 

0.02 U jCV 


Clarit y After: 

I_ 

i 

i 

"excure: 

Art '_facts: 

J i i 

SW-^4F

Bechtel Hanford, Inc. 


Richland, WA 99352 

April 21, 1998 

Attention: Joan Kessner 

SAF Number 

Date First Sample Received 

Date SDG Closed 

Number of Samples 

Sample Type 

SDG Number 

Data Deliverable 

CERTIFICATE OF ANALYSIS 

B98-061 

March 9, 1998 

March 16, 1998 

15 

Other-Cement 

W02275 

21 Day Summary 

°ivanterra 

Emironmrnra7 

sen'u es 

lc^ In ti 

I. Introduction 

Between March 9, and March 16, 1998, 15 21-day TAT other-cement samples were received 

by the Quanterra Environmental Se rvices Richland Laboratory (QESRL) for radiochemical and 

chemical analysis. Upon receipt, the samples were assigned the following laborato r y ID 

numbers to correspond with the Bechtel Hanford, Inc. (BHI) specific IDs: 

QESRL ID Ji BHI iD# YIATRI% DATE OF RECEIPT 

80316101 BON680 Soil 3/9/98 

80316102 BON681 Soil 3/9/98 

80318401 BON682 Soil 3/10/98 

80318402 BON683 Soil 3/10'98 

80318403 BON684 Soil 3/10/98 

80320601 BON685 Soil 3111198 

803 2 0602 BON686 Soil 3i 11.'98 

80320603 BON687 Soil 3x 11 "98 

80322201 BON688 Soil 3/12x98 

80312 1_02 BON689 Soil 3.12.'98 

80324401 BON690 Soil 3J13^98 

80324402 BON691 Soil 3; 1?x98 

80327201 BON692 Soil 3.16,98 

80327202 BON693 Soil 3, 16,98 

80327203 BON694 Soil 3116,98 

r1 

G0I)..


April 21, 1998 

Page 2 

II. Analytical Results/Methodology 

iivanterra 

EnOronmenral 

Souk , 

The analytical results for this report are presented by laboratory sample ID. Each set of data 

includes sample identification information, analytical results and the appropriate associated 

statistical errors. 

The requested analyses were: Alpha Spectroscopy 

Americium-241 by method RICH-RC-5062 

Plutonium-238, -239/40 by method RICH-RC-5062 

Uranium-234, -235, -238 b_y method RICH-RC-5062 

Gamma Spectroscopy 

Gamma Scan by method RICH-RC-5017 

Gas Proportional Counting 

Total Strontium b y method RICH-RC-5006 

Liquid Scintillation Counting 

Carbon-14 by method RICH-RC-5022 

Nickel-63 by method RICH-RC-5069 

Selenium-79 by method RD-3253 

Technetium-99 by method RICH-RC-5029 

Chemical Analyses 

Chromium Hex by EPA method RICH-RC-5005 

III. Quality Control 

The analytical results for each analysis performed under SDG WO-2 -2 75 include a minimum of 

two Laboratory Control Samples (LCS) and one method (reagent) blank. Any exceptions have 

been noted in the "Comments" section_ 

Quality control sample results are reported in the same units as sample results. 

(JO U.;


April 21, 1998 

Page 3 

IV. Comments 

Alpha Spectroscopy 

Q,P'uanterra 

Environmental 

Services 

Americium-241 by method RICH-RC-5062 

The LCS, batch blank, sample duplicate (BON680 and BON687) and sample results are within 

contractual requirements. 

Plutonium-238 -239/40 by method RICH-RC-5062 



Uranium 234, -235 -238 by method RICH-RC-5062 

The LCS, batch blank, sample duplicate (BON680) and sample results are within contractual 

requirements. The RPD values for sample duplicate BON693 were slightly greater than the first 

level of evaluation criteria but the values met the second level evaluation criteria. Rich Weiss 

gave approval to report the data on 4/6/98. 

Gamma Spectroscopy 

Gamma Scan by method RICH-RC-5017 

The LCS, batch blank. sample duplicate (BON680 and BON685) and sample results are within 

contractual requirements_ 

Gas Proportional Counting 

Total Strontium by method RICH-RC-5006 



Liquid Scintillation Counting 

Carbon-14 by method RICH-RC-5022 



Nickel-63 by method RICH-RC-5069 

The LCS. batch blank, sample duplicate (BON680 and BON688) and sample results are within 


G0Oit


April 1-1, 1998 

Page 4 

^%%uanterra 

F.mironm

O 

FORM I Date: 4/16/1998 

SAMPLE RESULTS 

LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/9/1998 10:30:00 AM 

LAB SAMPLE ID: 80316101 REPORT NBR: 4835 RECEIVED DATE: 3/9/1998 1:42:00 PM 

CLIENT ID: BON680 ORDER NBR: B98-061 MATRIX: OTHER 

ISOTOPE RESULT 

COUNTING 

ERROR(2s) 

TOTAL ERROR 

(2s) MDA 

REPORT 

UNIT YIELD RST/MDA RST/CNTERR 

ANALYSIS 

DATE 

ALIQUOT 

SIZE 

ALQ 

UNIT 

DETECTOR 

ID 

METHOD 

NUMBER 

TC-99 -5.03E+02 1.5E+03 4.8E+03 3.63E+03 pCi/sam 95.10% -0.14 -0.33 4/2/98 0.000414 SA LSC RICHRC5078 

AM-241 6.72E+03 1.2E+03 1.7E+03 1.57E+02 pCi/sam 74-90% (429) (5.4) 4/3/98 0.000368 SA ALPHA-SPEC RICHRC5057 

HEXCHROME 4.00E-03 00E+00 0.0E+00 200E-03 mg/L N/A (2.) N/A 3/10/98 100.0 ML SPECPHOTO EPA7196 

U-234 8.61E+01 1.0E+02 1.0E+02 1.19E+02 pCi/sam 80.30% 0.73 0.84 4/3/98 0000376 SA ALPHA-SPEC RICHRC5030 

U-235 0.00E+00 0.0E+00 8.8E+01 7.98E+01 pCdsam 80.30% 0 N/A 4/3/98 0.000376 SA ALPHA-SPEC RICHRC5030 

U-238 8.37E+01 1.0E+02 1.0E+02 1.35E+02 pCi/sam 80.30% 0.62 0.82 4/3/98 0.000376 SA ALPHA-SPEC RICHRC5030 

PU-238 5.26E+02 2.4E+02 2.SE+02 7.49E+01 pCi/sam 62.20% (7) (2.2) 3/31/98 0000368 SA ALPHA-SPEC RICHRC5010 

PU239/40 1.82E+04 1.4E+03 2.8E+03 1.26E+02 pCi/sam 62.20% (143.6) (12.8) 3131/98 0.000368 SA ALPHA-SPEC RICHRCS010 

AM-241 6.78E+03 1.0E+03 1.2E+03 N/A pCi/sam N/A N/A (6.6) 3/26/98 0.2355 SA GAMMA RICHRC5017 

CO-60 4.21E+04 7.SE+02 4.3E+03 N/A pCi/sam N/A N/A (56.3) 3/26/98 0.2355 SA GAMMA RICHRC5017 

CS-137DA 1.49E+06 4.9E+03 1.5E+05 N/A pCi/sam N/A N/A (305.4) 3/26/98 0.2355 SA GAMMA RICHRC5017 

EU-152 4.14E+04 2.0E+03 4.6E+03 N/A pCi/sam N/A N/A (21.) 3/26/98 0.2355 SA GAMMA RICHRC5017 

EU-154 5.81E+03 8.0E+02 9.9E+02 N/A pCi/sam N/A N/A (7.2) 3/26/98 0.2355 SA GAMMA RICHRC5017 

EU-155 -1.37E+02 6.9E+02 6.9E+02 1.06E+03 pCi/sam N/A -0.13 -0.2 3/26/98 0.2355 SA GAMMA RICHRC5017 

STRONTIUM 4.67E+05 1.0E+04 1.7E+05 1.79E+03 pCi/sam 97.00% (260.4) (46.8) 4/1/98 0000367 SA AS RICHRC5006 

C-14 1.90E+02 1.0E+03 1.6E+03 2.40E+03 pCi/sam 100.00% 0.08 0.19 4/9/98 0.00064 SA LSC RICHRC5022 

NI-63 4.16E+06 2.1E+04 5.0E+05 4.48E+03 pCi/sam 76.70% (928.9) (1969) . 4/3/98 0.000367 SA LSC RICHRC5069 

O SE-79 2.01E+03 2.0E+03 7.3E+03 4.60E+03 pCi/sam 71.50% 0.44 (1.) 4/1/98 0.000372 SA LSC RICHRC5043 

C. 

Number of Results: '18 

Comments:

FORM I Date: 4/16/1998 


LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/9/1998 1.45:00 PM 




COUNTING 

ERROR(2s) 

TOTAL ERROR 

(2 s) MDA 

REPORT 

UNIT YIELD RST/MDA RSTICNTERR 

ANALYSIS 

DATE 

ALIQUOT 

SIZE 

ALQ 

UNIT 

DETECTOR 

ID 

METHOD 

NUMBER 

TC-99 352E+00 1.4E+01 42E+01 323E+01 pCi/sam 95.10% -0.11 -0.26 3/31/98 0.0458 SA LSC RtCHRCS078 

AM-241 319E+00 2-3E+00 2.3E+00 1.08E+00 pCi/sam 87.10% (3) (14) 4/4/98 0.046 SA ALPHA-SPEC RICHRC5057 

HEXCHROME 2.00E-03 0.0E+00 0.0E+00 2.00E-03 mg/L N/A 1. N/A 3/10/98 100.0 ML SPECPHOTO EPA7196 

U-234 159E+02 2.5E+01 5.4E+01 4.10E+00 pCi/sam 19.80% (38.8) (6.2) 4/5/98 0.044 SA ALPHA-SPEC RICHRC5030 

U-235 8.15E+00 5.8E+00 6.3E+00 2.76E+00 pCi/sam 19.80% (3.) (1.4) 4/5/98 0.044 SA ALPHA-SPEC RICHRCS030 

U-238 1.83E+02 2.7E+01 6.2E+01 4.66E+00 pCi/sam 19.80% (39.4) (6.7) 4/5/98 0.044 SA ALPHA-SPEC RICHRC5030 

PU-238 0.00E+00 00E+00 5.2E-01 4.65E-01 pCi/sam 77.40% 0. N/A 4/3/98 0.046 SA ALPHA-SPEC RICHRC5010 

PU239/40 3.92E+00 1.6E+00 1.7E+00 7.84E-01 pCi/sam 77.40% (5.) (2.4) 4/3/98 0.046 SA ALPHA-SPEC RICHRC5010 

CO-60 4.22E+01 2.7E+01 2.8E+01 5.77E+01 pCi/sam N/A 0.73 (1.5) 3/27/98 0.0541 SA GAMMA RICHRCS017 

CS-137DA 4.95E+02 7.2E+01 8.7E+01 N/A pCi/sam N/A N/A (6.9) 3/27/98 0.0541 SA GAMMA RICHRCS017 

EU-152 1.87E+01 89E+01 8.9E+01 148E+02 pCi/sam N/A 0.13 0.21 3/27/98 0.0541 SA GAMMA RICHRC5017 

EU-154 1.14E+02 9.0E+01 91E+01 1.75E+02 pCi/sam N/A 0.65 (13) 3/27/98 0.0541 SA GAMMA RICHRCS017 

EU-155 -3.69E+01 65E+01 6.5E+01 101E+02 pCi/sam N/A -0.37 -0.57 3/27/98 0.0541 SA GAMMA RICHRCS017 

STRONTIUM 6.20E+02 3.2E+01 2.2E+02 1.34E+01 pCi/sam 9880% (46.3) (19.5) 4/2198 0.0476 SA AB RICHRC5006 

C-14 8.68E+00 1 4E+01 2.2E+01 3.30E+01 pCi/sam 10000% 0.26 061 4/2/98 0.0467 SA LSC RICHRC5022 

NI-63 4.47E+02 2.1E+01 8.1E+01 2.74E+01 pCi/sam 9930% (16.3) (21.6) 4/5/98 0.0458 SA LSC RICHRC5069 

SE-79 -5.63E+00 1.5E+01 5.6E+01 3.72E+01 pCi/sam 70.40% -0.15 -0.36 4/13/98 00464 SA LSC RICHRC5043 

C 

[Number of Results: 17 

C^ 

Comments:

FORM I Date: 4/16/1998 






TC-99 -2.99E+01 

AM-241 4.68E+00 

HEXCHROME 2.00E-03 

U-234 2.85E+01 

U-235 4.09E-01 

U-238 3.68E+01 

PU-238 0.00E+00 

PU239/40 2.37E+00 

CO-60 -2.12E+01 

CS-137DA 3.28E+02 

EU-152 -1.29E+01 

EU-154 -4.98E+01 

EU-155 1.26E+01 

STRONTIUM 7.92E+01 

C-14 3.73E+01 

NI-63 2.42E+02 

SE-79 -1.33E+01 

dumber of Results: '17 

G 

Cl) 

Comments: 

COUNTING TOTAL ERROR 

ERROR(2s) (2 s) 

3.0E+01 9.3E+01 

4.3E+00 4.3E+00 

0.0E+00 0.0E+00 

8.3E+00 9.9E+00 

1.2E+00 1.2E+00 

9.5E+00 1.2E+01 

0 0E+00 1 2E+00 

2.0E+00 2.0E+00 

3.9E+01 3.9E+01 

6.5E+01 7.3E+01 

9 0E+01 9.0E+01 

1.2E+02 1 2E+02 

8.4E+01 8.4E+01 

2.1E+01 3.6E+01 

3 3E+01 5.1E+01 

3.2E+01 1.0E+02 

3.7E+01 1.3E+02 

REPORT 

MDA UNIT YIELD 

6.98E+01 pCi/sam 95.10% 

3.83E+00 pCi/sam 81.70% 

2.00E-03 mg/L N/A 

4.01 E+00 pCi/sam 56.60% 

3.21E+00 pCi/sam 56.60% 

4.14E+00 pCi/sam 56.60% 

1.10E+00 pCi/sam 74.40% 

1.85E+00 pCi/sam 74.40% 

6.47E+01 pCi/sam N/A 

N/A pCi/sam N/A 

1 .51E+02 pCi/sam N/A 



3.35E+01 pCi/sam 94.50% 

7.60E+01 pCi/sam 100.00% 

6.16E+01 pCi/sam 95.20% 

8.78E+01 pCi/sam 75.40% 

RSTIMDA RST/CNTERR 

-043 -(1-) 

(1.2) (1 1) 

1 N/A 

(7.1) (3.4) 

0.13 0.34 

(8.9) (3.9) 

0 N/A 

(1-3) 

(1.2) 

-033 -0.54 

N/A (5.) 

-009 -014 

-025 -0.42 

009 0.15 

(2A) (38) 

049 (L1) 

(39) (Z5) 

-0.15 -0.37 

ANALYSIS ALIQUOT ALQ DETECTOR METHOD 

DATE SIZE UNIT ID NUMBER 

3/31/98 0.0206 SA LSC RICHRC5078 

4/4/98 0.021 SA ALPHA-SPEC RICHRCS057 

3/11/98 1000 ML SPECPHOTO EPA7196 

4/4/98 0.0243 SA ALPHA-SPEC RICHRC5030 

4/4/98 0.0243 SA ALPHA-SPEC RICHRCS030 


4/3/98 0021 SA ALPHA-SPEC RICH RC5010 


3/27/98 0.0537 SA GAMMA RICHRC5017 





4/2/98 0.0208 SA AB RICHRC5006 

4/2198 0.0204 SA LSC RICHRC5022 

4/5/98 0.0212 SA LSC RICHRC5069 

4/13/98 0.0183 SA LSC RICHRC5043

ISOTOPE 

TC-99 

AM 241 

U-234 

U-235 

U-238 

PU-238 

PU239/40 

AM-241 

CO-60 

CS-137DA 

EU-152 

EU-154 

EU-155 

STRONTIUM 

C-14 

NI-63 

SE-79 

Qlumber of Results 

G 

Comments 

RESULT 

-1.14E+03 

2 94E+03 

9 18E+01 

0 00E+00 

4 30E+01 

8 36E+01 

5.23E+03 

2 84E+03 

8.29E+03 

1 28E+06 

1 57E+04 

2 42E+03 

4 15E+02 

6 71 E+05 

7 01 E+02 

4.05E+05 

1.16E+03 

117 

FORM Date: 4/16/1998 




CLIENT ID: BON683 ORDER NBR: B98-061 MATRIX OTHER 


ERROR(2s) (2s) 

1.8E+03 5.8E+03 

7.3E+02 8.5E+02 

9.8E+01 9.9E+01 

0.0E+00 7.3E+01 

6.9E+01 7.0E+01 

9.7E+01 9.7E+01 

7 6E+02 1.0E+03 

5.4E+02 6.1 E+02 

3.7E+02 9.1 E+02 

2.3E+03 1.3E+05 

2.1E+03 2.6E+03 

4.6E+02 5.2E+02 

7.1 E+02 7.1 E+02 

1.2E+04 2.5E+05 

1 1E+03 1 7E+03 

6.7E+03 5.2E+04 

1.9E+03 6.9E+03 

REPORT 


4.39E+03 pCi/sam 95.10% 

1.23E+02 pCi/sam 98.10% 

1 22E+02 pCi/sam 92.90% 

6.61 E+01 pCi/sam 92.90% 

1.22E+02 pCi/sam 92.90% 

7 54E+01 pCi/sam 61.80% 

1.27E+02 pCi/sam 61.80% 







2.12E+03 pCi/sam 97.20% 

2 49E+03 pCi/sam 10000% 

4.29E+03 pCi/sam 8200% 

4.35E+03 pCi/sam 78.60% 

RST/MDA RST/CNTERR 

-0.26 -0.62 

(24-) (4) 

075 094 

0. N/A 

0.35 0.62 

(1.1) 087 

(41.1) (6.8) 

N/A (5.2) 

N/A (22.4) 

N/A (564.8) 

N/A (7S) 

(2.6) (5.3) 

0.35 0.58 

(3159) (54.2) 

0.28 065 

(94.6) (60.7) 

0.27 0.62 

ANALYSIS 

DATE 

4/2/98 

4/3/98 

4/3/98 

4/3/98 

4/3/98 

3/31/98 

3/31/98 

3/26/98 

3/26/98 

3/26/98 

3/26/98 

3/26/98 

3/26/98 

4/1/98 

4/9/98 

4/3/98 

4/1/98 

ALIQUOT ALQ 

SIZE UNIT 

0.000342 SA 

0.000355 SA 

0.00037 SA 

0.00037 SA 

0.00037 SA 

0.000355 SA 

0.000355 SA 

0.229 SA 

0.229 SA 

0.229 SA 

0.229 SA 

0.229 SA 

0 229 SA 

0.000349 SA 

0.000617 SA 

0.000359 SA 

0.000357 SA 

DETECTOR 

ID 

LSC 

ALPHA-SPEC 

ALPHA-SPEC 

ALPHA-SPEC 

ALPHA-SPEC 

ALPHA-SPEC 

ALPHA-SPEC 

GAMMA 

GAMMA 

GAMMA 

GAMMA 

GAMMA 

GAMMA 

AB 

LSC 

LSC 

LSC 

METHOD 

NUMBER 

RICHRCS078 

RICHRC5057 

RICHRC5030 

RICHRC5030 

RICHRC5030 

R ICHRCS010 

RICHRC5010 

RICHRC5017 

RICHRC5017 

RICHRC5017 

RICHRC5017 

RICHRC5017 

RICHRC5017 

RICHRC5006 

RICHRC5022 

RICHRC5069 

RICHRC5043

FORM I Date: 4/16/1998 


LAB NAME: QUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/10/1998 1:20:00 PM 




COUNTING 

ERROR (2 s) 

TOTAL ERROR 

(2 s) MDA 

REPORT 

UNIT YIELD RSTIMDA RST/CNTERR 

ANALYSIS 

DATE 

ALIQUOT 

SIZE 

ALQ 

UNIT 

DETECTOR 

ID 

METHOD 

NUMBER 

TC-99 -1.93E+01 2.9E+01 90E+01 6.91E+01 pCi/sam 95.10% -0.28 -0.67 3/31/98 0.0214 SA LSC RICHRC5078 

AM-241 301E+00 31E+00 3.1E+00 3.09E+00 pCi/sam 92.60% 0.97 098 4/4/98 0.0219 SA ALPHA-SPEC RICHRC5057 

HEXCHROME 2.00E-03 00E+00 0.0E+00 2.00E-03 mg/L N/A 1. N/A 3/11/98 100.0 ML SPECPHOTO EPA7196 

U-234 4.07E+01 98E+00 1 2E+01 2.37E+00 pCi/sam 63.30% (17.1) (4.1) 4/4/98 0.0226 SA ALPHA-SPEC RICHRC5030 

U-235 3.45E+00 2.9E+00 3.0E+00 2.70E+00 pCi/sam 63.30% (1.3) (1.2) 4/4/98 0.0226 SA ALPHA-SPEC RICHRCS030 

U-238 3.57E+01 9.2E+00 1.1E+01 3.50E+00 pCi/sam 63 30% (10.2) (3.9) 4/4/98 0.0226 SA ALPHA-SPEC RICHRCS030 

PU-238 0.00E+00 0.0E+00 1.1E+00 9.66E-01 pCi/sam 76.10% 0. N/A 4/3/98 0.0219 SA ALPHA-SPEC RICHRC5010 

PU239/40 1.28E+01 4.3E+00 4.6E+00 1.44E+00 pCi/sam 76 1 0% (8.9) (3.) 4/3/98 0.0219 SA ALPHA-SPEC RICHRC5010 

CO-60 -1.94E+01 4.5E+01 4.5E+01 7.58E+01 pCi/sam N/A -0.26 -0.43 3/27/98 0.05 SA GAMMA RICHRC5017 

CS-137DA 1.37E+03 1.2E+02 1.8E+02 N/A pCi/sam N/A N/A (11.6) 3/27/98 005 SA GAMMA RICHRC5017 

EU-152 -3.76E+01 9.4E+01 9.4E+01 155E+02 pCi/sam N/A -0.24 -0.4 3/27/98 0.05 SA GAMMA RICHRC5017 

EU-154 1.52E+01 11E+02 1.1E+02 197E+02 pCi/sam N/A 0.08 0.13 3/27/98 0.05 SA GAMMA RICHRC5017 

EU-155 6.76E+01 80E+01 8.0E+01 1.31E+02 pCi/sam N/A 0.52 0.85 3/27/98 0.05 SA GAMMA RICHRC5017 

STRONTIUM 1.30E+03 7.1E+01 4.3E+02 3.26E+01 pCi/sam 87.40% (40) (18.4) 4/2/98 0.0218 SA AB RICHRC5006 

C-14 -2.42E+00 2.9E+01 4.6E+01 7.00E+01 pCi/sam 100.00% -0.03 -008 4/2/98 0.0223 SA LSC RICHRC5022 

NI-63 2.47E+02 3.1E+01 9.8E+01 593E+01 pCi/sam 94.30% (4.2) (7.9) 415/98 0.0223 SA LSC RICHRCS069 

SE-79 3.29E-01 3.1E+01 1.1E+02 7.38E+01 pCi/sam 73.70% 0. 0.01 4/13198 0.0223 SA LSC RICHRC5043 

C-) 

(_Number of Resu lts: 117 

^t 

C-e 

Comments:

FORM I Date: 4/16/1998 



LAB SAMPLE ID: 80320601 REPORT NBR: 4835 RECEIVED DATE: 3/11/1998 11:57:00 AM 



COUNTING 

ERROR(2s) 

TOTAL ERROR 

(2 s) MDA 

REPORT 


ANALYSIS 

DATE 

ALIQUOT 

SIZE 

ALQ 

UNIT 

DETECTOR 

ID 

METHOD 

NUMBER 

TC-99 -801E+00 2.9E+01 9.1E+01 6.98E+01 pCi/sam 95.10% -0.11 -0.27 3/31/98 0.0213 SA LSC RICHRC5078 

AM-241 3.65E+00 3.6E+00 3.7E+00 2.47E+00 pCi/sam 83.00% (1.5) 0 ) 4/4/98 00207 SA ALPHA-SPEC RICHRCS057 

HEXCHROME 2.00E-03 0.0E+00 0.0E+00 2.00E-03 mg/L N/A 1. N/A 3/12/98 100.0 ML SPECPHOTO EPA7196 

U-234 3.50E+01 8.7E+00 1.1E+01 1.46E+00 pCi/sam 58.10% (24.) (4) 4/5/98 0.0257 SA ALPHA-SPEC RICHRC5030 

U-235 4.27E+00 3.1E+00 3.1E+00 2.17E+00 pCi/sam 58.10% (2.) (1.4) 4/5/98 0.0257 SA ALPHA-SPEC RICHRCS030 

U-238 5.12E+01 1.1E+01 1.4E+01 2.17E+00 pCi/sam 58.10% (23.6) (49) 4/5/98 0.0257 SA ALPHA-SPEC RICHRC5030 

PU-238 3.65E-01 8.0E-01 8.0E-01 1.59E+00 pCi/sam 80.20% 0.23 0.46 413/98 0.0207 SA ALPHA-SPEC RICHRC5010 

PU239/40 4.36E+00 2.6E+00 2.7E+00 1.07E+00 pCi/sam 80.20% (4.1) (1.7) 4/3/98 0.0207 SA ALPHA-SPEC RICHRCS010 

CO-60 5.67E+01 3.4E+01 3.4E+01 6.81E+01 pCi/sam N/A 0.83 (1.7) 3/27/98 0.0504 SA GAMMA RICHRC5017 

CS-137DA 2.82E+02 66E+01 7.2E+01 NIA PCs/Sam N/A N/A (43) 3127/98 00504 SA GAMMA RICHRC5017 

EU-152 6.01E+00 87E+01 87E+01 1.46E+02 pCi/sam N/A 0.04 0.07 3/27/98 0.0504 SA GAMMA RICHRC5017 

EU-154 689E+01 1.0E+02 1.0E+02 1.98E+02 pCi/sam N/A 0.35 0.66 3/27/98 00504 SA GAMMA RICHRC5017 

EU-155 3.04E+01 7.6E+01 7.6E+01 1.20E+02 pCi/sam N/A 0.25 0.4 3/27/98 0.0504 SA GAMMA RICHRC5017 

K-40 1.49E+03 12E+03 1.2E+03 NIA pCi/sam N/A N/A (1.2) 3/27/98 0.0504 SA GAMMA RICHRC5017 

STRONTIUM 4.78E+01 1.7E+01 2.3E+01 2.99E+01 pCi/sam 88.20% (1.6) (2.8) 4/2/98 0.0211 SA AB RICHRCS006 

C 

C-14 2.95E+01 3.3E+01 5.1E+01 7.60E+01 pCi/sam 100.00% 0.39 0.89 412198 0.0203 SA LSC RICHRC5022 

O NI-63 -303E-01 29E+01 89E+01 7.01E+01 pCi/sam 85.70% 0 -0.01 415/98 0.0208 SA LSC RICHRC5069 

F-^ 

5E-79 -117E01 3.3E*01 1.2E+02 7.94E+ 01 pCi/sam 73.50% -0.15 -0.35 4/13/98 0.0207 SA LSC RICHRC5043 

Number of Results: 18 

Comments:


TC-99 1 13E+02 

AM-241 3 74E+03 

U-234 7 12E+01 

U-235 5 94E+00 

U-238 2 27E+01 

PU-238 4 97E+02 

PU239/40 1 34E+04 

AM-241 3 72E+03 

CO-60 8.22E+03 

CS-137DA 1.36E+06 

EU-152 9 35E+03 

E U-154 1 85E+03 

E U-155 -1 56E+01 

STRONTIUM 4 33E+05 

C-14 6.59E+02 

NI-63 2.76E+05 

c1 

^ SE-79 7.68E+02 

~lumber of Results: '17 

Comments: 



10E+03 3.2E+03 

5.3E+02 7.7E+02 

6.6E+01 6.8E+01 

2.8E+01 2.8E+01 

3 8E+01 3.9E+01 

1.6E+02 1.7E+02 

8.2E+02 1.9E+03 

2.5E+03 2.5E+03 

2.7E+02 8.6E+02 

1.4E+05 1.4E+05 

1 SE+03 1.7E+03 

3.8E+02 4.2E+02 

7.7E+02 7.7E+02 

6.3E+03 1.6E+0S 

5 9E+02 9.1 E+02 

3.7E+03 3.5E+04 

7.8E+02 2.9E+03 

FORM Date: 4/16/1998 





MDA 

REPORT 


ANALYSIS 

DATE 

ALIQUOT 

SIZE 

ALQ 

UNIT 

DETECTOR 

ID 

2.40E+03 pCi/sam 95.10% 005 0.11 4/2/98 0.000626 SA LSC 

5.14E+01 pCi/sam 105.50% (72.8) (7.) 4/3/98 0.000836 SA ALPHA-SPEC 

898E+01 pCi/sam 73.10% 0.79 (1.1) 4/4/98 0.000839 SA ALPHA-SPEC 

8.35E+01 pCi/sam 73.10% 007 0.22 4/4/98 0.000839 SA ALPHA-SPEC 

7 20E+01 pCi/sam 73.10% 0.31 0.59 4/4/98 0.000839 SA ALPHA-SPEC 

5.00E+01 pCi/sam 6330% (9.9) (3.2) 3/31/98 0.000836 SA ALPHA-SPEC 

3.36E+01 pCi/sam 63.30% (398.7) (16.4) 3/31/98 0.000836 SA ALPHA-SPEC 

N/A pCilsam N/A N/A (1.5) 3/26/98 0.4107 SA GAMMA 

N/A pCi/sam N/A N/A (30.9) 3/26/98 0.4107 SA GAMMA 

N/A pCi/sam N/A N/A (10.) 3/26/98 0.4107 SA GAMMA 

N/A pCi/sam N/A N/A (6.4) 3/26/98 04107 SA GAMMA 

N/A pCi/sam N/A N/A (4.9) 3/26/98 0.4107 SA GAMMA 

1.25E+03 pCi/sam N/A -0.01 -0.02 3/26/98 0.4107 SA GAMMA 

8.16E+02 pCi/sam 99.90% (530.) (68.5) 4/1/98 0-000837 SA AB 

1.34E+03 pCi/sam 100.00% 0.49 (1 1) 4/9/98 0.001142 SA LSC 

2.00E+03 pCi/sam 76.00% (138.3) (74.3) 4/3/98 0.000831 SA LSC 

1.80E+03 pCi/sam 79.50% 043 0.99 4/1/98 0.00085 SA LSC 

METHOD 

NUMBER 

RICHRC5078 

RICHRC5057 

RICHRC5030 

RICHRCS030 

RICHRC5030 

RICHRCS010 

RICHRC5010 

RICHRC5017 

RICHRCS017 

RICHRCS017 

RICHRC5017 

RICHRC5017 

RICHRC5017 

RICHRCSW6 

RICHRC5022 

RICHRC5069 

RICHRC5043

FORM I Date: 4/16/1998 



LAB SAMPLE ID: 80320603 REPORT NBR: 4835 RECEIVED DATE: 3/11/1998 11'.57.00 AM 



COUNTING 

ERROR(2s) 

TOTAL ERROR 

(2s) MDA 

REPORT 


ANALYSIS 

DATE 

ALIQUOT 

SIZE 

ALO 

UNIT 

DETECTOR 

ID 

METHOD 

NUMBER 

TC-99 -9.47E+00 2.5E+01 7.9E+01 6.04E+01 pCi/sam 95.10% -0.16 -0.37 3/31/98 0.0245 SA LSC RICHRCS078 

AM-241 3.43E+00 3.1E+00 3.1E+00 186E+00 pCi/sam 93.80% (1.8) (1.1) 4/4/98 0.0245 SA ALPHA-SPEC RICHRCS057 

HEXCHROME 3.00E-03 0.0E+00 0.0E+00 2.00E-03 mg/L N/A (1.5) N/A 3/12/98 1000 ML SPECPHOTO EPA7196 

U-234 4.23E+01 1.1E+01 1.4E+01 282E+00 pCilsam 47.30% (16.1) (4.) 4/4/98 0.0272 SA ALPHA-SPEC RICHRCS030 

U-235 6.00E-01 1.3E+00 1.3E+00 2.62E+00 pCi/sam 47.30% 0.23 0.46 4/4/98 00272 SA ALPHA-SPEC RICHRC5030 


PU-238 8.22E-01 1.3E+00 1.3E+00 2.04E+00 pCi/sam 58.70% 0.4 0.65 4/3198 0.0255 SA ALPHA-SPEC RICHRCS010 

PU239/40 7.04E+00 3.6E+00 3.7E+00 2.23E+00 pCi/sam 58.70% (3.2) (2.) 4/3/98 0.0255 SA ALPHA-SPEC RICHRC5010 

CO-60 6.12E+00 3.9E+01 3.9E+01 6.99E+01 pCilsam N/A 0.09 0.16 3/27/98 0.0517 SA GAMMA RICHRC5017 

CS-137DA 1.48E+03 9.8E+01 1.8E+02 N/A pCilsam N/A N/A (151) 3/27/98 0.0517 SA GAMMA RICHRCS017 

EU-152 403E+01 9.2E+01 9.2E+01 1.59E+02 pCi/sam N/A 0.25 0.44 3/27/98 0.0517 SA GAMMA RICHRC5017 

EU-154 -4 46E+01 1.1E+02 1.1E+02 179E+02 pCi/sam N/A -0.25 -0.41 3/27/98 0.0517 SA GAMMA RICHRC5017 

EU-155 -1.89E+01 7.4E+01 7.4E+01 1 15E+02 pCi/sam N/A -0.16 -0.26 3/27/98 0.0517 SA GAMMA RICHRC5017 

K-40 1.91E+03 1.1E+03 1.1E+03 N/A pCi/sam N/A N/A (1.8) 3/27/98 0.0517 SA GAMMA RICHRC5017 

STRONTIUM 6.79E+02 5.1E+01 2.5E+02 3.46E+01 pCi/sam 86.30% (19.6) (13.3) 4/2/98 0.0241 SA AB RICHRC5006 

C-14 9.21E+01 3.0E+01 4.5E+01 6.40E+01 pCi/sam 100.00% (1.4) (3.1) 4098 00243 SA LSC RICHRC5022 

NI-63 1.60E+02 2.6E+01 8.0E+01 5.20E+01 pCi/sam 93.70% (3.1) (6.1) 4/5/98 0.0255 SA LSC RICHRCS069 

Fes+ 

SE-79 8.50E-01 2.7E+01 97E+01 6.33E+01 pCi/sam 74.30% 0.01 0.03 4/13/98 0.0257 SA LSC RICHRC5043 

C.) Number of Results: 18 

Comments:

FORM Date: 4/16/1998 






TC-99 -3.92E+00 

AM-241 1 42E+00 


U-234 3.81E+01 

U-235 1.44E+00 

U-238 4.34E+01 

PU-238 -5.63E-02 

PU239/40 1.06E+00 

CO-60 5.23E+01 

CS-137UA 6.18E+02 

EU-152 1 68E+01 

EU-154 -1.14E+01 

EU-155 2.57E+01 

K-40 5.80E+03 


C-14 2.28E+01 

c-) NI-63 7.60E+01 

C SE-79 -1.37E+00 

h-^ 

"Number of Resu lts: 118 

Comments: 



2.5E+01 7.7E+01 

2.1E+00 2.1 E+00 

0.0E+00 0.0E+00 

9.4E+00 1.2E+01 

2.0E+00 2.0E+00 

1 0E+01 1.3E+01 

8.0E-02 8.0E-02 

1.2E+00 1.2E+00 

3.6E+01 3.6E+01 

8.0E+01 1.0E+02 

86E+01 86E+01 

1.1E+02 1.1E+02 

7.5E+01 7.5E+01 

7.6E+02 9.6E+02 

3.1 E+01 7 5E+01 

2.6E+01 4.1E+01 

2.3E+01 7.1 E+01 

2 6E+01 9.4E+01 

REPORT 


5.82E+01 pCi/sam 95.10% 

2.97E+00 pCi/sam 86.60% 

2.00E-03 mg/L N/A 

3.39E+00 pCi/sam 5480% 

3.39E+00 pCi/sam 54.80% 

2.61E+00 pCi/sam 54.80% 

1.61 E+00 pCi/sam 72.60% 

9.52E-01 pCi/sam 72.60% 






172E+03 pCi/sam N/A 

3.47E+01 pCi/sam 73.80% 

6.00E+01 pCi/sam 100.00% 

5.05E+01 pCUsam 95.10% 

6.14E+01 pCi/sam 76.70% 

RST/MDA RST/CNTERR 

-007 -016 

048 0.68 

1- N/A 

(11 2) (41) 

0.42 0.72 

(168) (4.3) 

-0.04 -0.71 

(i.t) 087 

072 (1 5) 

N/A (77) 

0.12 02 

-006 -01 

0.21 034 

(3.4) (7.6) 

(6.) (6-8) 

0.38 087 

(1.5) (33) 

-0.02 -005 

ANALYSIS 

DATE 

3131/98 

4/4/98 

3/13/98 

4/4/98 

4/4/98 

4/4/98 

4/3/98 

4/3/98 

3/27/98 

3/27/98 

3/27/98 

3/27/98 

3/27/98 

3/27/98 

4/2/98 

4/2/98 

4/5/98 

4/13/98 

ALIQUOT ALQ 

SIZE UNIT 

00254 SA 

00255 SA 

100.0 ML 

0.0264 SA 

0.0264 SA 

0.0264 SA 

0.0255 SA 

0.0255 SA 

0.0507 SA 

00507 SA 

0.0507 SA 

00507 SA 

0.0507 SA 

0.0507 SA 

0.0254 SA 

0.0257 SA 

0.0259 SA 

00257 SA 

DETECTOR 

ID 

LSC 

ALPHA-SPEC 

SPECPHOTO 

ALPHA-SPEC 

ALPHA-SPEC 

ALPHA-SPEC 

ALPHA-SPEC 

ALPHA-SPEC 

GAMMA 

GAMMA 

eIDLllr_1 

CeL1S11ra 

GAMMA 

GAMMA 

AB 

LSC 

LSC 

LSC 

METHOD 

NUMBER 

RICHRCS078 

RICHRCS057 

EPA7196 

RICHRCS030 

RICHRCS030 

RICHRC5030 

RICHRCS010 

RICHRCS010 

RICHRCS017 

RICHRCS017 

RICHRC5017 

RICHRC S017 

RICHRC5017 

RICHRCS017 

RICHRC5006 

RICHRC5022 

RICHRC5069 

RICHRCSO43

FORM I Date: 4/16/1998 






COUNTING 

ERROR(2s) 

TOTAL ERROR 

(2 s) MDA 

REPORT 

UNIT YIELD RST/MDA RSTICNTERR 

ANALYSIS 

DATE 

ALIQUOT 

SIZE 

ALQ 

UNIT 

DETECTOR 

ID 

METHOD 

NUMBER 

TC-99 2.45E+02 9.7E+02 3.0E+03 2.22E+03 pCi/sam 95.10% 0.11 0.25 4/2/98 0.000677 SA LSC RICHRC5078 

AM-241 313E-03 6.6E+02 8.4E+02 140E+02 pCi/sam 86.50% (22.4) (4.7) 4/4/98 0.000655 SA ALPHA-SPEC RICHRCS057 

U-234 266E+01 43E+01 4.3E+01 755E+01 pCdsam 8150% 035 0.62 4/4198 0.000662 SA ALPHA-SPEC RICHRC5030 

U-235 0.00E+00 0.0E+00 4.5E+01 4.10E+01 pCi/sam 81.50% 0. N/A 4/4/98 0.000662 SA ALPHA-SPEC RICHRC5030 

U-238 5.81 E+01 6.1 E+01 6.1 E+01 6.92E+01 pCi/sam 81,50% 0.84 0.96 4/4/98 0.000662 SA ALPHA-SPEC RICHRCS030 

PU-238 214E+02 1.1E+02 1.2E+02 6.59E+01 pCi/sam 70.80% (3.2) (1.9) 3/31/98 0.000655 SA ALPHA-SPEC RICHRC5010 

PU239/40 6.89E+03 6.3E+02 1.1E+03 7.19E+01 pCi/sam 70.80% (95.8) (10.9) 3/31/98 0.000655 SA ALPHA-SPEC RICHRC5010 

AM-241 2.75E+03 4.7E+02 5.4E+02 N/A pCi/sam N/A N/A (5.9) 3/26198 0.42 SA GAMMA RICHRC5017 

CO-60 3.83E+03 1.8E+02 4.2E+02 N/A pCi/sam N/A N/A (21.7) 3/26/98 0.42 SA GAMMA RICHRC5017 

CS-137DA 6.16E+05 1.9E+03 6.2E+04 N/A pCi/sam N/A N/A (320.5) 3/26198 0.42 SA GAMMA RICHRC5017 

EU-152 6.96E+03 8.6E-02 1.1E+03 WA pCi/sam N/A N/A (8.1) 3/26198 042 SA GAMMA RICHRC5017 

EU-154 1 74E+03 2.0E+02 2.7E+02 4.53E+02 pCUsam N/A (3.8) (8.7) 3/26/98 0.42 SA GAMMA RICHRC5017 


STRONTIUM 4.06E+05 70E+03 1.5E+05 1.02E+03 pCi/sam 94.20% (3991) (58.2) 4/1/98 0.000661 SA AB RICHRC5006 

0-14 3.75E+01 6.0E+02 9.3E+02 1 42E+03 pCi/sam 100.00% 0.03 0.06 4/9/98 0.001081 SA LSC RICHRC5022 

c: 

NI-63 2.23E+05 3.7E+03 2.9E+04 2.42E+03 pCi/sam 77.30% (923) (60.) 413/98 0000675 SA LSC RICHRC5069 

O 

I,_ 

SE-79 -6.38E+02 10E+03 38E+03 244E+03 pCi/sam 76.00% -026 -0.63 4/1/98 0000657 SA LSC RICHRC5043 

G Number of Results: 17 

Cov ents:

TC-99 

AM-241 

HEXCHROME 

U-234 

U-235 

U-238 

PU-238 

PU239/40 

CO-60 

CS-137DA 

E U-152 

EU-154 

EU-155 

-8 74E+00 

3 67E+00 

9 OOE-03 

3 48E+01 

6.02E-01 

3.72E+01 

3.57E-01 

1.28E+01 

3.99E+01 

9.23E+02 

1 09E+00 

-1 13E+02 

-1 46E+01 

K-40 1.18E+03 


C 14 5.30E+01 

C) NI-63 1.99E+02 

O 

1-+ SE-79 1.80E+01 

CT) 


FORM I Date: 4/16/1998 





COUNTING TOTAL ERROR REPORT ANALYSIS ALIQUOT ALQ DETECTOR METHOD 

ISOTOPE RESULT ERROR(2s) (2 s) MDA UNIT YIELD RST/MDA RST/CNTERR DATE SIZE UNIT ID NUMBER 

Comments: 

2.7E+01 8.3E+01 635E+01 pCi/sam 95.10% -014 -0.33 3/31/98 0.0233 SA LSC RICHRC5078 

3.3E+00 3.4E+00 300E+00 pCi/sam 89.30% (1.2) (11) 4/4/98 0.0234 SA ALPHA-SPEC RICHRC5057 

0.0E+00 0.0E+00 2.00E-03 mg/L N/A (4.5) N/A 3/13/98 100.0 ML SPECPHOTO EPA7196 

9.2E+00 1.1E+01 2.75E+00 pCosam 54.00% (12.7) (3.8) 4/4/98 0.0251 SA ALPHA-SPEC RICHRC5030 

1.2E+00 1.2E+00 1.63E+00 pCi/sam 54.00% 0.37 0.5 4/4/98 0.0251 SA ALPHA-SPEC RICHRC5030 

9.5E+00 1.2E+01 2.75E+00 pCi/sam 54.00% (13.5) (3.9) 4/4/98 0.0251 SA ALPHA-SPEC RICHRC5030 

7.1E-01 7.2E-01 9.67E-01 pCi/sam 72.60% 0.37 0.5 4/198 0.0234 SA ALPHA-SPEC RICHRC5010 

4.3E+00 4.6E+00 1.44E+00 pCi/sam 72.60% (8.9) (3.) 4/3/98 0.0234 SA ALPHA-SPEC RICHRC5010 

4.2E+01 4.2E+01 7.63E+01 pCi/sam N/A 052 0.96 3127/98 0.0532 SA GAMMA RICHRC5017 

9.0E+01 1.3E+02 N/A pCi/sam N/A N/A (10.3) 3/27/98 0.0532 SA GAMMA RICHRC5017 

9.5E+01 9.5E+01 1.62E+02 pCi/sam N/A 0.01 001 3/27/98 0.0532 SA GAMMA RICHRC5017 

11E+02 1.1E+02 167E+02 pCi/sam N/A -0.68 -(1.1) 3/27/98 0.0532 SA GAMMA RICHRC5017 

8.7E+01 8.7E+01 1.42E+02 pCi/sam N/A -0.1 -0.17 3/27198 0.0532 SA GAMMA RICHRC5017 

8.4E+02 8.5E+02 N/A pCi/sam N/A N/A (14) 3/27198 0.0532 SA GAMMA RICHRC5017 

4.7E+01 2.3E+02 2.97E+01 pCi/sam 95.80% (20.6) (13.1) 4098 0.0234 SA AB RICHRC5006 

3.0E+01 4.6E+01 670E+01 pCi/sam 100.00% 0.79 (1.8) 4/2/98 0.0233 SA LSC RICHRC5022 

3.2E+01 9.8E+01 6.31E+01 pCi/sam 80.10% (3.2) (6.3) 46198 00246 SA LSC RICHRC5069 

3.2E+01 1.2E+02 7.52E+01 pCi/sam 69.20% 0.24 0.57 4113/98 0.0234 SA LSC RICHRCSO43

FORM I Date: 4/16/1998 






COUNTING 

ERROR(2s) 

TOTAL ERROR 

(2 s) MDA 

REPORT 


ANALYSIS 

DATE 

ALIQUOT 

SIZE 

ALQ 

UNIT 

DETECTOR 

ID 

METHOD 

NUMBER 

TC-99 282E+01 28E+01 86E+01 6.38E+01 pCi/sam 95.10% 0.44 0 ) 3131/98 00232 SA LSC RICHRCS078 

AM-241 2.31E+00 2.7E+00 2.7E+00 2.08E+00 pCi/sam 86.20% (1.1) 0.87 4/4/98 0.0241 SA ALPHA-SPEC RICHRC5057 

HEXCHROME 200E-03 0.0E+00 0.0E+00 2.00E-03 mg/L N/A 1. N/A 3113/98 100.0 ML SPECPHOTO EPA7196 

U-234 2.94E+01 7.9E+00 9.SE+00 2.12E+00 pCi/sam 65.10% (13.9) (3.7) 4/4/98 0.0249 SA ALPHA-SPEC RICHRC5030 

U-235 1.01E+00 1.5E+00 1.5E+00 2.12E+00 pCi/sam 65.10% 0.48 068 4/4/98 0.0249 SA ALPHA-SPEC RICHRC5030 


PU-238 0.00E+00 0.0E+00 1.2E+00 1.10E+00 pCi/sam 64.10% 0, N/A 4/3/98 0.0241 SA ALPHA-SPEC RICHRC5010 

PU239/40 6.11E+00 3.2E+00 3.3E+00 1.10E+00 pCi/sam 64.10% (5.5) (1_9) 4/3/98 0.0241 SA ALPHA-SPEC RICHRC5010 

CO-60 -276E+01 3.9E+01 3.9E+01 6.25E+01 pCi/sam N/A -0.44 -0.71 3/27/98 0.0504 SA GAMMA RICHRCS017 

CS-137DA 3.77E+02 8.5E+01 9.3E+01 N/A pCi/sam N/A N/A (4.4) 3/27198 0.0504 SA GAMMA RICHRC5017 


EU-154 344E+01 94E+01 9.4E+01 1 70E+02 pCi/sam N/A 0.2 0.37 3/27/98 00504 SA GAMMA RICHRCS017 

EU-155 2.20E-01 7.6E+01 7.6E+01 1.20E+02 pCi/sam N/A 0 0. 3/27/98 0.0504 SA GAMMA RICHRC5017 

STRONTIUM 1.36E+02 2.3E+01 5.1E+01 2.85E+01 pCi/sam 91.90% (4.8) (5.9) 4098 0.0241 SA AB RICHRC5006 

C-14 509E+01 30E+01 46E+01 670E+01 pCi/sam 100.00% 0.76 (L7) 412/98 00232 SA LSC RICHRC5022 

NI-63 8.95E+01 2.4E+01 7.3E+01 5.16E+01 pCilsam 102.30% (1.7) (3.7) 4/5198 0.0241 SA LSC RICHRCS069 

SE-79 -1.32E+01 3.3E+01 1.2E+02 7.98E+01 pCi/sam 68.00% -0.17 -0.4 4113/98 0.0223 SA LSC RICHRCSO43 

Qlumber of Results: 17 

O 

Comments:

C 

H 

FORM I Date: 4/16/1998 


LAB NAME: OUANTERRA, Richland SDG: W02275 COLLECTION DATE: 3/16/1998 8:30:00 AM 




COUNTING 

ERROR (2 s) 

TOTAL ERROR 

(2 s) MDA 

REPORT 


ANALYSIS 

DATE 

ALIQUOT 

SIZE 

ALO 

UNIT 

DETECTOR 

ID 

METHOD 

NUMBER 

TC-99 -1.27E+03 92E+02 29E+03 224E+03 pCi/sam 95.10% -0.56 -(1.4) 4/2/98 0.00067 SA LSC RICHRC5078 

AM-241 7.76E+03 1.0E+03 1.7E+03 138E+02 pCi/sam 96.40% (56.4) (7.5) 4/4/98 0.000667 SA ALPHA-SPEC RICHRCS057 

U-234 2.97E+01 4.4E+01 4.4E+01 6.23E+01 pCi/sam 83.00% 0.48 0.68 4/4/98 0.000664 SA ALPHA-SPEC RICHRCS030 

U-235 -1.24E+00 2.5E+00 2.5E+00 6.23E+01 pCi/sam 8100% -0.02 -0.5 414/98 0.000664 SA ALPHA-SPEC RICHRCS030 

U-238 2.60E+01 4.4E+01 4.4E+01 8.27E+01 pCi/sam 83.00% 0.31 0.59 4/4/98 0.000664 SA ALPHA-SPEC RICHRC5030 

PU-238 4.46E+02 2.0E+02 2.1E+02 9.00E+01 pCi/sam 54.10% (5) (2.2) 3/31/98 0.000667 SA ALPHA-SPEC RICHRC5010 

PU239/40 1.53E+04 1.2E+03 2.5E+03 102E+02 pCi/sam 54.10% (150.2) (13.1) 3131198 0.000667 SA ALPHA-SPEC RICHRC5010 

AM-241 7.27E+03 4.1E+02 8.4E+02 WA pCi/sam N/A N/A (17.7) 3/26/98 0.4048 SA GAMMA RICHRC5017 

CO-60 6-13E+03 2.5E+02 6.6E*02 N pCi/sam N/A N/A (25.) 3/26/98 0.4048 SA GAMMA RICHRC5017 

CS-137DA 766E+05 1.2E+03 77E+04 N/A pCi/sam N/A N/A (618.9) 3/26/98 0.4048 SA GAMMA RICHRC5017 

EU-152 3.30E+04 1.4E+03 3.6E+03 NA pCi;sam N/A N/A (22.9) 3/26/98 0.4048 SA GAMMA RICHRC5017 

EU-154 601E+03 5.5E+02 8.2E+02 N/A pCi/sam N/A N/A (10.9) 3/26/98 0.4048 SA GAMMA RICHRC5017 

EU-155 3.25E+02 4.4E+02 4.4E+02 723E+02 pCi/sam N/A 0.45 0.74 3/26/98 0.4048 SA GAMMA RICHRC5017 

STRONTIUM 4.56E+05 7.2E+03 1.7E+05 1.06E+03 pCi/sam 93.90% (430.5) (63.) 4/1/98 0.000683 SA AB RICHRC5006 

C-14 467E+02 6.5E+02 1.0E+03 1.50E+03 pCi/sam 100.00% 0.31 0.72 4/9/98 0.001022 SA LSC RICHRC5022 

NI-63 3.44E+05 4.4E+03 4.3E+04 227E+03 pCi/sam 81.30% (151.7) (78.) 4/3/98 0.000684 SA LSC RICHRC5069 

SE-79 -2.43E+02 9.6E+02 3.5E+03 2.29E+03 pCi/sam 82.80% -0.11 -0.25 4/1/98 0.000646 SA LSC RICHRC5043 


Comments:

ISOTOPE 

TC-99 

AM-241 

HEXCHROME 

U-234 

U-235 

U-238 

PU-238 

PU239/40 

CO-60 

CS-137DA 

EU-152 

EU-154 

EU-155 

STRONTIUM 

C-14 

NI-63 

SE 79 

RESULT 

5 17E+00 

5 54E+00 

1 40E-02 

3 33E+01 

3 54E-01 

1 95E+01 

0 00E+00 

1 03E+01 

2.65E+01 

1 32E+03 

1 62E+01 

1 56E+02 

4 84E+01 

1 34E+03 

1.22E+02 

8 09E+00 

1.97E+00 


ERROR(2s) ( 2 s) 

2.6E+01 8.3E+01 

3.9E+00 4.0E+00 

0.0E+00 0.0E+00 

7.9E+00 9.8E+00 

9.4E-01 9.4E-01 

6.0E+00 6.9E+00 

0.0E+00 1.0E+00 

3.7E+00 3.9E+00 

3.7E+01 3.8E+01 

1 .3E+02 1 9E+02 

1.0E+02 1 0E+02 

9.1 E+01 9.3E+01 

7.1 E+01 7.1 E+01 

6.9E+01 4.5E+02 

3.2E+01 4.7E+01 

2.6E+01 8.0E+01 

3.1 E+01 1.1E+02 

FORM Date: 4/16/1998 



LAB SAMPLE ID: 80327202 REPORT NBR: 4835 RECEIVED DATE: 3116/1998 12:15.00 PM 



0 

0 

Comments: 

MDA 

REPORT 


ANALYSIS 

DATE 

ALIQUOT 

SIZE 

ALQ 

UNIT 

DETECTOR 

ID 

6.21E+01 pCi/sam 95.10% 0.08 0.2 3/31/98 0.0238 SA LSC 

1.87E+00 pCi/sam 91.60% (3.) (1 4) 4/4/98 0.0247 SA ALPHA-SPEC 

2.00E-03 mg/L N/A (7.) N/A 3/16/98 100.0 ML SPECPHOTO 

2.63E+00 pCi/sam 6820% (12.7) (42) 4/4/98 0.0256 SA ALPHA-SPEC 

2.32E+00 pCi/sam 68.20% 015 0.38 4/4/98 0.0256 SA ALPHA-SPEC 

1.87E+00 pCi/sam 68.20% (10.4) (3.2) 4/4/98 0.0256 SA ALPHA-SPEC 

9.04E-01 pCi/sam 77.40% 0. N/A 4/3/98 0.0247 SA ALPHA-SPEC 

9.03E-01 pCi/sam 77.40% (11.5) (2.8) 4/3/98 0.0247 SA ALPHA-SPEC 

7.00E+01 pCi/sam N/A 0.38 0.71 3/27/98 0.0512 SA GAMMA 

NA pCi/sam N/A N/A (10.1) 3/27/98 00512 SA GAMMA 

1.69E+02 pCi/sam NIA 0.1 0.16 3/27/98 0.0512 SA GAMMA 

1.87E+02 pCi/sam N/A 0.84 (1.7) 3/27/98 0.0512 SA GAMMA 


296E+01 pCi/sam 83.20% (45.3) (19.4) 4/2/98 0.0247 SA AB 

6.50E+01 pCi/sam 100.00% (1.9) (3.8) 4/2198 0.0238 SA LSC 

6.22E+01 pCi/sam 81.50% 0.13 0.31 4/5/98 0.0246 SA LSC 

7.32E+01 pCi/sam 72.40% 0.03 006 4/13/98 0.0228 SA LSC 

METHOD 

NUMBER 

RICHRC5078 

RICHRCS057 

EPA7196 

RICHRC5030 

RICHRC5030 

RICHRC5030 

RICHRC5010 

RICHRC5010 

RICHRCS017 

RICHRCS017 

RICHRC5017 

RICHRCS017 

RICHRC5017 

RICHRC5006 

RICHRC5022 

RICHRC5069 

RICHRCSO43


TC-99 1.04E+01 

AM-241 3.42E+00 


U-234 4.54E+01 

U-235 9.73E-01 

U-238 4.12E+01 

PU-238 0.00E+00 

PU239/40 1.39E+00 

CO-60 4.71E+00 

CS-137DA 283E+02 

EU-152 -4.07E+01 

EU-154 1.48E+02 

EU-155 3.95E+01 

K-40 1.80E+03 


C-14 3.99E+01 

NI-63 7.75E+01 

C) SE-79 122E+01 

O 

)Yujnber of Results: 18 

C.1 

Comments: 

FORM Date: 4/16/1998 







2.7E+01 8.4E+01 

3 4E+00 3.5E+00 

0.0E+00 0.0E+00 

1.0E+01 1.3E+01 

1.6E+00 1.7E+00 

9.8E+00 1.2E+01 

0.0E+00 1.4E+00 

1.6E+00 1 6E+00 

3.7E+01 3.7E+01 

7.8E+01 8.3E+01 

9 0E+01 9.0E+01 

1.0E+02 1.0E+02 

9.0E+01 90E+01 

8.5E+02 8.7E+02 

2.4E+01 5.2E+01 

3.0E+01 4.6E+01 

2.8E+01 8.6E+01 

3.0E+01 1.1E+02 

MDA 

REPORT 


ANALYSIS 

DATE 

ALIQUOT 

SIZE 

ALQ 

UNIT 

DETECTOR 

ID 

6.27E+01 pCi/sam 95.10% 0.17 0.39 3/31/98 00236 SA LSC 

231E+00 pCi/sam 8250% (15) (1 ) 4/4/98 0.0224 SA ALPHA-SPEC 

2.00E-03 mg/L N/A 1. N/A 3/16/98 100.0 ML SPECPHOTO 

3.58E+00 pCi/sam 63.20% (12.7) (4.4) 4/4/98 00226 SA ALPHA-SPEC 

3.09E+00 pCi/sam 63.20% 0.31 0.59 4/4/98 00226 SA ALPHA-SPEC 

398E+00 pCi/sam 63.20% (10.4) (4.2) 414/98 0.0226 SA ALPHA-SPEC 

1.26E+00 pCi/sam 60.00% 0. N/A 4/3/98 0.0224 SA ALPHA-SPEC 

1.26E+00 pCi/sam 60.00% (1.1) 0.87 4/3/98 0.0224 SA ALPHA-SPEC 


N/A pCi/sam N/A N/A (3.6) 3/28/98 00524 SA GAMMA 

1.49E+02 pCi/sam N/A -0.27 -0.45 3/28/98 0.0524 SA GAMMA 

197E+02 pCi/sam N/A 0.75 (1.5) 3/28198 0.0524 SA GAMMA 


N/A pCi/sam N/A N/A (2.1) 3/28198 0.0524 SA GAMMA 

2.77E+01 pCi/sam 85.90% (51) (5.8) 4/2/98 0.0233 SA AB 

6.80E+01 pCi/sam 100.00% 0.59 (1.3) 412/98 0.0228 SA LSC 

6.22E+01 pCi/sam 89.90% (1.2) (2.7) 415/98 0.0222 SA LSC 

6.97E+01 pCi/sam 75.40% 0.17 041 4/13/98 0.023 SA LSC 

METHOD 

NUMBER 

RICHRC5078 

RICHRC5057 

EPA7196 

RICHRC5030 

RICHRCS030 

RICHRC5030 

RICHRC5010 

RICHRC5010 

RICHRC5017 

RICHRCS017 

RICHRC5017 

RICHRC5017 

RICHRC5017 

RICHRC5017 

RICHRC5006 

RICHRC5022 

RICHRC5069 

RICHRC5043

Quanterra Data Review C3eddist 

RADIOCHE.ÎIISTRY 

^xorle G4ver -atnoer r:r. ^3 I L 1 ^' 3 ^ ^ 4 ^ 3 aC^ î322 L ^5 a^ 

Ciem :D' 

No Datc — 

tau Saremie ^'umbcor SI7G: l.^ 22 7 

Method7m ?ammeters: YYl - 7• ti \ 

_ 

0 

Nam= C)'.a, r D e C en.. z„+ 

Item I Ycs (.0 I aeN) I ?UA(J) 

A. Callbnsfon I 

1. Is the nh'bratim dmmtam[im alluded Wtete mp6obk? I I 

& Sample Analrus 

1. Am _he satt role yields iNut acstttaoc c mu? I J 

2 Wes.ul sample holdins tiara ma? I / J 

7. Is the sar..pic .Milumttm Detacib le .iennv < the C. Deeatm Limit? I I I 

C- QC Sampiea 

I. Is ute Siaric i.id wtb= ameounce airma I / I I 

Li st^ .e `.Iinu:am - OtIaC ble A=WY CQ the olank rtsW S Ibe C urnnn Deuaion I I I / ! ` 

J. Is the aiank .quit < L: :he Cantraa Daman Imo? 

a. Is the aia > I;- the C.xtQae D • iirdt bee < C^ Dc m m Cinut? I ^_ 

`. Isthe.iari'.3ult>the Camrt Dace:m i.:mis ba :be smile rtauit

Comments n any -No' response: 

First L :ei 3e•.iett 

Second Lecd Re•.ie•xv 

Form d LS-078.2i%. 

Qaaatcra Data Review Chedciist 

RIDIOCHENUSTRY 

Work Cyder number ( or. SL^31 ^_ y I(o! ,S^CI(o "`22Z 244 ^.3^^^-- 

Cietn ID: R N r— 

Due oats: - G - 9 

Lab Sammie Number or SDG,i tr.! 

Method Test ?ammeter: f t a ut 

Z27^ 

Munn- Q L L L. r'r 

Rnnevl I Ye (•/) I `loft) I &A(1) I'Lard 

Review lJl 

A. CaUbmtIon 

1. Is the nhbtwbb docwnevacm inchtded Wore app6ethle? 

I 

I / 

a Simple AtWpis 

I. Am the sample vielda wmitm atzsatatre anena7 

I /^ 

Z W ere 311 sample holdms time nn^ 

I I 

3. Is the s ie Mnimum Detectable A=nr y < the C^ Detattna Lent? 

C. QC Samples 

1. Is the blank •leld Wthm •=cs, siren. 

:. Is the Minunum Detectable A=vnY for the Blanc rout S the Caaae Daaston 

Litrut? 

3. Is the blank . ^ it < L: the Caneacc Detemon L _.? 

S, Is the alw3 > I,- the C.Yne9G Dawson L 1t tta < C.IICYS Dc,— Llmnl? 

!. Is the olaruc It> the ComnG Desec'on :nut hotthe sa>Rle nstt

First Lc. ei 

Second '_z% -I 

Form d 1-64 i96. Ret 1 

Quzu= a Data Review Checklist 

RADIOCHE KISTRY 

Work Oraerypnoer ,ak 

^3^ 4 8031 ^1 ^3ao6 ^^zzz 8^3^'r X27 

Cicm!D' .tJ N --j_ 

Due Due: 4— 

Lab Sartmie ` umber or SOG: 

1lethod -M .'mntmurs: P •^ ^ 

Muni. 

Renew Item ( Yea (J) I !7o (J) I WA(J) 11'Sssei 

;ess^ (.0 

A. Cailbrauoit 

1. Is the calrlumas doaunau ation included where applicable? 

a Sempie .iadrsie 

I / 

1. Arc the sample yields within •^^mane citniat 

Z Were all sample holding:imn me? 

I ^^ 

7. Is :he zvrpie 11uumum De:stahle k=hN < the Cm Detection Limit^ 

C QC Samples 

1, Is the biarA '•+eid wthin ae-eovncc ct.—t . a 

f. 

T?Ithe ^•t^.lf:3ml Der[Cadlt.i4'.IVIN:Cf :h the C,lntl 

Detection a^:? 

ctC4an . J l but the sampie rmlh

Qumzm a Data Review Cheddist 

RADIOCHEMISTRY 

war< over -umaer ^, t: i 31(o I 3 i v F^3 a•o 3 Z zZ 8C3 a 7 

Clem fn . $1+Z 

Due our. Lk- (O - k 

Cab Sammie Number ar SDG: (P ZZ 7 

Nethed 7= is tsnnes: 

u,avc C: ^_CeM^.,-t 

A. CGllbradon 

1. Is the ralibn = doevmerpasim aebsdeb w e s¢eahl ? 

se„ICV lt® I Ye(J) I No(J) I VA(J) 

& Semple Arraign I 

1. Ate the sample neids sec" tt= aÔUptx esteriat 

I 

II 

17niew (J) 

I / 

II II 

Z. W ere all ==It holdio3 time inn? I ^ I j ^ I i 

3. Is Ne sample \Ivsirss,m, Dens-^bk .ieJnry < yeGmn Deserswn Ijmit^ I I j l— ^ I 

C QC Sampies I 

1. Is the blamer •.field within aetrar>re =t .a 

Is :he `du= Detectable Aesn,v far l le Sara rink S the Cc Des ern I 

Lirmt7 

3. Is the dia r=un < l.= the Cra¢,a Dâm tin? 

4. IS [he JINN > I,- the C.M?]C: DacJan i -1t II, < O,,,, a DQeGr41 LIIIYIT 

!. is the dark .a it > the Car, n L)d=on _:= hoebe samplensuh

Qaaatena Data Review Checklist 

RADIOCE9MMY 

Work Order„ambtlsk 8031 .3q T031G 03 0(0 8(3 D -a 3aNN o317^ 

C.iaa ID: U ^// 

Due Datc. 

Lab Satmk Number m SDO: 

GG 

'to Î 

w^ as -t S 

Mepmd Tea Pu® U 

Ô 

M. Mx 

Rin wltm Ye(J) HON) VA(V) Tiled 

A. Cailbradoa 

1. Is the dbalmdoc mausum u tchwad- Im M*kz [a? 

IL Sample Analysis 

1. M the sa iple yidda with= ameouac= abeia? !/ 3 / 

2 Were all sample bolding tesee an? I I I - 

3. Is the saaWie Minnu m Deeaahle .Acm y < the Conta ct Deua an Unav 

^v 

Date y^^ %^J 

Date: 

` 3 ` 

I 3 

C QC Sample 

1. Is the blank yield wigs acceptance ancris 3 

^tthe Mim nu n Dd=able Activity la the black ^ 5 the Ceetraa D etec tive ( 

I I I _ i 

3. Is the blank teals < L_ the C.smaa Ddectta Lunt? I 

3 

3 I r 

`, 

S. Is the blank > It' the Contact Ddemm Lim but < Catract Detection Lao I ( 3 I - 

5. Is the blank result > the Contract Deeom Lank but the savle renh

Qutm=Ta Data Rcview CLeddiu 

RADIOCIM0 1LSMY 

Wok O mer,mtsea r,t $ 316 1 8011V43 9° a()6 3:) ;t 

Chen ID* 

Dim Dare lily 

Lab Sammie Nmobw er SDCr. 

.Method Tea Psnsrm 

41sms 

I 

>n. â a "7 5 

RZME Item Yam (J) 140(01 ) I WA(J ) 1Îsed 

Rs+isr•!Jl 

A. Ca llbradam 

1. Is the sal3num doemameam ioduded Mus a*kabia? ^. 

S Sampee Asuiris 

1. An the sarmle?itidt - anseuome avmia? !/ 

1 Were all samplc bold* —m? 

3. Is the sur¢ie 4fakmem Daemhle Acuvdr < the Camas Datum t3mt? I I 3 

C. QC Samples 

1. Is the blank r cld wirhm scecomma m a 3 I I I 

2 Is the 4lutunum Daeamble Amvm (rr the blank rack S the Caara a Detetim 

[.unit? 

I 

3 

I /_ 

3. V the blank trsua < I!- :he Caatna Docc uau Unlit? I 

3 

/ 

s. Is the blank > Ir the Caeeraa Daaaeo 1= ba < C.srmaa Damask omit? I I ( 3 ' 

3. Is the blank :mh> the Cauraaa Dettsesm Lino bm the sampie nmlt < the Cavaa 

Detaitan Lirtut^. I f 3 

6. Is the i.CS rook wuhm a¢sprafoe vuaa? 

7. Is the LCS neldvdth in aaxponre cmrna 

8. Is the LCS Mirm Detecahk Acttrn:/ 5 the Camaa Deenim Lam? 

9. 415%4tSD rauln aM peld nm •^ r++^+ mtau7 

10. Duplicate wnple tesuus and r dd am s¢epuoce av I 

D. Other 

1. Are all ìomm nfommsm vsmded and ased? 

Are ail required forms Ned oLaC 

3. Corm= acbodaioa used? I 

4. Traractpuen ducked.' 

S. Were all calculaiau ducked at a nar>nam fsogo ? ei 

6. Unats Checked' 

Comments on any -No' response: 

First Lwe! 3etdav: L% Li- È^^{^t` Date: 

Second LL%--! Rrviewl Date: 

Form #: LS -038 .2 196. Rev 4 

3 

I I I j 

60 57

QUANTERRA LABORATORY NONCONFOR:N L-kNCE VIEmO (NCNI) 

PAGE 1 OF 2 

Project ID: 

Sample Numbers: 

r 

M 

NCM mriated by 

0 32 -7,202 D 03^7â 

Tests: —fô 

Matrix: y ^l u / D^ 7 

Analytical Area (cheek soorooriate area): 

LOG =: RD-98, 

• Sample control q GC Cl Wttchemistry l O-lData review 

• Organic preparation q HPLC q heals P'Rkadiochemistry 

• Inorganic p reparation q GC/MS q Reporting q Bioassay 

Nonconformance (check appropriate area): 

Holding Time rzolations (exceeded by days) QuAyAssurance/Quality Control 

Category 1. Laboratory Independent q 17. QC data repo rted outside of controls 

q I. Holding time expired in transit q 13. Incorrect procedure used 

q 2. Sample received > 48 hrs. or I/2 holding time has 

expired 

q 19. SOP intentionally modified tivith QA and Tech. approval 

q 3. Test added by client after expiration q 20. Imalid instrument calibration 

Category Il: Laborator y Dependent 

q 4. Instrument failure 

Cl 21- Insu ffi 

cient sample received for proper analysis 

Incomyror Incomplete Client Deliverable 

q 5. Analyst error q 2 Hardcopy deliverable error 

q 6. Login error q -13. Electronic deliverable error 

q 7. Miscommunication 

Reported detection limits eleti-ated due to: 

q 8. Other (complete description required) q 24. Sample matrix 

Category III: Analysis Reruns (OA, QC) q 2i. Insufficient sample volume 

q 9. 

IQ 

Surrogates 

Inte 

q 26- Other (complete description required) 

27. Other (specify): _ 

ZL CGh- `C 

rn al Standards 

q 11. Spike Reco • eries 

q 1 2. Blank Contamination 

Category Il'. .anal.sis Rerms (Conf+nrtation) 

q 13. Second column 

q 1 4. Contamination check 

q 15. Confirmation of matrix effects 

q 16. Other (complete desc ription required) 

Noti fi cation ( check appropriate area): 

Com>¢nts/Esplaînation 

Client noti fied by (name and date): Client "s name and respon s e 

d 

VtSu ` do ^, f _ 

GU! 71{7 Ê?L t / 

q jtf «Hung q by facsimile q process "as is" q re-_ t mple 

be telephone . Ap othe (explain) Z,2, I jo jli hold until q otSer (explain) 

Project Manager (signature and date): l f z 

0058

Corrective Action 

QUANTERRa LABORATORY NONCONFORMANCE MEMO (NCNI) 

PACE 2 OF 2 

Root Cause 1 nitkLI and date: 

LOGO: RD-93- 

1, hlrCC^ îiu^ s- ( n6o u)GnewPDtU^- ^r^¢>i^C - 

Corrective Action Initial and Date: (1q C 

Responsibility for performing CA assigned to: 

Actions to prevent recurrence Initial and Date: 

First Level Supenisor 

Responsible Manager: o / 

__Ouality Assurance Review 

Dy al/ omaly 

O Further action required: 

Assi gned to: 

QA signature: 

Corrective Action Ve rification 

11 Verified 

^' 4 

0 Cannot Verif} (specify reason): 1 ^ (` I 

Nonconformance demo Closure 

QA signature/date: 

Date: 

Date: 

Cl Deficienev O Rerun 

Date: 

/ 

n 

CO5 

_

Quanterra Data Review Cbeddist 

RADIOCHEMISTRY 

'Cork Che er nvmtser r a,: 1 I Sn31e FSO a S-03 2 2 Z SO 71 

1 

C:imt!D' 

Due Date. - 

Lab Samvie `:timber or SM. 

method -,m?aametcs: C 

Manx: 

Z. Z7 

Ramme Item 

,L Calib ration 

t. Is the calibration daautsemaomf urluded Weee anpiicaW 

I 

IL Sample ..A W7sis I 

1. Are the sarfrole vichh vmmma aemtaoae attersa7 

:. Were ill Saafple holding tines met' 

3. Is the SN.:^ to Meruratem Dee imcle Acu"N< the Camae D eseeem Lann7 I 

I 

Yet (!) I `!o (!) I WA(!) I ^ÎsW 

( f 

1l 

^_ 

f 

I I ^^/I 

I C QC Sunpies 

1. Is she burn '•teld w thin ^.c asma j 

:. lathe .`,1__-urrz Detactable .ae_•nty for she Defe ction 

Litfsif^. 

3. Is the oianx Tuft < IG the Cancan Deecvan L:mei 

4. Is the ours > I,: the C.xeaaa De' .n i:sesf ba < Cman Dese c,, Limit? I I f_ 

sr;e.11, 

!. 13 1he'JIarC :'31+I1 > Ltx C^- Dc %rC.IOn l:mn bm the s=%* l estdl < :he Ccnf 

Detection um.:' 

6. Is the i ZS cult wthm m=a' I I I i . 

7 . Is the :CS p,etd W then ]CL4N1C m1m. 

9. Is the LCS llmunum DCIL is 1 J"N < Lhc C as yh D et,,m LSLt? 

9, MS, MSD Buis and "sold ere: ac^[anc stem? 

10. DuPiiê sur.Ple real(: and ^seid mee. ac-Hang amsa? ^ I I ^ i 

D. Other 

I. .Are all Scnnr-ncrtnanoa indudd and noted? 

:. Are all ree_ud forma tiled out' I ^ I 

3. Curry me •_-odolog, used' 

a. Tat s ..p , cn cheekd'. I I I 

I 

7. Were ail n:alaneess aheeitd at a muumum fsequ , f 7 

6. Cn.0 cnccawd' I I / 

Commen: on on} "ò' resocnse: /U( A [ i-^, hk /u dr^S -/cr ^^L 1 _ 

First Ln.i R_•.-te•.v" 

Date 

Second Le.e!Rr.7e•.v- 

Form d LS S. ; 96 Rcc 

Date: 

0000 

I

First Lie! R.ne.v Date 

Second Leve! 2etie•.r 

Form O LS -013? /96, l 

Quanterra Dan Review C3eekku 

v 

RADIOCHEEi LIMY 

Work Ordermunberrsh î31g^ ^.}I(,I ,^}J^b Oj^j^ S^'î X 44 53 ^.3.) 

Client ID' f•f 

Due Datr. y — ì 

Lab Sumvie Vumbr or SDG: 

Method Tm paamens: 

Mama: I 

pas Item Yes (.0 *V) I WA(^/) 2Îasd 

Rass!!1 

A CallbmClom 

1. Is the calibruim doounammm i tchded.Me appiimbler 

IL Semple AimiTsis 

1. Are the sample Melds wahm aaxpummorsona? 

` f 

I 

I / 

2. Were all sauvle holding tnm on? I I I 

I Is the satstple Minimum Desemab ie Aaeite < the C•amsa Daeomm Limb? I I ' 

C QC Samples 

I. Is the blank Meld within a¢epaa: alum 

Z. Is the Misumum Daauble Aaivny for the Mani must S Ibe C.amact Detemon I 

Limit? I 

3. Is the blatu :sub < Ii= the Ceeffiaa Des>am L ou? 

a. I: the blank > 1 12 the Coma Daemon Lvb bu < Comma Deuam li®t? 

I ( /; 

I I I _ 

I J I 1 

S. Is the blank result > the Co runa Dana Lines but :be sample tub

QuanaTm Data Review Chedd ist 

RADIOCHE1IISMY 

W ork Ot numurtat 8o31,e 'F5-03DOC 3222 ,3.-)4 FC3a _7.x_ 

C' unt lD 

K ^,— 

Due Date: - la - Q Y 

Lib Samo!e Namur oe SDCr 

l.J q) 22 -7 S 

Nethad TeR ?atYRtei T TrtiP Sri 

Matnz 0 

A. Cillbnason 

' 

1. [s the olibatim dnaatmtatim ivrudd w.hee a, pwank? 

EL Sen 

AA&' sia 

Revmne It= I Yes (.0 I fb(J) I WA(^) I ~Ieved 

RMtN it l 

'°le the ' vi 

I I I i 

1. Are sample elds ndu, iteiat 

^.Wed all sple am haldig tea =? 

3. Is the San:pie Mitsomaa Deeraa!e Aa < the Camas Deeasv Sims^ I I 

C QC Sampies 

1. Is the b!anit '.ieid wIf= srntvtc = 

the M llllt'LmDctE le.A . N fO :he Aum.,. S:Sc CJIDIY['JC'i on 

". is 

3. Is the olank suit < l.= :be C. a Deeevon Ua 7 

I I I 

a. IS lh. 013 > I :he C.Imlf. Dneeaen L:ILI bn < C^ DecaiYO Lzma7 I ' I ^.^ 

!. Is the o!arx X12 > the Ca .. Jeecott Z 1= bee ^hc sa npie resod

Qoanterra Dua R rinr Checklist 

RADIOCFI DUSTRY 

wnrk order-^,n^,.t ^'t^31 b I ^c3 i 8 4 FC3ao^C 5D3 a^ `6C3,P -7 )- 

Cientll)* 

Due Due-- 

\_k 

- Cl 0 

Lab Surtnic Numhtr ar SDG: (,L Z2 -7 ^5 

Nahed —ea ?•^---T TO -r Q Sr 

.tune O 

Rene,. fleet I Yta(.0 I MoN) ( 

1. ton =ii 

i 

I. Is the nlihruim docamtcvatton inducted Wiere^c7 

R Semple.arm17s6 

I. Are the sueic sidle.Wun acGeptante mreriat 

I 

- Were 111 simple bolding tuna met? I / 

3. Is the s . to Amarr+mt Dete=ble iGlnty < DeCaman Desecuao Limn? 

C. QC Sempies 

I. Is the Mara '.l cld Wtlml aLCplylCe ^1[er.1 

Is:he IIr==M J

Quantem Data Review CSedtEu 

RADIOCHMMISTRY 

W«konuok ^'31^t ^î v 53o3a^^ 8^3aaa 8^3a - 7 a 

Cient ID- 

Due Dac. 

Lab Sammie *lumber or SDCr. 

A, J a a 7 S 

Method Tea parameters C - 1 Li 

\4atrim 

A. Callbrulos 

1. Is the calibration doammaom ecbadtd share appli able? 

S Semple Aasl7312 

1. Ara the sample viddis - acnnece anaria7 

times hem I Yea(.) No(1) I ;UA(.) 2-lavel 

Rsaieaal.\ 

2. Were all sample hold ing mm meteI / 

3. Is the satpie Mkum ma Detectable .iron) < the Caaa t Deemm Li aise? 

C QC Sunple 

1. Is the blank held within acmaas am eria 

I / 

2. Is the Vint mire Detectable Ac m iv the blank nsuh S ibe Cm 

Limit? 

a Detection I I 

f 

' I _ 

` 

i 

f 

3. Is the blank ;cult < lQ Ibe C.aueact Deueflon Lin? I I I I / i 

4. Is the blank > 1 R the Cacact Desom Lies bet < C vdria Detec oeu UnuL7 I I ' 

3. Is the blank vault > the Canna De sera s limn his the sample ratk < the Cacao 

Detcuon Umtl? 

I 

I I ^- 

6. Is the LCS result within a¢cpunc Ivan? I/ I I ' 

7. Is the LCS said within aonptm c ena 

B. Is the LCS M inimum Detectible Ass'm S the Carona Deuoos Lion? I I I 

9. MSi\fS r) .cults and y aid sheet acmuene cs ma? I I l 

10. Duplicate sample saints aid yi eld tots acceptance ancria? 

D. Other 

I. Ara all Noncoafimnanca ncludd aid acted? 

2. Are ail required Corms filed ate 

3. Cortex methodolo gy used? 

4. Transmpuan checked? I ^^ 

S. Were all calcttlatons ch ecked a a ev®a® frequency? I f ' 

6. Uni ts check ed? 

Comments on any -No' rspcnse: 

First L^:el Rabe% ^— Date: 

Second Ltvcf Review Date: 

Form ; LS-033,2!96. 

V14 r S 

006

Comm.it5 on am" No' resoc 0: 

First Lrrei Rr.ie:v: 

Second Letic! Actiie:r 

Form = LS-0 1 8.2 i96. 

Qunu=Ta Data Review Checklist 

RADIOCHL USTRY 

Wark Order-umta: Est O^'^^^7^ ^ 31 O ^^^lT-Ô ^^Z2^ ^3a^L. 

cian:n N.^ C 

Due oast: L 1y -C ! 

Cab Saenoie Number a SM t,J 2 Z 'T 

Method à[ .'aaametom S 'e - -7 

A. Calibradon 

1. Is the elibmm dawmeaduian inchnded *wc ag6cahk? 

M Sample AaW7 312 

Rrne+lt® Yea (J) `*(J) WA LgVel 

icriw (J: 

I 

Dauc A _ 

Dale 

I // 

1. Art the sample vields Imdun 

aarmaom entnar I I/ 

2. Were all sample holding tim es mn? 

I I I I 

3. Is the satr•ie Minimeam Dc=:.xole A=v < ftC.ma s Desectsm Lmd? 

C. QC Samples 

1. Is the bunk •deld . dun .^-. :tsntcc a:tea 

0. Is the.`.linurum Cor des: blank a®u Sdse Catm'aa Detection 

L nit" 

3. Is the mask âsuit < L: :he Canna aet,=a n L ma? I/ 

4. Is the Manic > I,-- the Cantne Dôn Lain bn< Ca mcn e Dcamomn Lamas? I 

'., fs Use blar3c ^3nll > Use Cantrac: Jenee:oo Lma he the sale nssl[

First Lz:,i Rv.ietc 

Second '_=^ e! R- iew- 

Form = LS-)',8.2/96. 

Qu=ern Data Review Check fist 

RADIOCHEaM 4-(;^ cr^ , 

J. were all :al.-llsstaru :Pecked at a :wmr:S n rsc epumv? 

6. Units checkd? 

COmmen Ls on any'-ò' resccns:: i1,'• ,LDL 

'es It" L^(,^ G"X— Q 

Date -^fJ 

D= Y 6 ^^ 

j 

6060

Qaaaterra Data Review C3eddist 

RADIOCHIJ. Y 

waeit order -umbe (It à'A3 i Fs ^{ 8C3 i ^! `6C'3 ^ c^SG;S ^ .^. a ^rG3 ^ ^f N ^t 3 3 7 

cient :D: t k -7 

Due Date: 

L . Y 

4 - 

Lab Samote Vumbe or SDQ 

Method Tea ?a=nswer: 7—C - 9 

Natnrc G +h P 

-22-7,.5 

Renew ltea I Yes (.1 ) I No (,0 I VA(.t) 

A. CAUbmtlon I 

1. Is the alibtmm dootmemommon mc!uded -tax agfehlst 

I /^ 

B. Sample Ameiyms 

1 . Are the sample yyields-was 

asreounm msaut 

:, Were all Sample holding—me? 

I 

I I / 

3. Is the sampic Minimum Dcw=ble iC.tnN n Detmsm Limis^. I ,'} 

C QC Semple, 

Y^ 

I ge LAvd l 

-CT ^ I^ ^ 

L is the hi= 1eid wtthta as = atma I I I 

L is t he Micur..um Da --r •. .iCtnty :or the blank arta 

S th Ca Damson 

I I - 

3. is the Mark ^11 < L- :he Can== _-aecvon Irma? I /sue I _ 

a. Is the oiu > I,: Itta Camas ',?ct¢:ton L .Vt but < C. Doccum Lunt? 

3. IS the D[wk : It > the Cams.-. C

Richland Laborato ry 

Quanterra Data Review Check List 

Work Order Number(sl: 9'U3 

Lab Sample Numbers or SDG: ^Z / 7 

Method/TestiParameter. e^f^ 

A. Initial Calibration 

METALS 

vyZ ^^ 

Review Item 

1. Performed at required frequency wih required number of levels? 

2. Correlation coefficient within QC limits? 

3. Initial calibration ve rification (ICV) analyzed immediately after calibration 

and results within QC limits? V 

4. Initial calibration blank(ICB) analyzed immediately after ICV and 

concentrations of all paramete rs < reporting limit? 

B. Continuing Calibration 

1. CC V analyzed at required frequency and all parameters within QC lirnits? 

2. CCB analyzed at required frequen cy and all results < reporting limit? 

C. Sample Analysis 

1. Were any samples with concentrations above the linear range for any parameter 

diluted and reanalyzed? 

Yes 

V) 

No 

(V) 

N/A 2nd Level 

Review ( 3 ^ 

2. Were all sample holding times met? i 

D. QC Samples 

1. All results for the preparation blank below limits? 

2. MS or MS/NISI) recove ries within QC limits and n/aRPD (forMSD) acceptable ^C 

3. LCS percent recove ry within QC limits and °/aRPD (for LCSD) acceptable? 

4. Analytical spikes within QC li 

mits where applicable? 

S. ICP only: One se rial dilution performed per SDG? 

6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy ? 

7. ICP only: Interference check samples GCSA, ICSAB) and FECAL analyzed at the 

re uired fre uencies and within 9C limits? 

page 1 of 2 

606

E. Other 

1. Are all nonconformances included and noted? 

2. Is the cormct date and time of analysis shown? 

Review Item ( Yes 

( ^) 

3. Did the analyst sign and date the frmt page of the analytical tmm? 

4. Correct methodology used? 

5. Transcrip tions chocked? 

No 

(V) 

N/A 20 Level 

Review (^) 

6. Calculations checked at minimum frequenc y? 3 ^/ 

7. Units checked? 

Comments on any "No" response: 

Analyst: Kw Lz e 7 ^ Ô n ^ Date: 

Second-Level Review: 12 Ie Date: 3/4/" 

Form No. CG-191. Rev. 2,1/97 

page 2 of 2 Go b 

i


Qanter a Data Review Check List 

METALS 

Work Order Numberts): 31ffzl S7 3)11 

Lab Sample Num bers or SDG: u/ .^275 4J 0 

Method/Test/Parameter. U+lo ur?L L Tl?-47f 


1. Performed at required frequency wih required number of levels? 

2. Correlation coefficient within QC li 

mits? 

Yes No N/A 2"d Level 

Review Item Review (^) 


and results within QC limits? L/ j 

4. Initial calibration blank(ICB) analyzed immediately a fter ICV and J 

concentrations of all parameters < repor ti ng limit? 


L CC V analyzed at required frequency and all parameters within QC limits? 

2. CCB analyzed at required frequency and all results < repot ting limit? 


1. Were any samples with concentrations above the linear range for any p arameter 

diluted and reanalyzed? v i' 

2. Were all sample holding times met? 

D. QC Samples i 

1. All results for the prepara ti on blank below limits? 

2. MS or MS/NiSD recove ries within QC limits and °/aRPD (for MSD) acceptable ^F 


4. Analy tical spikes within QC limits where applicable? 

5. ICP only: One se rial dilu tion performed per SDG? 

6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy ? 

7. ICP only: Interference check samples (ICSA, ICSAB) an d MCAL analyzed at the 

required frequencies and within limits? 

—I 

page 1 of 2 GUI U

E. Other 

1. Are all nonconformance included and noted? 

2. Is the correct date and time of analysis shown) 

3. Did the analyst sign and date the front page of the analytical run? 


5. Transcriptions checked? 

6. Calculations checked at minimum frequency? 


Comments on any "No" rssponsc: 

Analyst: -^?C, Lg_ '7^) ^G 

^ ^ 

^) 

Second-Level Review: 1/7?^^34/j/^ 

Form No. CG-191. Rev. 7, 1/97 

Review Item Yes No N/A 22° Level 

Review (/) 

Date: 3//l /9e 

Date: 31191?^ 

page 2 of 2 [ ^! 1

Richland Laboratory 


METALS 

Work Order Numher(s): Q a2 ] 9 7 

Lab Sample Numbers or SDG: /V 2 2-7 S t &-)C2291 

Method/Test/Parameter: Qk*t, L - rr 

A. Ini tial Calibration 

Yes No N/A 2°d Level 

Review Item (1) Review (V) 

1. Performed at required frequency wih requited number of levels? 3 / 



and results within QC limits? 


concentrations of all paramete rs < repor ti 

ng limit? / _I 

B. Continuing Ca lib 

ration 

1. CCV analyzed at required frequency and all parameters within QC limits? 

2. CCB analyzed at required frequency and all results < reporting limit? 


1. Were any samples with concentra tions above the linear range for any parameter 



D. QC Samples 

1. All results for the prepara tion blank below limits? j 

2. MS or MS/NiSD recove ries within QC limits and °/aRPD (for MSD) acceptable?^^^ 


4. Analytical spikes within QC limits where applicable? 

5. ICP only: One serial dilu tion performed per SDG? 

6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequency? 

7. ICP only: Interference check samples (ICSA, ICSAB) and HICAL analyzed at the 

required frequencies and vvithin C limits? 

page 1 of 2 

8 4 

60"tZ

E. Other 

1. Are a ll nonconformances included and noted? 

2. Is the correct date and time of analysis shown? 

3. Did the analyst sign and date the from page of the analy tical run? 


5. Transc riptions chocked? 

Rem Item Yes No N/A 224 Level 

Review (V) 

6. Calculations checked at minimum 5squmcy? 

7. Units checked? j 

Comments on any "No" m6ponse: 

Analyst: ^Q7^P ` 41 

d 3 

Second-Level Review: âl^f p 

Form No. CG-191. Rev. 2, 1/97 

Date: 3 z/ fzpz 

Date: 31145 

page 2 of 2 6 0 7 3 

I


Quarteim Data Review Check List 

METALS 

_^b!_31 i srLf ^_ 

Work Order Num ber(sl: ZbL gp 

Lab Sample Numbers or SDG: ^^ W O 

Method/Test/Parameter: 


1. Performed at required frequency wih requited number of levels? 


Yes No N/A 2°a Level 

Review Item (`) Review (v) 

3. Initial calibration ve ri fication (ICV) analyzed immediately after calibration 


4. Initial calibration blank( ICB) analyzed immediately after ICV and 

concentrations of all parameters < reporting limit? 


1. CCV analyzed at required frequen cy and all parameters within QC limits? 

2. CCB analyzed at required frequency and all results < repor ting limit? 


L Were any samples with con centrations above the linear range for any p arameter 

diluted and reanalyzed? v 

2. Were all sample holding ti 

mes met? 

D. QC Samples 

L All results for the prepara tion blank below limits? 

2. MS or MS/MSD recove ries within QC limits and °/d2PD (for MSD) acceptable? py 

3. LCS percent recove ry within QC limits and %RPD (for LCSD) acceptable? 


5. ICP only: One se rial dilu tion performed per SDG? 

6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequency ? 


re aired fre uencies and within C limits? `/ 

I 

3 

i ^^ 

page 1 of 2 60! 4 

—i 

_r 

P,

E. Other 

1. Are all nonconfonnances included and noted? 

Review Item Yes 

( ^) 

2. Is the correct date and time of analysis shown? 3 

3. Did the analyst sign and date the front page of the analytical rm? 

4. Correa methodology used? 

No 

(^) 

NIA 

(^) 

221 Level 

Review ( 3 ) 

5. Transcriptions checked? 3 j 

6. Calculations checked at minimum frequency? 4 

7. Units checked? C7 


Analyst: y O'XC e- ô^ 0 Date: 3/ ( 8/ p k 

Second-Level Review: ^^1. ^



N =ALS 

Work Order Numbedsl: 8C 3 

Lab Sample Numbers or SDG: &. b :-^ a O 

Method/Test/Parameter. y) 


1. Performed at required frequency wih required number of Levels? 


Yes No N/A 2"d Level 

Review Iten (V) Review (^) 

3. Initial calibration veri fication (ICV) analyzed immediately after calibration 

and results within QC limi ts? 

4. Initial calibration blaak(ICB) analyzed immediately after ICV and i 

concentrations of all paramete rs < reporting limit? 

3 

I 


L CCV analyzed at required frequency and all parameters within QC limits? / 3 

2. CCB analyzed at required fn quen cy and all results < reporting limit? 3 —^ 


1. Were any samples with concentrations above the linear range for any parameter 



D. QC Samples —i 

L All results for the preparation blank below limits? t/ v 

2. MS or MS/MSD recove ries within QC limits and %RPD (for MSD) acceptable4 ov v 

3. LCS percent recove ry within QC li 

mits and %RPD (for LCSD) acceptable? 

4. Analy tical spikes within QC limits where applicable? 

5. ICP only: One serial dilution perfo rmed per SDG? 

6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy? 

7. ICP only: Interference check samples (ICSA, ICSAB) and HICAL analyzed at the j 

required frequencies and within QC limits? 3 

3 

3 

— 

3 i 

page 1 of 2 / U

E. Other 


(3) 

1. Are all nonconformances included and noted? 3 j 




5. Transc riptions checked? i 

6 Calculations checked at minimum frequency? 



Analyst: Date: ,311 p k 

Second-Level Review: /),^ Date: 3 . 1-191y F 

Form No. CG-191. Rev. 2. 1/97 

No 

(-01) 

N/A 

(3) 

2=d Level 

Review ( 3 ) 

page 2 of 2 li 0 i i


^w° ` alters Data Review Check List 

METALS 

Work Order Num ber{s): Yo y y 

Lab Sample Numbers or SDG: 14,0 ,,?Q75 

Method/Test/Parameter. C & ^j Q 

A. Initial Calibra tion 

Review Item 

1. Performed at required frequency wih required num ber of levels? 


3. Initial calibration verification (ICV) analyzed immediately after calibration 

and results within QC limits? j 


concentrations of all parameters < reporting limit? 


L CCV analyzed at required frequency and all parameters within QC limits? t,-' 



1. Were any samples with concen trations above the linear range for an y parameter 



D. QC Samples 

L All results for the prepara tion blank below limits? 

2. MS or MS/NISD recoveries within QC limits and %RPD (for MSD) acceptable?; p'k 

3. LCS percent recove ry within QC limits and %RPD (for LCSD) acceptable? 


Yes No N/A 2°a Level 

Review (^) 

5. ICP only: One serial dilu tion performed per SDG? ^1 

3 

6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequency? 


required frequencies and within 2C limits? 

page 1 of 2 Go! u 

i

E. Other 




( ^) 

3. Did the analyst sign and date the fiont page of the analy tical tun? 


5. Transcrip tions checked? 3 

No 

(^) 

N/A 

(^) 

2—d Level 

Review (V) 

6. Calculations checked at minimum frequency? 3 i" 



Analyst: `,(^ X Le j1/^12a1^ 

Second-Level Review: 

Form No. CG-191. Rev. 2. 1/97 

page 2 of 2 

Date: 3 //L ^rfR 

Date: 3//E 

Go -, J


Quante"a Data Review Check List 

METALS 

Work Order Number(sl: X '. 

lab Sample Numbers or SDG: U) L2275 

Method/Test/Parameter: ' 

A. Ini tial Calibration 

1. Performed at required frequency wih required num ber of levels? 


Yes No N/A 2°d Level 

Review Item Review ( 3 ) 




concentrations of all parameters < reporting limit? 3 


1. CCV analyzed at required frequency and all parameters within QC limits? 



I. Were any samples with concen tra ti 

ons above the linear range for any parameter 


t/ 3 

2. Were all sample holding ti mes met? j 

D. QC Samples lj 

1. All results for the prepara ti 

on blank below limits? 

2. MS or MSQvISD recove ries within QC li 

mits and °/dtPD (for MSD) acceptable?!! 1 F 

3. LCS percent recovery within QC limits and °/gRPD (for LCSD) acceptable? I I —^ 

4. Analytical spikes within QC limits where applicable? 3 

5. ICP only: One serial dilu tion performed per SDG? 3 j _ 

6. ICP only: CRDL standard (CRI or CRA) analyzed at required frequen cy? 

7. ICP only: Interference check samples (ICSA, ICSAB) an d MCAL analyzed at the Lj 

re uired fre uencies and within C limits? 

page 1 of 2 

^. 

_I 

G 0 j 0

E. Other 




(^) 



5. Transcriptions checked? 

6. Calculations checked at minimum frequency? 



Analyst: 41 z i_e_ `7 ^0.^1 

^ 

^^ "" 

Second-Level Review: r pt A&d 

Form No. CG-191. Rev. 2, 1/97 

page 2 of 2 

Date: 

3 

No 

V) 

Dater IZ P% 

NIA 29° Level 

Review V) 

/ 

V0$t

CHAIN OF 

CUSTODY FORMS

C_ 

C 

or 

v 

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -01 Page 1 of ! 

Collector Company Contact Telephone No. Project Coordinator Data Turnaround 

R. Fahlberg Steve Ma rske 373 4 316 WEISS, RI. 

21 

Project Designation Slorpling Location SAF No. Days 

105-C Phase I & Phase If -Concrete Samples 100 Area B98-061 

Ice Chest No. Field Logbook No. Method of Shipment 

_^ - - C, — Iland deliver 

Shipped 'I (I 


Olfsite Perty rop No. Bill of Lading/Air Bill No. 


Radw.,m, c 

Sproul llandling and/or Sloragc 

SATIPLE ANALYSIS 

^^ Preservation 

rvâe 

Type of Container p 

No. of Cnnlainer ( s) - 

Volume \' 

(^/^ Sa i¢m 111 In 

^ J 'L 

SPed.l 

Imwnio^s 

Ci ^^^^J 

w 

11- 

Sample No Matrls• Sample Date Santple'fime s"'td v ^. qti` a5„tY [:'••^:, jg .r'n'3!^* , sl'^.rlt'°,:. 'f.^s 'â i aa q^%',`:- 

C, 

L 

BON680 CI Other Solid 

S 

SPEI LAI. INS 11 4 IRONS Matrix 

111 %IN III I'IOSSI..SSIOV Sign/Print Nawr. 

III I( -I' hlc0a6- 60 ttA lSupal0accl l eudl, Mcauq - 9421 - (CV ) , C6rumnmin llt, " 7146, 

s 

sk 

_ 

- 

s,,d 

sa.linan 

I(LIlP1 .Lcdlly (I - Y•/- D1 Iuuc Rua dIII 

-2 O 

U I..... Pill, 8080,iAi 1 

I 0 . I I54, I. 0 I 

1 ill.tia 0a S,,,,ou..ulY (e 0137, 

1551"A a .. 0 24I I 0 ryi. I Wlu 0wn 

bait6(11 

I mpie Il y a 

Vi t 152 

n . SO, 

sU 

si. 

- 

sWi4 

61,dae 

of na1 + 0 0lcluu^ 14c uJlq 

^^ 

10e1f5111uu 

- ^^(^ } C` `j 9 

. Mi LrCI 

r a ,j^0.1 

L3 Sr- 90 EDIT l Sr 

1, ¢^t s 

A 

" V , Can 

141w 1 uuLed 11 1Ito, nue wl scd it, I>.em' Inn e v q 

I(c 

^^ 

. 

a 

i 

m 

UI 

I 

- 

nil 

a s " I m 

ho- 

III - 111pe 

hall uyw.Lcl I10 U.uc l un. I(cco.cd II Ill.nc l llv. I I w ^ 

11111110A 111111 It nr.l Ito Iltic Uam^l lnm 

St( IOUs 

FIN'AI SVAII'Lf. 14 1.Iki'll 111.1 .0111, Ilalc/I inm 

I IISI'IISI I IfIN

C 

cc: 

li.- 

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -02 Page I of 

-'olleclor Company Contact Telephone No. Project Coordinator Data Turnaround 

R. Fahlherg Steve Marske 373 -4316 WEISS, RL 

21 Days 

Project Designation Sampling Location SAF No. 

103-C Phase 1 & Phase II -Concrete Samples 100 Area B98-061 

Ice Chest No. Fie ld Logbook No. Method of Shipment 

Hand deliver 

'hipped To Mile Properly Bill of Ladin Air Bill No. 


POSSIBLE SAMPLE IIAZARDS/11EAIARKS 

Radioaclim 

S pecial Ilandling and/or Storage 

SANIPLE ANALYSIS 

Prese valion 

None 


No. of Container(s) Z 

Volume 

IL 

sw acm t 11 In 

speci al 

m,wnrnns 

Sample No Mali:y • Sample Date Sample Time }-^ _, ` `.I z, =,gyp' = • s -:t(do. - 

BON681 j, -^ Other Solid — 3 ' ^," Z 

I SPF.CIA I. INSIRI C"II ONS Matrix 

HAIN OF PO SSE SSION 

ItcLw uuhcJ e" Dnm"Imo 

Sign/Print Names 

Re

Environmental 

Contractor 

Contractor 

Visa 

Team 


M. 

'.nrna! 

D. A. St. John r.0-19 

See Below 

°"M 1'ebruary 27.1999 

rtiaa S. L. Winslow 


X3-41/531-0700 

susurcr: CURIF ESTIMATE FOR S111PP1NGCON[:RETF. CORE SAMPLES 

CotQatration (obi/e) 

2.55 pCilg 

1.2F3 pCi/g 

4.95 pCi/g 

7.5E-1 pCi/g 

2.550 pCifg 

7.5E-2 pCi/g 

1.5 1 

1.46L'3 pCi/g 

CCN: 055088 

Job No. 22192 

Wnm•A.av Ap 

Div w• 

a, ion 

nn v 

c•n wn 

Swwn Cob Im 

The 1i111uwing calculations show that core sample: with a direct reading of equal to or Icss than 

400.000 dpm/1Merin' will be below the definitionorrulivactive material as defined in 49 CFR 173.403 

of 70 Bq/g (2F.3 pCi/g). Each sample will consist of contxete material from four, two inch core 

samples and enough water to arike a slurry consismacy. 'the distribution of radionuclides is hued on 

previous concrete samples rakcn from the below gtadie Fuel Storage Basin that would also he 

representative of these concrcec samples. 

(jiven: 

Cyiinder Volumc = itA Radius of concrete core (r) = I inch 

Concrete Density = 2.35 g/em' Height of cam sample taken (h) - 0.25 inches 

27 pCi = Dq Maximum 5rn:1 reading on core = 400,000 dpna/ I OOcm' 

2.'_2 dpm = pCi 

Calculations: 

V — (3.14) (1 in.)'(0 25in) = 0.78 in' (16.4 ciOin-' (4 con: samples) = 51.2 cm' 

(400,000 dpm/51.2 cm) (cm'/2.35 g) = 3.32E3 dpVg 

3.321:3 dpm/g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 Bq/g 

SI.W:dld 

°Co 

Percent Distribution(`7) 

0.17 

"'cs 

432 

EU 

82 

0.33 

1"Eu 0.05 

90Sr 17 

7Ai Ain 0.005 

239'rx'Pu 

0.1 

TU rAr-: 

('epics: 

S. 0. Marske X5-53 

P. A. Newman X3141 

RadCun Engineering file/LB XO-23 

Document and Into Services 010-09 

'0 

0085

Environmental 

Restoration ERC Team 

Contractor 


TO' D. A. St. John I.0-19 LATE: l-ebruary 27. 1998 

"O''' F'` ' See 13clow 

FROM: 

* Av 

S. L. Winslow 

RadCon Enginuing 

X3-41/531-0706 

suwECT: CURIE ESTIMATE FOR SHIPPING CONCRETE CORE SAMPLES 

Concentration_(^Ci/;> 

2.55 pCi/g 

I.2F.3 pCi/g 

4.95 pCi/g 

7.5E-1 pCi/g 

2.55E2 pCi/g 

7.5F.-2 pCi/g 

1.5 2C.Ug 

1.46E3 pCiig 

Job No. 22172 

wnan 0.epmrRpu.N .nU 

P+Ow w^ 

I 1 V w/, 

W n l0, 

CCN: 055081; 

s^+l..,cw. !Fw 

The ibllowing calculations show that core samples with a direct reading of equal to or less than 

400,000 dpm/100cm' will be below the definition of radioactive mate rial as defined in 49 CFR 173.40± 

of 70 Bq/g (2F3 pCi/g). Lach sample will consist of concrete materi al from [our. two inch core 

samples and enough water to make a slurry consistency. 'fhe dislrihution cdmdionuclides is based on 

previous concrete samples taken front the below grade Fuel Stora ge Bas in that would also be 

representative of these com:rctc samples. 

'ven: 

Cylinder Volume = nr'h Radius of concrete core (r) = I inch 

Concrete Density = 2 3 5 ylem' Ileight of care sample taken (h) - 0.25 inches 

27 pCi = Bq Maximum direct reading on :ore = 400.00 0 dpnl/lUUcn1` 


Calculations: 

V - (3.14) (1 in.) 2( 0.25in) = 0.78 in' (16.4 can `/in) (4 cure samples) = 51.2 cm' 

(400.000 dpm/51.2 cm) (cm'2.35 g) = 3.32E3 dpm/g 

3.3213 dpnn'g (pCi/2.2 dpm) = 1.5E3 pC'i/g or 55.4 Bq/g 

SI VAld 

Percent Distribution( 7o ) 

'"Co 0.17 

"'Cs 82 

1 1 Lu 0.33 

"°Eu 0.05 

"°Sr 17 

'°' Arn 0.005 

"°'="'Pu 0.1 

TOTAL 

Copies: 



RadCun Enginee ri ng File/LB XO-23 

Document and Info Se rvices 110-09 

V^Ô

F%jwI 1 

SAMPLE CNECX-IN LIST 

CaterTime Received: . ^ 151 SG* 

wcnc Order Number L' ? i ( ^' ^(GI Say 1R- C^^ Î 

Shipping Container IDk l SJ^ Chin dCustody; 

RFSHSOw-93-0003 - 

Revision 

^1 

(1 ^^' l 

1. Custody Sealsaod*Ong , I i ktar Yes IC II 

2 Custody Seals d*d and signed? Yes K,40 No I 1 

3. Chain-of-Custody recatd presenO 

GC 

Yes I 1 

4. Caalet temperaftae 

5. Vennici telpad* materials is Wet ( ; 3rY ( l 

6. 

Number of samples in shipping corainer 

7. Sample holding Imes exceeded? Yes [ ; No I 1 

8. Sammhave 

tape hazard Labels 

seats appropriate sample labels 

9. samples are_ 

_SLm good wnd ition lealdng 

broken _ have air bubbles 

10. Where any anomalies identified in sample receipt? 

11. Cescsiption of mana lies (nude sample numbers)_ 

Sample Custcdianllabaatorl '^ Date_ 

Yes I 1 No I 

Telephoned To: Ongy 

IA 

60S;

Frlrr 1 

SAMPLE CHECK-IN UST 

DateMme Received: SG#: 

^^c ^ sc ar-^--aoo_ - 

4" Sion 

Work Crder Number. l'^ ^^ SAF #:- 

Shipping Container ID: U d chair of Custody # I ^ (J - ^^ ^^ 

1. Custody Seals an shipping contain ritW. Yes I I 

2 Custody Seals dated and signed? Yes ( No [ 

3. Chain-of-Custody record present? Yes


I D-Mar-98 


BII ON14CI 3/9/19981:42:00 P7)2 1A 3/10/199811:23:38 BOM4CI 

(QUID 1HI+kg, 

3/10/1998 ^ :51 ANI BKG 

An]D t /10/1998 ' ,Alq: 5.00E-01 01 (Dpm/ 5.49E-01 (uCl/ 1.24E-0j 

,-Ppt mg:2.1 Unita: L Bet; ): 5.42E+01 So);--J.hE-0 3 

DI11 130 1,14C2 3/9/19981:42:00 PM QUAD2 1 B 3/101 19981123:38AN1 BON14C2 

LIQUID Bkg: 3/10/1998 8:43:51 A BKG 

A nI Dgt : 3/10 ToI Sr, AIy: 5.00E-0^ OE+01 Alp; (Dp V 738 -0 (uCU 8.07E-06 

/Pptmg: 2.6 Inks: /L m Bet( ,-^q): I.IIE+01 2.51E-04. 

30 16 9.49333333 841 27.233333 

i 

100 4 0.04 0 0.8 

2.47E+01 ± 2.3E+01 CAT OE+00 1. 

LIg )i 1'44+03 3 8.7E+01 I 2A ^^^L`^ 

w 6 

0.03 

(p 1.6 01 ± 2.4E 

Llg): 5.01E+02 .3E 

202 833333 - 

95 "-^ 0.95 

4T E+00 Lob 

I Alq 

11111 BON680S 3/9/1998 1:42:00 PM QU kD24D 3/1 0/'199811:23:51 AN1 BON680S 

30 1130 37.6066667 124390 4145.4333 

90G 100 6 0.06 

0.9 

I SOLID Bkg: 3/10/19988:43:55AN1 BKG 

AN Dote: 3/10/1998 Tot Sa,Alq: 1.63E+02 9.81E+01 Alp; (Dpm/ -1.71E+01 (uCU 4.27E-02 (pCV .7.83E+01 ±9.4E+00 CAT 1.6E+02 Lab 

Ppt mg: 98.1 / UNta:g mg Bel; Alq): 9.19E+03 So): 6.86E+00 Ljg): 4.22E+04 ± 1.2E+02 

III 

2.4E-03 

14c I-IC 

DIII BON681P 3/9/19983:15:OOPM QUAD2IA 3/10/199811:54:54AN1 DON68IP 30 5 0.12666667 96 2 4 

G a LIQUID Bkg: 3/10/1998 8:43:51 AN1 BKG 100 4 0.04 80 0.8 

An] Dote: 3/10/1998 Tot So, Alq: 1.80E+00 100E+01 Alp; ( )pm/ 3.23E-0 1 (uCU 2.62E-05 (pCU 1.45E+01 ± 2.4E+01 CAT 1.7E+00 lab 

I-pt mg: 69 Units: 1. / ml Bel; Alq): 4.79E+00 So): 3.88E-04 Ljg): 2.16E+02 ± 3.1E+01 I 2.3E-0t 

Alq 

BIII BON681S 3/9/19983:15:00 PM QUAD21B 3/101199811:54:54 AM BON681S 30 13 0.40333333 234 6.85 

GSOLID Bkg: 3/10/19988:43:51 ANt BKG 100 3 0.03 95 0.95 

AN Date: 3/10/1998 3'ot Sa,A1q: 1.90E+02 1.1511+02 Alp; (Dpnt/ 2.58E+00 (uCU 1.93E-03 (pCU 1.02E+01 ±5.5E+00 CAT 4.9E+00 lab 

Ppt mg: 114.5 Unite: g / mg Bet; Alq): 1.55E+01 So): 1.16E-02 Llg): 6.09E+01 + 4.6E+00 I , 1.6E+00 

DIII 13ON6801 : 3P)/19981:42.001'M QUAD24C 3/10/199811:23:51 AN1 11ON680P 30 43 1.39333333 3426 11339 

LIQUID llkg: 3/10119988:43:55 AM BKG 100 4 0.04 81 0.81 

AnlDate: 3/10/1998 'Pot Sa,Alq: 1.80E+00 LOOLWI Alp; (Dpntl 4.48E-0 1 (uCU 3.64E- 0 5 (pCU 2.02E+01 +2.2E+01 CAT 1.2E+00 tab 

Pp( mg; )A /^ Unite: I. nJ IRq Alq): 2.141:+02 So): 1.74E-02 Leg): 9.66E+03 + 1.7E+02 1 5.2E-03 

r 

^ 

'Î i^ 1) 9. Y , '17 1, I cA^4 

O 0-.4/nr-9N QDanterra Environment Se rvices, SCP V2.03 

CO ) 

Alq 

Ids 

I'll:

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-o61-03 vase ! '/ ! 

ullectur Company Contact Telephone No. Project Coordinator Data Turnaround 

R. Iahlhcr, 

Project Pro Designation 

I Des i , 

Steve Niarske 


373 -4316 WEISS, RL 

SAF No. 

21 Days 

105 C Vhax 18' Phase II -Conercre Samples 1(111 Area 898-061 

Ice Chest Nu. Meld I. ,ghouh No. Method of Shipment 

L- L J r _ Hand deliver 

Shipprd IF, 011silr 1'roperty No. Bill of fading/Air Bill Nu. 

I luanwira lncorpofFacd n IF 

POSSIBLI. SAN11'LL IJAZAlt DS/REMARKS 

RaJioaa i.c 

Special Ilandlln8 and/or Sturaye 

Presen'atiun 

I)pe of Container 

No. of ('ontalner ( s) 

\'olmne 

(^^^ 'y^ ^''^ 

111 

S:ANIP1.F 0% 

CIJLk>« -7, 

031 g â C^ c h i X0-5 

Sample No Nlalric Sample Dare Sample 'I 11 11 c 

BON682 Other Solid 

P 

IL 

sec uem (p m 

saeoal 

SPE('LU. INS IRE 'CI'IONS 

N1mriy 

I OI: POSNI.SSION ,'Ign/Prini Name, 

( 111( I N1n.d.-bnI''%'s .niF") ll aaJ l, Ntocl- w 74 71- I C V). C hmm moi l l° -119e, 

s 

SI. 

- soil 

- seammu 

1 cl Iqm ch

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -04 page 1 of ! 

Collector Company Conlact Telephone No. Project Coordinator Rata -turnaround 

R. Fahlberg Steve Marske 373-0316 WEISS, RI, 

Project Resignation Sampling Location SAF No. 21 Days 

105-C Phase I & Phase II - Concrete Samples 100 Area B98-061 

Ice Chest No. Field Logbook No. Melbod of Shipment 

L.°L — l 3 C ) r — 2 

Hand deliver 

Shipped 1'. 

Quanerre Incorporated 

POSSIBLE SAMPLE IIAZARRS/REMARKS 

OBske Property No., . 

AL-11-4 

r+aa. 

Bill of Lading/Air Bill No. 

A' 

Radioacl,e 

Preservation 

'pecial handling and/or Storage 

SA MPLF. ANALYSIS 

'Iype of Container 

No. of Container(s) - 

Volume 

P 

IL. 

5.^ m01in 

SaCn1 

10'^^.°1O°` 

03193 Chi g0318^ Pao(- 

Sample No Matrix Sample Date Sample Time ^ni 1111, ^`-E .-+p ;, ^. M ,+ '#„n c fr v ' ,. S+} 

BON683 O^ Other Solid /lJ S D ^l r'j7 X '^ 9 _ t 

11 UN 

01 PO.SSI SSION 

It i.... ..aJ lî /^^ ^Îi^9 un 

^^^ o ^ 3 

11eWignnh d ll/ 

SPF('L I. INS TI1VC110 11 S Mumix' 

Sign/Print Nwura S 

(I11(l'M

C 

l 

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-05 Page 1 of i 

Collector 

R. Fahlberg 

Company Contact 

Steve Marske 

Telephone No. 

373 -0316 


WEISS, RL 



21 Days 

105-C Phase I & Phase 11 - Concrete Samples 100 Area B98-061 


4- L — / 3 2 [land deliver 

'hipped "I o Offske Property No. Bill of Lading/Air Bill No. 



Radioactive 

S pecial Handling and/or Storage 


Preservation 


No. of Container(s) 

Volume 

r+oê 

p 

IL 

See Item ( 1) in 

Speaal 

Io:nom"'^` 

803183 ^^ gc^31^'4 ^^d 

Sample No Mavis Sample Date Sample Iime n^ 1L .E--;t' ry aii v`; ;/! 

BON684 3 Other Solid S/`/ `.r ^, `. '^ V 

CHAIN OF POSSESSIO N 

RJulgnuhnl n1 h,,, s^ U lc 5 

./^0< P 

RcLm mha fy IJeLLÌ ic 

Rcllnqul>heJ 11 1 Dale Tmm 

Sign/ 

i 

J Recce Ily 

Lcl.edIt, 

Remi.eJ Hp 

int Names 

/ 

1lalel1lnm 

amfllme 

v Dm,Tlnle 

ti 

SPECIAL INSTRUCTIONS Ma tr ix 

s 

I R 1 1 Nlo, is b010A (Super ace) ILead); Mercup - 7471 -(CV), Chromuun flea -7196, SG 

IV II, 8080 ( All i 1211 1lice, t SI t sc P) (Ce'ium 1 V C ,bah-60, Europium I S'_. SO 

L uy'w -U.L 1'.......n-139;. Ai w ......n-24 1 Isotopic P wo iiu . Isuwpic t)mnu m. Sell SI 

-1 G N' 

"lPn (f(Is'1 - 19 N^ ^/-6^ Sr-^^ -/o- - u^ / Sr, U 

Teoh 17q (^ bon 14, , 46 71/( 'ly Sean 1) 

or 

I

Environmental 

Restorati on 

Contracto ERC Team 


zO D. A. St. John r.0-19 b"rz0 February 

27. 1999 

1"Y1• '` See Below 

l 

ncoa: S. L. Winslow 

RadCun EngUla:ring 

S1. W:dld 

to Co 

137 CS 

Percent Distribution(r/o) 

0.17 

82 

132EU 

ueEu 

0.33 

0.05 

"Sr 17 

741 Ain 

209/zwpu 

0.005 

0.1 

TOTAL: 

X.1 -41 1531-0700 

suuecr: CURIE. ESTIMATE FOR SHIPPING CONCRETF. CORE SAMPLES 

Job '49. 22192 

wwvwll^Mwsrw '10 

D,DW NA 

il ♦ www 

a' Vole 

R11 

caw vw 

CCN: 055082t 

The lirllowing calculations show that con; sampicswith a diner reading of equal to or less than 

400.000 dpm/IOOcm z will be below the definition of radioactive material as defined in 49 CFR 173.40: 

e 

of 70 Bq/g (2F3 pCi/g). Lath sample will consist of concret inaterial from four. two inch core 

samples and enough water to make a slung consistency. 'Ile distribution of radionuclides is haled on 

previous concrete samples taken from the below grade Fuel Storage Basin that would also be 


(jivgn:: 

Cylinder Vulurm = nr'h Radius of camrlete corer) = I inch 

Concrete Density = 2.35 g/cm' Height of c:cee samplc talcen (h) - U.25 inches 

27 pCi = Bq Maximum dimt reading on core = 400,000 dpm/IUOcmz 

222 dpm = pCi 

Calculations: 

V-(3.14)(1 in.)-(025in) = 0.78in'(16.4cm'/irrj(4 core samples)=512 cm' 

(400.000 dpm/51.2 cm) (cm' 12.35 g) = 3.32E3 dp Wg 

3.321:3 dpm'g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 841g 

Conics: 



RadCon Engineering File/LB XO-23 


Cotltsatration (tom/0 

2.55 pCifg 

1.2F3 pCi/g 

4.95 pCilg 

7.513 -1 pCi/g 

2.55E2 pCi/g 

7.5F.-2 pCi/g 

1.5 VQr 

1.461'3 PCi/g 

X090

Figure 1 


DateTme Received: 3C//11'0 ICES 14 t /^ SG#:_ ^ 2 ^^^^ 

Work Order Number. 0 t ^^`T SAF #- 

Shipping Container 10: ^ C ^ h h6^ Chain of Custody # L - (L 

1. Custody Seals on shipping container intact? 

2. Custody Seals dated and signed? 

3. Chain•of-Custody record present? 


5. 

Vermiculite/packing materials is 


7. Sample holding times exceeded? 


J tape hazard labels 

_custody seals app ro priate sample labels 

9. Samples are: 

V .n good condition leaking 


10. Where any anomalies identified in sample receipt? Yes f 1 No [ -,/ 

11. Description of anomalies (include sample numbers): 

Sample Date: 

Telephoned To: On gy 

N, 

PFSH-SOW-93-0003 

Revision 5 

Yes [+40 11 

Yes ( èl^4o (1 

Yes ( No [ 1 

Wet [ 1 C ry tTr G-( , 

Yes (I No (I 

LU9`

Client Sample Screening Results 3 l0 

10-Mar-98 

CLIENTCODE 11) MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSB NETCPMB 

bhi BON682F 3/10/19981:05:00 PM QUAD2IA 3/10/19983:01:18PM BON682F 30 Is 0.56 69 1.5 

1 

/ I LIQUID Bkt: 3/10 1 1998 8:43:51 AM BKG 100 4 0.04 80 01 

A nt Date: 3/10/1998 Tut Sa, Alq: 1.80E 4 00 , LOOE+01 Alp; (Dpm/ 1.89E+00 (uCV 1.53E-04 (pCV 8.51E+01 ± 3.1E+01 CAT 2.9E-0 1 Lab 

_ 

Ppl mt: 1 L5 Unite: L 3' , ml Bet; Alq): 2.79E+00 So): 2.26E-04 Lit): 1.26E+02 + 2.6E+01 

I I^ 

4.0E-0f 

Alq 

ut 

Ant De / 0/1998 Tot a, Al 2.000 

pt m!;: j Un 13;/L 

1.00E+0 AI (DpM 0 L^+00 ( 'V O.00E (pCV .00E+00i* Num! CAT 3A)E+00 Lab 

I 

ml 1A; q): O.00Et00 )3^0.00E+00 LIlU :OOE00 ± qNu ! -^ 2.OE00 

1. 

Bill -BBN68'2S 3/10/19981:05:00 I'M QUAD2 1 B 31 10/19983:01:18PM DON682S 30 937 31.2033333 87485 2913.2167 

Ô(o$3 5 

SOLID Bkp 3/10/19988:43:31 AM BKO 100 3 O.OI 93 0.95 

AM Date: 3/10/1998 ToISa,Alq: 2.00E+02 9.15E+01 Alp; (Dpn3 2.39E+00 (uCl/ 2.35E-03 (pC9/ 1.18E+01 +6.3E+00 CAT 4.3Et00 Lab 

Ppt nq: 91.5 1 1,11 13: g / m8 net; Alq): 6 49E43 Se); 6.39E100 LIt): 3.I9E 4 04 ± 1.1!102 

111 

'v_ 3.1 F.-03 Alq 

LIt 

Bill BON683F 3/10/19981:05:00PM QUAD2 1 C 3/10/19983: 01 :ISPM BON693F 30 127 4.13333333 9212 306.17667 

M LIQUID Bkg: 3/10/1998 8:43:51 AM BKG 100 10 0.1 89 0.89 

An] Date: 3/10/1998 Tot Sa, Alq; 1. 11 0E+00 1.00E+01 Alpi (Dpm/ 3.34E+00 (4C7/ 2.71E-04 (pCY/ 1.lIEw2 f3.4Ew 1 CAT 1.7E-0 1 4b 

Pptmt: 7 3 Units: 1, 3 ml Bet; Alq): 6.06E+02 So): 4.91E-02 Lit); 2.73E+04 ±2.8E+02 I (/LBE-0 7 

^C 

Bill BON683S 3/10/19981:05:00 PA1 QUAD2 11) 3/10/19983:01.18 PM LION683S 30 5 0.02666667 75 1.68 

g0^68as SOLID Bkt: 3/10/19988:43:51 AM BKG 100 14 0.14 82 0.82 

' 1 1 D Anl Datc 3/10/1998 Tut Se, Alq: 2.00E+02 J/ 

8.53E+01 AI p; (DpM 6.13E-0 2 (uCY/ 6.30E-05 (pCY/ 3.23E-0 1 ± 3.3E+00 CAT 1.2E+02 Lob 

'll 

Pptmt: 85.3 

Units: g mg Bet; Alq): 3. 72E+00 Se): 3.93E-03 LIt): 1.96E+01 ±3.6E+00 I L S.IE+00 AIq 

I-It 

LI 

1 U-.1 far-98 Quanterra Environment Se rvices, SCP V2.83 I

(7-- 

C) 


11-Mar-98 

®x)11 I^ 


Bill BON684 3/11/1998 QUAD2 1 A 3/ 11 /19989:5104AM BON684 30 9 0.23333333 109 27716667 

C -' LIQUID Bkg: 3/11/19992:34:24 AM BKO 600 40 0.06666667 517 0.8616667 

Anl Date: 3/11/1998 Tot So, Alit : 2.00E+00 1.00E+00 Alp; (Dpm/ 1.04E+00 (uCB 9.38E-04 (pCl/ 4.69E+02 ± 3.9E+02 CAT 5.3E-02 Lab 

Ppt sing: 49,7 Units: L ml Bet; Alq): 5.94E +00 Sa): 5 . 35E-03 LI8): 2.67E +03 ±3.4E+02 11.9E-02 

BHI BON783 3/11/1998 QUAD21H 3/11/19989:51:34AM BON783 30 6 0.14333333 35 0.2383333 

LIQUID Bkg: 3/11/19982:34:24 AM BKG 600 34 0.05666667 557 0.9283333 

Ant Date: 3/11/1998 Tot Sa, Alq: 1.00E+01 1.00E+01 Alp; (Dpm/ 4.39E-0 1 (uCt/ 1.98E-04 (pCl/1.98E+01 ±2.IE+01 CAT 1 .3E 400 Lab 

Pptme: 0 Units: L , ml Bet; Alq): 3.72E-01 Ss): 1.68E-04 LI8): 1.68E+01 ± 1.7E+01 I 3 .0E+00 LIC 

C) 11-Mar-98 Quanterra Environment Se rvices, SCP V2.03 1 

'Iq

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST 698-061-06 

Collec Compan) Contact Telephone No. Project Coordinator Data Turnaround 

It Pahlbcrg ^(,( 

Steve N1a rske 373-4316 WEISS. RI_ 

Project Designation trampling Location 'AF No. 

105-C Phase I k Phase II - Concrete Samplcs 100 Area B98-061 

Ice If No. Field Logbook No. Method of Shipment 

— Z 

hand de li ver 

Shippcd'IL ll,kc Property No. Bill of La t in /Air Bill Nu. 

Quanlerru h 1 c0rpnmlad 

POS9BLL SAMPLE IL\ZARDSBEM:A RKS 

Itadluaclne 

Jpecial Han dling and/or Storage 

Presen'alion 

Iypc of Container 

rA 

rv o,l= 

No. of ('ontaincr(s) - 

'plu m e 

^^ /, 

5.\MI'Lh: :V^.^ \\:\11515 

Sample No Slamy ' Sample D at e Sample Mime 

BON685 C)' Other Solid ^.- /_ 3 

P 

I1. 

Sae uanlll nl 

Inwua arm 

SPI'.('L\1. INS I fit l (' IONS 

21 Days 

Pare 1 ! 

( \IN OI POS.SI'.SSION Sigel/1 1 1'1111 Names SS, II 

III II1'M.lal,,-o 110%ISI I Il IL cl l l.. ,id i. Nkc -7471- 1( V) . C hromlun, l 1c\-7106. SI SuIJO 11. 

a= I't It enXO ,AI a .tut 1 Sp 'I ascot ( ]. C (6,11-60 I_ p v m sal u 

L. 1.111

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-07 Page ! or ! 

( 'effector 

R. Fahlhcrg rLJ( 

Company Contact Telephone Nu. Project Coordinator Data Turnaround 

Steve hlarske 373-4316 WEISS, RL 

Project Designat en 'ampling Location SAF No. 

105-C Phase 13 Phase II - Concrete Samples 100 Area B98-061 

Ice Chest \'o.^l y^ p ^/1 r— / Field Logbook No. 3 


J M "9` 10 _ ^L (land deliver 

Shipped to 

Quante ira IncogwraleJ 

POSSIBLE SAMPLE IIA%ARDS/REI11ARKS 

RaJiaaaivc 

)ffske Property No 

Prne rvat on 

N.. 


N 

"type of Container 

P 


SA NIPIL .-ANA L}'SIS 

No. of Cunlalner ( a) - 

Volume 

IL 

S ec aan (I I ,n 

Spc ,xl 

loroou,nos 

21 Days 

X03, ^C^ m 

SanlpleNo. Matrix • SampleDale Sample Tinic rn, - S s - m R:j^ k>i d 9'p Fik'^,4?+.+i„^';}i• r ,'lfl r^'{t I+tom,,,(.`-^„t 

SON686 N Other Solid - )^_ f/ 

^d 0 (] 

SPECIAL INSTRUCTIONS Matrix 

AIN 0 F POSSESSION 

1, y shcJ N^ 

//]^ 

^S l ^^ V „â 

Sign/Print Names __ 

(1) ICI'Maa6- 6010A (S upen,acu)if eadl, Mercup-7471-(CV), Clo.on flex-)196, 

key a - Ihreûnc 1'Ui^ 5080 1 1 SJ " (Ian aSlx -211, 1 Ce' 137 C bah 60 L ru( um 15 1 - 

^^h.......,*1 1 : - I"s; - A" iv c,nn?JIla l,nc lhu r S.Iv 

^^ i ( 

S 

SE 

S1 

,I 

- 

- 

- 

So,i 

SNuncn, 

SoI,J 

ucLmgm.L.J B. Inec lw^^ 

.^ 

" I " nqI.11wu„n 

I

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -08 Page I f 

'olleetur Company Contact Telephone No. Project Coordinator Data Turnaround 

R. Fahlberg I Steve Marske 373-4316 WEISS, RL 


105-C Phase I k Phase II - ('o 11 crete Samples 100 

Area LL — 1 3 B98-061 


L L - _ Z 

Shipped 10 

Quantcrra Incorporated 

POSSIBLE SAMPLE IIALARDS/RE\L\RKS 

xodioaclive 

Special Handling and/or Storagc 

p 

^/p 

S\1111'1,L AN, 1,%SIS 


Hand deliver 

Offske Property No Bill of Lad in /Air Bill No. 

Preservalion 

rvon. 

'I ype of Container P 

Nn. of Container(s) 

V'nlu me 

I f. 

Sec i te m 10 in 

Specul 

Innmaiuns 

"/`loll / c-^^ 

Sample Na Matrix Sample Dale Sample'I'ime ?'>'^Y'S^D:"itP, ,hst°eft';a ,M. Li 

BON687 Other Solid S - - ^Y .^ U S ^Z C a 

21 

DAYS 

A^,^ 

'.9nuv{c,,+pT'f'.` 

SPECIA1. INSTRI1CI IONS Matrix 

11 %1'% 01 POSSESSION Sign Print Names 

fl) I(I'Alna6-eu IIÂ ltiupulâccl ll.eaul, Meaup- "TJTI-(CVj. Chroinmm lle^-T196, 

s 

9i 

- S'11 

- S

Environmental 

Restoration FJ^C Contractor Team 

D- mow+ A 

Interoffice Memorandum a' 

911 V 

TO ' 1:). A. St. John r.0-19 DA TE ' hebruary 27.1999 

n,•n:s' 

See Below raOW S. L. Winslow 

R ulCun Engineering 

X'+-4 1 /531 -0 706 

WJUECT: CURIE. FSTiMATE FOR SUPP1NC CONCRETE CORE SAMPLES 

CCN: 05508lt 

W° A 2Z'n 

awl e0^ orb 

The following calculations show that cur sunplawith a direct reading of equal to ur icss than 

400.000 dpm/10(km' will be below the definition of radioactive mate rial as de fi ned in 49 CFR 173.40; 

of 70 Bq/g (2F.3 pCi/g). Lach sample will consist of concrete material form four, two inch con 

samples and enough water to make a slutr • consissncy. The diianhution of radionuclides is biped un 

previous concrete samples taken front the below grade Fuel Storage Basin that would also he 


Given 

Cylinder Volume = arh Radius ofco=cte core (r) = I inch 

Concrete Density = 2.35 g/cm' Height of core sample taken (h) — 0.25 inches 

27 pCi = Bq Maximum tEmt reading on core = 400.000 dpm/100cat" 

2. 22 dpin = pCi 

Calculations: 

V — ( 3.14) (1 in.) `( 0.25ia) = 0.79 in' (16.4 cm 'in') (4 Lure satuplcs) = 512 cm' 

(400.000 dpni/5 L2 cm) (em'/2.35 g) = 3.32E3 d;mlg 

3.3213 dpm/g (pCi/2.2 dpm) = 1.5E3 pC'ilg or 55.4 Bq/g 

ti1.W:dld 

Percent Distrihution(`l) Concentration ( L Cih) 

°Co 0.17 2.55 pCi/g 

"'Cs 82 1.2F3 pCi/g 

"lieu 0.33 4.95 pCUg 

"'Eu 0.05 7.5E-1 pCi/g 

°0Sr 17 2.55 112 pCi/g 

"Ann 0.005 7.5E-2 pCi/g 

139124111 

Pu 0.1 L5- C 

Civics: 

S. Ci. Nlarske X5-53 


RadC'on Enginee ring File.!LB XO-23 

Document and Intb Services 110-09 

TOTAL: 1.4613 pCi/g 

Gido

Environmintil 

Contractor 

Contractor ERC Team 


TO' I). A. St John LO-19 DATE: 

Sec 13clow 

Corr=ration (pCi/0 

2.55 pCi/g 

1.2E3 pCi/g 

4.95 pCi/g 

7.5E-1 pCi/g 

2.55E2 pCi/g 

7.5F-2 pCi/g 

1 5 OCUM 

1.4613 pCi/g 

373 °"79 F"-02 

1êbruary 27. 1999 

At 

nto+t: S. L. Winslow 


X34 1/531-0706 

SU BJECT. C'URIF ESTIMATE FOR SJUPP1NGCONCRF.TE CORE SAMPLES 

Job No. 22171 

.^wY..YY.... b 

D\.0 . -A 

Ol e for 

n v 

CCN: 055088 

.Su^w\Cob !I!0 

The hollowing calculations Show that con: 5amplawith a direct reading of equal to or less than 

400.000 dpm/l0(km' will be below the definition of radivactive material as defined in 49 CFR 173.403 

of 70 Ay/g (2F.3 pCi/g). Lach sample will cunsistof concrete material itu n four - two inch co re 

samples and enough water to make a slurry consL*ncy. 'Fhe distribution of radionuc lides is based on 

previous concrete samples uJten front below grade Fuel Storage Basin that would also he 


(jiver: 

Cylinder Volume = n r'h Radius of concrete core (r) = I inch 

Concrete Density = 2.35 g/em `Height of com sumple taken (h) - 0.25 inches 

27 pCi = Dq Maximum Jima reading on core = 400.000 dprn/IUOcaY 

2.22 dprn = pCi 

('alUUldlions: 

V - ( 3.14) (1 in.)'(U 25in) = 0.79 in' (16.4 car/i n -')(4 cure simplcs) = 512 cm' 

(400.000 dpnr/51.2 cm') (cm' 12.35 g) = 3.32E3 dpn/g 

332L3 dpm/g (pCi/2. 2 dpm) = 1.5E3 pCi/g or 55.4 Bq/g 

ti1.W:dld 

°Co 

"'Cs 82 

02 E 

Percent Distribution(%) 

0.17 

0.33 

'"Eu 0.05 

"'Sr 

17 

W ,.iun 

taoawPu 

0.U05 

0.1 

TU'fAL 

('ones• 

S. (i. Marske X5-53 




6 16.4.

Oate/7me Received: 

Figure 1 

SAMPLE CHECK4N LIST 

~ ! ^^ I S Ll SGS Li ln Z^7S 

(j 

Work Order Number. ^1 ^^^^^L'^^^ SAF 

RFSH-SOW-93-0003 - 

Revision 5 

Shipping Container 1 0: 51)1 90 Chain ofCustody # ^ 7^^ ^ – ^L ^ ^^ô ^ L ^ 

1. Custody Seals on shipping container intact? Yes [ ] No ( ^ 

2. Custody Seals dated and signed? Yes [ ] No [ 11^ 

3. Chain-of-Custody record present? Yes W N or( ] 

4. Cooler temperature l 

L) 

S. Vermiculite/packing mate rials is Wet [ ] t ry (I 

6. 

Number of samples in shipping container. 

7. Sample holding times exceeded? Yes [I No (I 


tape hazardlabe 

astcdy seals _appropriate sample labels 


o good condition le akn9 


10. Where any anomalies identified in sample receipt? Yes [J'No [ ] 

11. Description of anomalies (include sample numbe# 

Sample CustodianlLaboratc ry: — L^_ ( a te: ^, 


I 'l

RFSH-SO W-93 -0003 

Revision 5 

Figure 1 _ 


OateMme Received: nn `^ SG#: 

b /^; ^nns^^ 

Work Order Number. 5^ ^ w tk i.^ tJLE' 

Shipping Container 10: Chain of Custody -616 

1. Custody Seals on shipping container irdact? Yes t /No (1 

2. Custody Seals dated and signed? Yes l7 No (1 

3. Chain-of-Custody record present? C Yes "b ( I 


5. Vermiculite/packing mate ri als is Wet I! D ry ( -r' 

6. Number of samples in shipping container: 

7. Sample holding times exceeded? Yes ( ] Vo [ } 

6. 

10. 

Sam s have: 

tae hazard labels 

^tody 

seals _appropriate sample labels 


in good condi tion leaking 

broken _have air bubbles 

Where any anomalies iden tifi ed in sample receipt? Yes (] No [, 

11. Desc ription of aromalies (include sample num bers): 

Sample Custodian/Laborato ry: ^jL 3/y1 ^J(Jjr`Z,/,/e: 

Telephoned 

IA 

pp 

C-1 03

n 

Q 0 3 X05 Cy r,-) D 3-)6& - Zed 


11-Afar-98 

/0 — rye ^^ 1 

CLIENTCODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSR NETCPMB 

Bill BON685 3/11/199812:00:00 PM QUAD23A 3/11/19981:02:54 PM BON685 30 3 0.025 44 0.525 

V I 

LIQUID Bkg: 3/11/1998234:41 AM BKO 600 45 0.075 565 0.9416667 

An] Dale: 3/11/1998 Tot Sa,Alq: LOOE 4 00 LOOI;f OO Alp; (Dpm/ 6.25E-0 2 (uCU 2.81 E-05 (pCl/ 2.81E+01 + 1.9Ei02 CAI' 8.9E-01 Lots 

Ppl mg: 2.9 / Units: L ml Bet; Alq): 9.83E-0 1 So): 4.43E-04 Ljg): 4.43E+02 

+2.OE+02 

Bill BON686 3/11/1998 12:00:00 PM QUAD23B 3/11/19981:02:54 PM BON696 30 1712 57 127510 4249.4083 

V LIQUID Bkg t3/11/1998 2:34:41 AM BKO 600 40 0.06666667 555 0.925 

Ant Dow 3/11 1 1998 To1Sa,Algi LOOEt00 1.00E+00 Alp; (Dpm/ 1.50E+02 (uCU 6.77E-02 (pC7/ 6.77E+04 t2.3E+03 CAT 3.7E-04 Lab 

Ppt mg: 95.5 UNb: L ml Bel; AI 9.32E+03 So): 4.20E+00 L 4.20E+06 + 1.2E+04 

111 

1.2E-06 Alg 

F—^ l-hinr- vN 011 BnlerrB Envlrunmcnl Se rvices, SCP V2.03 

G 

I 

I.IE-01 

Alit 

LI[


12-Afar-98 


BBI BON687 3/12/1998 

V 

LIQUID 3 

And Date: 3/12/1998 Tot St, Alq: 1.00E+00 3 

Ppt m8: 49.6Units: L 

/ 

QUAD21A 

Bke: 

1.00E+00 

nil 

3/12/199811 :01:02AM BON687 

3/12/1998 12:01:04 AM BKG 

Alp; (Dp W 8.39E-0 1 (uCl/ 3.78E-04 

Be(; AIql^ 3.27E+00 Sal: ) 1.48E-03 

30 7 0.18 74 1.54 

600 32 0.05333333 556 0.9266667 

(pC7/ 3 .78E+02 + 3.9E+02 CAT 3 6.6E-02 Lab 

L le)^ 1.48E+03 + 2.8E+02 I 3.4E-02 

Ci 

H 

C ( 12-Afar-98 Quanterra Environment Se rvices, SCP V2.03 I 

Alit 

Ide

^J 

J 

J 

-T 

Bechtel Hanford Inc CHAIN OF CUSTODY/SAMPLE ANALI'SIS REQUEST B98- 661 -09 pare ! ^( ! 

Collector 

R. I'allbere 

^y^ 

DD (A 

Company' Contact 

Steve Nlarskc 

"I"elephone No. 

373-4316 

Plotter( Coordinator 

WIiISS, BI" 


10?-C Phase I k Phase II - Cuncrcle Sanlplce 100 Area B98-061 

Ice Chest No. Field Loghonk No. 

_ — I '^ C3 

Nlethod of Shipment 

Hard deliver 

Shipped In Offshe Propero No. Bill of I.Ad inll/Air Dill No. 

Quanmrru Incorpo rated ^/ 

POSSIBLE SA NIPLE 11.1LA RDS/RF,NIARGS 

Nadioaclir. 


1. NN IA SIS 

L) I Cam ^C'3 -) r' ^ 

Preservation 

I ype of ( retainer 

No. of ( onlatner(s) 

\'olumc 

_ 'U^^1.^ 5«mm Ulm 

Symi.l 

Lou„ô„„ 

w( 

Sample NU. Nfalm Sample Dale smilplc I III1C 

11_ 

Daw Turnaround 

BON68B Other Solid ti' _ _ = (.i / _,:C .^ t J^- ^•' la C 

C11kIN OF POSSESSION 

Î 

^< "I .1.111 ”L. 

Sign/frill Names 

LA 

14ur. ^,I IIJ __ ^(,^ ( "1 _^ 

21 

Days 

SPE( I I I I, INS VIIC 1IONS Nlulri, 

11) ICI' Rlela6 - I , ,iv, i v, Uu mieeccl II eud Nlacul 1411 ChnnmuÎ Ile. - 1196 

KVI. 

111i.1.m , rXel 6:3 SC S4 ! /o - IS/ 

JJJ 

êC^nefûyv^ -9^l C^rLbv^ -(¢ 

NeI )1,.dIt. Ueielwr, Necrncdill U.ue lum / i ^Vl 

R .... yim...A H 'U,Ilc I Ka.anid lli Uem luu` 

L.\I1111

Bechtel Hanforfl Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 -10 Page i nr 

Collector Company Contact 7 elephone No. Project Coordinator Data Turnaround 

R. Fahlberg Steve Marske 3734316 WEISS, RL 

Project Designation Sampling Location 'AF No. 

105-C Phase I & Phase II -Concrete Samples 100 Area B98-061 

Ice Chest No. Field Logbook No. 7 


/ 7 / —/3 (D _ Z Iland deliver 

'hipped lo Offsite Property No.. Bill of Lading/Air Bill No. 


POSSIBLE SAMPLE IIALARDS/RENIARKS 

Radioactive 


Preservation 

'type of Container 

No, of Container(s) 

Volume 

SANII'LE AN.U.\'SIS I^ 

Sa ucm fIl n 

Speual 

Innmciinns 

3 

r 

II. 

a^ 

21 Days 

0 L, ''- G2 

Sample Nn. Matrix ' Sample Date Sample Time ° ;, i u a ,, d; • '.J: ,.:. t'd. ."f .'^rtA`. `Ht :.Sr yB lkl . , :`° C' ' . + y rr_ ' . :' '.. 

BON689 V Other Solid -12 - 131S 

SPECIAL INSTRUCTIONS Ma trix' 

CIIAIN OF POSSESSION Sign/1' it][ Names S - s,,,1 

(1) CPMemis- 6010A ISupnoxcl lLcedlMcraoy-/4/1-(CV), Chraniwn lien-/196. S[ - 5

Environmental 

Restoration ERC ream 

Contractor 


TO'' D. A. St. John LO-19 arc 

nrua' 

5).W:dld 

Set; Below Fa"` 

Percent DistrihutionM 

°Co 0.17 

(IT C." 82 

132 E 0.33 

'"Eu 0.05 

A7Sr 17 

'"'Ain 0.005 

'''"'"'Pu 0.1 

TDTAL: 

T_ -^7n 

l-ebruary 27.1998 

S. L. Winslow 

RadCun Engiw:cring 

X341/531-0706 

sualacr: CVRIK FSTIMATE FOR Stl1PP1N000NCUTF. CORE SAMPLES 

Job No. 22172 

v..,. J. A....r w 

P.D. wA 

CCN- 055088 

ov IO.0 

nn v. 

tae w. 

L..a. CeM 'rV 

The IbIlowing calculations show that con; sampltswith a direct reading of equal to or less than 

400.000 dpm/100cm' will be below the definition of riftwctive material as defined in 49 CFR 173.40-, 

of 70 By/g (2F3 901g). Lach sample will consist ofcoacrctc material from four. two inch co re 

samples and enough water to make a slurry consisxncy. '11w distribution of radionuclides is based on 

previous concrete samples taken front the below Vade Fuel Sloragc Basin that would also he 

representative of these cuncretc samples. 

(jiven: 

Cylinder Volume = nrh Radius of concrete core (r) = I inch 

Concrete Density = 2.35 gJcm' height of core sample taken (h) - 0.25 inches 

27 pCi = Bq Maximum &vet reading on con = 400,000 dpm/lUucalt 


Calculations: 

V-(3.14)(1 in.) `(025in) = 0.78 in' (16.4cm `/inj(4 van: samples) = 512 Lm' 

(400.000 dpm/5 L2 cm) (cm/2.35 g) = 3.32E3 dpm/g 

3.321:3 dpm/g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 kg 

C(Mics: 

S. (. Marskc X5-53 


RadCun Engineering He!LB XO-23 

Document and info Services 130-09 

Cona mtration (uC:V0 

2.55 pCiig 

1.2F3 pCi/g 

4.95 pCiig 

7.5E-1 pCilg 

2.55E2 pCi/g 

7.5F.-Z pCi/g 

1.5 OCUZ 

1.460 pCi/g 

nl 

0103

Environmental 

Job No. 22172 

Restoration 

Contractor a,.n,. w, 

Interoffice Memorandum"` w•~ a' iolt 

n w 

S WA 

S~ Cod. !m 

Concentration (pCi/") 

2.55 pCi/,v 

1.2F.3 pCi/g 

4.95 pCi/g 

7.5E-1 pCi/g 

2.55E2 pCi/g 

7.5F.-2 pCi/g 

1 5 nCi/g 

1.46L'3 pCiig 

CCN: 055081, 

r ERC Team -^- A ^° 

TO; I). A. St. John 1.0-19 °ATL` hebtuary 27. 1999 

' OM1'" Scc Below FROM: S. L. Winslow 

RadCua Engineering 

?634 1/531-0706 

suuecT. Cl:R1F: FSTfMATE FOR SHIPP1NCCONCRETE CORE SAMPLES 

The following calculations shnw that core s arnplcs widi a direct reading of equal trl or less than 

400,000 dpm/ 1 00em' will be below the de fi nitionofradioactive material as defined in 49 CFR 173.403 

of 70 Bq/g (2F3 pCi/g). Gach sample will consist of concrete mate rial from four, two inch co re 

samples and enough water to make a slurry coruiSrncy. 'I-he distribution of radionuclides is based on 

previous concrete samples taken front the below grade Fuel Storage Basin that would also he 

rcprescntative of these concrete sunples. 

Given: 

Cylinder Volutuc = nrh Radius of caucrcte core (r) = I inch 

Concrete Density = 2.35 elem' height of con: sample taken (h) — 0.25 inches 

27 pCi = Dq Maximn m liwt reading on core = 400.000 dpnt/1 Wcar 


Calculations: 

V — (3.14) (1 in.) `(0 25in) = 0.79 in' (16.4 cm'/iii) (4 core samples) = 512 cm' 

(400.000 dpm/5 L2 cm) (cm'/2.35 g) = 3 3 2E3 dtm/g 

3.32L3 dpm/g (pCi/2.2 dpm) = 1.5E3 pCi/g or 55.4 Bq/g 

51.W:dld 

mCu 

117 

C. 

Percent DistributionO 

0.17 

82 

"`flu 0.33 

1"Eu 0.05 

1'Sr 17 

'°'Ain 

11 91'4U 

Pu 

0-UU5 

0.1 

TO rAi 

Cn ies: 

S. (J. Marske X5-53 

P. A. Newman X3111 

RadCun Engineering file. !LB X0-23 

Document and into Services 110-09 

0109

Figure 1 

Î 

Date/Time Received: `l 

^.Z- 

Q 

^%1 ^v SGS., 

RFSH-SOW-93 -0003 

Revision 5 

SAMPLE CHECX-W UST _ v 

Work Order Number. 

SAF S ^(j CzQ3 ^j ^j–(,^¢ 1 - 

Shipping Container ID: "K-R . 

//}} 

chain o(Qstody S ^g 3 Dot ^1 -09 

^1rAq?, 

1. Custody Seals on shipping contairx intact? Yes [q/No ( I 

2. Custody Seals dated and signed? Yes B-INo (1 

3. Chain-of-Custody record present? Yes ( No (1 

4. Cooler temperature l 

o 

5. VerrnicufdeJpacking mate ri 

als is Wet [ Dry k/l )— 

in 

6. Number of samples shipping cadainer. 

7. Sample holding times exceeded? 2« Yes No [ 


tape `hazard libels 

_____custody seals _approprieie sample labels 

9. Sam les are: 

in good condition Ong 

broken Inge air bubbles 

10. Where any anomalies iden tified in sample receipt? Yes (j No 

11. Descrip ti 

on of anomalies (include sample numbers: 


C,li^

Figu re 1 


Revision 5 


S 

Date^me Received: , Î ^ l^^l / SG# l l^ ^l ^— 7 

1 

Work Order Number. SAF #: f5 1 — - 

Shipping Container ID: Chain of Custody if 

1. Custody Seals on shipping contakw intact? Yes [ 1,140' [ 1 

2. Custody Seals dated and signed? Yes [I No ( ] 

3. Chain-of-C ustody record preserd? Yes _ ,] No ( ] 


5. 

/` e 

"7 

VermicuWpacicing mate ri 

als is Wet [ [ C ry (^ 

6. Number of samples in shipping cmtainer. c 

7. Sample holding ti 

mes exceeded? Yes [ ] No [ ] 

8. Sa les have: 

Pe 

/ custody seals 

hazard labels 

_appropriate sample labels 

9. —8mptes are: 

in good condition leaking 


10. Where any anomalies identified in sample receipt? Yes [ ] No 

11. Desc ri ption of anomalies (include sample numbe rs): 

Sample Custodian/Laborato ry: 

Telephoned To: On. 

14 

C11i

(7) 

^ 96 . D3 1 C'-.n, 3 


13-Mar-98 

( J 

CLIENTCODE ID MATRIX RECEIVED DETECTOR ACQ DATE SAMPLE MINUTES CNTSA NETCPMA CNTSB NET CPMB 

Dill BON698 3/13/1998 QUAD2IA 3/13/199810:21:17 AM BON699 30 9 0.24142857 57 0.96 

O I LIQUID Bkg: 3/13/1998 1 :30:18 AM BKG 700 41 0.05857143 658 0.94 

An! Date: 3/13/1998 Tot Se, Algl 1.00E+00 , 1.00E+00 Alp; (DpM 1. 21E+00 (uCV 5.45E-04 (pCV 5.45E+02 t 4.1E+02 CAT 4.6E-0 2 Lab 

Ppt mg: 51.3 1^ Units: 1 1 ml Bet; Alq): 1.98E+00 Sa): 8.94E-04 Llg): 8.94E+02 ± 2.5E+02 I / 5.6E-0 2 Ni 

Bill 130N689 3/13/1998 QUAD2113 3/13/199810:21:17 AM I1ON689 30 661 21.9790476 47335 1576.8733 

OLIQUID Bkg: 3/13/1998 1:30:18 AM BKG 700 38 0.05428571 672 0.96 

And Date: 3/13/1998 Tot Sa, Alq: 1.00E+00 1.00E+00 Alp; (DpM 2.19E+01 (uCB 9.84E-03 (pCV 9.84E+03 + 8.5E+02 CAT 2.5E-03 Lab 

Ppt mg: 50 / Units: L / , ml Bet; Alq): 3JOE+03 Sa): 1.49E+00 Ljg): 1.49E+06 + 6.8E+03 

IIt 

/ 7.4E-05 

MLIL 

13 111 IION753 3/13/1998 QUAD2 1 C 31]3/199810:21:17 AM BON753 30 0 -0.0571429 84 1.9057143 

SOLID Bkg: 3/13/19981:30: 1 8 AAt BKO 700 40 0.05714286 626 0.8942857 

An] Date: 3/13/1998 Tot Sa, Alq: 2.50E+02 9.77E+01 Alp; (DpM -5.47E-0 1 (uC i/ -6.30E-04 (pCU -2.52E+00 ± 4.8E+00 CAT 2.5E+02 Lab 

Ppt mg: 97.7 Units: g 

/ 

/ mg Bet; Al Alq); 4.30E+00 Sa ) : 4.96E-03 L c)^ 1.98E+01 ± 3.2E+00 I / 5.0E+00 

Bill BON734 3/13/1998 QUAD2 113 3/ 13/199810:21:17AAI BON754 30 8 0.20666667 77 1.4709524 

SOLID Bkg: 3/13/1998 1:30:18 AM BKG 700 42 0.06 767 1.0957143 

And D ate: 3/13/1998 Tot Sa. Alq: 2.50E- +02/9.60E + 01 Alp; (DpM 1 .31E+00 (uCit 1.54E-03 (pCV 6.16E+00 ±5 .6E+00 CAT HAE+00 tab 

Ppt mp 96 Units: g mg Bel; Alq): 3.19E+00 Sa): 3.74E -03 Leg): IA9E +0 1 ± 3 . 1E+00 I / 6 . 7E+00 

BIII BON755 3/13/1998 QUAD22A 3/13/1998 10:21:21 AA1 BON755 30 3 0.05571429 70 1.4004762 

SOLID Bkg: 3/13/19981:30:26 AN] BKG 700 31 0.04428571 653 0.9328571 

Ant Dale: 3/13/1998 Tut Sa,Alq: 2.50E+02 9.61E+01 Alp; (DpM 2.80E-0 1 (uCl/ 3.28E-0 4 (pCi/ 1.31Et00 +4.5E+00 CAT 3.8E+0I Lab 

Ppt mg: 96.1 Units: g mg Bel; Alq): 2.98E+00 Sa): 3.50E-03 Ljg): 1.40E+01 ± 2.8 E+ 00 

/ 

I l 

Alq 

Ll g 

Llg 

7.2E+00 Alq 

LI g 

13111 11ON756 3/ 13 /1998 QUAD22B 3/13/1998 10:21:21 Mt 130N756 30 8 0.20952381 66 1.2314286 

SOLID nkg: 3/13/1998 1:30:26 AM BKG 700 40 0.05714286 678 0.9685714 

AN Hate: 3/13/1998 Tot Sa, Alq: 2.50E+02 9.73E+01 Alp; (DpM 1.32E+00 (uCI1 I.53E-03 (p(7/ 6.12E+00 ±S.OE+00 CAT 8.2Et00 Lab 

Ppt mg: 97.3 / Unitr. g / , mg Bet; Alq): 2.57E+00 Sa): 2.97E-03 LIg): 1.19E 4 01 + 2.5E+00 I / SAE+00 

Alq 

Llg 

1^-s 

ê 

ra 

13-h/ar-98 

Quanterra. Environment Se rvices, SCP V2.O3

G_ 

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-o61-I I Parc ! of I 

Collector 

n 

J !-.. "'aIF=> ^ y qh+ / RQ - A 


105-C Phase 1 A Phase II - Concrete Samples 

ornpany Contact Telephone Nu. 

Steve Marske 373-4316 

Sampling Location 1_ 

10O Area (os -c IMP twvc 3 


WEISS, RI, 

F No. 

098-061 


I 

r L_ '3 UC1 

Alethod of Shipment 

Iland deliver 

Shipped 'I u 


Bill of Lach/Air Bill No. 

POSSIBLE SAMPLE IIAZARIIS/REMARKS 

Radioaco,,, 



Olfsitc Property No. 

NA 

Preservation 

'I ype of Container 

Nn, of ('oriminer(s) 

/Vll/l"/ 

Volume 

/ J 

Nose 

I I. 

See imm I I)ir 

Special 

Insimcram 

N 


2 

^ Days 

-Ckk ivA 9 6-^)a425- 

Sample No - >j / 

rH 0 

mric • Sample Dole Sample Mime - ..... ! }'t gr ,. .2 

,,^, ..: 

BON690 G I Other Solid (3 MA (Z^l t'^ fJ Li I c 

SPECIAL INSTRIC I IONS 

t'ILMN OF POSSESSION Sign/Print Names 

. 

(1) KTMndls- 6010A(Sop,rlrace) I Lead), Mercwy-7471-(CV); C'hrumlum Ilea -7196, 

1t6 00p uhe li' lot 12541; Damns Spectroscopy Dam.Tu, Re ei B' Ddie,' n ICBs 6080 lA¢n D 

IC smm-U7 Cobal"O,Eur pion-152, 

^p 

oop, n 191. 1. , u n-1551, A e,c un-241 I I , ¢ Ismoprt 1r000000 s.1c 

î NqR rCJLI^.^ 5 C 

p %// 

P c mq^^^.hcd lb _._ li ci cl n, 1

c) 

H 

1Q 

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061 - 12 Paee ! 

Cullectur 

`1 

pp 

+tam -per & l i) -r / â IN I 


10 -C Those I k Phase II - conciew Sulllples 

Company Contact 

Steen hla rs ke 


10O Arca — I OS f- p Ilea ( +0 3 

Ice Chest Nu. Field Logbook No. 

EL -I IUA -6 L 

Shipped 7L 

Offs to Property No. 

Ouanicrra Incorpurmcd 

POSSIBLE SAi\IPLE IUZ\RDS/BENIARFS 

Badioaciice 

Special Ilandthig and/or Smreac 

BON691 

^03^G CAM 

Simple No I I I ) 

O.^ 

S:k1I 1 1.1; 

AN%11SIS 

h1A 

Prnscrcaliun 

Telephone No. 

373 -4316 


WEISS. RL 

SAF No. 

B98-061 


Iland del I%er 


w^ 


we -_-- 

2 nays 

'1'1'pe of Container i 1 

Nu. W 1loth... r'I'1^1 I _. 

\'plume 

IL 

see ueni lu in 

sn=.ml 

^03r^ 4^ - i^^(n( Ll- 

Iri% a .tialllple Pate Sample I II11C 

Other Solid 13 M RR ^/ Q ^(J ^^ —? 

-- 

_ - 

L 

- -1 

l I 

l f 

SPLCUL INSIRI I - IONS Main 

( HAIN OF POSSESSION Sign/Print Nit s s,,,i 

1111CI'MUa6-onl uq lS,ipuvecq lead;. Al t..... 74al- IC VL C6mauum lien-7190_ g. Spa 

Ita-1 ^,,, 

,d i, n, 

Nd nq ,I .J 

n Jp le4 1 UaI, Imm Re Dmclm,. I('0 - 8080 Ioi I I4 l ,G.iiiiin,i Stearn,- pp 1- in-13 7, C pbah60_f I n-15?- do s..i 

P 1 in-I,I P -hit A u_}i I. I. P . I I I ue I.ul, pl. li I i. Sale V r.. 

^CQ,eC/L 

13H92 

yg b3^ ^- .C- /3 ) 

- -- u.l- I ^„e p^ 'd - ,, .Ie 1,^ê I UC/cp-Y^., SelPn.If CM -7^1^ N^^jEe/-103; Sr-^FJ, Î ,I ^ 

90 7 15 

Te ^^lef L(^ ^q ' L'arbon -l¢ 

ff 

III, I- 1 m, ken nl P7 Ualc I me "ic v 

Hehn.pu,h ed ii, )a” lime Itacmled It, I)mo 1111, 

/ ^ ^ / /N ^^ nl I 

J3 I lu 

1—k \I (11(1 ft li. Inl. Dmc'l iiim 

Sf f l ION 

-- 

F IN \L 5 \\II'L f; 

UNI I ISI I If IM1 

U,pu..d nl.n,.,.l -. -.. - - - - b,p„^ I ^^ - - 

- 

- 

Uaie I ne 

,u o q 

i- ^x 

of 

i y...a..

Environmental 

Restoration ERC Team 

Contractor 1>.D. WA 

CCN: 055088 

fob Vo.2zt72 

W^Â^ a 

Interoffice Memorandum a' ^'' w° iWA w^ ran ^ 

S C 

SMw•CoA 11!0 

TO: D. A. St. John LO-19 °ATE: I ebnwy 27. 1999 

Scc Bclow MO.% S. L. Winsl ow 

RadCuu Engine ering 

X3-41/531-0706 

suuecT: CURIF. ESTIMATE FOR SJUPPINCCONCRETFE, CORE SAMPLES 

The following calculation simw that core sampleswith a direct reading of equal to or less IlLin 

400.000 dpm/1 00cm'will be below the definition ofradivactive material as de fi ned in 49 CFR 173.40; 

of 70 Bq/g (2F3 pCl/g). Lach sample will consistofeoncrete mate rial from flour, two inch core 

samples and enough water to make a slurry consisrncy. 'fhe distrihutiun of radionuclides is hased ern 

previous concrete samples taken front the below gmdt! Fuel Storage Basin that would also be 

represcniative of these cunercic samples. 

'iven: 

Cylinder Volume = nih Radius of co acte core (r) = I inch 

Concrete Density = 1 35 g/cm' height of care sample taken (h) - 0.25 inches 

27 pC; i =13q Maximum Jana reading on core = 400,000 dprni i UUcni' 

2?2 dpm = pCi 

Calculations 

V — (3.14) (I in.)'(U._5in) = 0.78 in' (16.4 ctrl'/in^ (4 care santplcs) = 51? cm 

(400.000 dpni/5 L2 cm') (cm'2.35 g) = 3.32E3 dim/g 

3.32L3 dpin"l; (pCi2 2 dpm) = 1.5E3 pCi/g or 55.4 Bq/g 

SINAld 

Percent Distribution(%) Conceatration (VOW, 

nCo 0.17 2.55 pCi/g 

"'Cs 82 1.2F.3 pCilg 

'''lEu 0.33 4.95 pCi/g 

"'Eu 0.05 7.5E-1 pC ilg 

°"Sr 1 7 2.55E2 pCi/g 

SA'Atn 0.005 7.5E-Z pCi/g 

'39n 'Pu 0.1 1 5 nCU 

Co ics: 

S. G. lvlarske X5-53 

P. A. Newnlatt X:>-4 1 

RadCon Enginee ri ng FildlLB X0-23 

Document and Into Services 110- 0 1) 

TU'fAL_ 1.46U3 pCi/g 

61 115

Figu re 1 


DateTme Received: d 3 51 Sc'k W uOb/^2 S 

Work Order Number. 

0^ 

Shipping Container ID: '^ ^ Chain of Custody # 

SAF # 13 I JGG-QP 


Revision 5 

1. Custody Seals on shipping container inta ct? Yes ( q-,K o 

2. Custody Seals dated and signed? Yes (q- o 

3. Chain-of-Custody record present?^ Yes ( o ( ] 


5. Vermicurde/packing mate ri 

als is Wet (] D ry 


7. Sample holding times exceeded? Yes [I No 14--' 

8. Samp have: 

tape _hazard labels 

custody seals !approp riate sample labels 

9. Samp are: 

ii^n good condition leaking 


10. Where any anomalies identified in sample re ceipt? Yes [ I No [q--^ 

11. Descrip tion of anomalies (in cl 

ude sample numbers): 

Sample ate: 6 

Telephoned 

?4 

G.

H 


13-Mar-98 

l3-Afar-98 

03^^3 LIB i^ 03,E 40 ". 


Blil BON690 3/13/1998 QUA 1324B 3/13/1998 1:15:37 PM BON690 30 7 0.17619048 71 1.3838095 

D' LIQUID Ilkg: 3/13/1998 1:30:14 AA1 BKG 700 40 0.05714286 688 0.9828571 

Anl Dale: 3/13/1998 Tot So, Alq: 1.00E+00 1.00E+00 Alp; (Dpi/ 5.84E-0 1 (uCB 2.63E-04 (pCl/ 2.63E+02 ± 2.6E+02 CAT 9.5E-02 Lab 

Ppt me: 1 1 5 Unib: L MI Bet; Alq): 2.64E+00 So): 1.19E-0 3 LI8): 1.19E+03 ± 2.5E +02 I / 4.2E-02 Alq 

LIE 

Bill 13ON691 3/13/1998 QUAD24C 3/13/19981:15:37PM BON691 30 2 0.00666667 30 -0.002857 

dZ- LIQUID Bkg: 3/13/19981:30:14 AM BKG 700 42 0.06 702 1.0028571 

AM Dote: 3/1 3/1998 Tot So, Alq: I.00E+00 LOOE+00 Alp; (Dpm/ 2.02E-02 (uCV 9.12E-06 (pCU 9.12E+00 + 2.0E+02 CAT 2.7E+00 Lab 

PplmB: 1.5 / UNin: L / , ml Be(; Alq): -9.36E-03 So): -4.21E-06 LI8): 4.21E+00 + 1.6E+02 I I.OE+00 Mq 

LIE 

Quanterra Environment Se rvices, SCP V2. 0 3 

p

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUES T B98-061 -I6 PaRe 

Collector/ / 

a/t r4 J1 RAld 

Project Dealgnation 

105 -C Phase 1 R Phase II - Concrete Samples 

Conlini ('unlact 7 elepbonr No. 

Steve Maroc J7J-4716 

ampling Location 

I OO Atea 

Project Cnordinalnr 

W11S. S, lit. 

AF No. 

1198-061 

I" Cheat Na Field Logbook No. .Method of Shipment 

Mpped To 

Quanterra Incorporate) 


Radloaetiv< 

peclal Handling and/or Storage 

{land deliver 

Offsiie Properly No. hill of LadinR/Air hill No. 

Prese rvation 

T) or of Container 

"°^° 

No. of Cnnldner( s ) 7 

Volume 

s^^^ Ce)Da^7S 


^03a ^'•I m g03X7,)- PC,4 

Sample No. Matrix • Sample Date Sample lime 

1. O Z Other Solid 3 —/6^ f U 

CHAIN OF POSSESSION Sign/Print Names 

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-14 Page 1 of ! 

Collector company Contact Telephone No. Project Coordinator Data 'turnaround 

to o+Mhrr 3 A!11 /1 Steve Marske 3734316 WEISS. RI. 

4 I 

Project Designation /'\, 

Sampling Location SAF No. 

105-0 Phase 1 & Phase 11 - Concrete Samples 100 Area B98-061 


Hand deliver 

- hipped To Offske Property No. Bill of Lading/Air Bill No. 

Quanterm Incorporated 

POSSIBLE SAMPLE HAZARDS/REMARKS 

Radioactive 

S pecial Handling and/or Storage 

S.-vNIPLE AN'AIA SIS 

Preservation 

Nape 

T) pe of Container P 

No. of Container(s1 

A'olume 

u. 

sec eem al i ^^ 

Special 

Inswnlo^. 

Sample No. Matrix Sample Date Sample How .. .»r a __ .., ^ 

BON693 02 Other Solid ._ 6 p 

21 Days 

CII N OF P SS.FSS ON 

R 

êry^^ pl 

y D 

^ ^ 

I?/ C 

Sign/Print Names 

A ^ 

h^ 

IJate'I c 

2 

/ 

?/ 

//' 

/_ 

SPECL%L INST] tIONS 

fll lU'Meia6-bU1041Jupenrao 1, 1.cad;-Memw.-74-1- ICVL Chronmunlie'- 71 96. 

PCBs roscopv Q,smm-137_ Cobalt-60, Lawtalim-152. 

Furop um I ^1 Cumpwm I n Ai enaum-?GI Imtopie Plwmuum. Isotopic lJrann lm_ Sale 

^ / 

/^ 

(Aj"V( — /^/3^ 9 

s 

St 

s0 

Si 

Matrix 

Snit S.Emc^ 

-- Solid 

= Sluay.^ 

6v Relinquished By Ua le71lnc Rece . ced B1 ^ryVL'^ 

lI..CC.. t_ 

)ale.Time l 

^^—^ ^^— ^^_ ^r - 

1) 

t 

- N'aâ 

- Olt 

Reli ted BS hale I mx Rewncd Bc Dale-lime 

echne-h'urv^ - Ì q 

J 

r, 4

Bechtel Hanford Inc. CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST B98-061-15 F! ,f 1 

Collector /^^ 7 

ISr1`fq .v+ 

^,y {^ ( 

Project Designation Sampling Location 

1051' Phase I & Phase II -Concrete Samplcs 

100 Area 

Compa nN Contact Telephone No. 

Steve Marske 373-4316 


WFISS. RL 

'AF No. 

B98-061 


Hand deliver 

Shipped I o 


POSSIBLE S,\htI'Lf: 11:\Z.\RDS/Kt:\I:\1265 

Radioacinc 

)(life Propert N .N o. Bill of Lading/Air Bill Nn. 

I'rescn'alion 

Tcpe of Container 

No. of Cunlainer(s) 

pecial Ilandling and/or Storage \. 1 rent 

nonr -- 

II. 

s.e urin U i ^ 

speâl 

SA M P[ E ANA 1.1 S IS °51N°°°` 

^03^? X11 Cl^ rti1 ^D^^^^^ ^^( 

Sample No Matrix " Sample (late Sample Time J- .. -- 

BON694 03 Other Solid 

l) 

S G 

N 

Data I urnaround 

S / }L 

21 Days 

SPECI:A1, IN'STRt'CI IONSNtaulx 

CI P IN OF 'OSSESSION Sign/Prins Names 

F / _ IulclNt 1 i. e 1 A.NI, ", - I I( I a rr,. 

s. ,.a,,. 

Sel ui' ^ 

I 

N.^^,^J 

qq pp )a l e linen kece b, Ual is I'( 11 41 80 1io i 1 Cin AI CCrtrs op C Is'. t b h 60 ( uuopiiiiii I'' so s.^ 

I.i ,hr .............^.:, ni..ic ._'41. I. n.pJlrno 6nopicLen n 

N-CLLL /b ^p'lyC^ lZ/5 C 

SJ< SI ,i1ue 

^7 q 

keLnquahed lac __-- Uom llmc aca-n u113.Deie'Iim^ 

--7,7. 

^^ 

l/lM 

rl f "^ { 

CC..^^ I 

clinqunacd I{, iLeo Ilwa kecur cJ b, Uam linen °`'r r { l//ti-e b^r / - 

ehnyuuhN U. Unir lnr,^ Remir ad I4 hntc lnn^ 

S1. C [ ION 

FIN.AI. tiA AII'Lt_ U I d Ata h o a 

DISPOSII ION 

_ 

1—all- 

/ A G^ 3 , cJ//.^ 

_ Unl .cJ B Uuc I unc 

Ua In.

Res Environmental 

Hestoratlon 

Contractor 

^^^ Team 


M D. A. ^4. John 1.0-19 

t 0M.N. 

See Below 

t'"TE: 

IRON: 

373 c'.17g 

1^cbruary 27. 1999 

S. L. Winslow AV 


X3-41/531-0706 

SUBJECT. CURIF ESTIMATE FOR SHIPPING CONCKETE CORE SAMPLES 

Job No. 22172 

D. D. »-A 

OC 10.c 

q w 

suww. cod. IM 

C C N: 055OHN 

The following Calculations show that core !iampleswith a direct reading of equal to or less than 

400.000 dpm/l 00cm'will be below the definition ofradivactive material as defined in 49 CFR 173.40; 

of 70 Bq/g (2F.3 pCi/g). Lerch sample will consist of concrete material Bonn four, two inch core 

samples and enough water to make a slurry consistency. 'Fhe dist ri bution al radionuclides is based on 

previous concrete samples taken from the below grade Fuel Storage Basin that would also be 


"vet : 

Cylinder Volume _ nr'h Radius of concrete core (r) = I inch 

Concrete Density = 2.35 g/Cm' Height of core sample taken (h) - 0.25 inches 

27 pCi = Bq Maximum tfrrect reading on core = 400.000 dpm/ 100cm1 

2.21 2 dpm = pCi 

Calculations: 

V - (3.14) (1 in.) 4(U.25in) = 0.78 in' (16.4 cot'/irrj (4 care samples) = 51.7-1 cm' 

(400.000 dpnl/5 1. 2 cm) (cm'/2.35 g) = 3.32EI dtm/g 

3.320 dpm/g (pCi/2.2 dpm) = 1.5E3 pCUg or 55.4 Bq/g 

SI . W Ald 

Percent Distribution(%) Cortcentration (VCi/g) 

"Co 0.17 2.55 pCi/g 

137 

Cs 82 1.2E3 pCi/g 

02Eu 0.33 4.95 pCi/g 

Èu 0.05 7.5E-1 pCi/g 

"'Sr 17 2.55E2 pCi/g 

Z41 

Ain 0.005 7.5F.-2 pCi/g 

2J'U2 4U 

Pu 0.1 L5 .i/ 

Co ies: 

S. G. Marske X5-53 



Document and Into Services 110- 09 

TD'fAL: 1.4683 pCUg 

G1^1

Figure 1 

SAMPLE CCK-IN LIST 

Date/TlmeReceived: ^^ ^^^^^ SG#: 

Work Order Number. 0 ^3 7 

r 

RFS H-SOW-93-0003 

Revision 5 

^ ^^0^ SAF #: oUî - 

Shipping Container lD: O) Chain of Custody # /^0 "(',&/- 

1. Custody Seals on shipping container intact? Yes eNo 

2. Custody Seals dated and signed? Yes KNo [ ] 

3. Chain-of-Custody record present? Yes [>r No [ ] 

O 


5. Vermiculite/packing mate rials is Wet [I Dn/^^ 


7. Sample holding ti 

mes exceeded? Yes [ ] No [4--- 


_ Llape 

custody seals 

hazard labels 

appropriate sample labels 

9. Samp s are: 

n good condition leaking 


10. Where any anomalies identified in sample receipt? Yes [ ] No 

11. Desc ription of anomalies (include sample numbers): 

Sample Custodian/Labor/ UL ^^ Llj4 

Telephoned To: On C/ 

I


17-Mar-98 


Bill B0HJI0 3/17/1998 QUAD21B 3/17/19989:38:04AA1 BOH1I0 30 11 0.32 107 2.6266667 

SOLID Bkg: 3/17/199812:19:30 A61 BKG 600 28 0.04666667 564 0.94 

Ant Date: 3/17/1998 Tot Sa, Alq: 5.00E+02 1.02E+02 Alp; (DpM 2.10E+00 (uC7/ 4.66E-03 (pCU 9.33E+00 ±5.3E+00 CAT 5.4E+00 Lab 

Ppt mg: 101.6 / );nits: G mg Bet; Alq): 5.73E+00 Sal: 1.27E-02 LIg): 2.54E+01 ± 3.4E+00 I 3.9E00 Alit 

Dill 13011/11 3/17/19')8 QIJAD21C 3/17/I9989:38:04AM 8011111 30 13 0.37333333 308 9.2816667 

SOLID Bkg: 3117/1998 12:19:30 A11 BKG 600 36 0.06 591 0.985 

An] Date: 3/17/1998 Tot Sa, Alq: 5.00E+02 9.95E+01 Alp; (Dpm/ 1.90E+00 (uCV 4.31E-03 (pCU 8.62E+00 ± 5.4E+00 CAT 5.8E+00 Lab 

Ppt mg: 99.5 Units: g mg Bet; Alq): 2.06E+01 Sa): 4.66E-02 Llg): 9.32E+01 +5.9E+00 I , LIE+00 Alq 

"It 

BHI BOHJI2 3/17/1998 QUAD21D 3/17/19989:38:04Abi BOHJI2 30 12 0.34666667 212 6.1383333 

SOLID Bkg: 3117/1998 12:19:30 A.\I BKG 600 32 0.05333333 557 0.9283333 

And Date: 3;17/1998 Tot Sa, Alq: 5.00E+02 9.91E+01 Alp; (DpM 1.98E+00 (uCU 4.50E-03 (pCU 8.99E+00 ±5.4E+00 CAT 5.6E+00 Lab 

Ppt me: 99.1 Units: g mg Bet; Alq): 1.36E+01 Sa): 3.10E-02 Llg): 6.20E+01 +4.9E+00 I ,- 1.6E+OU Alq 

LIg 

Bill BOHJ13 3/17/1998 QUAD22A 3/17/19989:38:08 AM BOH113 30 1 -0.0183333 346 10.638333 


Ant Date: 3/17/1998 Tot Sa, Alq: 5.00E+02 9.87E+01 Alp; (Dpm/ -7.95E-01 (uCU -1.81E-03 (PC[/ -3.63E+00 ±4.6E+00 CAT 5.0E+02 Lab 

Ppt me: 98.7 Units: g mg Bet; Alq): 2.30E+01 Sa): 5.25E-02 LIg): 1.05E+02 +6.IE+00 I 9.5E-01 Alq 

LIg 

Bill BOHJ 14 3/17/1998 QUAD22B 3/17/19989: 38: 08 AM BOHJ14 30 20 0.59666667 670 21.385 


And Date: 3/17/1998 'rot Sa, Alq: 5.00E+02 LOSE+02 ,Up; (DpM 2.83E+00 (uCi/ 5.91E-03 (pCU 1.18E+01 +S.IE+00 CAT 4.2E+00 Lab 

Ppt mg: 107.8 ))nits: g m g Bet; AI9h 4.74E+01 Se ) : 9.90E-02 L e): 1.98E•+02 ± 8.0E+00 

I 

S.IE-01 

LIC 

LIg 

Bill BON692 3/17/1998 QUAD22C 3/17/19989:3808AId BON692 30 7 0.19166667 310 9375 


AN Date: 3'17'1998 Tot Sa, Alq: 100E+00 1.00E+00 Alp; (Dpn,/ 2.40E-01 (uCV 1.08E-04 (pCU 1.08E+02 + 1.9E+02 CAT 2.3E-01 Lab 

Ppt mg: 04 Units: I, ml Bet; Alq): 1.73E+0i Sa): 7.81E-03 LIg): 7.81E+03 +4.9E+02 1 64E-03 Alq 

LIg 

CI 

F-+ 

T 17-Afar-98 Quanterra Environment Services, SCP V2.03 

C.7

L^ 

T J 


BHI BON693 3/17/1998 QUAD22D 3/17/19989:38:08 AM BON693 30 7 0.16166667 117 2.96 


Ant Date: 3/17/1998 Tot Su, Alq: 1.00E+00 1.00E+00 Alp; (Dpm/ 6.55E-0 1 (uCl/ 2.95E-04 (pCi/ 2.95E+02 ±3.7E+02 CAT 8.5E-02 Lab 

Ppt mg: 512 / URNS: L -! ml Bet; Atq): 6.09E+00 So): 2.74E-03 Llg): 2.74E+03 ± 3.4E+02 I LSE-02 

BID BON694 3/17/1998 QUAD23A 3/17/19989:38:12 AM BON694 30 6 0.11166667 57 0.8816667 

G 3LIQUID Bkg: 3/17/1998 12:19:48 AM BKG 600 53 0.08833333 611 1.0183333 

An] Date: 3/17/1998 Tot So, Alq: 1.00E+00 1.00E+00 Alp; (Dpm/ 5.45E-0 1 (uCV 2.45E-04 (pCl/ 2.45E+02 +3.8E+02 CAT 1.0E-0 1 Lab 

Ppt mg: 5$. 1 UNta: L / ml deh, Alq): 1.78E+00 Sa): 8.02E-04 Lg): 8.02E+02 ± 2.4E+02 

1 

6.2E-02 

LIIg 

BHl B0N8616 3/17/1998 QUAD23B 3/17/19989: 38: 12 AM BON8M6 30 119 3.92 5799 192.32333 

LIQUID Bkg: 3/17/199812:19:48 AM BKG 600 28 0.04666667 586 0.9766667 

And Date: 3/17/1998 Tot Sa, Atq: 6.00E+00 1.00E+01 Alp; (Dpm/ 7.45E+00 (uCU 2.01E-03 (pCl/ 3.35E+02 +4.OE+01 CAT 7.5E-02 Lab 

Ppt mg: 3.5 ,/ UNb: L ml Bet; Alq): 3.66E+02 So): 9.88E-02 Llg): 1.65E+04 ± 2.2E+02 1 , 3.0E-03 

BHI BON8Af7 3/17/1998 QUAD23C 3/17/1998938- 1 2ANI BON8M7 30 23 0.71833333 107 2.6683333 

LIQUID Bkg: 3 1 17/1998 12:19:48 AM BKG 600 29 0.04833333 539 0.8983333 

And Date: 

Ppt mg: 

3/17/1998 

5.9 ! 

Tot Sa, Alq: 6.00E+00 / 

UNb: L 

1.00 E+01 

ml 

Alp; 

Bet; 

(Dpm/ 2.18E+00 

Alq): 4.79E+00 

(uCl/ 5.89E-04 

So): 1.29E-03 

(pCl/ 

Llg): 

9.81E+01 

2.16E+02 

±2.7E+01 

+ 3.0E+01 

CAT 

I 

2.5E-0 1 Lab 

^- 

2.3E-01 

Alq 

LIg 

BHI BON8M8 3/17/1998 QUAD23D 3/17/199893812Abf BON 10,1 8 30 36 1.13666667 114 2.89 


And Date: 3/17/1998 Tot So, Alq: 6.00E+00 1.00E+01 Alp; (Dpm/ 3.46E+00 (uCl/ 9.36E-04 (pCl/ 1.56E+02 + 3.0E+01 CAT 1.6E-0 1 Lab 

Ppt mg: 3.5 / Un1b: I. / ml Bet; Alq): 4.83E+00 Sa): 1.31E-0 3 Lg): 2.18E+02 +2.9E+01 

I / 

2.3E-0 1 

AI 

Llg 

17-,Liar-98 Quanterra Envi ronment Se rvices, SCP V2.03 

!'^,71 i 

LIg 

LIg

1(ùanterra 

Soria 

BATCH SUMMARY/CHAIN OF CUSTODY 

ANALYSIS A^ _MATRIX 0 TYW'R DUE DATE y -6 -`t 

I^ R`t C-T--rnENr 

WORK ORDER SEQUENCE # CLENT COMhom 

J 03161 -1B 

QCBATMFEACrENTMANK 

6^+1 

J N a. -ix QC BATCBMAIM BI ANK 

J o b t b l -iM oQ 

(circle) 

J 2M or 2S 

(fie) 

D o3tbt -O^ 

!Sb3l6to\ J 1 `^ 

gu3 J$gO2 

803 Zo(o O Z. 

03 222.02 

$03 Z'7 2_O1 

Batched and QC updated bye on 3 •Z5-^ 

QC BATCHMAMUXREAC0;r 

SPOM 

QC BATC HMAIRDVREAGENT SPUKE 

Duplicate ofSamo # $0 3 t b 1 01 

Rec'd in Prep Lab by on Z" _W Sop# tLtF RCSot Rn'- 0 _ 

Rec'd in Sep Lab by v a/ on— Sop# Rn i 

Rec'd in Sep lab by on Sop# Rte= 

EDY ^P by 

on Ì - 3 - C 

Sop# i^ i C h ,l C 5 U 0 

^^ 11nn 

rr % 

by l an Sop# 6 ^Cl QQQ ^- Rid 6 

Rec'd in C.R j 3 'T 

Da ta Reviewed byon^ Sop# 6 Cr/ (sF?1^7. M-4 Z^ 

O riginal batch sheet complete akvl u n file to be filed with the FIRST listed work order number. 

FORM NO.: RC-52.1/98. Rev. 8 2Faceo n^,G c 

CRT 

RPT u .TS = ^C^^S^ S(^ ^2u^ o s o^ O e yccw^ -^ nor rc 1 sA 

CT 

= \c0 

GI^,, 

c,T- =N 5 T = A-s p ^ ^ —

\^ ^c CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 10-Mar-1998 

Page 1 

' CUSTOMER: BHI SAMPLE DELIVERY GROUP 

^p 

11ATRIX OTHER ^ BATCH NUMBER 

CUSTOMER 

LIES ID DUP ACCOUNT ID COMMENTS 

5A, A^ 

Ser)_ 

__°_______=====ESJA625 ---------- == 

To3^b1\S IQO129 ) 

1 ) 80316101 ESJA626 II BON680 O.000S6 8- 

Pr.11/2 4 /91 91,11/29.98 

2 ) sea t 6t62 6H f s vriooi 

— '7t p?^16101 

ESJA627 p.oco3' 73 

JÂjCQTIONS (Initial !. Date) 

9 

1) INITIATED l ^ l !D 5) COUNTINC/MEASUREMENT LAB 

SOPS) # 

SOP (5) # 

2) PREP LAB RECEIVED l9scY o.L 6) DATA REVIC:WED AND 

ANALYTICAL_ PREP STORED 

SOP(.`' .-) ;# {iy Np^So3 0 

3) SAMPLE REMAINDER STORED 3-2S-7,y 

SOP (s) I) , xo- 

4) SEPARATION 1-AD RECEIVED 

ìiiP i S) ,^ 

SOPS) # 

_ 

-- 

UIZu

lV 

V i 

l ` Ûlx CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 11-Mar-1998 

1Î V Page 1 

^Y • 

CUSTOMER: DHI 

SAMPLE DELIVERY GROUP (,ôaa-7.^ 

W0 

j 

MATRIX OTHER V -W/ HATCH NUMBER 03 

1 ) 

2 ) 

3 ) 

CUS 1'OMER 

OES ID DUP ACCOUNT ID COMMENTS 

5 A, M*L 

CS r^ 

80318402 E SJA628I BOP4's 3 0.00 0355 

Pt.11 /24 / 91 81-11/24.98 

863r "^' -I3PI^ 89)1684 

ACTIONS (Initial & Date) 

1) INITIATED 

Wu- 

^^ 

a) SCP(Si # 

5) COUN T INWM-A- ,_RE', FNT . La 

EDP (5) # _-- 

2) PREP LAD °E'`lVFD 6) 0-A-A R;-:'J(1- ED AND 

- ---- ANfiLYT7CiiL FP,EP STORED 

SCF(S) ff (^ H(mac SO 3^ 

Off,(• - 

3) L E R E l , tA'_NDER S--0RE0 3.26siP - Qws 

4) SEPAR?iTION LAC RE:_:=i`.'I) 

soli (^) 's ..rte 

iiUri 5; ii 

V ti

CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 12-Mar-1995 

Page I 

;j CUSTOMER: BHI SAMPLE DELIVERY GROUP 03 0,^ 

O 

-a^/^/^- 

MATRIX : OTHER ^ U -Ov I BATCH NUMBER 03 'a^ 

CUSTOMER 

QES ID DUP ACCOUNT ID COMMENTS 

SPrrwM 

1 ) 0a296Q! — -BFII 900160w 

2 ) 80320602 ESJAG29 

Pr.11124/9' E%.11124.98 

I BON636 0 .00083b 

3 ) 80220 699 BI IT B6P 16E3 

ACTIOj4S (Initial °. Date) 

1) INITIATED Â ^5) COUNTING/PIEASUREPIENT LAD _ 

nnj^ 

SOP (S) it /\j—) SOPS) # 

2) PREP LAD RECEIVED 3-11^_ rl k a,< 6) DATA REVIEWED AND 

ANALYTiCP,I. PREP STORED 

SOP (S) 9t ?JSagC5o 'S--o 

3) SAMPLE REMAINDER STORC{D -3 (,AP' °C 

4) SEPARATION; LAO PECEIP -D 

SO(' i S) It ... 4.. 

SOP (8) !1 

SOP(S) # 

Gl^î

l)^- 

G 

U 

CUSTOMER: BHI 


Page 1 

SAMPLE DELIVERY GROUP 

^( 

MATRIX OTHER (^' BATCH NUMBER 03 o 

CUSTOMER 


S ^ Aug 

1 80322201 

3 •^ 

2 ) 80322202 I BON689 0.000GS5 

------------- --------- ------------ ----- - -- ------------- -- 

ACTIONS (Initial `z Date) 

^^.)l/ 

1) INITIATED zo V1 ;51g9 5) C'UNTINC/MEA5UREi •1ENT LA3 

SOP(S) # SDP(S) # 

2) PREP LAB RECEIVED 3-L9- '^t 1' orc 6) DATA REVIEWED AND 

ANALYTICAL PREP STORED 

SOf (s) ;ir^ttg:cam 

SOP( 

3) SAMPLE REMAINDER STORED 3-_zb-Q Fos 

4) SEPARATION 1- A0 RECEIVED 

SOP(s) 4 J^ 

SOP(S? It 

)n 

6121

I ) ° 1 . 

^1 -,CIlO 

USTOMER: BHI 

MATR D: : OTHER 

- AMFL.E CELIVER' : .-R - 1 -11' 

B A T:H NUM'-R 

93 

CUSTOMF_R 

OES ID OUP ACCOUNT ID COMMEN-"5 

Sl:- A JJ,4^ 

1 ) 80327201 D ' , - I 00116 172 C.000(o ^- 7 

3 4 SQQQ' " a4 •arc n 01.i(-aa 

-------- 

irtitiaL '< Dc'.:e 

P, g L 

1INITIATED Jo 

"' S) C .^.ÎNTi": /;1-ASURE"iF_NT -`.3 — 

EOP (5) # ^SOf (S `'. 

2) FR=P LAB RECEIVED 1)-TA REVD: *WED AND 

ANALYT'CiAl- PREP STORED 

3) S-,ÎPL.E R7- )T r•d nF--F c-I it L- 

4) -cr ARri 1. i^fJ i_."' LV:_LJ 

L6'^t W^ 

b0P(E` # 

- 

61;;0

G, o, aanterra 

S^ 


ANALYSISA--z-yr mmix dMINF-L DUE DATE -b- ct8 

S w RRy 

_ WORICORDER SEQUENM0 CLIENT coheAwn 

J cJ-sI Fr 9 -IB QC BATCH REAG'FNT WAka 

J N 14 ix QCBATCHMATRi 3-e& 

I O 31&4 -IMot© 

(ank) 

j -2M or 2S 

D O3 Zoe 

(aide) 

_off 

QCBATCHMATRIX/R C NT 

SPUM 

^S 0:s t^401 03 zsR 

^b -5 16102 1'4 

$03 zo6ol b3 2 S^ 

^t7322201 -^' 1" 

Ô TJ 2'-1`l 01 bZ 

$03 2 r ? bz 

03 

Batched and QC updated by ^ on 5-is -'JY 

Rec'd in Prep Lab by -.p a on 3-t5 4 

Rec'd in Sep Lab by > on-]? 

Rec'd in Sep lab on 

ED/^PP^y ^^ on Y- 3 -^^ S 

^/ J 

QC BATCH MATRDMMACENT SPHO 

Duplicate of L ple #_3T3 zo 603 

Sop# 1Z^cs1QCSr) Re47_ 

n, 

Sop# ^1C^^C S^ Rn'^ 

Rev3 

Sopy fZ i C N TIC JO^2 Retii 

Rec'd in C.R. by on Sop# Red 

Data Reviewed by on Sop# 

L2Rna 

^7y 

Original batch shee and complete calculation file lobe Wed with the FIRST fisted work order number- 

FORM NO.: RC-52,1/98, Rev. 8 

IZ^ utj.T-s S PF 5^ ^^ 3/ÛG^ C^ 

CT Tw nE = too Mw ^^G^ ^l _ p i /. 

5'c__ 

-^.r 

- ,; J 

CT 1.rJS i = {^S Q^L 

- 

C^^ 

l 

^_ ys 

`-

_ __ - 

. 

sA A.nK 

_ Sq 

Sb3184i6 ESJA 6 13 -___- 

___ 3o3 or LiL% IQ0188 1 

ES JA614 

Pr.11/24/97 81.11/24.98 _- -- 

5.LS 

ESJA615 O.ou — 

Pr.11/24/97 11.11/24.98 

3'l9-zs DvL 

(Z- mac. t"Z c So .3-0 

3-25rih" oar 

N 

6134

^^" ^^ ^^^ 

_. = i _. - ^ ___^ 1G-I°lar1`19:3 

ESJA616 

Pr.11/24/97 EX. 11/24.98 

' 0 

w 

S A, A.Ae- 

rs 

Gl 33

_ ^'^ ^'^ -GC S I D3- - 

------- ------ - 

ESJA617 

__._ Pr.11124/91'5,11/24.98 

SPF A^^ 

ESJA618 0•ozys -- 

ESJA61 

Oo3Zo6o3 Pr 1112419'x•11124.98 

k;x 

-S-2 5 -E.Y V^- 

Y+ 

o•OZVS 

-- 

61"4

- - - _ 

PA 

ESJA620 

Q ^ 

Pr. 11 124191II .11/24-98 

^J( 

3.x54(' 

Sri ^ 

^QZSS 

3-1911fi- out = 

IZ ^Lh+RCSJ(Sb -- - 

r 

Odt------ - . 

y 

G1^^

^ Lk c^ 

U7^-ao j 

ESJA621 

Pr,11/24/91 88.11/24.98 

ESJA632 

Pr.11124197 81.11/24.98 

On 1, 

3— L'( —kt ouc, 

R ^ N-2c So ^3^ 

3-251'i_Y p^^ 

G1-J6

cl 

sp^ "A4- 

ESJA623 O.C)?-Lk-7 

Pr. 11/24/97 91.11124.98 

ESJA624 0 - P- Z-14 

Pr.11/24/97 81 .11/24.9 8 

jo 

2 5 --cL 

G I I-)

C%ivanterra 

Emimnmlmd 

Senxu 


ANALYSIS Peso MATRIX o ihF--e- DUE DATE q-C `t8 

s^^ RRy 

WORK ORDER SEQUENCE CLIENT COMMENTS 

J oil Sr y -1B 

bbl 

QC BATCH REAGENT BLANK 

1 f-i (4 -1X QC BATCH MATRIX BLANK 

J t m l" -IM oQ 

(Ckk) 

J lq -2M or 2S 

(cycle) 

D 0 3 Z.ob ' 03 

QC BATCH MATRDUREAGENT 

SPIKE 

So^1^401 03 zs A, 

^b3l6toz 

a la 

$ p 3 z.obol 03 5 4 

ÎJTa?-Z2ol 

N la 

Fr 0 ,6 02 

$03?rl?4b'z- 

03 

Batched and QC updated by w - on 3- 2. s-4X 

Rec'd in Prep Lab by :]^ aL on-3 t°r 4d 

Rec'd in Sep Lab by---O on ^' ) 

Rec'd in Sep lab by on 

(E^/CPPT by Its on 3 C g 

QC BATCH MATRM REAGENT SPIKE 

Duplicate of Sample # %' 03 7. 06o3 

S 0134 RICS-1QCSOV3 Rev#_ 

Sop#.0 ^r,^ ^'S 7 

Sop# 

Rev# 

^/ 3/ ^t ( Rev# 

Sop# _ !C ( (^ U 3 1 Rev# 

Recd in C.R. by on^'^/9^ Sop#a1 C1711eDL,)X 9 Rev# J 

Da ta Reviewed by on I I T Soo_ ^'C 2p-2— Rev# 

Original batch sheet and omplete calculation fi le to be filed with the FIRST fisted work order number. 

FORM NO.: RC-52,1/98, Rev. 8 

Rf ^ urn= ê_^(5r« 

Lr T^ V-+^ = 2.00 

C- T- =n 5T = 

f-- L 

G I J 8

- 

3b3 fr`11B ESJA613 

_ 3oswAIS I2HI225 1 

ESJA614 p.pZio 

Pr.11/24191 91.11/24.90 

-Doc 

"-° - 

ESJA615 - _ -- -- 

Pr.11124191 6%.:1124.90 

3-1q 1t F ova 

^ \-ce+acSo%3-'Z:5 

3•zs 1t^ o t 

r^ 

p.ozi9 

G1i9

v't_J 

ESJA616 

___Pcll/24/918%.11/24.98 

25 -`L 

5R- RNAL 

Ìrjr-19' , U 

C1•t0

f308 -CIO 

-- - - ESJA617 - -- -p.OZd'1 

Pr. 11/24/97 81.11/24.98 

.--- 

_ - .5 zs ax 

ESJA618 

Pr.11/24197 81.11/24,98 

-- - ESJA619 

D032o603 Pr.11/24/97 81.11124.98 

3 lg 'Uv- 

c^^ ^H2cSOCs ô 

3^ZS-42r o^ 

N^ 

0 •oZ`1S 

- ----- 

U14.i

SISSî -SS^^-- 

-- ESJA620 

Pt,11/24/91 U.11/24.98 

h I) S 

R ^c uri c so ^S -o 

J-zS ìFs^ 

O.O ZSS 

Ll^^

-- - 

_ ESJA621 O.OZ3`F 

Pr.11/24/91 Br nne as 

- -------- -. ESJA622 

Pr.11/24/91 IX.11/24.98 

R^ceF2c5a,3-^ 

3-2-5-tir o„ cl 

N 

Y ^

Olb / 

3 -Zs 'Y 

ESJA623 - -- 

Pr.11124197 3%.11/24.98 

ESJA624 

Pr.11124 191 31.11/24.98 

R^^2cso^3^ 

3-25-ì e- out 

5H- Avtm 

Q' OZ^ 1 

x_02 zV 

6l ti

N.rmanterm 

se.^ 


ANALYSIS Pu00 MATRIX 0 TtW±j DUE DATE y-6-cLk 

tip"( CS m wr 

WORK CRDER SEQUA a # amir COmmem 

J o 5 l b l -1B QC BATCH REA(EN M ANK 

J N 1n. -ix QCBATCHMAMUSAW 

J o 3 L 61 -imam 

(dale) 

J N 2M or 2S 

(drde) 

D o3ibt -Qt 

p^Tj 16101 ^' 1" 

go3 t8`{o2 

8o3 Zob oZ 

p3 22.Z02 

$03 Z'7 L0^ 

Batched and QC updated by-î ec on 3 Z5-% 

3• 

QC BATCH MATRDOMAGENT 

SPIIKE 

QC 13ATCH MA2RDORFAGENT SPM 

Duplicate of Sample # $A 3 -IN lb 

Rec'din Prep Lab by ^ on 3_ 19_4 Sop#RtCt Q-So13 Re,4 0 

? C 

Recd in Sep Lab by on 76 Sop# L' ^' C c yCJ 

7 !^ÎZ ^7 =e 

/,'C S7v 

Recd in Sep lab by on Sop# Rn: 

PPTby 

v 

on-3 Sop# Zict^ t• 39 Rn= 1 

Recd in C.R by on 31 3>1 14 Sop# r hi poa7 r R ^^ 

jptq-1- i--K 

Data Reviewed by on 11' Sop#__ SC yam- JL,î J 

L 

O riginal batch sheet complete calculation file to be filed with the FIRST Lsted work order number. 

FORM NO.: RC-52, M8, Rev. 8 

2^ w = e a-Z I SA 

Gr S.v9 7 = i`kect 

— { — 

StH ^QAC ^, v.. ,S o^DRy cew.e...Tj ô .— to Tel S-`/^^.^ 

6145

I 

^3^^^ 

CHAIN-OF-CUSTODY B4TC1-i ANAL`(`.ilS RECORD 10-Mar-1998 

D9Page 1 

CUSTOMER: BHI E;At1P!_E DELIVEPY GROUP 

MATRIX : OTHER ^ ^ BATCH NUMBER O^'Jbl 

CUSTOMER 


.5,4 AuAI 

( ^s" 

__====3b3i6^=a ESJA625 _______-______-----= 

So3i6l Ls14HI326 l 

1 ) 80316101ESJA626 I BON6(30 p-0Ob36 

ouStsio( ESJA627 

2 ) F^p Pr.11/24/91 EI.11/24.98 

3 •u 

------------- ------ - ------------- -- 


1) INITIATED^ 5) COUNTING/MEASUREMENT LAD _ 

SOP(S) # _ SOP(S) # — 

2) PREP LAB RECEIVED 3 -09 4Y WI, 6) DATA REVIEWED AND 

ANALYTICAL. PREP STORED 

SOP(S) # îcc+-¢cSO^b=o 

SOPS) # 

-3) SAMPLE REMAINDER STORED 3 -zc^r pn 

4) SEPARATION LAD RECEIVED 

90 p ( 01) f ^'^ 

S u p (F) 3 

0146

)CUSTOMER- BHI 

MATRIX : OTPER 

OES TD 

PUI;,O# 

CHf;IN-OF-C'_! STODY SWCH ANALYSIS RECI ]RD 11-Mar-1998 

^ 

q 


ID[ BATCH NUMBER 

CUSTOMER 

DUP ACCOUNT ID 

S h Awe 

1 ) BB8iB4i1 8i-ITrÔC BA^!E}-:^ 

^ .L 6 4Y 

2 ) 80318402 ESJA628 I 1301,4 683 0.0003155 

Pr.11/24/9 1 91.11/24.98 

3 ) 8A8184HS 43itI3 ,-, --"-'3d 

JJ^^^^//'^^ 

4it^ ^?S 

Page 1 

OL^Ts7F— 

COMMENTS 

RC TIONS (Initial !, Date) 

Q 

1) INITIATED ^^^ 5? c; UNTI'i^/MEASURE:`?ENT LAD 

SOPS) # SOP (S) # 

2) FREP LAB RE(,E T_ V F.) T S- k9 Y orL_- 

SUP (`:) , ._ R^trf^4So ^3 o 

3) 5=MPLE REi4Fl 17 ii'^:!* ST,-RF_O 3!Lb•^Y^ 4 

4) SEPARATION t.:=,C RF.0=IV.0 

,'tNALYTIC:'I_ PRE? STORED 

SOPS) # 

Ciî

0 /qg 

CUSTOMER: BHI 

MATRIX : OTHER 

1 ) 

QES ID 

*41 PUISO 4-" 


Page 1 

^/^ SAMPLE DELIVERY GROUP 

1319-v" ) BATCH NUMBER 

booms 

03 -xi.10 

CUSTOMER 

DUP ACCOUNT ID COMMENTS 

SA- AWAi 

------------------------ 

3-Lb 

2 ) E303206O2 ESJA629 I BON6360.0O0£eb6 

Pr.11/24191 8.11124.98 

3 ) "QO32 B er6 5 514 r-^nTeaa^ 

3,Zy 

------ ---------------------------------- 

A(^ TIGHS (Initial Datc) 

1) INITIATED 

l 

1^l^D à) COUNTINO/MEASUREMENT LAB 

SOPS) 4k '/U1/V S7i'(S? m 

2) PREP LAB RECE' !)ED 75-t- p yvc 6) DATA P.EVI.vJEE AND 

ANALYTICAL_ PREP STORED 

3) SAI•iPLE REiMAIitD'i--F ST'JR' r) S,Z6-9S 

4) SEFARATION LAP RECEP.: L` 

SOP (3) # 

6:.40-

(^ ^Q 

*#* PUISO*# 


Page I 

CUSTOMER: BHI 


MATRIX 

Q /p 

OTHER Koo 

/ BATCH NUMBER 03'(29,;? 

1 ) s2ee 

CUSTOMER 

GES ID DUP ACCOUNT ID COMMENTS 

SR A+A,l 

3-x6 ,W 

2 ) 80322202 I BON6E90.00o655 

- -- ------- ------------------- - ----- ---------------- -- 

ACTIONS (Initial '< Date) 

3 

1) INITIATED "1^^ 5? t:'UPITINr/M,=AStRci iENT - 8 __ 

SOPS) if SOPS' it - 

2) PREP LAB RECEIVED _3- (gkY o^ h) DATA REVIEWED AND 

ANALYTICAL ?REP STORED 

90F(S) is _1Z cH?cS^^3a 

SOPS; # 

3) SAMPLE REMAINDER STORFD 3 -26 -2 P c-t^ 

4) SEPARAT I ON _1;B PFi;= :`Jta; 

9 0P(S) it Â 

SOP (3) ;i 

6149

^ CHAIN- O=-CUST77-`'( B?TCI- ANAL''P'iS RECORD 17-Mar-1995 

i l 

Page 1 

CUSTOMER: BHI SAMPLE DELIVERY GROUP 

/I)/^ ^f 

W(/^/ 

MATRIX OTHER kJ `s - Ob / BATCH NUMBER Oc/ -az l OS 

CVSTOm 

GES ID DUP ACCOUNT ID 

5A. ANA-, 

COMMENTS 

(D rr> 

1 ) 60327201 J " I BON692 0 •ooa^ 7 

2 ) 80'12720 2 BI iI 3 uAYBON69a 

3 )^B09272 39 BH; °"` 80W.694 

'ur 

6'4 

3•zc 

------ ------------------------------- 

ACTiO 0IS (Initial & Date) 

1) INITIATEDO 5) C UN-I".=%i9EASURE''EMT Lr;3 

SOPS) # __.J>!^ SOP(-) # 

2) PREP LAB RECEIVED 3-( 9t -iY - 71^^ . 

SOPSS) i) ^tc^+ac5y3 ^ 

3) SAMPLE REi"RI !')EP °.TOR-n 

4) SEPARATION L.-' 

:;C AP i ::^) nJ ^ 

r_ rc":; ) 

f,) 0,T„ REV r -_JED nMD 

Ai'iALY-iCAI- PREP STORED 

50f iS) # 

Gl;,o

RPj 

R 1'. ,'uanterra 

s^ 

BATCH SUMMARYICHAIN OF CUSTODY 

ANALYSIS o-o MATRIX 0M %V*, DUE DATE 4A-b-aS 

S t-v RRy 

WORK ORDER SEQUMgCE 0 C[ma COMMe (g 

J-:3-S1&`4 4B3 

O ^l I 

QCBATCHREAGe rffiAW 

J N 14 -I% QC BATCH MATRM SAM 

1 031Fsy -1M ot© 

(dide) 

QC BATCHMATRUVRFACENr 

SPIIM 

J 2M or 2S QC BATCH MATRDORFAGENr win 

D O 32'1 z.. 

Z Duplicate of Sample# $032'^ Zo z 

80 TS 1t4o1 03 zsR 

Fo3lbloZ 

a la 

$03 zo601 03 2 SA 

^032Z201 

.^ la 

Fr0b z yy ol oZ 

^03 Z'12bZ 

03 

Batched and QC updated by -DVc on 5-is-qY 

Recd in Prep Lab bY- oc- on 3 -ter 4d 

Sop#- '-uC C -U 

Rev# Q_ 

Rec'd in Sep Lab by ^ .^ one^ - 36 SF Sop# &i &kf ,S 6 3 6 R--v# C` 

Recd in Sep lab by 

/CPPT by 

pp 

on 

^ 

Sop# 

Sop# 

Rev# 

i 3) Rev# 

Rec'd in C.R. by f j ' a0 an Vw ^t Sop# a0»> r Rev# o 

^n 

Data Reviewed by i^ on' (^ GI gyp# 

O ri ginal batch sheet an complete calculation file to be filed with the FIRST fisted work order number. 

FORM NO.: RC-52,1/98, Rev. 8 S^ 

t ^x^ra c ^^ 2 ti c-Ait1C û3 

= po- L /S ic^ 

LT S tV 5T = At5 PEC- 

0151

_ 

S A-AuA-L 

_-_-__ESI27495 -- 

X31 y` 

` -- 

s_o y9 

EQIE316 

\ 

---__ So3 y _os 

^fr`1_ 0.03^34ode, 

lS .._... . _..,..,, fs a 1 -__ _ _-----_----- 5.ov^ 

— 

ESI27496Ci•ozv3 

_ ,. _ 

Pr. 73113/97 8x.:'_!13/9A 5.0 op 8 

s ss•t 

- ESI27497 6.0?z6 5 ^-7 1 ^ — 

P [.1?! 13 / 91 3x,'.2!' 3'9B 

2^c \+ec5^ \3 ^ 

r ^- 

_ 

- 

_- 

G15

ESI27498 

9r.12/13197 31.12 /13/9 2 

r^ 

e+C 

'-QUO 1 

-vU •. JF;^ ^^ lrC _—__ 

5 A An Al 

SPe 

S-061-7 

- 

FE 

c153

AN+_'.,1 PECCPD—filar-194(3 

5 P, P ~ AIL 

ESI27499 -- — o.ozS7 

Pr,"/:: /97 ?a./:3133 

S-ZA4r 

ESI27500 - -- — - 

_ O .o^4Z 

l9 -4k 

V^^c rFecSo i3-o 

3-L6 ALP 

61-34

^1 v F7- 1 ,f - 

^cl C^ 

5{f A.AI 

ESI27501 O•oab l - 

Pr.12/ 11 '3,1 

--- --- - 

1 3a:12/13/98 

.. 

S- 0 5 9 So 

OdC- 

- - - - - - - - --- 

•xL'E1' 

nl^^ 

- - - 3-Zl-q-a' 

{ZlCµ2CSo^3^ ---- -- - 

tiw 

C 15

- _ ESI27502 0.0ZS1 

Pr,12/13/97 Ba,12!13/93 

ES I27503 G 

Pr.;J'3/97 s"a 12/13/?8 

3 -4t c^^ 

`tZ is t+^CCSa rS-o 

_ —_ _ 3-^b 2k art 

N ^' 

S o(o 17 

s 91 ^^ 

-. 

_..---- - 

6156

---------- ESI27504 

..___L7o32'r ZO2 ESI27505 

_ 

ESI27506 

1-2b-4Y o« 

^v 

$ k "At 

------ --- — 

p.oz a6


4 0 A A31s ut y0 MATPJX on-WA DUE DATE 9-6-9 

T5R`( Cam WT- 

_ F9 )P% CstDER 

1 Va __._ _ _- — 

l0 3 t 6 t -1M oQ 

SEQUFNM# QgNf COMMENTS 

-1B QC BATH REAGENT BLANK 

-IX QC BATCHMATRIX BLANK 

(arcle) 

I -2M or 2S 

(ar de) 

Do3tbt -fit 

^S17 -516 1 01 "' t ° 

gu3 1$`ôZ 

8o3 Zob oz- 

-6 2ZZOz 

$03 Z'TZO\ 

Batched and QC updated by^cz_ on 3 -25-alr/ 

Rec'd in Prep Lab by on 

Rec'd in Sep Lab by 

74 


3- 

_ onoa -a C -9 F 

Re 

(EL)/CPPT by /b on q /3'q g 

QC BATCH MATRDUREAGFNP 

SPDM 

QC BATCH MATRUMA(ENI SPUM 

Duplicate ofsample #X03 t b t o l 

Sop#RK-t''RCSot^ ReO Q 

Sop^ÎC,.^P[' .sago R^?Q 

sops >2i CL-ec 57 3q Rcn'- 

Rec'd in C.R by on Sops Rte= 

Data Reviewed by / ' ^C^ ' p ^^ 

Cl k y Sops -1 L I ^^ C E ^c Z R- 

Original batch sheet and mplm ration file to be filed with the FIRST' rioted work order number. 

FORM NO.: RC-52. 1/98. Rev. 8 1 ^— Qxtr 2^- ., ,^ 

i 

4 z w 5 R,CNQ^_ °3•. 

5ET fRA^-no.J iS OF PRy ^c.w,a-..^^ nôT 0^" l^rn{ SR.5-L6-`LS^ 

C^T^-J i2a D.ru.o c0`3"- - 

R.PT llwtn = FCi-`spt CTTtw.Ec200 = IBS L G158


Page 1 


MATRIX OTHER 

N-1611 

BATCH NUMBER (/' 

CUSTOMER 


SA-AuAL 

SI 7507 

^3 \61^^ ` ._ 

_______=_______-___________________________ 

i S.oS fG 

503161LS EQIE317 ^S_p3S'o•^26797 l 1 .5.03^"J. 

1 ) 80316101 ESI27508 Pr.1211?191 37.1211i/9P 

I BON680 C^-oOV376 

S_ 0 S ]lp 

2 RWI 89N68} 

ESI27509 

_____ O03t6101_?r..2113/97_°1.:2i'.'.r 19_____________ 


1) INITIATED III 5) COUNTING/MEASUREMENT LAB 

SOPS) # SOP (s) # 

2) PREP LAB RECEIVED 3 _l q a k oc r- 6) DATA REVIEWED AND 


SOPS) #6 ^^t42LSo^3^ 

SOP (9) # 

3) SAMPLE REMAINDER STORED 

]UI ' 1 ^J ) iI N 

4) SEPARATION LAD RECEIY[-D 

^)O('iS? tt 

6150

^CUSTOMER: 

CHAIN-DP-CUSTODY BATCH ANALYSTS RECORD 11-Mar-1998 

Page 1 

BHI^^// 

SAMPLE DELIVERY GROUP Ôa375 

MATRIX : OTHER 8q S-aj I BATCH NUMBER 

CUSTOMER 


SA- A+.JkIL- 

-------------- ------- -- ----------====^sr^^===___-----------------____ 

1 ) A01 8401SHI -- bo'^ 

2 ) 80316402 ESI27510 I BON603 0 -000 -6-70 

3 ) 

Pr,1211 3 '7 7 38.11!11/P2, 

3 ;4tY 

S_ 05 7(p 

---- - - ------ ----- - ------------------------ 

ACTIONS (Initial '< Date) 

1) LNITIATED 

SOPS) #t 

3^î I 

Ô 

io— Y l 

5) (;DtJNTIN>;'i1EAStJREPii_NT LaB 

COPS) # 

2) PREP LAB RECEIVED h) DATA RE4'I`. WED AND 

AtdAL'f 1 lC A(_ PREP STORED 

SOP (S) is 50k3--p 

so? (5) # 

3) SAMPLE REMAINDER STOR-D 3.2k_ -q^tPlk, 

SOP (3) ii 

4) SEPARATION LAB RECEIVED 

FjOF' (3 ) ;i 

ît;lJ

CUSTOMER BHI 

MATRIX OTHER eq -G(; J 

CHAIN—OF—CUSTODY BATCH ANALYSIS RECORD 12—Mar-1998 

Page 1 

SAMPLE DELIVERY GROUP -75 

QES ID CUP ACCOUNT 

1 ) sum 

2 ) S0330602 ES I27511 I BON-5,96 0 -000 1r 'S9 

raft 

BATCH NUMBER O3 ^ T^ r 

CUSTOMER 

ID COMMENTS 

so, ai m- 

====== 

61- 71-01-45 (init=_a1 & Cate) -------- — 

1) INITIATEC ^_^^^[^^ S) CCUNTI'dG%P! cA UREÌEiiT L:1L+ 

SOP(S) ii ^l/^ScP(5; 

2) PREP LAD RECEI`.'ED, 6) PATH REVI:..iE_, AND 

3) SAMIPLE iENl ii!DFR STORCn 

ìOP(^ ) 4S I\ - 

4) SEPARATION L A'_1 REi- El')' L) 

u-,P(°! 

G161

^ 3 CH A IN-OF-C'.JST^=^DY BATCH AN ALYSIS RECORD 13-i1ar-199 8 

' `^ 

Page 1 

` CUSTOMER: BHI 

SAMPLE DELIVERY GROUP ^-Z5 

MATR I X : OTHER 

QQ ^n 

l u w BATCH NUMBER 

1 ) 

CUSTOMER 

DES ID DUP ACCOUNT ED COMMENTS 

32,i,R^' 

2 ) 803?2202 ESI27512 I BQi•46og 0•0006(-2 

v., 2i?' :1. 121 :3/ca 

S,o3â 

— ---- — —ACTiDidB (Inii;iai '< Date) ------------ — 

1) INITIATED h"_/ 5? C UNTi' ;MEAS)REi1ENT LAB 

SOP(S) g 11^^ ^SGT ;Si k 

2) PREP LAB RECEIVED 7 _' 1'1-1Y_16) UAia 'EviF:' E7 FiN_ 

Ai.IN^'r'T; ÂL °JE? STCRD __..__._ 

3) SAMPLE REMr^ T.N i )ER STORCO 

4) SEPARA T: I,;N !. RCEI ij_i) 

SOPS) #A —^'- 

5CJl(cl. ^ 

50F'iSi sk ___ 

G16C.

II 

CHr+I N -OF-C':JSTODY BaT(;H AN-CYSTS RECORD 17-Mar-199£; 

Pa a 1 

CUSTOMER: BHI SAMPLE DELIVERY GROUP W 0020 

MATRIX OTHER( v" I BATCH NUMBER Da ^^ 

CUSTOMER 


SA• PNni 

1 ) 80327201 ESI27513 I SON692 0-00066 

2 ) 

3 Roaa7292 Bill--SON", ^4 

-- - -- 

/r 

03 i 

ACTIONS (Initial & Date) -- --------- - 

1) I NITIATED ^ ^. :' _ „'i1 --- 

SOP(S) # 4 -- 

2) PREP LAB P,ECEIYED 3:x`1 F h) OAT= PEYI WED AND 

ANALY 7 ICA1_ PREP STORED 

SOP (S) R Ott 2C 13^ 

SOP (S) # 

3) SAMPLE PENAINDEFR S?OR D __Zb_^LY OTC 

4) SEPAR I) TION LAP, RECF-:IVF-0 

GOYO i; ^ 

i70P (t ) i! 

ciss

uanflerra 

J o3I bt 

S riaa 


AC ALYSIS MATRIX OTrWA DUE DATE y-6-9-- 

-r!,2Y CS=m Ekm 

WORK OMM SEQUE NCE # CUENr COM1mm 

QCBATCHREAGENTHIAMC 

Afl, IX 

EAC3- 26 -4 1 

J N %x -1X QCBATCHMAIRIXEILM 

1 o b t 61 -1M oQ 

(fie) 

on 

I} 

QCBATCHMATRDURFAGWr 

2IM 844 C-oo 1 

J N tA. -2M or2S QC BATCH MATRDURF GWr SPUM 

Do3tbt _Ot 

DSO -St6lo1 "' 1 a 

gv3 L$ào2 

803 Zo(o pZ 

03 2-2.?-Oz 

$O3 z-7Z.0 \ 

Batched and QC updated by- - ^Dvt on 3 -Z5-ul 

Rec'd in Prep Lab by -err— on 3 -w 

Rec'd in Sep Lab 

Dapii eate of Sample #g0 3 t 61 01 

R tC+eCs0t-7 1 

W-' R tc-t 5() Rn'--^_ 

Rec'd in Sep lab on Sop# Rey; 

ED/CPPT by on Sop# Rn: 

Rec'd in C.R- by / oa 3 2G Q Sop# 

Data Reviewed by 

Rev-,- 

RIC /f 7 Reo O 

n 

r/ Sop#_f'(ZC Low) ^ ^ 

C- 

O riginal batch sheet and mplete calculation fi le to be filed with the FIRST rived work order number. 

FORM NO.: RC-52- IM, Rev. 8 C 00 nT -r k yr E = 4500jo u n., =m S:r= C ^ 2 

JP, ^ tarn trs = ^CC / SA G-Lc Z5 

CR'1 

SR k pRy ^^ ^..- X02 ^, „o- ^^ s^ 

G1G^


Page 1 

Li CUSTOMER: BHI SAMPLE DELIVERY GROUP 

MATRIX OTHER BATCH NUMBER 

QES ID 

06% Ix 

1 ) 80316101 

2 ) 

ACCTIONS (Initial & Data) 

1) INITIATED p^'I ' l 5) COUNTING/MEASUREMENT LAD 

SOP(s) 0 IJ SOP(3) # 

2) PREP LAD RECEIVED 6) DATA REVIEWED AND 

RK rrR^SO^?'1 ANALYTICAL PREP STORED 

SOP(s) # R \cHtccSo 13-0 

SOP (S) # 

3) SAMPLE REMAINDER STORED 3- 2-S-4Y o.^, 

SOP(s) if r 


L 

DUP ACCOUNT 

CUSTOMER 

ID COMMENTS 

SA oncE..+,y' (S i}) 

iw ====o..ems====e—=itai==o------s^^==o^ 

K FahE O rMr+h 

SOP( cl ) 4 

CO r\r Tiw f- _ 5 ) , I e-O =ZS) PC, /S^ 

1030 

NfG cool 0-1 w.*. 91 %L" LSt (^N L6/y1fjP Q^^91D 

BHI BON680 o4vruMtYY 103,0 C,z355 /-G zeoe "e 

G. 16

Q^^- q' ^ 

CUSTOMER: BHI 


1 ) 

OES ID 

CHAIN-OF-CUSTODY BAT -, F l ANALYSIS RECORD 11-Mar-1998 

Page 1 

^ 

j 


II BATCH NUMBER Vt/ 

CUS I'OMER 

DUP ACCOUNT ID Sq COMMENTS 

s A A. AA. aRTc 

2 ) 80310402 BHI B01•4683 0.2z4utomacggottSG L( ^09^1 

3 ) -86^^946aS•s5-tc OUTPn i n 

1 , 14 

i ON5 (I 1 1 i t i a l '. Date) 

1) INITIATED _^/ 0 5) C7UNTIN,/MEASUREMENT LAB 

SOP (5) # Xa E A SOPS) # 

2) PREP LAD RECEIVED 3_IQ--4-K off_ 6) DATA REVIEWED AND 


SOPS) R __R>^+44 0 -^ 

3) SAMPLE REMAINDER STORE;U 3_25-4Y oaf 

SOP ( S ) SI 

4) SEPARriTIOfd LAB RE;; ['':) -- 

(,OVv7T T/ 01 e = 5U) 

b, eo = 2s ) P G^S^ 

SOi'(^) # 

6166

I J 

CHAIN-OF-CUSTOD`' BAI --,- ANAL' . ' 'l i S RECORD 12-Mar-1998 

Page 1 

/ CUSTOMER: BHI Elid'IPI_E :DELIVE` : Y GROUP 

MATRIX : OTHER p'(i(1 BATCH NUMBER d3-^ 

C US'r OMER 

GES ID DUP ACCOUNT ID SA 

1 ) X93=^ r_nt c 3.2.SA' NW; $HHthF3^ 

sR 

COMMENTS 

2 ) 80320602 BHI BON6061 (M' X 1wo o•'k 107 G3 Z6rh,^R9 g I /03 

3 ) 89829 92 yHf E) E) 

ACT! DO , ' ( Initial & 0.3t2) 

J 7' 

1) INITIATED ^^((^^ / ^Û 5) COUNTINOiMEASUREMENT LAD _ 

SOP(S) 4 _ND S^F'(5) # 

2) PREP LAB RECEIVED 3_L^_Q o_rL_ 6) DATA REVI WED AND 

2^rtac So Z-I ANALYTICAL PREP STORED 

SOP (S) # _ i^kr^?CSo^3 0 

SOP(°„ # 

3) SAMPLE REP1ATMrEP STDPI-') ^^zs 4t__os^ 

4) SEPARATION LAD RECL-l ki: D 

c16

CHAIN-OF-CUSTODY B%T." ANAL'ii S RECORD 13-Mar-1998 

Page 1 

/ ^^^ 

I V t CUSTOMER BHI SAMPLE OELIVEFiV GROUP L(J( 

27s- 

MATRIX : OTHER BATCH NUMBER 03 d^ 

OES ID DUP ACCOUNT 

CUSTOMER 

ID 

SA- 

i ) '^922e^^.=`^'}ê^s•z $fIF $9HiS8B 

s P. rw^C 

2 ) 80322202 BHI BON689t2'^"* l3`S O.vzco 


COMMENTS 

1) INITIATED `// "/^ Gl 5) C,OUNTIN9/MEASL'REt1ENT LAB 

SOPS) # IJ 117v^ SOPS) ;! 

2) PREP LAD RECEIVED _

AUSTOMER 

MATRIX 

BHI 

rAi".'A -x :^ 

CHAIN-OF-CL B,4TC1' ANAL' `.aIS RECORD 17-Mar-1998 

OTHER j-/ &W 

SAMPLE:'JELIVER`/ GROUP 

BATCH NUMBER 

Page I 

D^^ S 

o ^5-;rZa 

CUSTOMER 


SA SR- n^n^ 

---------------------------------------- ^^ _____ `SIN- ) 

1 ) 803E720t CHi EOi964211oh'+HR. o83a O.4oyS(^ ^ 

G ) 

3 ) —eose-7,R 

oar - Z -c 

HT 1391v69q 

1) INITIATED - 1 -' F 'NT LAG 

2) PREP L.rQ "c: is iE T'dED 3 -49 AY - 9v5 h) OATA RE`.-'IF:'AED AN'_) 

F2.c rt 2a5o 1-7-1 AN-?LY-iC at_ = RE= ST )R=D 

3) =, 7 NFI_E i;Eit.f Ir;:,. .r S' I?+.) _3 -25 Y 

/ 

Co^^^ ^rrc r = soy G^^ - zs c, ^^ C,^ se 

2,/4141P9^ 

^_ 

6161

^!s'aanf-errs 

F nimnn 

S nim 

BATCH SUMMARYICHAIN OF CUSTODY 

AtIALYSIS n .' MATRIXo=_DUE DATE 

Sw RRy 

PORK ORDER SEQUENM # Q1EN7 cch owlem 

1 oil& y -IB 

6 

QC BATMREAGENrN AW 

1 N Iq -IX QC BATCBMATRIXB[Aw 

1 031&H , -1moom 

( cirde) 

1 t4 -2M or 2S 

(drdc) 

QC BATCBMATRDUREAGENr 

SPUM 

QC BATCBMATRDQREAGENr SPIKE 

D 03 bolo "Ol - 

Dupli=cofSample # go3zo601 

Ff 03 I LA 01 03 Z SR 

$b31blOZ 

a la 

$Ozo6ol b3 2 s^ 

$0322201 

FfOb 2'-1ì 0\ 

$03 Zr12bZ 

la 

p'Z 

03 

Batched and QC updated by Atli` on -5-aS-4Y 

- 3• 5-4d' 

12\LC{-RCSo ^7 \ 

Rec'd in Prep Lab by a or.- on 3 -1°r 2 Sop#3 tCN --X Reo C) 

Rec'd in Sep Lab on Sop# Re+ 

Rec'd in Sep lab on Re%-J 

ED/CPPT byon Sop# R e%-J 

Rec'd in C. R. by 

on-— Sop#-KCN200 )O Z ReO^_ 

Data Reviewed by on ^/ ? lip# ^C^^12^7 Rn^^ 

O riginal batch sheet 

lT-'T^' `77-^^^ y -U^ 

complete calculation file to be tSlMed \vrth th j 

e FIRST fisted work order number. 

FORM NO.: RC-52,1/98, Rey.$ 

/ ^Q (^ 7 ( n / 

(Coo 

(T^ o = too 

c r s ,j s-F =GAR 

UUl 

G ^ i J

SA 

SR Av RL - 

Soat&4i8 - -- -: _--- 7 ---- 

25Ntk22045 1 --^j.^ 7- /77R ^ 7^0^ 

Sob1FSN15 QCAG387 o9FEBgK?zap 1 (ZL McvgY oil< 

..... - ..; lO rrN^t41f eg35 0.0537 

3-lq 

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a-asac 

- .. ^ -. wv..4R.9Y t32o --O-oSOO -___. ---- 

VKiZ^ci4AC 

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3/ 26 ^1 5f 

17MAR 4 8' /C6 

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SA- 

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ItmRCgflo83o O.oSoy GG .__z 7j^jQ-QJT^ô 

__—_DOSZobol __wp _ _ .__ _ o,os¢T 67 _27^^ R98 16^3^ 

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7Z ^c cr,;zc Sv « -I 

2 ^^rt-ttc S o t3 ^ 

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Gov^^ ^«r - ôo^ 6c^ _ g oo A-7 Pc, /sue 

IlntMCgKt3aS o.oS^l^7 yi ^bh'^ aJ O0"" 

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6173

--- —... — 

--VOL S- Lot Dw- - 

4Y 2i r.rwF Otti'r 

{Zkc tN-zc SoV3-^ — - - — 

= 3 LS-4d oat 

G C) U ,l t- ^;^ e = 600, feu = / Oo-. c, P c,/sue 

J N(. 

G17^^

ti\ ^ 

- -.. 3 - iS -`L8ij 

jute ^ So ^T -I 

R.c^+ltc Sc^3-O 

3 -25 -`-r Ddt 

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or3s^ C1 ft) - 

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l6mnagX loz5 o-oSLy - C -3 .2817ygF^1E' /^3 / 

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eo a,^ Scu - - 

3-ig-2k oR 

Ric n Q^Sp^"1 -^ 

2.c-eKCgo.3 ^ 

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ANALYSIS^ MATRIX DUE DATE 444-8 

S LV RRy 

_ WORK ORDER SEQUIIAM / CLIENT combaRm 

I v3l&y -1B 

6 H-t 

QC BATCH REAGENT MAW 

J ^1 -ix QC BATCH MATME AM 

I Oil& i -1M 

(crcle) 

J „ l4 -2M or 2S 

D 032Kg 

(drde) 

of 

^50 1 €y ol 03 zsR 

^b3 16102 

a IA. 

$03 i? 0601 b3 2 SA 

201 

Ala 

Fs03R 14'1 oZ 

^0 T.7 Z'12bZ 

O-^ 

Batched and QC updated by yt on 3-t s -Q 

QC BATCHMATRDURFAWIT 

ED/CPPT by on SOP# 15-4 

Recd inR C. by on N GfJ Sop#_f.'1^N2^ Rn3 C^ 

Da ta Reviewed by ! on 7 3-if Cnml 11^ 

9 CIFAAZ 

sY-' J q I. l y 3 ^. 

QC BATCH MATRDJRFAGeTr SPIIM 

Duplicate of Sample # %702 Lt uc t 

Recd in Prep Lab by at on 3-tit Qd Sop# -IS: ZO-- RM 0_ 

Rec'd in Sep Lab by 

Op 

7.T n 1 on Sop# i t ti R c 00 E 

RL,-4 

Rec'd in Sep lab by on Sop# ReS i 

O riginal batch sheetAnd complete calculation file to be fi led with the FIRST rested work order numb, 

FORM NO.: RC-52. 1/98, Rev, 8 

X: PrnQ- dI A PR '^. 1 3: U 

G1lt 

n

-- 

- ---'^p3lfr4ti3-ESF14249 

,. - --- 

3b318'4lS EQGF263 _ )L 0 

---- ------ 

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_- 

_ 

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N V^ 

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74. 168 o2^1^R 

^_ GG.--- 

- --- - -- — -- ---- 

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3.a5N 

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qy.q o.oî^ SC. OZA-PR9Sf 6g/s 

(Z ^Ltt(ZC SJ ^1^_ 

N 

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ESF14254 $(3 O.OLVI 6,4 622 {}1'/ l ^ ^^TS 

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silo Xdi^zO_ ^9 0 o hEc SS7bT3S3 

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2 57 ^1 ? o, uZ3a 6D OZR ^Y_pf£1s 0/ 

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ANALYSIS -7-sr MATRIX DUE DATE y-6-4.R- 

T1tN !'fenEntr 

WORKORDER SEQUENCE# MINT CODS 

1 161 -1B 

^t+1 

QC BATC HREAGEN T W A M 

J nj1A -1X QC BATCH MAMIX ff-ea 

J - 0 3161 -1M aim 

(°=IC ) 

J 2M or 2S 

(aide) 

D o3tb1 -01 

QC BATCH MATRDC/RF.AGENI' 

SPUM EQGp;(, 9 'ec-193f 1.1ti349^^ 

QC BATCH MATRM71AGENP SPUM 

Duplicate of Sample #S0 3 1 b 10 1 

x'0316 1 01 "' 1 °' _ 

gv3 l$`{02 

803 i;o^ oZ 

a3 2zZ.oz 

X03 ^'7 ZO1 

Batched and QC updated by^vt on 3 -Z5-%K 

Rec'd in Prep Lab by ^ on -3 -n -w SVOJR ^^ t* Q-S O t Red n 

Rec'd in Sep Lab by - 12on ;1 1 $^¢ , S c }L ^^'[' Rn -Z 

Recd in Sep lab by on Sop3 r " / F R^ 

ED/CPPT by 

.4 

1 on 

sopit_—L-_ R 

Recd in C.R. by / on SopdîC f^/^L^^n ^ -4 , 

Data Reviewed by a3-Y^ $opi frJ^C^" AZ- Re,'^ 

O riginal batch sh and complete calculation file to be filed with the FIRST listed work order number. 

17MM NO.: RC-51 1/98, Rev. 8 

SA fRM-na ^ ^S off' aRy C.evre.^Z^ No: of TOM1 SA Ij yJ h (•^ 

3/ 3i^4 Y 

5 R s^9 

x;18

^ vtp/ 

rx* -C)-A '--Cq *** 


Page 1 

CVSTOMER: BHI SAMP1- DELIVERY GROUP ( D f^J^^^ 

MATRIX OTHER n r BATCH NUMBER 111 

^/Ixv CUSTOMER 

GES ID DUP ACCOUNT ID 

PVT „n Sft a„^ 

COMMENTS 

]0316\^$ ESF?4_51 =__----___________------- 

G^.C, ( 

____(ofCIA 

IOAgg )/Z3 

So3lbttS EQGF264 

1 ) 80316101 ESF '_ 42,' 2 I BON680 q-).D bL 

-Do3l6\ol ESF14253 QS.! n.000366 (ip 


1) INITIATED ^^ 5) COUNTING/MEASUFEF'ENT LAD 

SOP(S) # 40 SOPS) # 

2) PREP LAB RECEIVED 6) DATA REVIEWED AND 


SOP (S) # Q^L+-2^ 50 ^^-7 

SOP (S) # 

3) SAMPLE REMAINDER STORED 3_Zb^Lt^ 

4) SEPARATION LAD RECEIVED 

SOP (S) 4 - \° 

SOP(5) 4 

G 

1 

C18J


1 Page 1 

11, 

CUSTOMER: BHI 

J SAMPLE DELIVERY GROUP 


^^(( 

U-^t BATCH NUMBER O j 

1 ) 

CUSTOMER 


P P'r w'f- s R ^ 

S•u 

2 ) 80318402ESF142^4 II BON633 G^.^ o -oou3V9 (.¢ 1,410R4^1 /lli 

3 

iq 

AC 

3u^ 

IONS ( 1:111: a1 0: T)-1 

------ --- 

T 

1) INITIATED 5) COUNTiNC/NEASURENENT LAB 

SOP(S) 0 jVnD SOPS) # 

2) PREP LAB RF_CEIVED 3 •19_TY_ wet b) DATA REVIEWED AND 

ANALYT?CAI_ PREP STORED 

3) SAMPLE REi`1A'NDER STOR 1) -z6-LR Ot 

4) SEPARATION L 4 3 RECEIV(I) 

SOP (5) # 

GIS5

CHAIN-OF-CUSTODY BATCH AID.-,LYS;IS RECORD 12-Mar-1998 

I tq) 

Page 1 

fvfL CUSTOMER: BHI 

/I) 

SAMPLE DFLIVERY GROUP IND ]^7 

MATRIX 

n^ 

OTHER ^ /^ lJ1 BATCH NUMBER 0^ r 

CUSTOMER 

0ES ID DUP ACCOUNT ID P T.,c Sar ^^ COMMENTS 

1 j—ffB3Re6ei A(+1 5 B6WbE35 

2 ) 80320602 ES-14265 

v. ô • , .. 

I 

,:a 

BON686 ZF j.j O coOF5 7 0bg 8' / Zz- 

3) L-893@ B 60 3 BI I I O1^ B II 'J^ 

AC-IONS (T t i d a l '< Date) ------ ------- 

I 

1) INITIATED LAB 

2) PREP LAB RECEIVED 3_,l9_•9P.^^ 6) DATA REVD=tiED AND 

ùr(S) 4S Fjv_-*,^C J\3^ 

3) SAMPLE REN(kiN i)E:R ST P Pt=D _ -2b-z% oJ^ 

4) SEFARATION L.AE Ri:CEiV>.D 

SOP (S) if _------- 

Ocf' (0) iF 

ANALYTIC I_ PREP STORED 

SOP(Si

-$*t _-AL-SR c44 


l) Page 1 

1 2CUSTOMER: BHI 



_/)/p v^-^' I BATCH NUMBER D3'a3^ 

GES ID DUP ACCOUNT 

CUSTOMER 

ID 

wZ' SA- ANA^ 

APT 

COMMENTS 

1 ) 80322201 ---81i^ `"--a te BêH6c65 

2 ) 80322202 °SF14_5o lI BON639 Gy.Z 0. 000"6 6C. i ApR 1zz^ 

------------ --------- ------ - ------ -- 

ACTIONS CTIOi JS (Initial & Date) ----------- 

1) INITIATED < 3 5) COUNTING/MEASUREMENT LAL+ 

2) PREP LAB RECEIVED aL-t9-9g _ 5) DATA FEVIE-WED AND 

A.NALYTI;P.I_ PRE° STDRED 

3) SAMPLE REMAINDER STOR. D 3_Z6=4T _p^ 

4) SEFARATiOi: LAP RECEI'-TGh 

SOp(G) R 

Gigs

3 l / CUSTOMER 

MATRIX 

-** TOTAL-SR # -I* 


9 e 

EHI SAMPLE DELIVERY GROUP 

OTHER rl -LV I BATCH NUMBER 

CUSTOMER 


r ^r 

Lh.r.^ CsA^ ------- 

1 ) 80327201 BHI BON692 Q3.1 O-0006&T^ 6D //}iie4$ 12.Zl 

2 

3 ) 

f ------ - -ACTIG10S (Initial & Date) - ------- -- 

1) INITIATED 1) GOUPJTiPJG/hIEASUREi`f:-NT LAP 

SOP(S) 4 SOP (5) t -- 

2) PREP LAB RECEIVED 6) DATA PEV1EWED AND 

r`.NALYTICAL PREP STCRED 

501 1 (S) # $_^^±^2c So i3^ 

SuP(5) # 

3) SAMPLE RENAI-'NDER STCRPn 3 Lb-4g out 

4) SEPARATION! LAD P.ECEIV'_D 

- 

cis, j

%uanterra 

.Sb.iCV 


ANALYSIS C-1 q MATRIXo+DUE DATE y -6-9k 

t!^R`( r-rr-mEnlr 

WORK ORDER SEQUENCE a amir CONAENIS 

J- 03161 -10 Wj,;AJ QCBATC$REAGEM'BIAW 

J . Û. D^ I (ro iX QC BATCHMAMUX IS AIS 

J o 316 t IM oQ 

J- 

D o31b1 

(dtde) 

2M or 2S 

(dude) 

01 

^'p3161o1 '^ 1 " 

gn3 LBôZ 

g03 F-06 pZ 

b3 Z? 02 

$03 z-2z0^ 

Batched and QC updated by-î e^ on 3 -2 

3• 

QC BATCH MATRDUREAt3Nr 

SPUM 

QC BATCHMATRUMEAG NT SPUCE 

Dupticade of Sample H 8`0 3 t 61 01 

Rec'd in Prep Lab by on 3- H -w S0 05L1C- C-So 1 i Rn,= 0 

Rec'd in Sep Lab by uM , on #-G fe Sop#12(_ e-- SG,2.) Rni / 

Rec'd in Sep lab by on 41 SOP# _ RnLj— 

ED/CPPT on Sop# Rni 

Rec'd in C.R by on yl, l+r So p(__, 

Data Reviewed by - ^`^ l^ Sop# e- ^4 Z 

O riginal batch sheet an complete calculation file to be filed with the FIRST Esttd work order number. 

FORM NO.: RC-52. I/98. Rev 8 

S4 FRAc c10 

i s 0-^ O R y 5 0 L- o, Nor o^ 1 S; 

&L-L- s 02 1 = Gi9i1 

Rn

CHAIN-OF-CUSTODY BATCH ANALY;l S RECORD 10-Mar-1998 

Page 1 

'J 

CUSTOMER: BHI 

SAMPLE DELIVERY GROUP I/ ^^ 

MATRIX 

Q 

OTHER ^ ^ u -D0 l 

/`^) 

BATCH NUMBER ll -0I 

CUSTOMER 


sa aaa^ 

---------------- ---------------------------- 

1 ) 803161010.000 1040 BHI SON660 

2 ) 80216192 Biii 130H681 

^..3•i6 

1) INITIATED 

D031b 4o l 0_•000blg 

it 

3 


^ 5) COUNT IN /MEASUREi•4ENT LA3 ___ 

SOPS) # SOP(S) i4 

2) PREP LAB RECEIVED 3_-v =L -ci^j^.^ Ei) 4)jT;n REVIh.WED ANO 

,04l%LY I i L FRS? STGRcD 

SOP ( ) ) if R - 

SOP (S) # 

3) EA'NPLE REf!AINiiER SIOR I=D s-2S-qY _o L 

4) SEPAROTION LAB RECEIVED 

SOH (5 i 4 

L191

CHAIN-OF-CUSTODY BATCH ANAL`SIS RECORD 11-Mar-1998 

1 3 ^1 Page 1 

CUSTOMER: BHI SAMPLE DELIVERY GROUP ^ 

Q 

MATRIX : OTHER f ^ lam' i BATCH NUMBER o3'IS 

CUSTOMER 


gp dal 

1 ) 603E 8481 7" ac 3-zs 

I?I13 $9PF6^^ 

2 ) 80010402 0.0006\ 7 DHI BON6 33 

3 ) ^ BE)S I BR6S T'°` 3 ' Fill! BER16 j4 

----------------------------------------nr 

I%i') ri 

1) INITIATED `) CCUNTI'?G!i IcA5UREi`lEi T L.AB 

SCP ( S ) 4 SOP (S) ## 

2) PREP LAD ^.__ :." - 5-t5 9^ S___ b) hATA REVIEWED AND 

t^.iINALYTICAI_ PREP STORED 

SOt' (5 i ;E Ri^H RC S9 ^3 -o — 

GOP (7) 

3) SAMPLE RE?A 7 ^'0^° '-TSJ,;" h 3_z5- ciY O(t -- 

4) E /?i i,l IiJIli L.'?L' FL t.t I'i -11 

-- 

619

1 / 1 

CHAIN—OF—CUSTODY BATCH ANAL"S IS RECORD 12—Mar-1998 

Page 1 

I/ CUSTOMER: BHI SAMPLE DELIVERY GROUP 

MATRIX : OTHER HAW BATCH NUMBER 

(,^ 

CUSTOMER 


SR AUkI 

%A 

2 ) 60320602 0 .00 1 1 4c BHI BON686 

3 ) (36226692 _ 

i-u ^Lr _R 41 uQW687 - 

- -- ------- -------- -- ---- ------------------------------- ---- 

IJACTIONS (Initial ?< Date) 

ff 

1) INITIATED ^ t _ vC 5) COUNTiW,/M=ASURE;'lENT LAI3 

SOP(S) 4 SOP(S) # 

2) PRE? LAD REC E IVED 3=1.^^K. D^^ 6) DATA RE'J[t_WED AND 

IgALYTIC `)L PREP STORED 

SOP (5) t# ^t^So ^3 

3) SAr.PLE REMAINDER STOR^_0 

4) SEPAR A TION L=° 9E-,-E`4's_,) 

SC P 13) 4 wW. 

F) 

(JigJ


Page 1 

31 / CUSTOMER: BHI SAMPLE DELI`,lERY GROUP WQ^^^^ 

MATRIX : OTHER M8-bul BATCH NUMBER 

1 ) 

CUSTOMER 


5 A Au A^ 

zs 

2 ) 80322202 0. 00 t O 2S l BHI BON639 

------------- ----------- --------------- — -- 


1) INITIATED(-1 U) COUNTING/MEASUREMEidT LA3 

2) PREP LAB RECEIVED -j°1-gH_°nc S) DATA REVIEWED AND 


SOPS) H Rjct" 

SOP (3) n 

3) SAMPLE REMAINDER STORED 3_ zS '^K Oaf 

4) SEFARATION LAD RECEP;`;i) 

SUP (5 ) ;' _ _ —^W---- 

SCP (^:) It 

61,9,1


Page 1 

/ CUSTOMER: BHI WIPLE DELIVERY GROUP 

MATRIX OTHER -oCQ, BATCH NUMBER 

CUSTOMER 

QES ID DUI' ACCOUNT ID COMMENTS 

-SA AmPrc_ 

1 ) 80327201 (0 .00lozz DHI BON692 

2 ) , 20=7202 VY^-3 . 2 5 tL1( 8 1693 

3 ) —Be -327E 3 ° L4 -Hi BON694 

719g 

1-a' 

`^J ^ 

1) INITIATED _ 3 > CuUid^ ;'=Ci IG1SU°EPIE^JT Ld7 

2) PREP LAD RECEIVED 3-l^L-RY_D _ > DATA REV IE!:ED AND 

Arl.ALYTICAI_ FRET STCt?HD 

3) SAMPLE R i''.,a;i;L'=R ".: i_'I

i..T":}1M1frt::l 

Sen+:rx 


ANALYSIS 5F.-77 MATRIX C) T^ DUE DATE_a -6 -Ur 

^R`( CS=m Etvr 

WORK ORDER MQMCE s CENT Comme T$ 

J 03161 - 113 QC BATCiREAGUITBtANK 

J ^ tw -1X QC BATCH MAT= BLANK 

J o 3 t 61 

J N In 

- 1m aim 

(code) 

-2M or 2S 

(mde) 

QC BATCH MAIMMAGENT 

SPUCE 

QC BATCH MATRDUREACENT SPLICE 

Do-6tb1 -01 -_ 

Dt>Q lirate of Saittple B g0 3 l 61 01 

FSb3l6 l o1 '^ 1 `^ 

gub l$ 1oZ 

8o3 zob oZ 

03 2ZZ02 

$03 

Hatched and QC updated by-^dt on 3 LS-LJ 

Rec'd in Prep Lab by ean 3 A _ Sopiig tL g-SO t 3 Re%- 

Recd in Sep Lab by l A on ^^ ^^ Sop3 C^ ^^ L ` R n^ 

Rec'd in Sep lab by on Sop# Rcv 

ED/CPPT by on SopB p Rn 

Recd in C.R. by !^ on 3 31 SOP# 7^ Ic- ^G l R^ ^^ 

3,70-,- 

Da ta Reviewed by on Sop! ^^^' Cc [ R^ 

O riginal batch sheet add complete calculation file to be filed with the FIRST Eved work order number. 

FORM NO.: RC-52.1/98. Rev. 8 

50. tS of 1 {Lj CS-,: WN ') tvoT of- set 

CWT 1^^ -. Rab^•F ^ a.LQ. 

LiÛ

I 

CHAIN-OF-CUSTODY B,4TCFi ANAL Y 51S RECORD 10-Mar-1998 

Page 9 1 

CUSTOMER: BHI ^/'y SAMPLE DELIVERY GROUP W D ^^ 

MATRIX : OTHER I3 ^ (/ {may I BATCH NUMBER 

CUSTOMER 

0ES ID DUP ACCOUNT ID COMMENTS 

S(} Auk 

1 ) 80316101 ° _ _ = ' )' _JN680 o-oco3 ra 

2 ) 863t6ie _ _ I e 

1) INITIATED 

13^ti6a 


^ ^5) CSUNTIN•f,/MEASURE-,KENT LAB 

SOPS) # 410- i^ SUP(S) ?k _ 

2) PREP LAB RECEIVED 6) DATA REVIEWED AND 

ANALYTIC ;)_ PREP STnRED 

SOP (S) Sk ^^tE2C5 o^T» 

SOP(S) u 

3) SAMPLE REMAINDER STDREO 3-Z6 0.8 q^ 

SOF'(S) i; V- 

4) 

n 

SEPARATION LAB RECEivi -0 ^^^(^^!^ ^^^^\\ 

SOP3,^ÎT^4^ 

^^19,

! 

**^^ SE-79 *** 


CUSTOMER BHI 

Page 1 

SAMPLE DELIVERY GROUP (,voa07 

MATRIX OTHER I BATCH NUMBER 03-1 

CUSTOMER 

GE3 ID DUP ACCOUNT ID COMMENTS 

5{} A"4tz- 

1 ) 3,Lb 

3 

80318402 I BON633 O •oeo357 

----Y 

5 

-- ------ ^ îr T I OI •aS (I n i t i a 1 `. D.^ ^: a) ------------ 

1) INITIATED / ` )^ :) COUNTI`JG/iÌaASUREiÌENT LAB 

SOPS) # SOP (s) # 

2) PREP LAB RECEIVED 3-g-9^0^_ 6) DATA nEVIEWED AND 

3) SAMPLE REMAINDER STORED _3-26 `^k_OyC 

4) SEPARATION LAB RECEI'V, 

n^ 


SOP(S) # 

G L J ,j

*n 5F-79#r 

I,^ 

^ 

V 

q li^ 


Page 1 

CUSTOMER: BHI 

V hf' 

MATR IX OTHER /y . 1 

I'\ l 

SAMPLE DELIVERY GROUP OQQ7.S 

BATCH NUMBER O3 -°Cy 

CUSTOMER 


S!! AwA - 

1 ) 805Efto s'f c5 

2 ) 80320602 -- I B 0N61360. 000 rs50 

3) eeszewe Bi )l3 "^- BE)H687 

- -- ----------------- ------- 

ACTION-- (Iuitiai & Date) 

1) INITIATED _ ^(^?7D^ 5) COUNT iNC!t1EAS'.JRE'tENT LAB 

SOP(S) # S010 (S) t# 

2) PREP LAB REC_eVEG 3 _lg _fig ,_ 6) DATA REVD - WED AND 

FiN.^- Y i.AL =RE P STOR E71) 

SOPS) 4 F^^Cti C50^3 0 

Soe (s) # 

3) SAMPLE REMAIfdDER ST07v:D 3.26-`^rr 

4) S EE cAR.fTI^CN 

Sr)^ c :^) ,i ,^^ 

l 

^l l n i^

^CHAIN-OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998 

Page 1 


MATRIX : OTHER ^(^ ^ BATCH NUMBER 0v _Z/92 

CUSTOMER 


S tOr AN A k- 

---------------------------- ----- 

1 ) C $ 

3.7bRTf 

2 ) 80322202 - - : II BON 639 0.000657 

1 CTIOi.3S (Initial Data) 

1) INITIATED / ^1 `) CCUNT?NC;/ IN IEASUREPIC 'i\iT LAD 

2) P R EP L AB R EI` iEC 3.1^g$ b) I IATA ,EVI; WED AID 

SOP (S) # R'CH-Re5013-0 

3) SAMPLE REMAIPIDER STOR'1) 3_- 26 "2'? r--A. 

4) SEPARATIuP"! LAL 

AiNALYTICAI.. P R EP °_.T04Ei 

^Pc 

G; 3 0

W A^ 

CUSTOMER 

MATRIX 

EHI 

OTHER Û cb I 

h^^ SE:-!9 

^^n 



BATCH NUMBER 

^^(^ ^7 Page 1 

I.W^ I 

o3-a7a 

CUSTOMER 


5^4 ANR^ 

1 ) 80327201 ' " eC= ` ' I BON692 O-0006°tb 

3.26'45 " 

3 ) ^69327^ P+f 13—^^tl^`^Q ^'.At'^,5^4 

------ -- - --- ---- ---- -- - --------------------------- 

'^CTI0PJ:3 (Inibxal ', Dace: 

1) INITIATED 5) COVivT-NS/MEASUREMENT LAD 

SOP(S) J^'3 5i7P(5) R 

2) PREP LAB RE Ei•1 D 3-)5_= jy^ 6) DATA REV!'-W;ED AND 

(`,N1LY7-,-j`j PREP STORED 

Sop 1. 3 i K R%L'wfC 4501 3 -i7 

SOP ( 0 ) 

3) SAMPLE Ri_i', i' i;GP STOP! D 'b -26-43 V+ 

4) EEPARAT10iI LA-r `?=r'EIY,-D 

G^G^

(j..%"uanterra 


ANALYSIS TL . Q MATRIX O TlifA DUE DATE L -6 `Lk 

r,a`4 rV-rn FIUT 

WORK ORDER SEQUENCE # CLINT 

J-. 0316 1 -1B QC BATCHREAGE"NP BLANK 

J - N ^ k -ix QCBATCHMATMBLANK 

1 0 3161 -1M 0(a) 

(circle) 

1 -ZM or 2S 

(aide) 

Do3tbt -fit 

^Sb-Sl6lo1 "' 1 °' 

QC BATCHMA 

SPDM 

p GEgr 

QC BAT CHMATROGRFAGENT SPIKE 

Duplicate of Sample # $0 3161 01 

gv3 tB^lOz I - 

g03 i_06 02 

go3 2zZO2 

$-03 Z: '7Z0\ 

Hatched and QC updated by^_ on 3 -2 5-%^ 

Rec'd in Prep Lab by -- vr.- on 3 -H -W Sop>9RtCttRCSoI^ M-2 C)_ 

Rec'd in Sep Lab by 6TL1) 

on 312- 411 Y 

Rec'd in Sep lab by /L( — on SOP# Rte: 

ED/CPPT on SOP# R.t - 

Rec'd in C . R_ by---4- on 'f I i k r SOpag _ tZ r tilts, 7 ,o t Rn-4 o 

Da ta Reviewed by on 

sop# t^ 

^F`T^ ^Re1d 

O riginal batch sh t and complete calculation file to be filed with the FIRST Gsted work order num be r. 

FORM NO.: R -52. 1/98_ Rev 8 

SCE ^--RA

J r 

CHAIN-OF-CUSTODY HATCH ANALYSIS RECORD 10-Mar-1998 

ql/1 Page 1 

1) INITIATED 

SOP (S) # 

"Do3 16) b 1 O-00038Z 


oaa^7 


MATRIX OTHER VuI BATCH NUMBER 

/, 

_1(Î 

CUSTOMER 


SA, Afjn^ 

1 ) 80316101 0.000yrt BHI BON680 

2 ) R0314410:2 LZtc 5-25 9d I I BON 681 

5) COUNTING/MEASUREi`1ENT LAB 

SOP (5) # 

2) PREP LAB RECEIVEll 3-i9 - CC _ 6) DATA REVIEWED AND 


SOP (S) # ^R-L4A^\J^:^) 

SOP (s) # 

3) SAMPLE REMAINDER STORED•z51t 


SOPS) B J w 

SOP' (S) !k 

vL,.^J

n/ ^j\x CHAIN-OF-CUST011`r' BAICFi ANALìTiIS RECORD 11-Mar-1998 

UU ,J` U 

Page 1 

, I TOMER: BHI 

-j 

501PLL DELIVERY GROUP W6422 / 

llV// MATRIX OTHER g- BATCH NUMBER LCJ 

1 ) 

CUSTOMER 

OES ID SDAU pACCOUNT (D COMMENTS 

2 ) 60318402 0-00034Z BHI BONE03 

3 ) seaâ4e^ 0at3•z54k -IT 

1) INITIATED 

/ 

tiC 

01dS (Tuitial I< Date) 

-1 

U 5) COUNTING/MEASURE4IENT L D 

SOPS) # r-! SOPS) 4 

2) PREP LAD RECEIVED 3-Ict-4^^SL 6) DATA =.EVCEWFID AND 


SOP (s) 4 R1ctFScLî^^-o 

3) SAMPLE REMAINI)ER STOR`--r ) 

C^ ^^ (J i If rJ 

4) ===;RATIO;•! L B RE.C==VC0 

o^(s a 

L20el

:r Tr-99 

CHAIN--OF-CUSTODY BATCH ANALYSIS RECORD 12-Mar-1998 

` Page 1 

l• 

/ CUSTOMER: BHI 


MATRIX 

^Q 

OTHER ^^ D` BATCH NUMBER LEA OWE 

^-st 

CUSTOMER 


5A AQ At 

1 ) 9a-3:0601 --Z)0C -s•u Ski; BGW609 

2 ) 60320602 0-00°6a6 BHI BON636 

3 ) QQ-2ncn- 1 -pe 3 • 2,5 am; 

_ ^l_Ap:T C1=5 

13 ,90CA97 

1) INITIATED _) t^b COUNTING !NEISUP,Ei'IEhIT LAB 

SOPS) 4 oWG SOI'iS? T 

2) PREP LAD RECEIVED ^_-1q-^^^` 6) DATA RE"'IcWEL' AND 

ANALYTICAL PREP STDRED 

90F`-) 4 R^t}iZC v\3 ^ 

SC i'' Ie/ '^ 

3) SAMPLE REMAIiÒEF ST7RL 1) 

4) SEPARATION LAD RECEIV:T) 

I 1 _`) 'It 

LL-VJ

GvJ ^) 

^ 

II 

VIA// 

CUSTOMER 

MATRIX 

BHI 

CHAIN--OF-CUSTODY BATCH ANALYSIS RECORD 13-Mar-1998 

Page 1 

SAMPLE DELIVERY GROUP IJDo^^7S 

OTHER IO^(/(^ I BATCH NUMBER 

CUSTOMER 

QES I 1) DUP ACCOUNT ID COMMENTS 

'S4 quq^ 

1 ) 89a2229 } B)a4 BQW;$38 

2 ) 80322202 0-00°6 77 BHI 13 01.4609 

ACTIONS (ILtitial & Date) 

^j 

1) INITIATED 5) CUNTING/MEASUREMENT LAB 

SOP(S) # SOP (S) # 

2) PREP LAB RECE.'.VED ?Zlc]. ^ 

SOf' S) i5 _F 

Ur TA di:b!ED %)i;-: 

!i'1-'LYT.Gt\L PREP S 7 0R="D 

c+ Q _ i3 -Q) 

3) SAMPLE PENAI`CER STORi=O 3_ZS ^^ûL 

G20G

CÌAIN-OP-CUSTODY BATCH ANALYSIS RECORD 17-Mar-1996 

Page 1 

1 i 


MATRIX OTHER ^ BATCH NUMBER 

OES Ill DUP ACCOUNT 

CUSTOMER 

ID COMMENTS 

S y A+jf4fr 

------------------ - --------------______________________________________ 

I ) 80327'-101 0_00ob !o BHI BON692 

2 ) BHi 

----------- -- -- -- ----- - --- - -------------- - - 

lACCjTICNS (I) itiai D-i-) 

1) INITIATED +)^ i ;_.H?_?I !NI \SURE`:1F.NT LAR 

6OP(S) #_^ L ^! SO? (S) 

21 PREP LAB :R c.(;=iVED I ` -`Z$ DDS b) i) ATA REV ( f:WFD AND 

AidALV'_:AI_ of^cp ST'^ftED -__ 

3) SAMPLE F'EV-J ;Ii : i?E? S T OR :D 3.25-4^_f^t^ 

4) ScP:ARr1Ti:=?; _-- YD:C= ' .t:+: 

SCf' (B i ;; 

)!) 

U2 o

' l i uani'erra 

E _l,st8 

S Tiv 


AVALYSIS TC -9 MATRIX DUE DATE LI -b-`c8 

st_%j R-&y 

19 ORK ORDER SEQUENM # QdENi' C lzg mm 

1 oil&`V -1B 

cs t+i 

QCBATCHREAGENI'BLANK 

J ata. _Ix QCBATCHMATRDMHIAMC 

J O31 h-4 _IM 099) 

J N 

(dsde) 

lq 2M or 2S 

(drde) 

D 03 iky -Ol 

QC BATCH MATRI)WEACENT 

SPUM 

QC BATCH MAIRDUREAGENT SPIIM 

Duplicate of San* #i $703 1840 1 

^SOÎ&4ol 03 

-a la 

Wn 227 

^b3 1b102 

$0b2.o6o1 b3 2- 5A 

$03a22o1 

S-0 -5 P- bZ 

^ro3 Z 12b2 

,., l a _. 

OTC 

Batched and QC updated by 'wL on 5-2--s-1Y 

Rec'd in Prep Lab by -7z> eL on 3 -t°t Aqv 

Rec'd in Sep Lab by_ 1Wl on >> 2 9 Si 


ED/CPPT by on 

Sop# a CtA 2CSbv3 RCO 0 

Sop# A^ C I7 R C 1 6615 Rev* 

{, 

^ Rev# 

Rec'd in C.R- by it on 3Sop# f` /c ,Q y^ryyl ) Rev 

Data Reviewed by on ^- Z' Sop# f ` L W ( Ma 2Rn-4__ _ L 

Original batch sheet and I 

complete calculation file to be filed with the FIRST fisted work order number. 

FORM NO.: RC-52,1/98, Rev 8 

Revd 

6 206

cclaq 

w^'M t+s

_ 

SF^ Aa A^ 

Jll,! ''CUTS 

G^1C

^!^ n"mil 12^^ 1 ?5 

P, ^LrKZC S o i3 ^ 

5 25 -Z 

^l

Get

SAr A-&) A^ 

621 J

jS A- 

V-D 

621=

CLIENT: 

PROJECT ID: 

BHI_45 

SAP B98-061 

Cr+6 CHAIN OF CUSTODY 

MATRIX: OTHER DUE DATE: 03/31/98 

SDG W02275 BATCH: 03-184 

SAMPLE # CLIENT ID COMMENTS 

W803184 01A BON682 

W803184 02A BON683 

W803184 03A BON684 

Comments: 

q QC REQUIRED 

INITIALS DATE ^ SOP# 

COC INITIATED L^ 7 , N/A 

SAMPLE PREPARATION 3/1 1 gz RICHWC5003 Rev 2 

SAMPLE ANALYSIS 3 ^ RICHWC5003 Rev 2 

DATA REVIEW RICHWC5003 Rev 2 

L^-1J

CLIENT: 

PROJECT ID: 

CS+6 CHAIN OF CUSTODY 

BHI_15 MATRIX: OTHER DUE DATE: 

SAP B98-063 SDG W02261 BATCH: 


W803216 01A BON894 (^, ^j b8,5) 

W803216 02A BON895 (^Gy 3) 

W803216 03A BON896 C' JG ,kj ypl 

Comments: 

El QC REQUIRED 

04/01/98 

03-216 

INITIALS DATE SOP# 

COC INITIATED ^j(C^ N/A 

SAMPLE PREPARATION RICHWC5003 Rev 2 

SAMPLE ANALYSIS RICHWC5003 Rev 2 

DATA REVIEW 

3 !^ Cyy RICHWC5003 Rev 2 

C^lU

CLIENT: 

PROJECT ID: 

BHI_45 

SAY B98-063 


q QC REQUIRED 

MATRIX: WATER DUE DATE: 03/31/98 

SDG W02261 BATCH: 03-186 


W803186 01A BON783 

Comments: 


COC INITIATE D N/A 

SAMPLE PREPARATION 

^ 

RICHWC5003 Rev 2 

li 


DATA REVIEW 3 Q RICEWC5003 Rev 2 

G

CLIENT: 

PROJECT ID: 

BHI_45 

SAF B98-061 

Ci+6 CHAIN OF CUSTODY 

MATRIX: OTHER DUE DATE: 

SDG W02275 BATCH: 


W803272 OIA BON692 


04/06/98 

03-272 

W803272 02A BON693 ?o32,790/ 

W803272 03A BON694 

Comments* 

COC INITIATED 


'31 -7 /9 9 

SAMPLE PREPARATION 36l RICHWC5003 Rev 22 


a !6 

N/A 


DATA REVIEW RICHWC5003 Rev 

G^:1^ 

it 

it

CLIENT: 

PROJECT ID: 

Ci+6 CHAIN OF CUST0DY 


SAF B98-063 8DG W02281 BATCH: 

SAMPLE # I CLIENT ID ( COMMENTS 

W803279 01A BON898 C ^0Y0 > 

Comments: 

COC INITIATED y _ 


04/06/98 

03-279 


r/, `/ b 



DATA REVIEW RICKWC5003 Rev 2 

N/A 

^"^.j

CLIENT: 

PROJECT ID: 



SAY B98-061 SDG W02275 BATCH: 

SAMPLE # CLIENT ID ( COMMENTS 

W803206 01A BON685 

04/01/98 

03-206 

QC REQUIRED 

W803206 02A BON686 

a-LD î41eL ,- 1ficGI uulwl-luL-( r3r) L 

W803206 03A BON687 grj32^ld^^ 

Comments: 


COC INITIATED 7^= N/A 



DATA REVIEW RICEWC5003 Rev 2 

G4.

CLIENT: 

PROJECT ID: 



SAP B98-063 SDG W02261 BATCH: 

SAMPLE # CLIENT ID I COMMENTS 

W803216 01A I BON894 C r3 .Qb8& l 

W803216 02A BON895 

(pO 

W803216 03A BON896 C'JG/ l ^^^ 

Comments: 

3 ) 

q QC REQUIRED 

04/01/98 

03-216 


COC INITIATED ^^ ^7 N/A 



3 ^z^ ^C 

3/1 



DATA REVIEW 3 / 4 Y RICHWC5003 Rev 2- 

nn^ 

^^1

CLIENT: 

PROJECT ID: 

BHI_45 

SAF B98-061 

Cr+6 CHAIN OF CUSTODY QC REQUIRED 


SDG W02275 BATCH: 03-222 


W803222 01A I BON688 

W803222 02A BON689 

Comments: 

80 A) 


COC INITIATED ^- __^( N/A 


3 13 1q - RICHWC5003 Rev 2 

SAMPLE ANALYSIS Tfo 3 13 4 RICHWC5003 Rev 2 


7 .^ r

CLIENT: 

PROJECT ID: 



SAF B98-063 SDG W02281 BATCH: 


W803242 01A I BON897 

Comments: 

QC REQUIRED 

04/03/98 

03-242 


COC INITIATED / N/A 



DATA REVIEW 

3/Na 


M 3 9 1 ,^, IRICHWC5003 Rev 2 1

CLIENT: 

PROJECT ID: 

BHI_45 

SAF B98-061 

Cr+6 CHAIN OF CUSTODY QC REQUIRED 


SDG W02275 BATCH: 03-244 


W803244 01A BON690 

W803244 02A BON691 

Comments: 

I IALS DATE SOP# 

COC INITIATED ^' /,^ N/A 


SAMPLE ANALYSIS 3r/9 RICKWC5003 Rev 2 

DATA REVIEW 7j lb 

^^ RICHWC5003 Rev 2 

i

CLIENT: 

PROJECT ID: 

BHI_45 

SAF B98-061 


0 QC REQUIRED 


SDG W02275 BATCH: 03-161 


W803161 01A BON680 

W803161 02A BON681 

Comments: 


COC INITIATED ^^ N/A 

SAMPLE PREPARATION 3/Old RICHWC5003 Rev 2 


DATA REVIEW 34497 RICHWC5003 Rev 2

CLIENT: 

PROJECT ID: 



SAF B98 - 063 BDG W02261 BATCH: 


W803216 01A BON894 l rJG/-) (a^GJ 

W803216 02A BON895 ( J30 ^,-/ by3 ) 

W803216 03A BON896 

Comments: 


04/01/98 

03-216 


COC INITIATED 7 N/A 

SAMPLE PREPARATION 3/^^/ 8 RICHWC5003 Rev 2 II 


31& 

— 



G^t_v 

I

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