SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

SAF-RC-047 

100 & 300 Area Component of the 

RCBRA Sediment and Tissues 

FINAL DATA PACKAGE 

COMPLETE COPY OF DATA PACKAGE TO: 

Jill Thomson HO-23 KW 7/19/06 

INIT W UDATE 

Jeanette Duncan H9-02 KW 7/19/06 

INITIAUDATE 

COMMENTS: 

SDG K0303 SAF-RC-047 

Rad only Chem only X Rad & Chem 

X Complete Partial 

Waste Site: 600-132/600-190 

1607-H2 

116-N-3 

1607-D2:1 

Borrow Pit 24 

Yakima Ridge II 

Vernita Upriver on South Side 

McGee Ranch 

Saddle Mountain 

Central Plateau Shrub Steppe 

r -),:'03SS 

AUG 0 7 2006 

EDMC 

100-D-22 

Borrow Pit 23 

600-131 

100-D-48:2 

100-D-49:2 

M

4DIVLI 

1 

Joan Kessner 

WC-Hanford 

3190 Washington Way 

MSIN H9-03 

Richland, WA 99354 

Subject: Analytical Data Package 

Dear Ms. Kessner: 

VdM 

\ 

N V 

Enclosed are the hard copy analytical reports for the batch number/fraction indicated 

(marked X) in the following table: 

LvLIBatch ................._................................._ # . 06041-904 

. ..................._... i. . ..._...... . ............._...._K0303....... 

SAF # RC-047 

lte Received 

# Samales.._ .. 

Volatiles 

Semivolatiles 

4/28/06 

............._...................1.5.............. 

SOLID 

Pest/PCB 

PAH 

O/KRO/GRO 

........._.......__...._...-.-._._ 

GC Alcohols 

Herbicides 

Metals 

X 

The electronic data deliverable (EDD) will be emailed shortly. If you have any 

quest Rns, please don't hesitate to contact me at (610) 280-3012. 

OrleM S. Johnson 

Project Manager 

r.\group\pm\orlette\tnu-hanford\data\b_ltrs. doc 

208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-3000 • Fax (610) 280-3041

Lionville Laboratory, ry, Inc. 

PEST/PCB- ANALYTICAL DATA PACKAGE FOR 

TNUHANPORD RC-047 K0303 

DATE RECEIVED: 04/28/06 LVL LOT # :060 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

06/02/06 

1191920-- 

N RECEIVED 

^^` 206 

CLIENT ID LVL # MIX PREP # COLLECTION EXTR /PREP ANALYSIS 

J11KK8 001 SO 06LE0455 04/05/06 

J11KL5 002 SO 06LE0455 04/05/06 

Ji1KL6 003 SO 06LE0455 04/03/06 

J11KM0 004 SO 06LE0455 04/05/06 

J11K 42 005 SO 06LE0455 04/03/06 

J11KM3 006 SO 06LE0455 04/03/06 

J11KM4 007 SO 06LE0455 04/03/06 

J1iKM5 008 SO 06LE0455 04/03/06 

J11KM6 009 SO 06LE0455 04/03/06 

J11KV1 010 SO 06LE0455 04/05/06 

J1lKV2 Oil SO 06LE0455 04/05/06 

J11 1,21 012 SO 06LE0455 . 04/03/06 

J11L23 013 SO 06LE0455 04/03/06 

JlIL25 014 SO 96LE0455 04/05/06 

J11L36 015 '50 06LE0455 04/03/06 

JIIL36 015 MS ,$0.061:80455 09/03/06 

J11 1,36 015 MSD S0 06180455 ' 04/03/06 

LAB OC: 

PBLKJM MB1 S 06LE0455 N/A 

PBLKJM MB1 HS S 06LE0455 N/A 

PBLKJM M131 HS _N/A 

L 

06/23/06 

06/23/06 

06/23/06 

06/23/OE 

06/23/06 

06/23/06 

06/23/OE 

06/23/OE 

06/23/06 

06/23/OE 

06/23/OE 

06/23/OE 

06/23/OE 

06/23/OE 

06/23/OE 

06/23/OE 

06/23/OE 

06/23/06 

07/07/06 

06/23/06 

000000001

Case Narrative 

Client: TNU-F-IANFORD RC-047 W.O. #: 11343-606-001-9999-00 

LVL #: 06041-904 Date Received: 04-28-2006 

SDG/SAF # K(3303/RC-047 

CHLORINATED PESTICIDES 

Fifteen (15) solid (composed of mice) samples were collected on 04-03,05-2006. 

The samples and their associated QC samples were extracted on 06-02-2006 and analyzed 

according to Lionville Laboratory SOPS based on SW846, 3rd Edition procedures on 06-23-2006 

and 07-06-2006. The extraction procedure was based on method 3540C and the extracts were 

analyzed based on method 8081A. 

The following is a summary of the QC results accompanying the sample results. Lionville 

Laboratory Inc (LvLI) certifies that all test results meet the requirements of NELAC except as 

noted below: 

1. All results presented in this report are derived from samples that met LvLI's sample 

acceptance policy with the exception of some discrepancies, which were documented on 

the Sample Receipt Checklist. 

2. The sarnples were received outside extraction holding time. Samples were also extracted 

outside holding time due to the refrigerator (ID # R003) malfunction. A copy of the 

Sample Discrepancy Report (SDR) has been enclosed. 

3. The soil sample results were reported on a wet-weight basis. All samples were extracted 

using reduced sample volume due to the nature of the sample matrix. A copy of the 

Sample Extraction Record has been enclosed. 

4. All samples and their associated QC samples received Florisil and Copper-Sulfur cleanups 

according to Lionville Laboratory SOPS based on SW846 methods 3620B and 3660A 

respectively. 

5. The method blank was below the reporting limits for all target compounds. 

6. Seventeen (17) of forty (40) surrogate recoveries were outside acceptance criteria. A copy 

of the Sample Discrepancy Report (SDR) has been enclosed. 

The results presented in this report relate only to the analytical testing and conditions of the samples at receipt and during storage. All pages of this report are integral parts of 

the analytical data. Therefore, Us report should only be reproduced in its entirety of 2 g pages. 

208 Welsh Pool Road • Exton, PA 19341- 1313 a (610) 280-3000 • Fax (610) 280-3041 

8laM1

7. Two (2) of twenty (20) blank spike recoveries were outside the accept ance criteria in the 

pre-Florisil cleanup fraction. Eleven (11) of twenty (20) blank spike recove ries were 

outside the acceptance criteria in the Flo risil cleaned fraction due to the cleanup procedure. 

A copy of the Sample Discrep ancy Report (SDR) has been enclosed. 

8. Eleven (11) of for ty (40) matrix spike recoveries were outside accept ance criteria. A copy 

of the S ample Discrep ancy Report (SDR) has been enclosed. 

9. All samples required dilution due to the nature of the sample ma trix and high concentration 

of non-target analytes. The reporting limits were adjusted to reflect the necessary dilution. 

10. The initial calibrations associated with this data set were within acceptance criteria. 

11. The continuing calibration st andards analyzed prior to sample extracts were within 

acceptance crite ria. 

12. LvLI is NELAP accredited by the state of Pennsylv ania and holds over 20 additional state 

accreditations. For a complete listing of accrediting authorities and the corresponding 

analytes/methods, ple ase contact your Project Manager. 

13. I certify that this sample data package is in compli ance with SOW requirements, both 

technically and for completeness, other than the conditions detailed above. Release of the 

data contained in this hard-copy data package has been authorized by the laboratory 

Manager or a designee, as verified by the following signature. 

nt.iel 

J ry M an ager 

Lionville Laborato ry Incorporated 

som4lgoup\daW\put\NU hanford\0604-904s.pst 

208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-3000 • Fax (610) 280-3041 

3 i^lo^ 

Date 

.88.09801 f

Lionville Laboratory Sample Discrepancy Repo rt (SDR) SDR #: ob ec. IA-41 

Initiator. Jo ^%. L--0-- Batch: o b O 4 L qa `t Parameter 

Date: "1 l • b Samples: Ppss Matrix: 

Client: 1-n .. Method: swwdmcAwwcLpt Prep Batch: 

Fri. . 

n+oYy 

1. Reason for SDR 

a. CDC Discrepancy _ Tech P rofile Error Client Request Sampler Error on C-O-C 

_ Transc ri p ti on Error _ W ro ng Test Code _ Other 

b. General Disc repancy . 

_ Missing Sample/Extract _ Container B roken _ Wrong Sample Pulled _ Label ID's I ll egible 

_ Hold Time Exceeded _ Insufficient Sample _ Preservation Wrong _ Received Past Hold 

Improper Bottle Type _ Not Amenable to Analysis 

Note* : Verftd by [Logan] or (Prep Group) (drds)...stgnatureldaw 

c. Problem (Include all relevant specific results; attach data if necessary) 

SPt,.^PtY 3i t r3 

S-f•vscl-vs 21c..^K1. 

A ►t;a D» t lt^ ic t ^ gS 

SPP.PVtt e c CL 1 11 adT rt cY ♦. mo t a Z 

2. Known or Probable Causes(s) 

3. Discussion and P roposed Action Other Desc ri p ti on: 

_ Re-log 

_ Entire Batch 

Following Samples: 

_ Re-leach 

_ Re-extract 

_ Re-digest 

_ Revise EDD 

Change Test Code to 

_ Place On/Take Off Hold (circle) 

4. Pr eat Manager Instructions ... -^ 

_ Concur Proposed Action 

_ Disagree with P roposed Action; See Instruction 

_ Include in Case Narra tive 

_ Client Contacted: 

Date/Person 

_ Add 

Cancel 

(» 1 ! . 

S. Final Action ... slgnatunadate: V NEW Other Explana ti on: 

verified re-pog][leach]lextmct][digest][an ( e) 

/ Included in Case Narrative 

_ Hard Copy CDC Revised 

Electronic COC Revised 

_ EDD Correc ti ons Completed 

When Final Action has been recorded, forward original to CIA Specialist for distribution and filing. 

Route Distribut ion of Completed SDR Route Distribu ti • Ini 

on of Completed SDR 

ti ator 

• Lab General Manager. M. Tay lor 

X Project Mgr. Stone/Johnson 

Data Management S 

_ 

_ _ Metals: Beegle 

_ _ Inorganic: Per rone 

_ _ GC/LC: IGger 

ti lwell 

— 

_ MS: Rychlak/Daley 

Sample Prep: BeegleNger _ _ Log-in: Per ry 

_ _Admin: 

Other. 

GA-105,A-0805 

GO MM

"aw"Vurc L-auvrdwly Qdlliplrd LASGrepollGy mepOrr tzoum) 

Initiator. Orlette Johnson Batch: Parameter: 

Date: !17 06 Samples: Mat ri x: 

Client: t Method: swwerlucnwwicLP/ Prep Batch: 


a. COC Discrepancy _ Tech P rofile Er ror Client Request Sampler Error on C-O-C 

Transcription Error _ Wrong Test Code _ Other 

b. General Discrepancy 

_ Missing SampVEx tract _ Container B ro 

ken _ Wrong Sample Pulled _ Label ID's Illegible 

Hold Time Exceeded 

_ Improper Bottle Type 

Insufficient Sample 

_ Not Amenable to Ana lysis 

Preservation Wrong 

X Other 

— Received Past Hold 

Note: Verified by [Log4n] or [Prep Group] (circle)... signature/date: 

c. Problem (Include all relevant specific results; attach data if necessa ry) 

On 5110!06 sample storage refrigerator ID# R003 malfunctioned and was not holding the required sample storage 

temperatu re of 4°C +/- 2'C 


Broken motor 

3,. Discussion and P roposed Action Other Description: 

_ Re4og At the time of malfunc tion R003 was used for storage of samples received 

_ En tire Batch for extractable organics, metals and wet chemist ry (except TOC) analyses. 

Following Samples: All samples were removed fr om R003 to another refrigerator on 5/1006. 

_ Re Aeach R003 was tagged out on 5/10/06, repaired on 5/12/06, and we have 

_ Re-extract certified that R003 Is maintaining the required sample storage temperatu re. 

_ Re-digest 

Revise EDD 

— Change Test Code to 

_ Place OnlTake Off Hold (cir cle) 

4. Project Manager Instructions ... signature/daw 

Concur with Proposed Action 

sagree with Proposed Ac ti 

on; See Instruction 

clude in Case Narrative 

Client Conta 

Date/Person 

_ Add' 

Cancel 

5. Final Action ... signature/date: 

6/^`^^ 

414110 Other Explana ti _ enfied re-{log][leach][extract][digest][an 

Included in Case Narrative 

_ Hard Copy COC Revised 


_ EDD Corrections Completed 

on: 

When Final Action has been recorded, forward original to QA Specialist for distribution and filing. 

Route Distribu ti 

on of Completed SDR Route Distribu ti 

X Initiator 

X Lab Manager. I. Daniels 

X Project Mgr. Stone/Johnson 

Data Management: Stilwell 

_ Sample Prep: BeegleNger 


_ _ Metals: Welsh 

Inorganic: Perrone 

_ GC/LC: Kiger 

_ MS: Schneider/Daley 

— _ Login: Per ry 

Admin: 

— Other 

NM1 05-A-0805 

999000905

vLI 

DATA QUALIFIERS 

GLOSSARY OF DATA 

U = Indicates that the compound was analyzed for but not detected. The minimum detection limit for the 

sample (not the method detection limit) is reported with the U (e.g., l0U). 

B 

E 

= Indicates an estimated value. This flag is used in cases where a target analyte is detected at a level 

less than the lower quantification level. if the limit of quantification is 10 ug/L and a concentration 

of 3 ug/L is calculated, it is reported as 3J. 

I = Interference. 

I 

ABBREVIATIONS 

This flag is used when the analyte is found in the associated blank as well as in the sample. It 

indicates possiblelprobable blank contamination. 

Indicates that the compound was detected beyond the calibration range and was subsequently 

analyzed at a dilution. 

Indicates an interference on one analytical column only. Result is reported from remaining analytical 

column. 

BS = indicates blank spice in which reagent grade water is spiced with the CLP matrix spicing solutions 

and carried through all the steps, in the method. Spice recoveries are reported. 

BSD = Indicates blank spike duplicate. 

MS 

MSD = 

DL 

NA 

Indicates matrix spike. 

Indicates matrix spice duplicate. 

Indicates that recoveries were not obtained because the extract had to be diluted for analysis. 

Not Applicable. 

DF z Dilution Factor. 

NR 

NS 

Not Required. 

Not Spired. 

SP = Indicates Spiked Compound. 

P = This flag is used for an PESTICIDE/PCB target analyte when there is greater than 25% 

difference for detected concentrations between the two GC columns (see Form JQ. The 

lower of the two values is reported on Form I and flagged with a 'T". 

D = T'his flag identifies all compounds identified in an analysis at a secondary dilution factor. 

C = This flag applies to a compound that has been confirmed by GUMS. 

NPM = 

No pattern match for multi-component target analytes. 

000000006

uaVUâaa pYVapYVa7, 11,Y• 

Pesticide/PCBs by GC, CLP List Report Date: 07/07/06 15:01 

RFW Batch Number: 0604L904 Client• TNURANFORD RC-047 K0303 Work Order: 11343606001 Page: 1 

Cust ID: J11KK8 Ji1KL5 J11KL6 J11KM0 J11KM2 J11KM3 

Sample RFW#: 001 002 003 004 005 006 

Information Matrix: SOLID SOLID SOLID SOLID SOLID SOLID 

D.F.: 4.00 4.00 4.00 4.00 4.00 4.00 

Units: UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG 

Surrogate: Tetrachloro -m-xylene 139 * t 110 t 159 * $ 108 t 153 * t 114 t 

Decachlorobiphenyl 124 * t 102 t 138 * t 97 t 125 * 97 t 

........... ---------°_______________°_....... fl ........ ====fl= ........ ===fl====—= .... fl.'"==_=`===fl==.=_ ....... f 1 

Alpha - BHC 20 U 18 U 16 U 18 U 14 U 18 U 

gamma - BHC (Lindane) 20 U 18 U 16 U 8.8 J 14 U 18 U 

Beta-BHC 20 J 18 U 20 18 U 14 U 64 I 

Heptachlor 19 J 18 U 16 U 18 U 14 U 18 U 

Delta-BHC 20 U 18 U 16 U 18 U 18 18 U 

Aldrin 16 J 18 U 18 17 J 16 11 J.I 

Heptachlor epoxide 20 U 18 U 16 U 18 U 14 U 18 U 

gamma-Chlordane 20 U 18 U 16 U. 18 U 14 U 18 U 

Endosulfan i 20 U. 18 U 16 U 18 U 14 U 12 J 

alpha -Chlordane 20 D . 18 U 16 U 18 U 14 U 18 U 

4,4'-DDS 20 U _ 18 U 16 U 18 U 14 U 18 U 

Dieldrin 20 U 18 U 16 U 18 U 14 U 18 U 

Endrin 20 U 18 U 16 .0 18 U 14 U 18 U 

4,4'-DDD 20 U 18 U 16 U 18 U 14 U 18 U 

Endosulfan II 20 U 18 U 16 U .18 U 14 U 18 U 

4,4'-DDT 20 U 18 U 16 U 18 U 11 J 18 U 

Endrin aldehyde 20 U 18 U 16 U 18 U 14 U 18 U 

Endosulfan sulfate 20 U 18 U 16 U 18 U 14 U 18 U 

Methoxychlor 20 U 18 U 16 U 18 U 14 U 18 U 

Endrin ketone 20 U 18 U 16 U 18 U 14 U 18 U 

Toxaphene 200 U 180 U 160 U 180 U 140 U 180 U 

U= Analyzed, not detected. J- Present below detection limit. B = Present in blank. NR= Not reported. NS. Not spiked. 

t= Percent recovery. D. Diluted out. I- Interference. NA= Not Applicable. *= Outside of EPA CLP QC 

ti 

m

A.ionv", a a,auuracury, iuc. 


RFW Batch Number: 0604L904 Client: THURANFORD RC-047 X0303 work Order: 11343606001 Page: 2 

Cust ID: J11KM4 J11KN5 J11KM6 JllKV1 JllKV2 J11L21 

Sample RFW#: 007 008 009 010 011 012 


D.F.: 4.00 4.00 4.00 4.00 4.00 4.00 


Surrogate: Tetrachloro-m-xylene 122 * t 104 t 173 * t 177 * t 200 * t 124 * k 

Decachlorobiphenyl 101 t 92 t 143 * t 140 * t 155 * t 96 t 

---__...... °__ ......... _________ .......... ___f1 ...... _===== f1=====__=====fl=====_...... fl ...........= f1=====__=====f1 

Alpha-BHC 20 U 15 U 14 U 18 U 14 U 19 U 

gamma-BHC (Lindane) 20 U 15 U 7.3 J 18 U 15 J 19 U 

Beta-BHC 46 19 .1 44 51 38 .I 16 J.I 

Heptachlor 20 U 15 U 14 U 18 U 14 U 19 U 

Delta-BHC 12 J 15 U 14 U 40 14 U 19 U 

Aldrin 12 J 15 J 14 U 14 28 19 U 

Heptachlor epoxide 20 U 15 U 14 U 18 U 14 U 19 U 

gamma-Chlordane 20 U 15 U . 14 D 18 U 14 U 19 U 

Endosulfan I 20 U 15 U 14 U 18 U 9.8 J 19 U. 

alpha-Chlordane 20 U 15 U 14 U 18 U 14 U 19 II, 

4,4'-DDE 20 U 15 U 14 U 12 J 14 U 19 U. 

Dieldrin, 20 U i5 II 14 II 18 U 14 U 19 U: 

Endrin 20 U 15 U 14 U 18 U 14 U 19 U 

4,4'-DDD 20 U 15 II .". 14 II _18 U I 19 U. 

Endosulfan II 20 U 15 U 14 U 18 U 14 U 19 U 

4,4'=DDT 20 U 10 J 14 U 18 U 19 19 U 

Endrin aldehyde 20 U 15 U 14 U 18 U 14 J.I 19 U 

Endosulfan sulfate 20 U 15 U 14 U 18 U 14 U 19 U 

Methoxychlor 20 U 15 U 14 U 32 14 U 19 U 

Endrin ketone 20 U 15 U 14 U 18 U 14 U 19 U 

Toxaphene 200 U 150 U 140 U 180 U 140 U 190 U 

U- Analyzed, not detected. J. Present below detection limit. B= Present in blank. NR= Not reported. NS= Not spiked. 

V- Percent recovery. D- Diluted out. I. interference. NA. Not Applicable. *= Outside of EPA CLP QC 

4 

m 

M 

M 

m

uiuura W ua Wv 06Vcy, auc. 

Pesticide/PCBs by GC, CLP List 

Report Date: 07/07/06 15:01 

RFW Batch Number • 0604L904 Client-, TNUHANFORD RC-047 K0303 Work Order- 11343606001 Page-, 3 

Sample 

Information 

Cust ID: 

RFW#: 

Matrix: 

D.F.: 

JIIL23 

013 

SOLID 

4.00 

JIIL25 

014 

SOLID 

4.00 

J11L36 

015 

SOLID 

4.00 

J11L36 

015 MS 

SOLID 

4.00 

J11L36 

015 MSD 

SOLID 

4.00 

PBLKJM 

06LE0455 -MIDI 

SOIL 

1.00 

m 

mm 

m 


Surrogate: Tetrachloro-m-xylene 81 % 133 * $ 116 % 117 $ 149 * $ 113 $ 

Decachlorobiphenyl 67 $ 109 $ 87 $ 90 $ 135 * $ 97 $ 

............................................. fl== ---------- fl ..... __=.... fl ... ==__=====fl== = ......... fl ............ fl 

Alpha-BHC 16 U 16 U 17 U 76 t 91 $ 0.33 U 

gamma-BHC (Lindane) 7.9 J.I 16 U 17 U 91 $ 112 $ 0.33 U 

Beta-BHC 46 .I 14 J 17 U 91 % 119 $ 0.33 U 

Heptachlor 16 U 16 U 17 U 99 $ 116 $ 0.33 U 

Delta-BHC 16 U 16 U 17 U 68 $ 64 $ 0.33 U 

Aldrin 16 U 16 U 17 U 90 $ 119 % 0.33 U 

Heptachlor epoxide 16 U 16 U 17 U 93 $ 113 $ 0.33 U 

gamma-Chlordane 16 U 16 U 17 U 84 $ 119 $ 0.33 U .. 

Endosulfan I 16 U 16 U 17 U 94 $ 136 * $ 0.33 U 

alpha-Chlordane 16 U 16 U 17, U 94 $ 132 * $ 0.33 U 

4,4'-DDE 16 U 16. U 17 U 95 V 141 * $ 0.33 U 

Dieldrin 16 U 16 U 17 U 91 $ 132 * % 0.33 T ... 

Endrin 16 U 16 U 17 U 111 _ $ 157 * $ 0.33 U 

4;4'-DDD 16 U 16 U 17 ,U 102 t 197 *. % 0.33 U 

Endosulfan II 16 U 16 U 17 II 94 $ 134 *$ 0.33 U 

4,4'-DDT 16 U 16 U 17 U 79 $ 43 $ 0.33 U 

Endrin aldehyde 16 U 16 U 17 U 10 * % 5 * $ 0.33 U 

Endosulfan sulfate 16 U 16 U 17 U 58 * t 28 * $ 0.33 U 

Methoxychlor 16 U 16 U 17 U 107 $ 75 $ 0.33 U 

Endrin ketone 16 U 16 U 17 U 79 $ 72 $ 0.33 U 

Toxaphene 160 U 160 U 170 U 180 U 180 U 3.3 U 

U- Analyzed, not detected. J- Present below detection limit. B- Present in blank. NR. Not reported. NS= Not spiked. 

$. Percent recovery. D. Diluted out. I= Interference. NA. Not Applicable. *- Outside of EPA CLP QC 

m 

CD


RPW Batch Number, 0604L904 Client: TNMLUMORD RC-047 K0303 Work Order- 11343606001 Page r 4 

Cust ID: PBLKJM BS PBLKJM BS 

Sample RFW#: 06LE04SS -MB1 06LE0455-MB1 

Information Matrix: SOIL SOIL 

D.P.: 1.00 1.00 

Units: UG/KG UG/KG 

Surrogate: Tetrachloro-m-xylene 82 $ 94 $ 

Decachlorobiphenyl 90 t 98 t 

.............. ...=...... --- _____________===== fl==........ ..f1-...=__=====fl=====_......fl............ fl .... ........ fl 

Alpha-BHC 62 $ 95 $ 

gamma - BHC ( Lindane) 53 t 100 $ 

Beta-BHC 25 * $ 106 $ 

Heptachlor 75 $ 91 % 

Delta-BHC 4 * $ 103 t 

Aldrin 77 $ 90 $ 

Heptachlor epoxide 35 * t 95 $ 

gamma-Chlordane 64 $ 102 $ 

Endosulfan I 35 * t 106 t 

alpha-Chlordane 73 t 99 $ 

4,4'-DDE 84 t 125 * t 

Dieldrin 16 * t 101 t 

Endrin 19 * t 101 $ 

4,4'-DDD 69 $, 142 * t 

Endosulfan II 5 * $ 101 t 

4,4'-DDT 77 t 141 $ 

Endrin aldehyde 5 * t 95 t 

Endosulfan sulfate 3 * $ 107 % 

Methoxychlor 20 * t 165 $ 

Endrin ketone 4 * t 109 % 

Toxaphene 3.3 U 3.3 U 

U. Analyzed, not detected. J= Present below detection limit. B. Present in blank. NR= Not reported. NS= Not spiked. 

%. Percent recovery. D= Diluted out. I. Interference. NA. Not Applicable. *= Outside of EPA CLP QC 

P 

1^1 ^ 

m 

m

Lionville Laboratory, Inc. 

Extract. Date: 06/02/06 

Test: 0606 

LIMS Report Date: 06/22/06 

SAMPLE EXTRACTION RECORD 

Extraction Batch No: 06LE0455 

Cleanup Date: 06/21/06 

Solvent: DCM,HEXANE 

Analyst: MF 

Analyst: EL 

Sheet no.: 1 

Method: **** ^' 0^3^0 m M 

Client: TNUHANFORD RC- 047 K0303 m M 

Adsorbent: FLORS m 

Client Name Initial Surr. Spike Final Fins bplit uec: a U/u 

Sample No: Client ID WT/VOL Mult. Mult. VOL VOL Mult. YIN Solids FACTOR 

0604L904- TNUHANFORD RC-047 K0303 

001 H J11KK8 2.0 1.0 10 1.0 N 5000.0 

002 H J11KL5 2.20 1.0 10 1.0 N 4545.4 

003 H J11KL6 2.56 1.0 10 1.0 N 3906.2 

004 H J11KM0 2.17 1.0 10 1.0 N 4608.3 

005 H JllKM2 2.86 1.0 10 1.0 N 3496.5 

006 H J11KM3 2.18 1.0 10 1.0 N 4587.2 

007 H JllKM4 2.00 1.0 10 1.0 N 5000.0 

008 H J11KM5 2.67 1.0 10 1.0 N 3745.3 

009 H J11KM6 2.86 1.0 10 1.0 N 3496.5 

010 H J11KV1 2.19 1.0 10 1.0 N 4566.2 

011 H J11KV2 2.86 1.0 10 1. 0 N 3496.5 

012 H JlIL21 2.15 1.0 10 1.0 N 4651.2 

013 H J11L23 2.52 1.0 10 1 .0 N 3968.2 

014 H JlIL25 2.50 1.0 10 1.0 N 4000.0 

015 H JllL36 2.30 1.0 10 1.0 N 4347.8. 

015 HS J11 1, 36 2.18 1.0 1.0 30 1.0 N 0.0 4587.2 

015 HT JlIL36 2.18 1.0 1.0 10 1.0 N 0.0 4587.2 

06LE0455-MB1 H PBLKJM 30.0 1.0 10 1.0 N 100.00 333.3 

06LE0455-MB1 HS PBLKJM 30.0 1.0 1.0 10 1.0 N 100.00 333.3 

Comments: 

Surrogate: 250 UL OLM PSURR 89915602 

Spike: 250 UL FULL LIST PEST SPIKE 89915001B 

s Transferred Relinquished By Date Time Received By Date Time Reason for Transfer {

Lionville Laborato ry Use Only 

1 p Lci() 

Custody Transfer Record/Lab Work Request Page t of a 101vLl 

FIELD PERSONNEL: COMPLETE ONLY SHADEDYEAS 

^1 

See SRC 

Client 714Lk 1-6 ey(-0rp gc-o47 

Est. Final P ro). Sampling Date 

Refrigerator) 

I/rype C 

- m 

on / 

Project# /LAG?(^î^^ ^^'W`7 '^^ 

Project Contact/Phone # 

tainer 

Volume 

Liquid 

L17uld 

Bond 

arm 

m 

Lionville Laborato ry Project C 1 ^Manager 

QC "^ Del J ,TAT l.c, D 

Date Recd Lk ,d 8-0(, Date Dus ^' r" ,^. 

Preservatives -^^ 

ANA LYSES 

REQUESTED -^ O 

> 

OR 

Q 

Z 

In 

NI 

m a 

m 

x 

lj 

D.. - 

INORG 

O 

2 

2 

- 

MATRIX 

1 Lionville Laboratory Use Only j 

CODES: 

Melrla 

Date Time 

n 

S - Son Lab 

OC Matrix 

Client ID/Description 

Chosen 

Collected Collected h 

SE - Sediment ID 

so - Sans 

t31 

c^ ^^ < 

1^ 

SL. Sludge 

CL 

W. Water MS I MSD 

O 

C 

0- Oil 

Air 

A- 

DS 

Drum 

Salida 

DL • Drum 

1 y'S' x 

V 

b 

L*lcw '{aaê f as 

L • EFfrC.P 

LoodialB 

WI • Wipe 

^( X 

X. Other 

F. Fish 

w 

m 

a a 

la 

o3 

x X 

X 

/^ 

x 

X 

X 

mi 

J 5 

j t VnLo 

^( 

X A 

X 

x X 

Special Instruction: 

o to J x x x 

}C^4.1" D NS: 

1 v 

^....- n V r -A'00 1. MAI V ca) C 

i^ t'1i^1 Ct,o p^,r3^ 0.Y. ê -^5t, z. 

(Y1tws PC8,$ voc.. 9. , 

D 

1. go 

^ d *low - eo( S V,; 4JU d uZJJLA-yft1eAa1:S 

PCB, PrS4 Sdoc . Kc^'tjJ^/iA7RtX`— n. 

Re li nqu ished 

by 

Roe~ 

by 

Dale Z 

Relinquished 

by 

Received 

M 

two Time 

Relinquishedd 

.. 

by 

Received 

by 

Date Time 

x 

^^ aYo Zrl3 %; r 

WASTER 

m

I 


b 

Client I J 

Custody Transfer Record/Lab Work Request Page of ---;I- 

FIELD PERSONNEL: COMPLETE ONLY SHADED AREAS 

Refrigerator # 

Est. Final P rol. Sampling Date 

Project # 

Project Contact/Phone # 

A 

_.. 

C 

NRype Comeiner 

Volume 

Liquid 

Lionville Laborato ry Proj 

OC Del 

anger A-06 

TAT 

Prcservetivee 

Sd lid 

Liquid 

I 

IVIVLi M 

Sad m 

ORGANIC INORG 

Date Recd Date Due 

ANALYSES 

REQUESTED —^ p 

> 

Z 

CO 0- 

p 

_ 

m 

Mm 

V 

Z 

j IJemiils laborato ry Use Only 1 

MATRIX 

CODES: 

9 - 505 Lab 

SE- Sedime nt 10 

SO - So 

Client ID/Deacnptlon 

Matrix 

QC 

Chosen 

(^ 

Meolx 

Dale Time 

Colleted Collected 4' 

U) 

-^ 

L',o 

^C1 

VT 

^' 

li 

d 

SL- Sludge 

W- Water 

D. 

% t 

Cl- 

D5 

MS I MSD 

O 0 

C 

A - Air nil, J11y a 

DS. Drum 

solids 

DL- Drum 

Liquids 

L- EPflCLP 

Leaalate 

06L ,) I 

J1 L 13 

s- S0 0 

X 

X 

X " 

X X 

X- ^ 

F- Fish 

Specia l Instruction: 

015 J 11-x(0 ojs X ?^ X 

DATEIREVISIONS: 

c^° ra y%, ' 

I ^_• =(^^ RISC-tY^, (^^' ^ r ^ c ^ c 

J ) / L^ 3. 

RsUnquiehad ReexNad 

Ralingtdehad ReaeWitt! 

DateTim 

Thee 

ReUrtqulshod Retxdved 

by by by by by by 

•d^ 

e. 

5. 

6. 

pale Time 

0 

9 

m

Washington Closure Hanford CHAIN OF CUSTODYISAMPLE ANALYSIS REQUEST RC"047-259 

Po L or 1 

Collector 

Company ContactTelephone No. Protect Coordinator 

TR NLINCI(MAN 

Pelee Code 9]v Data Turnaround 

TILLER, B. JOAN KFSSNER 375.4688 KESSNER, JH 

Proiect Desianadon Sampling Location SAF No. Air Quality q 45 Days 

loo & 300 Are Component of the RCBRA Sediment and Ti 600-13216OD-190 OFFAL RC-047 m 

lee Chest No Field Logbook No. COA Method of Shipment m 

g;ee QZ ^D,J — EL-1595 BESRAS6520 FED ESC l9 

Shipp Offsite Property No.2 Ô^,s>, ? BL L g/Air 111111I No. 

E .LINE SERVICES LIONVIILE 

V.7 J SEE PC 

POSSIBLE SAMPLE HAZARDS/REMARKS 

POTENTIAL RADIOAC77VE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-266 PW I of 1 

Collector Conmany Contact TdeOBone No. Protect Coordinator 

fee 

TRIER, B. TR KLIN K JOAN KESSNER 375.4688 KESSNER, III 

Price Code Data Thrnaund in 

9N ro 

45 Days m 

leer Deshmation 

Semolina I.aeaBon 

$AF No. 

Air Quality 

100 d: 300 Area Component of the RCBRA Sediment and Ti IBBÎFdb OFFAL ^G D 7—//Z 

RC-047 

m 

9 

No. y^L, Flel k No. COA Method of Shipment 

m 

111.11595 I595 BPSRA56520 FED Px m 

SI Oftaite Properly No. ÔÔ^ 2Q BI Bill of Ladisu/Alr Bill No. 

EBEKLINE LIONVI t n ` 7 SEE OSPC 

PO EIJAZARDSMEMARKS 

POTENTIAL RADIOACTIVE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC•047-267 I PASO I of 1 

Collector 

T[tSER, B. TR KLINCKMAN 

Company Contact 

LOAN KESSNER 

Telephone No. 

3 15-1688 

Protect Coordio.tor 

KESSNER, JH Prim Codt 9N Data 1Lrnatrounl^ 

Air Quality q 45 Days 

lect Designa ti on Sa Hxw Lamson SAY No. 

100 A 300 Area Component of the RCBRA Sediment and Ti'. 116-N-3 OFFAL RC-047 m 

r 

Ice Chest No- Field t.oehook Na COA Method of Shiasssml 0 

Shipp 

ER2 SERVICES LIONVI 1 F 

POSSIBLE SAMPLE HAZARDS MFMARKS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-271 j Pw I of I 

onectar 

TR.LER, B. TR NLIN 

^rolect Draienaaon 

100 & 300 Area Component of the RCBRA Sediment and Ti 

Ice Cheat No.r 

t^,eC' 

SI 

BEdR ESERV L10NVnJC 


POTENTIAL RADIOAC77VE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047473 I NP I at l 

Collector 

Company Conta 

TN KLINCKMAN 

ct Tel ep hone No. Protect Coordi nator 00 

Price Code 9N Data Turnarm-st 

TILLER, Bt JOAN KESSNER 375-MBB KESSNER. IH 

rolecl Dex^nW on Sawnslin se Location SAF No. Air Quality q 45 Day, 

100 & 300 Area Component of the RCBRA Sediment and Ti BORROW PIT 24 OFFAL RC-047 ,D 

Field Loabook No. COA Method of Shioment - m 

Ice Chest No. 

xee- ,Z ',3Q,,f^ 

El, 1595 BESRAS6520 FED EX m 

Shipp Ofls1k Property Na / Bi ll orLadiuWAtr Bill No, 

ERUNESERVIM UONVILLE 60 ,3 SEEOSPC 

POSSIBLE SAMPLE IiAZARDS/REMARKS 

POTEN77ALRADIOACTIVE .DOTIJUITS 

Preservation 

- 

Special handling and/or Storage 

Type of Container 

COOL 4C "MATRIX COMPOSED OF MICE" 

No. of Conlalner(s) 

SAMPLEANALYSIS 

Volume 

Is_r-164 W 3c 3 

Samp le No. Mat ri x • Samp le Date Samp le Time - ,; .. 1,. -. 

Coal 4C NO. Car14C Cod IC Cwl4C 0ae14C 

aG G/P a? aG aG AG 

I 1 0 0 0 0 

_2509 109 Ise Sells 509 50g 

See ram(1)u Seesm(Dsr Saaon(3)1n PIs-1012 Pwkides . sm-VOAsms 

W1W Slacbl ant 9270A rTCL) 

Inmanbna Inamlim. 

J11KM2 OTHER SOLID Q 3 Z5,& X +X ' 

18W V 

. _ V,_ WW lit_ 

CHAIN OF POSSESSION 

Relinquished By/Remwed from,y 

E•as L e/ 

'nnui i C'icw 

Doe/17me 

GeV-î 3o 

Date/fine 

Sisnmrint Nam es 

Ell d In 

S 

eive y/Srared In 

Dat^me 

p 

Dm^nn 

w 

SPEC IAL INSTRUCTIONS 

NOTE: FLerane- perform Gamlm Spec Wen auubip b attle to tionvilk La bs, if pmsible nainam 4 C 

cooky. liowilkt patpmneu4.PCB,PFST,SVOC In this ade'aa rxrpleu avaiYIs Caranct Joan 

Kaaaaer upon reeeipl. 

Matrix 

srnhd 

1 

su 

^+• 

Relinquished By snowd From 

^1 /,TOO 

D ae 

ÊU 

ltcciwd By/Sk n 

AA 

(1)Ganarw Spw-tpulllisi)IAerericiom241,Animooy-125,Berylaum7,Ccsiuw134,Cesium-137, 

CaWlt-60.Emapi IS'IEmvpiam154,Evopinm.ISS,Pdmiurn40,Radmm-224,Radim 329. 

W. 

m'' w li B e dprom - 

-^L 

clinquisled By/Rcnvwd From 

D"^'ne 

DatrJFime 

Rec ' B 

Received By 

In 

In 

yÛ 

1 7-y.+10 

;7 

130 ore 

.0` 

DotHFbre 

RulerdurnlOb. Urasawn- 235. (lanum2391 

(2) SUmsiu 89.90 - TOW Sr; hmopic; TbrAan ( T7nr unr232); Isotop ic Unnium I Unnium23323J. 

Ummuro-235. U sasft -2391: hmpie o ROroaitan 

(3) ICP Mwh -6010 tFUR tm) lAlu ii inum. Animooy. Anenk. Barium Beryl) wm Bisnuolt annual 

Cadmium. Cakimlt Owoesimn Cobalt Copper. Ivan. Lcad. fidwaR Magnesium Manganese, 

Molybdenum Nickel, Plospborus, Patassiorn Seknlum SWCOW, Silt y, Sodium Swmhmt TMl9u 111. 

Ten, Unnis m. Vanadium, Zinc); Mercu ry - 7471 - (CV) 

MasprsdW 

rat u. Lam, 

r•TI.^* 

WW'. 

ubwa 

a.V" .a 

X. 

Relinquished ByrRemaved From Duerr," Received aylSiomd in Dolarkre 

S e^/^ -( )c-G ^' C) 7) 

LABORATORY 

SECTION 

Rceived By Title •l'C 

Dale/linx, 

FINALSAMPLE Dirpaal McdW Disposed By Dare fine 

DISPOS IT ION 

SHI-EE-0 11 (08129/2005)

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-274 Par I a L 

Rector 

TILLER, B. TR KLINCKMAN 


JOAN KESSNER 

Telephone No. 

375-4688 

Protect Coordinator 

KESSNER. IN Price Code 9N 

o+ 

Data Turaarour^ 

rolecl Deaianation Samulins Location SAF No. 

100 & 300 Am Component of the RCBRA Sediment and Ti YAKIMA RIDGE 11 OFFAL RC-047 

Ice Chest No. 

D2:Saf 

Air Quality C] 

45 Day m 

Field Logbook No. COA Method of Sldoment m 

EL- 1595 BESRAS6520 FEDP.X m 

hinned TA OffAtc Property No. OOÔ 7 ^ n BID of LadindAir BIII No. 

BERU NESERVIC LK)NVILE /y 7 v SEE OSPC 

POSSIBLE SAMPLE IIAZARDS/REMARKS 

POTENTIAL RADIOA C77VE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-275 wp I of L 

Collector 

T ILLER, B. TR KLINCKMAN 

roiect Deslanation 


Ice Chest No. p 

02 -^ S 

S I 

BEIdN RESBRViCFS ONVRIE 

POSSIBLE SA ZARDS/REMARKS 

P07ENTMLRADIOACTIVE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-276 I Nse I of I 

Ilector 

TILLER, B. TR KLINCKWIAN 

Company Contact Telephone No. 

JOAN KESSNER 375-4688 

Proled Coordinator 

KESSNER, IH Pd«Code 9N Data Turnsroum-' 

N 

Air Quality q 45 DaySm 

sect DeataaaUon Saaoline Lo ca tion SAF No. 

100 A 300 Area Component of the RCBRA Sediment and Ti MOM RANCH OFPAL RC-047 (fl 

Ice Chest No. t^ 

Field Loehook No. COA Method erShlonnent m m 

Pfi G ' O z 

EL-1595 BESRAS6520 FED EX 

SkglilLd To °ffi Pro 

i1e 

p erty No. 

S LIONVILLE 

POSSIBLE SAMPLE HAZARDS/REMA RKS 

POTENTIALRADIOAL77VE

Washin gton Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-277 P-P L of i 

actor 

TILLER, B. N KUNCKNIAN 

roiect Designation 


JOAN KESSNER 

Samollo a Loca 

Telephone No. 

375.4688 

Prolect Coordinator 

KESSNER, III 

price Code 9N 

Air Quality El 

Data TurnaroualN 

N 

45 Days@ 

ti 


on 

SADDLE MOUNTA IN OFFAL 

SAF No. 

RC-047 m 

tee Clint No. 

^^t^ ` Q-z- SV3r 

Field Logbook oo No. 

COA Metbod orshioml 

EL. 1595 BESRAS6520 FED EX 

Sh TO Otfsite Property No. BW of Ladine/Air BIB No. 

BE LINE SERVIC LIONVILLE 14 3 3 D SEEOSPC 


POTEN77ALPADIOAC77VE

Washin)Iton Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-322 Poll- 1 of I 

olleclor 

TILLER, U. 

TR KLIRCKMAN 

Coamanv Contact 

JOAN xessNER 

Telenbone No. 

37s-46// 

Prefect Coordinator 

KESSNER JH 

, 

p ace Cade 

9N 

Data TurnarounN 

45 Days 

Prefect Designation Sampling loca tion SAFNo. 

AirQuty ali El 

100 & 300 Area Component of the RCBRA Sediment and Ti 100-D-48:2 OFFAL RC-047 m 

Ice Cbest No. 

Field Logbook No. COA Method of Shis nsent 

• "C -0,Z E1r1595 BESRAS6520 FED EX 

SW To OfhtlePronertrNo. ^D /D ^^/, 

g/AirBillNo. 

E RIJN LIONVILLE G l/ 

HISEEOSPC 

POSSIBLE SAMPLE HAZARDS.WMARKS 

POTENTIALRADIOACTIVE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-323 Page 1 of 1 

Collector 


ComwnV Contact 

Tdeohone No. 


Prulect C serdhudor 

KESSNER, JH Price Code 9N Data 7ltrnaroslrN 

45 Mpg 

Air Quality 

y 

test Designation Samoiine Location SAF No. 

100 & 300 Am Component of the RCBRA Sediment and Ti [DO-D-49:2 OFFAL RC-047 m 

Ice Chml No. Field Loibook No. CIA Method of Shlmstent m m 

El 1595 BFSRAS6520 FED EX 

Sitipped To OffAtc Properly No. 

ERLME SERVI / LK)NVILLE 


POTEA7MLRADIOAC77VE

Washington Closure Hanford " " CHAIN OF CUSTODY/SAMPLE -ANALYSIS REQUEST RC-047-328 P-P 1 of 1 

Collector Comoanv Contact Telephone No. Protect Coordinator 

TILLER, B. TR KLINCKMAN LOAN KESSNER 375-4688 KESSNER, IH Prim Code Data 9N 

Trrn Yausffl 

in 

roleel Dedenstion Sanmlhan Loca tion SAF No. 

Air Quality p 45 DayC 

100 R 300 Arta Component of the RCBRA Sedim ent and Ti 116-DR-I.DR-21100-D-22 OFFAL RC-047 M 

Ire Chest No. N^3 c ^ 

ii `(- 0 .2 - i9 

Std 

ERLBJE SERVICES LIONVILLE 


Field Leabook No, 

EL. 1595 

OHsile Property No. V lO6O 

COA 

BESRAS6520 

3v 

Method of Shi pment 

FED EX 

Bill of Ladina/Alr Bill No. 

SEEOSPC 

m 

m 


Was1iini:lon Closure Hanford (CHAIN OF CUSTODY/SAMPLE ATIA LYSIS REQUEST RC-047.330 Pnta 1 of I 

Collector 

TTLLER, B. TR KLINCKMAN 

elect Deslanalion 

100 & 300 Area Component of the RCBRA Sediment and Tt 

Ice Chest No. A2 -^pSJ 

Af kC 

Company ContactTelephone No. 

JOAN KESSNER 375.4688 

SomBline Loca tion 

BORROW PIT 23 OFFAL 

Field El 1595 is No. 

BESRAS6520 

Proied Coordinator 

KESSNER, III 

SAP No. 


Method Shinment 

FED F-X 

Price Code 9N 

Air Quality q 

Data Turnarou" 

N 

45 Days" 

0 

m 

CD 

m 

^^ D 3 3 D 

SB Offsite Prooertr No. 2 Big Sdi B Air IB No. 

EBERLINE SERVICES L.IONVRLE 

POSSIBLE SAMPLE IIAZARDB/REMARKS 

POTEIIMAL RADIOACTIVE cDOTLIMf1S 

Special IIandling and/or Storage 

COOL 4C 'MATRIX COMPOSED OF MICE' 

SAMPLE ANALYSIS 

Preselvotion 


No. of Contain er(s) 

Volume 

s^Gs^- KA3U'^ 

Sample No. Matrix • Sample Date Somple Time 

cw14c Nan o,w 4C cow 4[ Coot 4C coni 4c 

aG GIP GIP aG sG a0 

I 1 a o 0 0 

250mL log 15S SOS S0g 568 

Switun Min Sn Nnm(ne ICPMmuh- PWiidn• PM-1011 Smni-VOA- 

SP.M SpmYl 6010(&l Poor 8770A 1T'CU 

1 

Imnue ont. Imt n Lin); 

M__y - 

7471 -(M 

JIIL23 OTHER SOLID R Q 3 /3frJ X K 

CHAIN OF POSSESSION Sign/Print Names SPECIAL INSTRUCTIONS 

Matrix 

NOTE: FLer6au-p erfm Gump Spec does baml tip boale to Lionville 

Relinquished BY/Retnossd 

laba, Upon" nisimain 4 C 

e•vl 

From /^ Daadfirre vy 

Dmrjme 

In ow—_ 

coo ling. L2umole: parum mls, ea PCBPS ,PTSVOC in sus urdcr as samplele 

EAS LOCKED STO C y -(a'jv aniu Conran Con Jean 

O r7 

slit d.s 

Kusrty upon mgip[. so-sda 

us As4elrtored' (,..IeA/ Dame 

ReeeisM BY/Smned In Datelrinrc sasu4s 

UU 

y - G (1) Game Spec- (Full Usti (Americium,241. Aadmony-1 25, BerYl ium7, Cfth m 134, Cesiurrv137, 01 

v 

Cebali-60, Eaapbu 152, FAt Wk p 154, Eaopium 155, Paarsium-40, Radinm226, Radiumng, wdi 

Rclinquis dB etmeed Front DaWI'mx 

Recdred By N ^rc 

Raheahan106,Unnho 235,Uranium^23 11 ) ôs.pun,r,m, 

(2)Sooai.49,90 - Total Sr, lsotopie Thorium JT7wrium-232 1 : Isotopic Ura ni um(Urariltm!33PU, ol.Oam L npw 

Dmtda M. Umwum-251 1; hsnayie Pusonium 

T•T .. 

Rel i d B e eve From 

Retzived B d In. none 

h ex e$cw*^ y^r^ 6 Êi^) 

- Fv r.P.. 

Reli wahe /Re Rpm Datertine B In 

^( a^3o 

• 

Relinquished By/Rennrcd From L1areTime Received By d In 132MMW 

^GiuL (^C 3G^ 

LABORATORY Received By Title DrteMvne 

SECTION 

FINAL SAMPLE Disposal Method IRspucd By DatelTime 

DISPOSITION 

RHI-EE-011 (08/29/2005) 

% Ono

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047.332 peso -I 1 

ollector 

TI LER, n. TR KLINCKMAN 

roieetDestin ation 

100 lit 300 Area Component of the RCBRA Sediment and Ti 


JOAN KESSNER 

SamulituLoation 

600- 131 OFFAL 

Telephone No. 

375.4688 


- 

ID;SSNP.R, JH Prim Code 9N Data Tur tarsti- 

SAFNo. 


45 

Air Quality E] Daysm G) 

Ice Cheat No.//^^â Field Logbook No. COA Method or Shhument m 

'Age- ^ (f L7,,,$^ EL-1595 BESRAS6520 FED EX m 

Shlnped To OMIte Property No. Bill Ladino/Air Bill No. 

INESERV 1LIONVIILE . 06033v SEE OSPC 

POSSIBLE SAMPLE IIAZARD6/REMARKS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS RE WEST RC-047-343 1ka 2 of 1 

olleclor 

TILLER. B. TR KLINCKMAN 

Company Contact Telt Rahn No. 



KF-SSNER, JH Price Cade 9N 

Data Tumamuna0 

(y 

oiect Desiamtion Samnlna Laration SAF No. 

Air Quality E] 

45 Days m 

100 & 300 Area Compon en t of the RCBRA Sediment and Ti CENTRALPL.ATBAU SHRUB STEPPE OFFAL RC-047 m 

Ite Chest No.rQ 

Field Logbook No- COA Method of SWotllmt m 

, L EL-1595 BFSRAS6520 FED EX 

m 

^—QZ -'^,S 

5W Offsite Properly No.^^^^jj 

14 O 

6 D 

BERLBJE SERVICES LIONVILLE 

POSStIlMNIVERE HAZARDSMEMARKS 

33p 

Bid of Ladina/Air Bill No. 

SEE OSPC 


SR-002-B 

13. VOA, TOC, TOX free of headspace? 

14. QC stickers placed on bottles designated by 

client? 

15. Shipment meets LYLI Sample Acceptance 

Policy? (identify all bottles not within 

policy. See reverse side for po licy) 

16. Project Manager contacted concerning 

discrepancies? name/date (or samples 

outside criteria) 

vLl 

Lionville Laboratory Incorporated 

SAMPLE RECEIPT CHECKLIST (SRC) 

r 

CLMNT: 'T^1U. ^r c- Date: 

MV,,/Beatch#: 

Order / Proj ect# / p 

OW# I Release #: R)c - p^^l 

C)( 

1. Samples Hand Delivered."r Shipped 

2. Custody seals on coolers or shipping 

container intact, signed and dated? 

3. Outside of coolers or shipping containers am 

free from damage? 

4. All expe ct ed paperwork received (coc and 

other client specific information) scaled in 

plastic bag and easily acce ssible? 

o ^^L^ 1 Sample Custodian: 

NOTE: EXPLAIN ALL DISCREPANCIES 

S. Samples receiv cool r ambient? Z ) 

6. Custody seals on sample containers intact. 

signed and dated? 

7. coc signed and dated? 

a. Sample containers are intact? 

9. All samples on coc received? A ll samples 

received on coc? 

10. All sample label information matches cm? 

11. Samples properly preserved? 

12. Samples received within hold times? 

Short holds taken to wet lab? 

Sd Yes O No 17 No Seals 

res O No 

Jd Yes 0 N 

/O'-- ONo 

t(Yes O No 

Yes ONO 

lW 

J2(Ycs q No 

O Yes 

O Yes 

O Yes 

aYes 

• No IldN/A 

• No CIA 

0 N 11 

i er^F,. 

13 No 

Airbill# '7ga7 x565 1" 

[YYes O No O No Seals Comments 

//4 Yes q No 

7 

Yes O No 

Temp —T - 3 °C Cooler # SA LOS-1b_:^) 

ONO 

D'+satpaocics 

000000029

PBLKJM MB1 

PBLKJM MB1 BS 

Lionville Laboratory, Inc. 44 2 

PCB ANALYTICAL DATA PACKAGE FOR 

TNUKANFORD RC-047 K0303 

DATE RECEIVED: 04/26/06 LVL LOT # 

CLIENT ID LVL # MTX PREP # COLLECTION EXTR/PREP ANALLYSIS 

J11KK8 001 SO 06LE0455 04/05/06 06/02/06 06/22/06 

Ji1KL5 002 SO 06LE0455 04/05/06 06/02/06 06/22/06 

J11KL6 003 SO 06LE0455 04/03/06 06/02/06 06/22/06 

J11KM0 004 SO 06LE0455 04/05/06 06/02/06 06/23/06 

J11KM2 005 SO 06LE0455 04/03/06 06/02/06 06/23/06 

Ji1KM3 006 SO 06LE0455 04/03/06 06/02/06 06/23/06 

JL1KM4 007 SO 06LE0455 04/03/06 06/02/06 06/23/06 

J11KM5 008 SO 06LE0455 04/03/06 06/02/06 06/23/06 

J11KM6 009 SO 06LE0455 04/03/06 06/02/06 07/06/06 

J11KV1 010 SO 06LE0455 04/05/06 06/02/06 06/23/06 

J11KV2 011 SO 06LE0455 04/05/06 06/02/06 06/23/06 

JlIL21 012 SO 06LE0455 04/03/06 06/02/06 06/23/06 

,7111,23 013 SO 06LE0455 04/03/06 06/02/06 06/23/06 

JIIL25 014 SO 06LE0455 04/05/06 06/02/06 06/23/06 

JlIL36 015 "S0 06LEb455 04/03/06 06/02/06 06/23/06 

J111,36 015 MS So 06LE0455 04/03/06 . 06/02/06 06/23/06 

JIIL36 015 MSD '96"06LE0455 04/03/06 06/02/06 06/23/06 

LAB QC: 

N/A 

N/A 

06/02/06 

06/02/06 

06/22/06 

07/06/06 

000000001


Client: TNU-I IANFORD RC-047 W.O. #: 11343-606-001-9999-00 

LVL #: 0604L904 Date Received: 04-28-2006 

SDG/SAF # K0303/RC-047 

PCB 

Fifteen (15) solid (composed of mice) samples were collected on 04-03,05-2006. 

The samples and their associated QC samples were extracted on 06-02-2006 and analyzed 

according to Lionville Laboratory SOPs based on SW846, 3rd Edition procedures on 06-02,23- 

2006. The extraction procedure was based on method 3540C and the extracts were analyzed based 

on method 8082. 

The following is a summary of QC results accompanying the sample results. Lionville Laboratory 

Inc (LvLI) certifies that all test results meet the requirements of NELAC except as noted below: 


acceptance policy with the exception of some discrepancies, which were documented on 

the Sample Receipt Checklist. 

2. The samples were received outside extraction holding time. All samples were extracted 

outside holding time due to the refrigerator (ID # R003) malfunction. A copy of the 


3. The soil sample results were reported on a wet-weight basis. All samples were extracted 

using reduced sample volume due to the nature of the sample matrix. A copy of the 

Sample Extraction Record has been enclosed. 


5. One (1) of thirty-eight (38) surrogate recoveries was outside acceptance criteria. A copy of 

the Sample Discrepancy Report (SDR) has been enclosed. 

6. All blank spike recoveries were within acceptance criteria. 

7. All matrix spike recoveries were within acceptance criteria. 


The results presented in this report relate only to the analytical testing and conditlom of the samples at receipt and during storage. All pages of this report are integral parts of 

the analytical data. Therefore, this report should only be reproduced in its entirety of 2 7 pages. 


nefnneos+r.-r

9. The continuing calibration standards analyzed prior to sample ex tracts were within 

acceptance criteria. 

10. LvLI is NELAP accredited by the state of Pennsylvania and holds over 20 additional state 


analytes/methods, please contact your Project M anager. 

11. I ce rtify that this sample data package is in compliance with SOW requirements, both 

technically and for completeness, other th an the conditions detailed above. Release of the 



lain paniels ^ 

Lab ratory M anager 


s m\r:\group\data\pesknu hmford\0604-904.pebs 


_)/010 4. 

Date 

c7

Lionville Laborato ry Sample Discrepancy Report (SDR) SDR#: 8 16 be ' L 4, 

Initiator Jo %N. Batch: 

Parameter. PY s3 , P UR 

Date: 'T1-1 to 6 

Sampl Matrix: •. d w t 

Client: Ttv.J Metho Prep Batch: nb e o^,^ 

4-E=e 


a. COC Discrepancy _Tech Profile Er ror Client Request — Error on C-O-C 

Transcription Error _ Wrong Test Code Other 


Missing Sample/Extract _ Container B roken —Wrong Sample Pulled _ Label ID's Illegible 

Hold Time Exceeded _ Insufficient Sample _ Preserva ti on Wrong _ Received Past Hold 

_ Improper Bottle Type _ Not Amenable to Analysis 

Note * : verified by [Lo In] or [Prep Group] (circle)... signaturaldate: 

c. Problem (Include all relevant specific results; attach data if necessa ry ) 

It 

sr%^ tf rf G mot! 11 af'T /'f cJ .....t.^k a Z 


3. Discussion and Proposed Action Other Descrip ti on: 

_ Re-log 

_ En ti re Batch 


_ Re-leach 

_ Re-extract 

_ Re-digest 

_ Revise EDD 



4. Project Manager Instructions ... signature/date: 

Concur with Proposed Action 

_ Disagree with P roposed Action; See Ins truction 

_ Include in Case Narrative 


Date/Person 

_ Add 

Cancel 

5. Final Ac tion... signature/date: 

— 

Other Explana tion: 

Verified re-[log][leach][extractildigest][an y0sl 016e) e) 

_ Included in Case Narrative 

_ Hard Copy COG Revised 

Electronic COG Revised 


When Final Action has been recorded, forward original to QA Specialist for distribu tion and filing. 

Route Distribution of Completed SDR Route Dis tribu ti 

X Ini 


ti 

ator 

X Lab General Manager. M, Taylor 

X P roject Mgr. Stone/Johnson 

Data Management: S 

_ 

_ _ Metals: Beegle 

_ _ Inorganic: Perrone 

_ _ GC/LC: IGger 

ti 

lwell 

_ Sample Prep: Beegle/Kiger 

_ MS: Rychlak/Daley 

_ _ Login: Per ry 

Admin: 


QA-105-A-0805 

4û 1 

wl^ 

7/7/6 

000000004

Lionville Laboratory Sample Discrepancy Report (SDR) SDR #: 06PM001 

Initiator. Odette Johnson Batch: T Parameter: AW AVA, Y°^ 

Date: /1706 Samples: Mat ri 

x: 

Client: Method: swaesnacAVVwrcm P rep Batch: 


a. COC Disc repancy _ Tech Profile Error _ C li 

ent Request Sampler Error on C-O-C 

Transcription Error _ Wrwg Test Code _ Other 


_ Missing Sample/Extract _ Container B roken Wrong Sample Pulled _ Label ID's Illegible 

Hold Time Exceeded 

Improper Bot 

Insufficient Sample Preservation Wrong _ Received Past Hold 

tl 

e Type _ Not Amenable to Analysis X Other 

Note: Verified by [Log-In) or [Prep amp[ (drde) ... signeture/daw. 

c. Problem (Include all relevant specific results; attach data If necessa ry) 

On 5110/06 sample storage refrigerator ID# R003 malfunctioned and was not holding the required sample storage 

temperature of 4'C +/- 2°C 

2. Known or P robable Causes(s) 

Broken motor 

3..Discuss[on and P roposed Action.... Other Description: 

_ Re-log At the time of malfunction R003 was used for storage of samples received 

_ Entire Batch for extractable organics, metals and wet chemist ry (except TOC) analyses. 

Following Samples: All samples were removed from R003 to another refrigerator on 5/10/06. 

_ f e-Ieach R003 was tagged out on 5/10106, repaired on 5/12/06, and we have 

_ Re-extract certified that R003 is maintaining the required sample storage temperature. 

_ Re-digest 

_ Revise EDD 



4. Project Manager Instructions ... signaturefdate: 

Concur with P ro posed Action 

gree with Proposed Action; See Instruc 

r 

ti on 

^/ nclude in Case Narrative 

Client Conte 

Date/Person î del l.t^ fGy^D^p 

_ Add 

Canoel 

S. Fine -Acdon..sgnatureaate: 

nfied re-[log][leach][extract] 

KÎhcluded in Case Narrative 


Electronic CDC Revised 

_ EDD Co 

est)[analysi ] circi ) 

Other Explanation: 

rr ec ti 

ons Completed 

When Final Action has been recorded, forward original to OA Specialist for dis tribu tion and filing. 

Route Distribution of Completed SDR Route Distribution of Completed SDR 

X Initiator _ _ Metals: Welsh 

X Lab Manager. I. Daniels Inorganic: Perrone 

X Project Mgr. Stone/Johnson _ GC/LC: IQger 

Data Management: Stilwell _ MS: Schneider/Daley 

_ Sample Prep: BeegleNger _ Log-in: Per ry 

Admin: 


oA-105-A-DW5 

069960005

19 

rNnn1r L10oFAIOF'r /^' 




sample (not the method detection limit) is reported with the U (e.g., IOU). 

Indicates an estimated value. This flag is used in cases where a target analyze is dete cted at a level 

less than the lower quantification level. If the limit of quanti fication is 10 ug/L and a concentra tion 

of 3 ug/L is calculated, it is reported as 31. 

B = 'Ibis flag is used when the analyte is found in the associated blank as well as in the sample. It 

indicates possible/probable blank contamination. 

E = Indicates that the compound was dete cted beyond the calibration range and was subsequen tly 

analyzed at a dilu tion. 


I 

ABBREVIATIONS 

Indicates an interferen ce on one analytical column only. Result is reported from remaining analytical 

column. 

BS = Indicates blank spike in which reagent grade water is spiked with the CLP matr ix spiking solutions 

and carried through all the steps in the method. Spike recoveries are reported. 

BSD 

Indicates blank spike duplicate. 

MS = Indicates matr ix Spike. 

MSD = Indicates matrix spike dup li cate. 

DL = Indicates that recoveries were not obtained because the extract had to be diluted for analysis. 

NA = Not Applicable. 

DF 

Dilu tion Factor. 

NR = Not Required. 

NS = Not Spiked. 

SP = indicates Spiked Compound. 

P _ This flag is used for an PEsnCIDE/PCB target analyte when there is greater than 2S°/, 

difference for detected concentra ti ons between the two GC columns (see Form X). The 

lower of the two values Is reported on Form I and flagged wi th a "P". 

D = This flag identifies all compounds identi fied in an analysis at a secondary dilution factor. 

C = This flag applies to a compound that has been confirmed by GOMS. 

NPM = 

No pattern match for multi-component target analytes. 

000000006

PCBs by GC,Report Date: 07/10/06 11:35 

RFW Batch Number: 0604L904 Client: TNUBANPORD RC-047 K0303 Work Order, 11343606001 Paae • 1 

Cust ID: J11KK6 J11KL5 J11KL6 J11KM0 J11KM2 J11KM3 

Sample RFW#: 001 002 003 004 005 006 


D.F.: 1.00 1.00 1.00 1.00 1.00 1.00 


Surrogate: Tetrachloro-m-xylene 93 $ 85 $ 71 t 87 % 78 $ 105 & 

Decachlorobiphenyl 102 $ 88 $ 92 % 90 % 97 Ir 104 $ 

. . ............. . ........... _____________===== f1...... =====-fl===°=_=== ... f1 ..... ___==== £1=====__===== f1=====__='==°fl 

Aroclor-1016 200 U 180 U 160 U 180 U 140 U 180 U 







Sample 

Information.: 

Cust ID: J11KM4 JllKM5 J1lmd Ji1KV1 JllKV2 J111,21 

RFW#: • 007 006 009 010 011 012 

:Matrix: SOLID '.SOLID' SOLID SOLID SOLID SOLID- 

D.P.: 1.00 1.00 .1.00 1.00 1.00 1.00 

Units: UG/KG UG/KG /KG UG/KG UG/KG UG/KG 

Surrogate: Tetrachloro -m-xylene 100 $ 88 % 100 % 120 * $ 105 $ 93 $ 

Decachlorobiphenyl 97 $ 83 $ 96 $ 116 $ 107 $ 99 $ 

....... ...................................... fl ...... _=====fl==== ........ fl --- ......... fl............ fl............ fl 


Aroclor - 1221 200 U 150 U 140 U 180 U 140 U 180 U 




Aroclor - 1254 200 U 150 U 140 U 180 U 140 U 180 U 


U= Analyzed, not detected. J- Present below detection limit. B. Present in blank. NR= Not reported. NS= Not spiked. 

$= Percent recovery. D= Diluted out. I= Interference. NA= Not Applicable. *• Outside of EPA CLP QC U^r 

ti 

m 

m 

m 

G 

m 

CD

PCBs by GC Report Date: 07/10/06 11:35 

RFW Batch Number: 0604L904 Client: TNQBANFORD RC -047 K0303 Work Order: 11343606001 Paae• 2 

Cust ID: JlIL23 J111,25 JlIL36 JIIL36 JlIL36 PBLKJM 

Sample RFW#: 013 014 015 015 MS 015 MSD 0GLE0455-MB1 

Information Matrix: SOLID SOLID SOLID SOLID SOLID SOIL 

D.F.: 1.00 1.00 1.00 1.00 1.00 1.00 


Surrogate: Tetrachloro-m-xylene 93 W 95 8 87 t 103 t 100 %. 82 t 

Decachlorobiphenyl 94 t 112 93 %- 108 W 98 t 88 %, 

........_____________====fl..===._,..... fl.=..=_.=.... fl............ fl ......... ...fl --- .----- =..fl 

Aroclor-1016 160 U 160 U 180 U 100 $ 94 $ 13 U 




Aroclor-1248 160 U 160 U ISO U 180 U 180 U 13 U 


Aroclor-1260 160 U 160 U :180 U 104 W 96 13 U 

Cust ID: PSLKJM BS 

Sample RFW#: 0M0455-MB1 

Information Matrix: SOIL 

D.F.: 1.00 

Units: UG/KG 

Surrogate: Tetrachloro-m-xylene 94 W 

Decachlorobiphenyl 88 % 

............................................. fl ... = ........ fl. ....... = .... fl ............ fl=====__=====fl.=.......... fl 

Aroclor-1016 80 t 

Aroclor-1221 13 U 





Aroclor-1260 81 t 

U= Analyzed, not detected. J= Present below detection limit. B. Present in blank. NR= Not reported. NS= Not spiked. 

W= Percent recovery. D= Diluted out. I= Interference. NA= Not Applicable. •= Outside of EPA CLP QC 

1 

m 

CD 

M 

G 

m


Extract. Date: 06/02/06 Extraction Batch No: 06LE0455 Analyst: MF 

766L: 3FCF) Cieaiiup Z, Lc: Ai.alyst: iiF 

LIMS Report Date: 07/10/06 Solvent: DCM,HEXANE 

Sheet no.: I 

Method: **-• m mm 

Cl RC-,47 K0333 

m Adsorbent: FLSLA m Client Name pH Initial surr. Spike Final Final Split GPC % C/D 

Sample No: Client ID WT/VOL Mult. Mult. VOL VOL Mult. Y/N Solids FACTOR 


001 J11KKB 2.0 1.0 10 1.0 N 0.00 5000.0 

002 J11KL5 2.20 1.0 10 1.0 N 0.00 4545.4 

003 J11KL6 2.56 1.0 10 1.0 N 0.00 3906.2 

004 011KMO 2.17 1.0 10 1.0 N 0.00 4608.3 

005 J11KM2 2.86 1.0 10 1.0 N 0.00 3496.5 

006 J11KM3 2.18 1.0 10 1.0 N 0.00 4587.2 

007 J11KM4 2.00 1.0 10 1.0 N 0.00 5000.0 

008 J11KM5 2.67 1.0 10 1.0 N 0.00 3745.3 

009 J11KM6 2.86 1.0 10 1.0 N 0.00 3496.5 

010 J11KV1 2.19 1.0 10 1.0 N 0.00 4566.2 

011 JllKV2 2.86 1.0 10 1.0 N 0.00 3496.5 

012 JlIL21 2.18 1.0 10 1.0 N 0.00 4587.2 

013 Ji1L23 2.52 1.0 10 1.0 N 0.00 3968.2 

014 JlIL25 2.50 1.0 10 1.0 N 0.00 4000.0 

015 J111,36 2.17 1.0 10 1.0 N 0.00 4608.3 

015 -S J111,36 2.17 1.0 1.0 10 1.0 N 0.00 4608.3 

015 -T J111,36 2.18 1.10 1.0 10 1.0 N 0.00 4587.2 

06LE0455-MB1 PBLKJM 30.0 1.0 10 1.0 N 100.00 333.3 

06LE0455-MB1 -S PBLKJM 30.0 1.0 1.0 10 1.0 N 100.00 333.3 

Comments: 

Surrogate: 250 UL OLM PSURR 89915801 

Spike: 250 UL AR1660 89915602 

(Extracts Transferred I Relinquished By Date Time Received By Date Timei Reason for Transfer 

m

Lionville Laborato ry Use Only Custody Transfer Record/Lab Work Request Paget of of lu^ LI 

Est. Final Prol. Sampling Date 

Project # !^ l-,yl _^^/^rJ- of 

Project Co rdacUPtwne # 

Lionville Laborato ry Project Manager 

QC Del ^T d TAT 

Date Recd Lk •d s o(, Dale Due .^/J 71 '/rt'-" 

MATRIX 

CODES: 

S- Soli 

SE • Sediment 

Letr 

ID 

SO - So li 

d 

SL • Sludge 

w - Wafer 

O- oil 

A - J it 

DS- Drum 

Scads 

OIL- Drum 

Liquids 

L- EP/TCLP 

Leschele 

an • wipe 

X • Other 

F- Fish 

Client ID/DaaMpllon 

FIELD PERSONNEL: COMPLETE ONLY SHADED /AREAS 

See SRC 

/^ m 

u 


#Mpe Conminer 

volume 

Preservatives 

ANALYSES 

REQUESTED 

Liquid 

So lid 

Liquid 

So li 

d 

c 

ac 

Chosen 

d" 

Date Time 

Col le 

cted Collect 

10 to lJ1116V 1I 1 1. 4 I'll 

Special Instructions: V'VL =CQn', lic"A\¢,L DNS: 

^l'^YTLÎ p t^L 

mC^cy15 , PCQ , SiÔC . * 

`l-d^4^ cto.Dw `''`.r3, aY. le.-Pes^^ z. 

Me- A-CJS PCB, PCIA, SVOCL . K' 

ReanquleMd Roe~ 

by r by 

Onto 

Time 

1,1 

3. 

4. 

>I a^=lal III 

j LloWlis Laboralory U se 

X, 

r/ 

Re linquished wed 

by by 

,.;QMP0.sjJ 0 f 

WASTE" 

CD 

CD 

J Î•^^^ /^Jr 

Dale Time


Custody Transfer Record/Lab Work Request Pag e—I.4- of ---^l 

^V^1 

b a ^ô^- 

I- 

FIELD PERSONNEL: COMPLETE ONLY SHADEDREAS 

m 

C lient r^ C °" m 

Est. Final P ro). Sampling Date X/type Container 

liquid 

S 

m' 

m 

Project # 

Project GontaeVPhone # 

^^ 

(J 

vaum. 

LigWd 

- 

m 

Lionville Laboratory Pro] 

OC Del 

- anager 

TAT 

G 

- 

Preservatives 

Solid 

ORGANIC INORG 

ANALYSES 

Date Recd Date Due 

REQUESTED -^ O 

> 

Z 

m 

Amy 

a q I E U 

MATRIX 

1 LbrMae laboratory Use Only 1 

CODES: 

matrix 

S. SON 

SE. Sedent im 

SO - Sae 

SL- Sludge 

W. Water 

ob 

C lient ID/Descrlptton 

OC 

Chosen 

In 

Matrix 

Date 

Collected 

T[ma 

Copxlea ^S 

:^ 

V+ 

O 

$ 

`' 

VT 

h 

Y] 

O O- oil 

MS I MSD 

à 

A - Air 

DS- Drum 

Solids 

DL. 

o 

NJ 

oZ^ - + 

L- EP/TC I. 

WI Woe 

^^ Lai a - , ..:: -x 

-.. x -. 'x -K 

PLeadwe s so o x t x 

X - Other 015 J 1 ^—ZG 015 X x X 

F - Fish 

Special Instructions: 

DATEMEMSIONS: 

`SL. "r.J^ 1rL l r j )" f lir 2. 

r^^r^^^ 

J 7 r(L 3. 

ReiingWehed Received 

Deis Thrre 

Refirmpieiled Received 

.Data Time 

Re li by by by M 

nquished 

by 

Received 

by 

1 y 

4. 

5. 

8. 

Ow 71rM

Washineton Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS RE VEST I RC-047-259 JPPF I -f 1 

Collector 

TR KLiNCKMAN 

TILLER, B. 

Company ContactTelephone No. 

JOAN KESSNBR 375-4688 

Proleel Coordinator 

KESSNFl2, IN 

Price Code 9N Data Turnaround 

45 Days m 

Project Designation 

100 & 300 Arcs Component of the RCBRA Sediment and Ti 

Sampling Location 

600-1321600-190 OFFAL 



Air Qualify [] y m 

m 

lee Chest No y Field Loebook No. COA Metiaod of Shinmeat m 

^^_ 133.111595 BESRAS6520 FED EX 0 

Sl pv OfTsile Properly No. ^ 7 Bi ll of lAdiwJA ir Bill No. 

RLINE SERVIC5 LIONVILLE 1-99464!f 7 2 d SEE OSPC 

POSSIBLE SAMPLE HAZARDS/BEMARKS 

POTEKTIALRADIOACTIVE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-266 g F J or s 

(lector 

TILLER, B. TR KLINC 


JOAN KESSNER 

Telephone No. 

375-4688 

Proled Coordinator 

KESSNER, JH Price Cade SIN 

Dafa Turnaround M 

roieel Designation Sampling Loca tion 


100 & 300 Area Component of the RCBRA Sediment and Ti .1004f-Iii, OFFAL] ^G O ^^}.Z 


Ice ChatNo- 

Âe / ' 

Fid No. COA Method of Shiosnenl 


SI Ta Oftyite Properly No. Big of Lodinx/Air Bill No. 

EBERNE LI 

LIONVU.F ^906a33 40 

SEE 

POS E RAZARDSIREMARKS 

POTEMIALRADIOACTIVE DOTLIMITS 

SpecialIfandlinganNorStorage 


SAMPLE ANALYSLS 

Preatrwlion 


No. of Conlailter(s) 

Volume 

spry koao_3 

c v44C None Ce"I/C C °"1K Gautac I C- 1 4C 

AG GIP GIP aG aG aG 

( ) o a a a 

250& log 15g 306 505 50S 

Swean( I) in Sxitem(2) k Sw G)m PCBs -1082 Patietlw- Snoi-VOA- 

Sprciw Spxid Spaial SRI 9270A(TCL) 

1.100. I,wwiow. Immnb"s 

A.ir QusRty 

Sample No. Mat rix Sample Date Sample Time 4 ._,-I - - , ,• r 

b 

J11KL5 OTHER SOLID APR 0 5 2006 Ci X h 

45 Days m 

CHAIN OF POSSESSION Sign/Print Names SPECIAL INSTRUCTIONS 

NOTE: Fbedi w. peripm Gamto Spec th 

Matrix 

Relinquished By/Ringd Fiwn Date/(Imev a y/51ap111n /t^ _ Oy DaleJlitee 

en m nship hank b Lionville Lahs, if pwsbk rmimin d C 

.6l. 'ms's 

O 

A LOCKED STO AGE y' 

io i(3o coding. Lionville: perform acing. PCB,PESTSVOC is Bds order as snopk is available. Contact loan Kessner upon receipt. 

>.^ 

Rhe4 9nn &.e,# Daternnm Received By/Stored In Date/fme 

y/ 

swsgv' 

(1)Gamm Spec-(Pollliag lAmericium yAl, Andmany-125, Be W.W. 

rylliuna7,Cesium134,Cesiuml37, 

Cobalt-6t1.Fjumpivn•15? rsuo pium154.rar*um155,Pdassium4O.Radhw 226,Radhw 221- o'nl 

Relinqu ished By/Re fran.J; Dw sce Received By/St o 

Ina 

q^ Rulhemun- 106, Undmo-235, Unrliuo-2181 

apa,pmsoar 

r^ as I ' "N (2) Shonimn89,90 -- Total Sr, Isoto pic Thorium I Thmium2J'_): Isotopic Uranium I UmmInt-233P34, p.an.n ewe, 

Unnirwa233, Unnom2J g 1: isdopie Pouor:um 

T.T. 

Retie d By p d IeT 

Received ByfSlmd In Da me 

ttO 

(3) ICP Mpsk 7I - 60101PWI IJsU ( Aluminum Animoily. Anenk, Buiam Beryllium, Bum FPO ph, Koran, 

wl.ww 

tx ' Gdmium Calcium, Cnorlwuo Coba lt, Copper. Iran, lend, Ulh)um Magnesiwn Man 

I}raeao 

Ppar, 

v.vam,. 

Relirq hed tl /Renaved DatNl'ine Reai B d In Date?ime Molybdenum Nicke l. Phosplmus, Porassivm Selenium Sikcoa Silver, Sodium Stmnims Tlullus, x.oue 

QC Tin, lhlftii , Vanadium 2'iwl: Mercury - 7471 - (CV) 

Relinquished Byl itemoved From DakTne Reaped By d in Date(fine 

S' 

azV 

^Q 30 3 

LABORATORY Rea).ed By Tit le UatoTme 

SECTION 

FINAL SAMPLE Disposal Me th od Disposed By Danrtime 

DISPOSITION 

BHI-EE-011 (0812912005) 

m 

m 

m

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS RE QUEST RC-047-267 P+6e L 4t I 

Collector - 

TILLER, B. iR KLINCKMAN 

Comoan Contact 

JOAN KESSNER 

Telephone No. 

375-4668 


KESSNER, JH 

Code 9N Data Tntvutrouata 

lect Deienaaon Swmlim Location SAF No- 

Air Quality q 

45 Days m 

100A 300 Area Component of the RCBRA Sediment and Ti ' 116-N-3 OFFAL RC-047 m 

Ice Chest Na Field Loabook No. OA Melted of S1Jlrmwl m 

EL-1395- BESRAS6520 FED EX 

m 

Shipa 

ERl.B4E SERVICES LIONVIILE 

POSSIBLE SAMPLE IIAZARDS/REMAR IIS 


Washington Closure Hanford CHAIN OF CUSTODYISAMPLE ANALYSIS REQUEST I RC-047-271 1 pir 1 of I 

Collector Company Contact Telephone No. Proled Coordinator uIf77 

price Code 9N 

Data Turnarons,,.i 

TILLER, B. TR BLIN JOAN KESSNER 375 -4685 KESSNER, JH 

m 

rolect Designation Sawlina Lwalkn SAF No. 

45 

A it Quality q Days 

100 & 300 Area Component of the RCBRA Sedim en t and n 1607.D2:1 OFFAL RC-047 

Ice Chest No./^ r 

fJ 

4rRC' eQ - 

Field Loabook No. COA Method of Shipment m 

EL-1595 BESRAS6520 PEDEX m 

S1 Offsile Property No. AOIO l 2^ Bill of Ladf WAir BBI Na 

ERLINESERVICES LK)NVIUE /^ P JJ SEEOSPC 

POSSIBLE SAMPLE WARDS/REMARKS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS RE VEST RC-047473 Ra t i 

Collector 

Company Contact Telephone No. Protect Coordinator 

TILLER, B. TA KLINCKMAN 

JOAN KESSNER 375-4688 KESSNER. JH 

Price Code 9N 

Data urnarou T^f 

Protect Dellenation 

100 &300 Area Component of the RCBRA Sediment and Ti 

Satnotine Loca tion 




Air Quality E] 45 Day (OD m 

Ice Cheat No. pry 

/Z ,C ^- 

L ,+ 

,z ' 3 QJ 

Field L.nehook No. 

EL-1595 

COA 

DESRAS6520 

Method of Shipment 

FED EX 

- 

m 

m 

Shlu ORsue Property No. O O 

B ll OL S A ir BillI N 

BERLINE SERVICES LIONVILE /^^^ 

POSSIBLE SAMPLE IIAZARDS/BEMARKS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047.274 P4a I or 1 

Collector 

TRIER, B. TR KLINCKMAN 

Cotma tv Contact 

JOAN KESSNER 

Telephone No. 

375-4668 

Protect Coadb a w 

KESSNER, IN Price Code 9N Data Turnarounttoted 

Dedenation 

100 & 300 Am Component of the RCBRA Sediment and Ti 

Sampling Loca tion 

YAKIMA RIDGE B OFFAL 



Air Quality q 

45 Days% 

l9 

Ice Chest No. Field Logbook No, COA Method of S hIpment m 

^^1 ['-02','^^ EL-1595 BESRAS6520 FP.D EX 

m 

Shl ORslle Property No. Bill of Air Bi ll No. 

BER ME SERVICES LIONVfILE J ll E OSPC 

POSSIBLE SAMPLE IIAZARD&MMARKS 

POTENTIAL RADIOACTfVE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-275 I Pw 1 of J 

Collector 

Continently Contact T el ephone No. Protect Coordinator 

TILLER, B. TR KLINCOAN JOAN K 12SSNER 375-4688 KESSNER, JH Price Data 

Pr 9N TssrnaroushhhD M 

Protect Deelanasbp Semo lina Location SAP No. 45 

Air Quality [] Days 9 

Y 0 

ICn & 300 Arm Componem of the RCORA Sediment and Ti VE.RNTTA UPRIVER ON SOUTH S IDE OFFAL RC-047 0 

Ice Chest No. n 

4êC- Field Loebook No, COA 

m 

Method of Shimswlt 

e%2 

EL, 1595 BESRAS6520 FED EX 0 

Si o Offsfle Property No. BIB of LadindAir Bill No. 

BERLINE SERVICES IONVBLE h'06o 33o SEE OSPC 

POSSIBLE SAMPMUZARDSMMARM 

POTENTIAL RAVIOAC77VE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-276 P'I2 1 of 1 

oilector Company Contact 

TILLER, R. TR KLINCKMAN JOAN KESSNER 

Telephone No. 

375-4688 


KFSSNER, JH Fria ce ('ode 9N Data Twuaramaa` 

45 Days% 

ofett Dalana llon 

100 & 300 Arcs, Component of the RCBRA Sediment and Ti 

Sanmliat Location 

McGEE RANCH OFFAL 



Air Quality q 

(5J 

Ice Chat No.C^ 

^C'OZ -3-D 

Field Logbook No. 

EL-1595 

COA 

DESRAS6520 


PEDEX 

m 

m 

Sh' To Onatle Property No. Bi ll 

of Ladine/Air Bill ERE L ES VI LIONVILLE 060330 

No. 

SEE OSPC 



Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-277 w>R 2 nr 1 

olleetor Company ContactT el _ 

ephone No. Prolect Coordinator 

TILLER, B. N KLINCKMAN JOAN KESSNER 375-4688 KFSSNER, III 

^,^,nv,^^ v 

Prim Code 9N 

N 

'rolect Deaienmlon Sampling Location SAF No. 

45 Day s.0 

Air Quality q 

100 & 300 Am Component of the RCBRA Sediment and Ti SADDLE MOUNTA IN OFFAL RC-047 m 

Ice Chat No. AeC- e2. sV3 

Field Loehook No. COA Method of Shipment M 

EL 1595 BESRAS6520 FED EX m 

ShinuedTo Dil le Property NO. RERLMESERVIC LIONVILLE 3 3 o 

BID Lading/Air ill Air No. B 

BID of 


PO'FENTUL RADIOACHVE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC•047422 Paso I of I 

(lector 


Project Dedenatlon 

100 & Me Area Component of the RCBRA Sediment and Ti 

Ice Chest No. n ^---^ 

Coaaanv Contact 

JOAN KESSNER 

Semolina Location 

IWD48:2 OFFAL 


Telephone No. 

375-4689 

- 

Project Coordinator 

KFSSNER, III 



Price Code 9N 

Air Quality q 

Data Turoarosu-+ 

(y 

45 Days 

m 

9— 

EL . 1595 

COA 

BESRAS6520 


FED EX 

SI' To Offsile Property No. /^ Z p'l Bill ELa^dAirBBINo. 

E RLIN LIONVILL6 /' G c/Jf/ 



Washington Closure Hanford CHAIN OF CUSTODUSAMPLE ANALYSIS RE UEST RC-047-323 Page I of I 

Collector 


Protect Dalenalion 

100 & 300 Ara Component of the RCBRA Sediment and Ti 

Ice Chase No. 

£j^C-01 

Sd^ 

Conmanr Contact 

JOAN KESSNER 

Samolina Loca tion 

100-D-49:2 OFFAL 

Flekt Loarbook No, 

EI. 1595 

Teleohom No. 

375-4688 

COA 

BESRAS6520 

Proieet Coordinator 

KESSNER, IH 

SAP No. 


Method of SNoment 

FED EX 

price Code 911j 

Air Quality q 

Data TurnarounlV 

N 

45 Days 

m 

m- 

m 

m 

SI'ued To 

•^R ME SERVO L10NVILIE 

Oefatte Property No. 

,900033 o 

Bill of Ladina/Air Bill No. 

SEEOSPC 


POTENTIAL RAVIOACTNE

Washington Closu re Hanford " CHAIN OF CUSTODY/SAMPLE-ANALYSIS REQUEST RC-047.328 J or 1 

Collector 


'roles( Deslewtion 

100 & 300 Area Component of rile RCBRA Sediment and M 

Company Conta ct Telephone No. 


Sampling Location 

116-DR-1,DR-2/100-D-22 OFFAL 

Proiect Coordinator 

KESSNER,JH 



Price Code 9N Data 7WrnarouWJ 

a 

Air Quality p 45 Days 

m 

Ice Chest No. p^r^ r Field Loaboolc No. COA Method of Shipment m 

AlIC- 0.2 '^7 OJr EGI595 BESRAS6520 FED EX m 

Shtp 

BERLINE SERVICES LIONVIUB 

POSSIBLE SAMPLE RAZARDS/REMARKS 


Washington Closure Hanford 

Collect" 


Protect Dalena ion 

100 & 300 Am Component of the RCBRA Sediment and Ti 

tee Cheat No. f'r2c^ D2 5a5f 

.. 

OF CUSTODY/SAMPLE -ANALYSIS REOUEST RC-047-330 J PW 1 -1 t 


JOAN KESSNER 

Telephone No. 

375-4688 

Proleet Coordmalor 

KESSNER, III Sanitation Lo 

Price Code 91V Data Tprnaraucy 

N 

cati on 


SAP No. 


Air Quality El 

45 Day s% 

m 

Field Loebook No. 

EL-1595 

COA 

BESRAS6520 


FED EX 

0m 

m 

S Otfa(te Property No. Bill /2 2 Air Bill No. 

EBERLINE SERVICES L.IONVILLE 

603 3 D 

SEE OSPC 

POSSIBLE SAMPLE HAZARDSIREMARKS 

POTEN77ALRADIOAC17VE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-332 P'2° 1 of 1 

Collector 

Company Contact Telephone No. Prolect Coordinator 

TILLER. B. TR KLINCKMAN LOAN KESSNER 375-468R KPSSNBR, JH 

Psiee Code 9N Data Tax'oarourU} 

Protect Des iena llon Semolina Location SAF No. 45 Day .RD 

Air Quality q 

100 & 300 Arca Component of the RCBRA Sediment and Ti 600-131 OFFAL RC-047 

Ice Chest No. r^^_D^ Lorlsook No. meow FEDPX shipment 

M 

—50 ,i ..^ BESRA56520 

9— 

Shipped To Offshe Property No. ,y O v 

Bill of LadloNAir Bill No. 

E SERVI / LIONVILLE ff'(J 3 SEE OSPC 

POSSIBLE SAMPLE IIAZARDSIREMARKS 

POTENTIAL RADIOACTIVE ^DOTLIMITS Preservation 

Special handling and/or Storage 



C-1 IC None c"°I .e eaal4C Caat

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-N7-343 aF i of 1 

Collector Company Contact Telephone No. Profixt Coordinator 

«Code Data 9N Turnaromsifl 

TILLER, B. Tfl KLINCKMAN JOAN KESSNER 375.4688 KP35NER, IH 

led Designation Samsdine Location SAF No. Air Quality E) 45 Daysm 

100 & 300 Area Cmnponent of the RCBRA Sediment and Ti CENTRAL PLATEAU SHRUB STEPPE OFFAL RC-047 m_ 

f5] 

Ice Chest No.r Field Logbook No. COA Method of Shinmml 

G c -192- —,Sdj 

EL. 1595 BESRAS6520 FED EX 

m 

S^BERLINE 

Offsite Property No.,^0 / Bill Bill 

O33D 

BI Na. 

SERVIC LIONVILLE !^ f7 SEE 

POSSIBL LE HAZARDS/REMARKS 

POTEAWALSADIOACT/VE fime 

SECTION 

FINAL SAMPLE Disposal Method Dispo se d By Datemem, 

DISPOSITION 

SHI-EE-011 (06129/2005)

Lionvi ll 

e Laborato ry Incorporated 


( 

CLIENT: `-NaaRr^ oc,^ Date:` 

Order / Project# / 

SAF# w# / Release #: RC o' \^ 

v Batch 9: rl,N ) n ,\, 

1. Samples Hand 



3. Outside of coolers or shipping containers am 


4. All expected paperwork received (coc and 

other c li 

ent speci fic information) sealed in 

plastic bag and easily accessible? 

5. Samples receiv cool r ambieut? y Q 

6. Custody seals on sample containe rs intact, 


7, coc signed and dated? 

8. Sample containers are intact? 



10. All sample label information matches coc? 




SR-002-B 



client? 

15. Shipment meets LvLI Sample Acceptance 

Policy? (Identify all bottles not within 



discrepancies? name/date (or samples 


vLl 

EXPLAIN ALL 

/ 

O No 

/Q Yes q No 

17 3es 0 No 

O No Sash Comments 

Tetup 7 .3 IC 

S 

^d Yes O No O No seats 

1 93 

11 Yes 

/^Y4 

I(Yea 

Yes 

Yes 

O Yes 

Oyes 

O Yes 

Ye 

U Yes 

Sample Custodian: 

ONO 

O No 

O No 

ONO 

O No 

O No 

O No /^11`NlA 

ONO 94 A 

ONo 

Airbill# '7 q a7 °^ 5 OS 

ONo 0 N 

Diseeepsoeks 

Cooler# SAW - 1a^ 

000009027

Lionville Laboratory, Inc_ 

INORGANIC ANALYTICAL DATA PACKAGE FOR 

TNUHANFORD RC-047 K0303 

N 

vd\lE^ 

N\- ZD 

DATE RECEIVED: 04/28/06 LVL LOT # :060 E 

CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS 

J11KK8 

SILVER, TOTAL . 001 SO 06LO324 04/05/06 05/25/06 05/27/06 

SILVER, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06 

SILVER, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

ALUMINUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/30/06 

ALUMINUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/30/06 

ALUMINUM, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/30/06 

ARSENIC, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

ARSENIC, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06 

ARSENIC, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06 

BORON, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

BORON, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06 

BORON, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

BARIUM, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06 

BARIUM, TOTAL 001 REP SO 06LO324 0.4/05/06 05/25/06 05/27/06 

BARIUM, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06 

BERYLLIUM, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/30/06 

BERYLLIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/30/06 

BERYLLIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/30/06 

BISMUTH, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06 

BISMUTH, TOTAL REP 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06 

BISMUTH, TOTAL SPIKE 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

CALCIUM, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06 

CALCIUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06 

CALCIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

CADMIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

CADMIUM, TOTAL 001 REP SO 06L0324 .04/05/06 05/25/06 05/27/06 

CADMIUM, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06 

COBALT, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06 

COBALT, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06 

COBALT, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06 

CHROMIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

CHROMIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06 

CHROMIUM, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06 

COPPER, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/30/06 

COPPER, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/30/06 

000000001



TNUHANPORD RC-047 K0303 

DATE RECEIVED: 04/28/06 LVL LOT # :0604L904 


COPPER, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/30/06 

IRON, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06 

IRON, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06 

IRON, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

MERCURY, TOTAL 001 SO 0600086 04/05/06 05/03/06 05/04/06 

POTASSIUM, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06 

POTASSIUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06 

POTASSIUM, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06 

LITHIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

LITHIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06 

LITHIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

MAGNESIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

MAGNESIUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06 

MAGNESIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

MANGANESE, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06 

MANGANESE, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06 

MANGANESE, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

MOLYBDENUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

MOLYBDENUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06 

MOLYBDENUM, TOTAL ,001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

SODIUM, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06 

SODIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06 

SODIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

NICKEL, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06 

NICKEL, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06 

NICKEL, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

PHOSPHORUS, TOTAL 001 SO 66LO324 04/05/06 05/25/06 05/30/06 

PHOSPHORUS, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/30/06 

PHOSPHORUS, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/31/06 

LEAD, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

LEAD, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06 

LEAD, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06 

ANTIMONY, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06 

ANTIMONY, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06 

ANTIMONY, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

SELENIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

SELENIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06 

SELENIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

000000002




DATE RECEIVED: 04/28/06 LVL LOT # :06041,904 


SILICON, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

SILICON, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06 

SILICON, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

TIN, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

TIN, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06 

TIN, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06 

STRONTIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

STRONTIUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06 

STRONTIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

THALLIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

THALLIUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06 

THALLIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

URANIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06 

URANIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06 

URANIUM, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06 

VANADIUM, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06 

VANADIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06 

VANADIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

ZINC, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06 

ZINC, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06 

ZINC, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06 

J11KL5 

SILVER, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06 

ALUMINUM, TOTAL 002 SO 06LO324 04/05/06 05/25/06 05/30/06 


BORON, TOTAL 002 SO 06LO324 04/05/06 05/25/06 05/27/06 



BISMUTH, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06 

CALCIUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06 

CADMIUM, TOTAL 002 SO 06LO324 04/05/06 -05/25/06 05/27/06 


CHROMIUM, TOTAL 002 SO 06LO324 04/05/06 05/25/06 05/27/06 




000000003






MERCURY, TOTAL 002 REP SO 0600086 04/05/06 05/03/06 05/04/06 

MERCURY, TOTAL 002 MS SO 0600086 04/05/06 05/03/06 05/04/06 

POTASSIUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06 





SODIUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06 

NICKEL, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06 

PHOSPHORUS, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/30/06 

LEAD, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06 

ANTIMONY, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06 

SELENIUM, TOTAL 002 SO 06LO324 04/05/06 05/25/06 05/27/06 


TIN, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06 




VANADIUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06 

ZINC, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06 

J11KL6 

SILVER, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/27/06 




BARIUM, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06 

BERYLLIUM, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/30/06 




COBALT, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06 


COPPER, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/30/06 

IRON, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06 



000000004







MAGNESIUM, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/27/06 






LEAD, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06 




TIN, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/27/06 



URANIUM, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/27/06 


ZINC, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06 

J11KM0 



ARSENIC, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06 




BISMUTH,_TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06 


CADMIUM, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06 





MERCURY, TOTAL 004 SO 06CO086 04/05/06 05/03/06 05/04/06 


LITHIUM, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06 



000000005





CLIENT ID /ANALYSIS LVL # MIX PREP # COLLECTION EXTR/PREP ANALYSIS 





LEAD, TOTAL 004 SO 061;0324 04/05/06 05/25/06 05/27/06 



SILICON, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06 

TIN, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06 


THALLIUM, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06 

URANIUM, TOTAL 004 _ SO 06L0324 04/05/06 05/25/06 05/27/06 



J11KM2 













IRON, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06 





MANGANESE, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06 

MOLYBDENUM, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06 



000000006







LEAD, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06 




TIN, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06 

STRONTIUM, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06 





J11KM3 













IRON, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/27/06 










LEAD, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/27/06 


000000007


INORGANIC . ANALYTICAL DATA PACKAGE FOR 






TIN, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/27/06 






JllKM4 













IRON, TOTAL _ 007 SO 06LO324 04/03/06 05/25/06 05/27/06 










LEAD, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06 




TIN, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06 

000000008





CLIENT ID /ANALYSIS LVL # M7% PREP # COLLECTION EXTR/PREP ANALYSIS 






J11KM5 



























TIN, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06 




000000009



TNUHANFORD RC-047 X0303 





J11KM6 













IRON, TOTAL 009 SO 06L0324 04/03/06 05/25/06 05/27/06 






MOLYBDENUM, TOTAL 009 SO 06LO324 04/03/06_ 05/25/06 05/27/06 




LEAD, TOTAL 009 SO 06L0324 04/03/06 05/25/06 05/27/06 




TIN, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06 






J11KV1 


000000010







ARSENIC, TOTAL 010 SO 061,0324 04/05/06 05/25/06 05/27/06 
























TIN, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06 


THALLIUM, TOTAL 010 SO 06LO324 04/05/06 05/25/06- 05/27/06 



ZINC, TOTAL 010 SO 06L0324 04/05/06 05/25/06 05/27/06 

S11KV2 




BORON, TOTAL Oil SO 06LO324 04/05/06 05/25/06 05/27/06 

000000011

Lionville Laboratory, Inc, 







BISMUTH, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/27/D6 




















TIN, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/27/06 


THALLIUM, TOTAL Oil SO 06L0324 04/05/06 05/25/06 05/27/06 



ZINC, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/27/06 

JlIL21 








000000012



TNUHANFORD RC-04.7 K0303 


















LEAD, TOTAL 012 SO 06L0324 04/03/06 05/25/06 05/27/06 




TIN, TOTAL 012 SO 06L0324 04/03/06 05/25/06 05/27/06 





ZINC, TOTAL 012 SO 06L0324 04/03/06 05/25/06 05/27/06 

JIIL23 











000000013








IRON, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/27/06 














TIN, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06 



URANIUM, TOTAL 013 'SO 06LO324 04/03/06 05/25/06 05/27/06 


ZINC, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/27/06 

JlIL25 













IRON, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06 

000000014












SODIUM, TOTAL 014 - SO 06L0324 04/05/06 05/25/06 05/27/06 



LEAD, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06 




TIN, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06 





ZINC, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06 

J11L36 













IRON, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06 




000000015




DATE RECEIVED: 04/28/06 _ LVL LOT # :0604L904 



MANGANESE, TOTAL 015 SO 061,0324 04/03/06 05/25/06 05/27/06 









TIN, TOTAL 015 SO 06LO324 04/03/06 05/25/06 05/27/06 





ZINC, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06 

LAB QC: 

SILVER LABORATORY LC1 BS S 061,0324 N/A 05/25/06 05/26/06 

SILVER, TOTAL MBl S 06L0324 N/A 05/25/06 05/26/06 

ALUMINUM LABORTORY LC1 BS S 06L0324 N/A 05/25/06 05/30/06 

ALUMINUM, TOTAL MB1 S 06LO324 N/A 05/25/06 05/30/06 

ARSENIC LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

ARSENIC, TOTAL MBl S 06LO324 N/A 05/25/06 05/26/06 

BORON LABORATORY LC1 BS S 06LO324 N/A 05/25/06 05/26/06 

BORON, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

BARIUM LABORATORY LC1 BS S 06LO324 N/A 05/25/06 05/26/06 

BARIUM, TOTAL MB1 S 06LO324 N/A 05/25/06 05/26/06 

BERYLLIUM LABORATORY LC1 BS S 06LO324 N/A 05/25/06 _ 05/30/06 

BERYLLIUM, TOTAL MB1 S 06LO324 N/A 05/25/06 05/30/06 

BISMUTH, LCS LC1 BS S 06LO324 N/A 05/25/06 05/26/06 

BISMUTH, TOTAL MB1 S 06LO324 N/A 05/25/06 05/26/06 

CALCIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

CALCIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

CADMIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

CADMIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

COBALT LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

000000016






COBALT, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

CHROMIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

CHROMIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

COPPER LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/30/06 

COPPER, TOTAL MB1 S 06L0324 N/A 05/25/06 05/30/06 

IRON LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

IRON, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

MERCURY LABORATORY LC1 BS S 0600086 N/A 05/03/06 05/04/06 

MERCURY, TOTAL MB1 S 0600086 N/A 05/03/06 05/04/06 

POTASSIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

POTASSIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

LITHIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

LITHIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

MAGNESIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

MAGNESIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

MANGANESE LABORATORY LCl.BS S 06L0324 N/A 05/25/06 05/26/06 

MANGANESE, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

MOLYBDENUM LABORATOR LCl BS S 06L0324 N/A 05/25/06 05/26/06 

MOLYBDENUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

SODIUM LABORATORY LC1 BS S 061,0324. N/A 05/25/06 05/26/06 

SODIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

NICKEL LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

NICKEL, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

PHOSPHORUS LCS LCl BS S 06L0324 N/A 05/25/06 05/30/06 

PHOSPHORUS, TOTAL MB1 S 06L0324 N/A 05/25/06 05/30/06 

LEAD LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

LEAD, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

ANTIMONY LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

ANTIMONY, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

SELENIUM LABORATORY LC1 BS S 06LO324 N/A 05/25/06 05/26/06 

SELENIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

SILICON LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

SILICON, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

TIN LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

TIN, TOTAL MBl S 06LO324 N/A 05/25/06 05/26/06 

STRONTIUM LCS STANDA LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

STRONTIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

THALLIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

000000017






THALLIUM, TOTAL MB1 S 06LO324 N/A 05/25/06 05/26/06 

URANIUM LABORATORY LC1 BS S 06LO324 N/A - 05/25/06 05/26/06 

URANIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

VANADIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 

VANADIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

ZINC LABORATORY LC1 BS S 06LO324 N/A 05/25/06 05/26/06 

ZINC, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 

000000018

Client: TNU-HANFORD RC-047 WON: 11343-606-001-9999-00 

LVL#: 0604L904 Date Received: 04-28-06 

SDG/SAF4: K0303/RC-047 

METALS CASE NARRATIVE 

The following is a summary of the QC results accomp anying the sample results. Lionville Laborato ry 

(LvLI) certi fi 

es that all test results meet the requirements of NELAC except as noted below. 

All soil samples are repo rted on a dry weight basis unless requested by the client, required by the method, 

or noted otherwise. 

This narrative covers the analyses of 15 solid samples. 

2. The samples were prepared and analyzed in accordance with methods checked on the attached 

glossary. The samples are reported on a wet weight, às received' basis. 

All samples were rerun for Aluminum, Be ryllium, and Copper, along with the Phosphorous 

analysis, due to sample matrix. The matrix spike of sample J11KK8, and samples J1 1L21 and 

J11L23 were rerun for Phosphorous due to high concen trations. 

3. All analyses were performed within the required holding ti mes. 

4. All Ini ti al and Con ti nuing Calibration Verifications (ICV/CCVs) were within the 90-110% con trol 

limits (80-120% for Mercury). 

5. All Ini tial and Continuing Calibration Blanks (ICB/CCBs) were within con trol limits (less than the 

PQL). 

6. The preparation/method blanks for 2 analytes were outside method c riteria (less than the Prac ti cal 

Quantitation Limit (3X the IDL), or samples greater than 20X MB value). Refer to the Inorganics 

Method Blank Data Summary . 

a). The MB results for Aluminum and Uranium were greater than the Prac ti cal Quantitation Limit 

(PQL) (3 x the (IDL) Instrument Detection Level) and al l samples read less than 20 ti mes the MB 

concentration for Aluminum. However, no corrective ac ti on criteria for MBs were provided in 

SW846 method 6010B. The sample results were repo rted herein "uncorrected" for the levels 

found in the MB. All samples were below the IDL for Uranium. 

All ICP Interference Check Standards were within con trol limits. 

The re su lts presented in this re port relate only to the analytical testing and conditions ofthe samples at receipt and during storage. All pages ofthis re po rt are 

integral pads ofthe analy tical data The re fo re , this report should only be reproduced in its entirety of ^C pages. 

208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-3000 • Fax (610) 280-3047

8. All laboratory control samples (LCS) were within the 80-120% control limits with the ex cep ti on of 

Silicon at 69.6%. Refer to the Inorganics Laborato ry Control Standards Report. Associated 

sample results may be bi ased low. 

9. The matrix spike (MS) recove ries for 5 analytes were outside the 75-125% control limits. Refer to 

the Inorganics Accuracy Repo rt . 

10. For analytes where the ICP MS is out-of-control, a post-diges tion MS (PDS) and serial dilution are 

performed. A PDS w as prepared at meaningful concentration level for the following analytes: 

Sample ID Element 

PDS 

Concentra 

PDS 

ti 

on (pob) %Recovery 

J11KK8 C al cium 12,000 115.6 

Iron 2,000 95.3 

Phosphorous 6,000 104.1 

Silicon 1,100 100.3 

Zinc 100 117.1 

11. The duplicate analyses for 16 analytes were outside the 20% Rela ti ve Percent Difference (RPD) 

control limits. Refer to the Inorg anics Precision Repo rt . 

12. For the purposes of this report, the data has been reported to the Instrument Detection Limit (IDL). 

Values between the IDL and the Practical Quantitation Limit (PQL) are acquired in a region of 

less-certain quantification. 

13. LvLI is NELAP accredited by the state of Pennsylv ania and holds over 20 addi ti onal state 

accreditations. For a complete listing of accredi ti ng authorities and the corresponding 

analytes/methods, ple ase contact your Project M anager. 

14. I certify that this sample data package is in compli ance with SOW requirements, both 

technically and for completeness, other than the condi ti ons detailed above. Rele ase of the data 

contained in this hard-copy data package h as been autho rized by the Laborato ry Manager or a 

designee, as verified by the following signature. 

aniels 

I_JLôvatory Manager 


ijw/m04-904 

vLl 

c, )g1,^ 

Date 

10 4W.

METALS METHOD GLOSSARY 

The following methods are used as 'reference for the digestion and analysis of samples contained within t 

Lot#: 66() 4L4aN r 

Leaching Procedure: -1310 -1311 -1312 ,_Other: 

CLP Metals_ Digestion and _ Analysis Methods: _ILM03 .0 -ILM04.0 

Metals Digestion Methods: _3005A _3030A 3015 3020A x 3050B 3051 200.7 -SS17 

__Other: 

Metals Analysis Methods 

EPA 

SW846 EPA STD MTD OSWR USATHAM , 

Aluminum 46010B _200.7 -99 Antimony 

Arsenic 

Ba rium 

Beryllium 

Bismuth 

Boron 

Cadmium 

Calcium 

Chromium 

Cobalt 

Copper 

f 6010 -7041' -200.7 -204.2 

)oC 6010B -7060A -200.7 _206.2 -3113B 

)r, 6010B -200.7 

)^- 6010B 200.7 

--106010B' _200.7' 

)C6010B -200.7 

-IC 6010B -7131A' 200.7 213.2 

)C6010B -200.7 

^6010B _7191' -200.7 218.2 

40010B 200.7 

6010B -7211 

-1620 

99 

-99 

99 

99 

99 

-99 

-99 

-99 

-SSI7 

-99 

:200.7 

Iron 

Lead 

Lithium 

Magnesium 

Manganese 

Mercu ry 

Molybdenum 

Nickel 

Potassium 

Rare Earths 

Selenium 

Silicon 

Silica 

Silver 

220.2 

ZC 6010B _200.7 

6010B -7421 5 200.7 -239.2 -3113B 

6030$ _7430' _200.7 

6010B 200.7 

6010B ll 200.7 

7470A 3_)(7471A3 -245.1?2455' 

-y601 0B -200.7 

60101 -200.7 

1,60101 -7610' 200.7 _258.1' 

_6010B' _200.7' 

)C6010B -7740' -200.7 -270-23113B 

)L4010B' 200.7 

_6010B 200.7 

^C 6010B -7761 

-1620 

-1620 

-1620 

-1620 

-99 

-^ 

-99 

99 

99. 

-99 

-99 

-99 

-99 

_99 

-99 

-99 

-99 

_99 

S Sodium 

Strontium 

Thallium 

Tin 

Titanium 

Uranium 

Vanadium 

Zinc 

Zirconium 

200.7 -272.2 

6010B _7770' _200.7 -273.1' 

^6010B 200.7 

K6010B -7841' 200.7 279.2-200.9 

Y 6010B -200.7 

6010B 200.7 

6010B' 200.7' 

6010B _200.7 

6010E 200.7 

-6010B' 200.7' 

-1620 

-1620 

99 

99 

-99 

99 

-99 

99 

-99 

-99 

_99 

Other. W d 

/ 

Method: 60/06 4m.mws.om . 

000000021

METHOD REFERENCES AND DATA QUALIFIERS 

U = Indicates that the parameter was not detected at or above the reported limit. The 

associated numerical value is the sample detection limit. 

" = Indicates that the original sample result is greater than 4x the spike amount added. 

MB = Method or Preparation Blank. 

MS = Matrix-Spike. 

MSD = Matrix Spike Duplicate. 

REP = Sample Replicate 

LCS = Laboratory Control Sample. 

NC = Not calculated. 

Not included in the method element list. 

2. Modified Hg: Hgl and Hg2 require less total volume of digestate due to the 

autosampler analysis. Sample volumes and reagents for mercury determinations 

in water and soil have been proportionately scaled down to adapt to this semiautomated 

technique. The sample volume used for water analysis is 33 mL. For 

soils, approximately 0.3 grams of sample is taken to a final volume of 50 mL 

(including all reagents). 

3. Flame AA. 

Graphite Furnace AA. 

L-W1 -033/N-04/98 

000000022


INORGANICS DATA SUMMARY REPORT 06/08/06 

CLIENT: TNUHANPORD RC-047 K0303 LVL LOT #: 0604L904 

WORK ORDER: 11343-606-001-9999-00 

REPORTING DILUTION 

.SAMPLE SITE ID ANALYTE RESULT UNITS LLMIT FACTOR 

: e 

-001 J11KK8 Silver, Total 0.07 u MO/KG 

0.07 '6i `2.0 

Aluminum, Total 26.2 MG/KG 2.2 1.0 

Arsenic, Total 0.58 u MG/KG 0.58 1.0 

Boron, Total 0.45 MG/KG 0.23 1.0 

Barium, Total 4.4 MG/XG 0.02 1.0 

Beryllium, Total 0.02 u MG/KG 0.02 1.0 

Bismuth, Total 0.49 u MG/KG 0.49 1.0 

Calcium, Total 9790 MG/KG 1.6 1.0 

Cadmium, Total 0.07 u MG/KG 0.07 1.0 

Cobalt, Total 0.13 u MG/KG 0.13 1.0 

Chromium, Total 0.41 MG/KG 0.12 1.0 

Copper, Total 2.6 MG/KG 0.21 1.0 

Iron, Total 94.3 MG/KG 3.3 1.0 

Mercury, Total 0.02 u MG/KG 0.02 1.0 

Potassium, Total 2680 MG/KG 2.2 1.0 

Lithium, Total 0.1 MG/KG 0.03 1.0 

Magnesium, Total 471 MG/KG 0.92 1.0 

Manganese, Total 3.0 MG/KG 0.03 1.0 

Molybdenum, Total 0.28 u MG/KG 0.28 1.0 

Sodium, Total 1340 MG/KG 0.72 1.0 

Nickel, Total 0.23 u MG/KG 0.23 1.0 

Phosphorus, Total 6060 MG/KG 0.86 1.0 

Lead, Total 0.30 u MG/KG 0.30 1.0 

Antimony, Total 0.42 u MG/KG 0.42 1.0 

Selenium, Total D.63 MG/KG 0.46 1.0 

silicon, Total 42.9 MG/KG 2.2 1.,0 

Tin, Total 1.0 a MG/KG 1.0 1.0 

Strontium, Total 10.9 MG/KG 0.01 1.0 

Thallium, Total 0.67 a MG/KG 0.67 1.0 

Uranium, Total 0.84 u MG/KG 0.84 1.0 

Vanadium, Total 0.14 MG/KG 0.09 1.0 

Zinc, Total 46.6 MG/KG 0.15 1.0 

000000023

SAMPLE SITE ID 

002 J11KL5 



CLIENT: TNUMANFORD RC-047 K03O3 LVL LOT M: 0604L9O4 

WORK ORDRR: 11343-606-001-9999-00 


ANALYTR RESULT UNITS LIMIT FACTOR 

silver, Total 0.07 u MG/KG 0.07 1.0 


Areenic, Total 0.58 U MG/KG 0.5E 1.0 


Barium, Total 3.1 MG/KG 0.02 1.0 


Bismuth, Total 0.49 u MG/KG 0.49 110 



Cobalt,. Total 0.13 u MG/KG 0.13 1.0 



Iron, Total 122 MG/KO 3.3 1.0 








Nickel, Total 0.23 a MG/KG 0.23 1.0 


Lead, Total 1.5 MG/KG 0.30 1.0 


Selenium, Total 0.86 MG/KG 0.45 1.0 

Silicon, Total 44.8 MG/RG 2.2 1.0 

Tin, Total 1.2 MG/KG 1.0 1.0 

Strontium, Total 10.4 MG/[CG 0.01 1.0 

Thallium, Total 0.67 u MG/KG 0.67 1.0 

Uranium, Total 0.84 u MO/KG 0.84 110 



606090624

CLIENT: TNUHANFORD RC-047 K0303 

WORK ORDER: 11343-606-001-9999-00 

SAMPLE SITE ID ANALYTE 

-003 J11KL6 Silver, Total 

Aluminum, Total 

Arsenic, Total 

Boron, Total 

Barium, Total 

Beryllium, Total 

Bismuth, Total 

Calcium, Total 

Cadmium, Total 

Cobalt, Total 

Chromium, Total 

Copper, Total 

Iron, Total 

Mercury, Total 

Potassium, Total 

Lithium, Total 

Magnesium, Total 

Manganese, Total 

Molybdenum, Total 

Sodium, Total 

Nickel, Total 

Phosphorus, Total 

Lead, Total 

Antimony, Total 

Selenium, Total 

Silicon, Total 

Tin, Total 

Strontium, Total 

Thallium, Total 

Uranium, Total 

Vanadium, Total 

Zinc, Total 


INORGANICS DATA SUMMARY REPORT 06/DB/06 

LVL LOT 8: 0604L904 


.RESULT UNITS LIMIT FACTOR 

0.07 u MG/KG 0.07 1.0 

102 MG/KG 2.3 1.0 

0.59 u MO/KG 0.59 1.0 

0.55 MG/KG 0.23 1.0' 

2.D MG/KG 0,02 1.D 

0.02 u MG/KG 0.02 1.D 

0.49 u MG/KG 0.49 1.0 

9590 MG/KG 1.6 1.0 

0.07 u MG/KG 0.07 1.0 

0.13 u MG/KG 0.13 1.0 

0.45 MG/KO 0-12 1.0 

2.7 MG/KG 0.21 1.0 

115 MO/KG 3.4 1.0 

0.01 u MG/KG 0.01 1.0 

2780 MG/KG 2.2 1.0 

0.00 MG/KG 0.03 1.0 

467 MG/KG 0.93 1.0 

5.7 MO/KG 0.03 1.0 

0.28 u . MG/KG 0.28 1.0 

1310 MG/KG 0.73 1.0 

0.27 MG/KO 0.23 1.0 

5890 MG/7W 0.86 1.0 

2.4 MG/KG 0.30 1.0 

0.42 u MG/KG 0.42 1.0 

0.81 MO/KG 0.45 1.0 

45.3 MG/KG 2.2 110 

1.7 MG/KG 1.0 1.0 

7.0 MG/KG 0.01 1.0 

0.67 u MG/KG 0.67 1.0 

0.85 u MG/KG 0.85 1.0 

0.14 MG/KO 0.09 1.0 

40.5 MG/KG 0.15 1.0 

099090625


INORGANICS DATA SUMMARY REPORT 06108106 

CLIENT: TNDHANFORD RC-047 K0303 LVL LOT #t 0604L904 

WORK ORDER: 11343-606-001-9999-00 


SAMPLE SITE ID ANALYSE RESULT UNITS LIMIT FACTOR 

-Fez _zz a ....................... z _ 

-004 J11KM0 Silver, Total 0.07 u MG/KG 0.07 1.0 



Boron, Total 0.23 u MG/KG 0.23 1.0 








Copper, Total - 3.6 MG/KG 0.21 1.0 

Iron, Total 142 MG/KG 3.4 1.0 



Lithium, Total 0.07 MG/KG .0.03 1.0 

Magnanium, Total 583 MG/KG 0.93 1.0 

Manganese, Total - 6.6 MG/KG 0.03 1.0 

Molybdenum, Total '0.28 u MG/KG 0.28 1.0 



Phouphorue, Total 5590 MG/KG 0.86 1.0 




Silicon, Total 52.6 MG/KG 2.2 1.0 







000000026



CLIENT: TNUMANFORD RC-047 K0303 LVL LOT 6: 06D4L904 

WORK ORDER: 11343-606-001-9999-00 


SAMPLE SITE ID ANALYT6 RESULT UNITS LIMIT FACTOR 

-005 Ji1KM2 Silver, Total 0.07 u MG/KG 0.07 i 1.0 





Beryllium, Total 0.02 u MG/KG 0,02 1.0 

Bismuth, Total 0.49 a MG/KG 0.49 1.0 

Calcium, Total Salo MG/KG 1.6 1.0 



Chromium, Total 0.46 MG/KG 0.12 110 





Lithium, Total 0.07 MO/KG 0.03 1.0 



Molybdenum, Total 0.28 u MG/KG 0.28 110 











Uranium, Total 0.8S u MO/KG 0.85 1.0 

Vanadium, Total 0.09 u MG/KG 0.09 1.0 

Zinc, Total 59..5 MG/KG 0.15 1.0 

996099627

CLIENT: TNURANFORD RC-047 K0303 

WORK ORDER: 11343-606-001-9999-00 


-006 J11KM3 

ANALYTE 

Silver, Total 



Boron, Total 

Barium, Total 





Cobalt, Total 


Copper, Total 

Iron, Total 







Sodium, Total 

Nickel, Total 


Lead, Total 


selenium, Total 


Tin, Total 





Zinc, Total 



LVL LOT #: 0604L904 

REPORTING 

RESULT UNITS LIMIT 

0.07 u MG/KG 0.07 

45.1 MG/KG 2.3 

0.59 u MG/KG 0.59 

0.23 u MG/KG 0.23 

3.2 MG/KG 0.02 

0.02 v MG/KG 0.02 

0.49 u MG/KG 0.49 

7450 MG/KG 1.6 

0.07 u MG/KG 0.07 

0.13 u MG/KG 0.13 

0.47 MG/KG 0.12 

2.5 MG/KG 0.21 

192 MG/KG 3.4 

0.02 u MG/KG 0.02 

2620 MG/KG 2.2 

0.09 MG/KG 0.03 

394 MG/KG 0.93 

4.4 MG/KG 0.03 

0.28 u MG/KG 0.29 

1450 MG/KG 0.73 

0.34 MG/KG 0.23 

455D MG/KG 0.86 

0.30 u MG/KG 0.30 

0.42 u MG/KG 0.42 

0.75 MG/KG 0.45 

71.5 MG/KG 2.2 

1.2 MG/KG 1.0 

4.2 MG/1(G 0.01 

0.67 u MG/KG 0.67 

0.65 u MG/KG 0.85 

0.18 MG/KG 0109 

46.5 MG/KG 0.15 

DILUTION 

FACTOR 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.D 

1.0 

1.0 

1.0 

1.0 

1.0 

996999628

Lionville Laboratory, Inc, 


CLIENT: TNUHANPORD RC-047 KO303 LVL LOT 41: 06041,904 

WORK ORDER: 11343-606-001-9999-00 


SAMPLE SITS ID ANALYTB RESULT UNITS LIMIT 

:: 

PACTOR 

-007 J13KM4 Silver, Total 0.07 u MG/KGx 

0.07 "'• 1.0 



Boron, Total 0.23 a MG/KG 0.23 1.0 





Cadmium, Total 0.07 u MO/KG 0.07 1.0 




-- Iron, Total 117 MG/KG 3.3 1.0 








Nickel, Total 0.54 MG/KG 0.23 110 









Orenium, Total 0.64 u MG/KG 0.84 1.0 



000000029

CLIENT: TNURANPORD RC-047 K0303 

WORK ORDER: 11343-606-001-9999-00 


-008 JIIKMS Silver, Total 



Boron, Total 

Barium, Total 





Cobalt, Total 


Copper, Total 

Iron, Total 


Potannium, Total 





Sodium, Total 

Nickel, Total 

Phosphoru0, Total 

Lead, Total 




Tin, Total 





Zinc, Total 



LVL LOT 8: 06041,904 


RESULT UNITS LIMIT FACTOR 

........ ...... 

........ 

0.07 u 

MG/KG 

.......... 

0.07 

1.0 

70.8 MG/KG 2.2 1.0 

0.58 u MG/KG 0.69 1.0 

0.26 MG/NG 0.23 1.0 

4.5 MG/KG 0.02 1.0 

0.02 u MG/NG 0.02 1.0 

0.46 u MG/KG 0.48 1.0 

12800 MG/KG 1.5 1.0 

0.07 u MG/KG 0.07 1.0 

0.13 u MG/KG 0.13 1.0 

0.84 MG/KG 0.12 1.0 

3.2 MG/KG 0.21 1.0 

233 MG/KG 3.3 1.0 

O.D2 u MG/KG 0.02 1.0 

2920 MG/KG 2.1 1.0 

0.13 MG/KG 0.03 1.0 

566 MG/KG 0.91 1.0 

7.4 MG/KG 0.03 1.0 

0.27 u MG/KG 0.27 1.0 

1560 MG/KG 0.72 1.0 

0.96 MG/KG 0.23 1.0 

7290 MG/KG 0.65 1.0 

0.51 MG/KG 0.29 1.0 

0.41 u MG/KG 0.41 1.0 

0.79 MG/KG 0.44 1.0 

91.7 MG/KG 211 1.0 

1.1 MG/KG 1.0 1.0 

7.2 MG/KG 0.009 1.0 

0.66 u MG/KG 0.66 1.0 

0.83 u MG/KG 0.83 1.0 

0.40 MG/KG 0.08 1.0 

61.9 MG/KG 0.15 1.0 

000000030



CLIENT: TNUNANFORD RC-047 K0303 LVL LOT R: 06041,904 

WORK ORDER: 11343-606-001-9999-00 


SAMPLE SITS ID ANALYTR RESULT UNITS LIMIT FACTOR 

-009 J11KM6 Silver, Total 0.07 u MG/KG 0.07 1.0 


Arsenic, Total O.SB a MG/KG 0.58 1.0 




Bismuth, Total 0.49 u MG/XG 0.49 1.0 

Calcium, Total 17900 MG/KG 1.6 110 





Iron, Total 158 MG/XG 3.3 1.0 

Mercury, Total 0'.02 u MG/KG 0.02 1.0 

Potassium, Total 2930 MG/XG 2.2 1.0 


MagneelUM, Total 605 MG/KG 0.92 1.0 


Molybdenum, Total 0.28 u MG/XG 0.28 1.0 

Sodium, Total 1690 MG/KO 0.72 1.0 

Nickel, Total 2.9 MG/KG 0.23 1.0 


Lead, Total 0.31 MG/XG 0.30 1.0 





Strontium, Total 10.2 MG/KG 0,01 1.0 

ThalliuM, Total 0.67 u MG/KG 0.67 1.0 




000000031



CLIENT: TNURANFORD RC-047 X0303 LVL LOT 4: 06O4L904 

WORK ORDER: 11343-606-001-9999-00 


SAMPLE SITE ID ANALYTe RESULT UNITS LIMIT FACTOR 

-010 .711XV2 Silver, Total 0.07 u MG/KG 0.07 Lc 1.0 


Areenie, Total. 0.56 u MG/RG 0.56 1.0 








Chromium, Total 0.61 MG/R& 0.12 1.0 

Copper, Total 3.0 MG/KG 0.21 110 






Manganese, Total 4.5 MG/KG 0.03 110 




Phosphorus, Total 5270 MG/KG a.86 1.0 






Strontium, Total 6.8 MG/ICG 0.01 1.0 


Uranium, Total 0.84 u MG/XG 0.84 1.0 


Zinc, Total 67.5 MG/1(G 0.15 1.0 

000000032

CLIENT: TNUMANPORD RC-047 K0303 

MORK ORDER: 11343-606-001-9999-Ob 

SAMPLE SITE TO AKALYTS 

-011 J11KV2 Silver, Total 



Boron, Total 

Barium, Total 





Cobalt, Total 


Copper, Total 

Iron, Total 







Sodium, Total 

Nickel, Total 


Lead, Total 




Tin, Total 





Zinc, Total 



LVL LOT #: 0604L904 



0.07 u MG/KG 0.07 1.0 

55.7 MG/KG 2.2 1.0 

0.58 u MG/KG 0.58 1.0 

0.26 MG/KG 0.23 1.0 

4.7 MG/KG 0.02 1.0 

0.02 u WKS 0.02 1.0 

0.48 u MG/KG 0,48 1.0 

17400 MG/KG 1.5 1.0 

0.07 u MG/KG 0.07 1.0 

0.13 u MG/KG 0.13 1.0 

0.61 MG/KG 0.12 1.0 

2.8 MG/KG 0.21 1.0 

190 MG/KG 3.3 110 

0.01 u MG/KG 0.01 1.0 

3020 MG/KG 2,1 1.0 

0.10 MG/KG 0.03 1.0 

727 MG/KG 0.91 1.0 

7.0 MG/KG 0.03 1.0 

0.27 u MG/KG 0.27 110 

1550 MG/KG 0.72 1.0 

0.24 MG/KG 0.23 1.0 

9420 MG/KG 0.85 1.0 

0.46 MG/KG 0.29 1.0 

0.41 u MG/KG 0.41 1.0 

0.89 MG/KG 0.44 1.0 

69.3 MG/KG 2.1 1.0 

1.4 MG/KG 1.0 1.0 

16.3 MG/KG 0.009 1.0 

0.66 u MG/KG 0.66 1.0 

0.83 u MG/KG 0.83 1.0 

0.25 MG/KG 0.08 1.0 

78.6 MG/KG 0.15 1.0 

000000033

CLIENT: TNUNAMFORD RC-047 K0202 

WORK ORDER: 11343-606-001-9999-00 

SAMPLE SITE ID ANALYTB 

-012 JIIL21 Silver, Total 



Boron, Total 

Barium, Total 





Cobalt, Total 


Copper, Total 

Iron, Total 







Sodium, Total 

Nickel, Total 


Lead, Total 




Tin, Total 





Zinc, Total 

Lionvilla Laboratory, Inc. 


LVL LOT M! 06041,904 



0.07 u MG/KG 0.01 1.0 

41.9 MG/KG 2.2 1.0 

0.56 u MO/KG 0.58 1.0 

0.23 u MG/KG 0.23 1.0 

5.4 MG/KG 0.02 1.0 

0.02 u MG/KG 0.02 1.0 

0.49 u MG/KG D.49 1.0 

18900 MG/KG 1.6 1.0 

0.07 u MG/KG 0.07 1.0 

0.13 u MG/KG 0.13 1.0 

0.70 MG/KG 0.12 1.0 

2.9 MG/KG 0.21 1.0 

172 NO/KO 3.3 1.0 

0.01 u MG/KG 0.01 1.0 

2680 MG/KG 2.2 1.0 

0.13 MG/KG 0.03 1.0 

691 MG/KG 0.92 1.0 

4.9 MG/KG 0.03 1.0 

0.28 u MG/KG 0.28 1.0 

1600 MG/KG 0.72 1.0 

0.23 u MG/KG 0.23 1.0 

10600 MG/KG 5.1 6.0 

0.33 MG/KG 0.30 1.0 

0.42 u MG/KG 0.42 1.0 

1.2 MG/KG 0.45 1.0 

54.5 MG/KG 2.1 1.0 

1.1 MG/KG 1.0 1.0 

17.6 MG/KG 0.01 1.0 

0.67 u MG/KG 0.67 1.0 

0.84 u MG/KG 0.84 1.0 

0.20 MG/KG 0.09 1.0 

78.3 MG/KG 0.15 1.0 

000000034

CLIENT: TNUHANFORD RC-047 K0303 

WORK ORDER: 11343-606-001-9999-00 

SAMPLE SITS ID ANALYTE 




Boson, Total 

Barium, Total 





Cobalt, Total 


Copper, Total 

Iron, Total 

Mercu ry , Total 






Sodium, Total 

Nickel, Total 


Lead, Total 




Tin, Total 

St ro ntium, Total 




Zinc, Total 



LVL LOT #: 0604 1,904 



0_07 u MO/KG 0.07 1.0 

53.9 MG/KG 2.2 1.0 

0.58 u MG/KG 0.58 1.0 

0.23 u MG/KG 0.23 1.0 

5.7 MG/KG 0.02 1.0 

0.02 u MG/KG 0.02 1.0 

0.48 u MG/KG 0.48 1.0 

18400 MG/KG 1.5 1.0 

0.07 U MG/KG 0.07 1.0 

0.13 u MG/KG 0.13 1.0 

0.65 MG/KG 0.12 1.0 

2.7 MG/KG 0.21 1.0 

177 MG/KG 3.3 1.0 

0.02 u MG/KG 0.02 1.0 

2900 MG/KG 2.1 1.0 

0.09 MG/KG 0.03 1.0 

656 MG/KG 0.91 1^0 

5.7 MG/KG 0.03 1.0 

0.27 u MG/KG 0.27 1.0 

1590 MG/KG 0.72 1.0 

0.29 MG/KG 0.23 1.0 

10300 MG/KG 5.1 6.0 

0.61 MG/KG 0.29 1.0 

0.41 u MG/KG 0.41 1.0 

0.64 MG/KG 0.44 1.0 

67.5 MG/KG 2.1 1.0 

1.3 MG/KG 1.0 1.0 

12.7 MG/KG 0.009 1.0 

0.66 u MG/KG 0.66 1.0 

0.63 u MG/KG 0.83 1.0 

0.20 MG/KG 0.08 1.0 

67.1 MG/KG 0.15 1.0 

000000035



CLIENT: TNGHANFORD RC-047 K0303 LVL LOT #: 0604L904 

WORK ORDER: 11343-606-001-9999-00 


SAMPLE SITE ID AMALYTB RESULT UNITS LIMIT FACTOR 

-014 JIIL26 Silver, Total 0.07 u MG/KG 0.07 .1 .0 







Calcium, Total 14300 MG/KG 1.5 110 












Sodium, Total 1610 MG/KG 0.72 1.D 












Zinc, Total 106 MO/KG 0.15 1.0 

000000036

CLIENT: T14URANFORD RC-047 K0203 

WORK ORDER: 11343-606-001-9999-00 


-015 7111,36 Silver, Total 



Boron, Total 

Barium, Total 


Biemuth, Total 



Cobalt, Total 


Copper, Total 

Iron, Total 


Potaaaium, Total 





Sodium, Total 

Nickel, Total 


Lead, Total 



silicon, Total 

Tin, Total 





Zinc, Total 



LVL LOT 8: 06041,904 



0.07 u MG/KG 0.07 1.0 

30.1 MG/KG 2.2 1.0 

0.58 u MG/KG 0.58 1.0 

0.23 u MG/KG 0.23 1.0 

6.0 MG/KG 0.02 1.0 

0.02 u MG/KG 0.02 1..0 

0.49 u MG/KG 0.49 1.0 

11200 MG/KG 1.6 1.0 

0.07 u MG/KG 0.07 1.0 

0.13 u MG/KG 0.13 1.0 

0.48 MG/KG 0.12 1.0 

2.7 MG/KG 0.21 1.0 

114 MG/KG 3.3 1.0 

0.02 u MG/KG 0.02 1.0 

2690 MG/KG 2.2 1.0 

0.08 MG/KG 0.03 1.0 

429 MG/KG 0.92 1.0 

3.5 MG/KG 0.03 1.0 

0.29 u MG/KG 0.28 1.0 

1490 MG/KG 0.72 1.0 

0.36 MG/KG 0.23 1-0 

6620 MG/KG 0.86 1.0 

0.30 u MG/KG 0.30 1.0 

0.42 u MG/KG 0.42 L.0 

0.97 MG/KG 0.45 1.0 

56.8 MG/KG 2.2 1.0 

1.5 MG/KG 1.0 1.0 

6.7 MG/KG 0.01 1.0 

0.67 u MG/KG 0.67 1.0 

0.84 u MG/KG 0.84 1.0 

0.18 MG/KG 0.09 110 

41.4 MG/KG 0.15 1.0 

000000037

Lionville Laboratory, T.C. 

INORGANICS METHOD BLANK DATA SUMMARY PAGE 06/06/06 

CLIENT: TNURANPORD RC-047 X0303 LVL LOT k: 0604L904 

WORK ORDER: 11343-606-001-9999-00 


SAMPLE SITE ID ANALYTB RESULT UNITS LIMIT FACTOR 

SLANKL 06LO324-MB1 Silver, Total 0.07 u MG/KG 0.07 1.0 





Beryllium, Total 0.02 u MG/XG 0.02 1.0 

Bismuth, Total 0.61 v MG/XG 0.51 1.0 

Calcium, Total 1.6 u MG/XG 1.6 1.0 



Chromium, Total 0.13 a MG/KG 0.13 1.0 

Copper, Total - 0.56 MG/KG 0.22 1.0 

Iron, Total 3.5 u MG/KG 3.5 1.0 

Potassium, Total 2.3 u MG/KG 2.3 1.0 


Magnesium, Total 0.97 u MG/KG 0.97 1.0 

Manganese, Total 0.03 u MG/KG 0.03 1.0 


Sodium, Total 0.76 u MG/KG 0.76 1.0 

Nickel, Total 0.24 u MG/XG 0.24 1.0 

Phosphorus, Total 0.90 u MG/%G 0.90 1.0 



Selenium, Total 0.47 u MG/KG 0.47 1.0 

Silicon, Total 2.3 u MG/KG 2.3 1.0 




Uranium, Total 3.6 MG/KG 0.88 1-0 


_ Zino, Total 0.16 u MG/KG D.16 1.0 

BLANKS 0600086-MB1 Mercury, Total 0.02 u MG/KG 0.02 1.0 

000000038

CLIENT: TNUNANFORD RC-047 K03O3 

WORK ORDER: 11343-606-001-9999-00 

SAMPLE SITU ID ANALYTB 

-001 J11KK8 Silver, Total 



Boron, Total 

Sari., Total 





Cobalt, Total 


Copper, Total 

Iron, Total 






Sodium, Total 

Nickel, Total 


Lead, Total 




Tin, Total 





Zinc, Total 


INORGANICS ACCURACY REPORT 06/08/06 

LVL LOT M: 06O4L904 

SPIKED INITIAL SPIKED DILUTION 

SAMPLE RESULT 

AMOUNT 

4R9COV FACTOR(SPK) 

....... 

4.4 

....... 

O.07u 

...... 

4.8 

....... 

91.7 

.......... 

1.0 

200 26.2 190 91.5 3.0 

179 O.58u 190 93.2 1.0 

90.6 0,45 95.2 94.7 1.0 

199 4.4 190 97.1 1.0 

4.2 O.02u 4.9 87.5 1.0 

454 O.49u 476 95.4 110 

900 9790 2380 677.1+ 1.0 

4.4 O.O7u 4.8 91.7 110 

43.7 O.13u 47.6 91.8 1.0 

16.6 0.41 19.0 95.8 1.0 

23.9 - 2.6 23.8 89.1 1.0 

252 94.3 95.2 165.1 1.0 

070 2680 2380 100.3 1.0 

106 0.1 95.2 111.2 1.0 

980 471 2380 105.4 1.0 

50.1 3.0 47.6 98.9 1,0 

87.5 0.28u 95.2 91.9 110 

850 1340 2380 105.2 1.0 

44.9 O.23u 47.6 94.1 1.0 

500 6060 476 1553 * 6.0 

44.7 O.3OU 47.6 93.9 1.0 

43.3 0.42u 47.6 91.0 1.0 

174 0.63 190 91.1 1.0 

177 42.9 95.2 140.4 1.0 

83.3 1.0 u 95.2 87.5 1.0 

LIS 10.9 95.2 112.2 1.0 

L74 0.67u 190 91.6 1.0 

lie 0.84u 238 91.7 1.0 

44.7 0.14 47.6 93.6 1.0 

LOS 46.6 47.6 131.5 1.0 

000000039


INORGANIC$ ACCURACY REPORT 06/06/06 

CLIENT: TNURANPORD RC-047 KO3O3 LVL LOT tl: 06O41,9O4 

WORK ORDER: 11343-606-001-9999-00 


SAMPLE SITE ID ANALYTE SAMPLE RESULT AMOUNT 4RECOV PACTOR(SPK) 

-002 S11KLS Mercury, Total 0.16 O.02u 0.16 99.4 ' 1`0 

966696049


INORGANICS PRECISION REPORT 06/08/06 

CLIENT: TNUNANPORD RC-047 K0303 LVL LOT M: 0604L904 

WORK ORDER: 11343-606-001-9999-00 

INITIAL DILUTION 

SAMPLE SITE ID ANALYTE RBS13LT REPLICATE RPD FACTOR(REP) 

-001REP JS11UC8 Silver, Total 0 . 07u 0 . 07u NC 1.0 •• 

Aluminum, Total 26.2 67.2 87.8 1.0 

Arsenic, Total 0.58u 0.58u NC 1.0 

Boron, Total 0.45 0.26 54.6 1.0 

Barium, Total 4.4 4.6 4.4 1.0 

Beryllium, Total 0.02u 0.02u NC 1.0 

Bismuth, Total 0.49u 0.49u NC 1.0 

Calcium, Total 9790 17500 56.6 1.0 

Cadmium, Total 0.07u 0.07u NC 1.0 

Cobalt, Total 0.13u 0.13u NC 1.0 

Chromium, Total 0.41 0.71 54.0 1.0 

Copper, Total 2.6 2.6 0.00 1.0 

Iron, Total 94.3 287 101.1 1.0 

Potassium, Total 2680 2740 2.1 1.0 

Lithium, Total 0.1 0.17 56.4 1.0 

Magnesium, Total 471 667 34.4 1.0 

Manganese, Total 3.0 5.4 57.1 1.0 

Molybdenum, Total 0.28u D.2RU NC 1.D 

Sodium, Total 1340 150D 11.0 p 1.0 

Nickel, Total 0.23u 0.29 -iC' l^ 1.0 

Phosphorus, Total 6060 9340 42.6 1.0 

Lead, Total 0.30u 0.42 JN.- 1.0 

Antimony, Total 0.42u 0.42u NC 110 

Selenium, Total 0.63 0.82 25.5 1.0 


Tin, Total 

42.9 

1.0 u 

64.9 

1.1 

40.8 

,?1C 

Y^ 

Tr 

1.0 

1.0 

Strontium, Total 10.9 13.3 19.6 1.0 

Thallium, Total 0.67u 0.67u NC 1.0 

Uranium, Total 0.84u 0.84u NC 1.0 

vanadium, Total 0.14 0.29 72.1 1.0 

Zinc, Total 46.6 69.2 39.0 110 

000000041


INORGANICS PRECISION REPORT O6/OSI06 

CLIENT: TNURANPORD RC-047 K03O3 LVL LOT k: 06041,904 

WORK ORDER: 11343-606-001- 9999-00 


SAMPLE SITE ID ANALYTE RESULT REPLICATE RPD FACTOR (REP) 

-0O2REP J1lKL5 Mercury, Total O.O2u 0.O2u NC 1.0 

699690042


LCS1 06L0324-LC1 

ANALYTB 

Silver, LCS 

Aluminum, LCS 

Arsenic, LCS 

Boron, LCS 

Barium, LCS 

Beryllium, LCS 

Bismuth, LCS 

Calcium, LCS 

Cadmium, LCS 

Cobalt, LCS 

Chromium, LCS 

Copper, LCS 

Iron, LCS 

Potassium, LCS 

Lithium, LCS 

Magnesium, LCS 

manganese, LCS 

Molybdenum, LCS 

Sodium, LCS 

Nickel, LCS 

Phosphorus, LCS 

Lead, LCS 

Antimony, LCS 

Selenium, LCS 

Silicon, LCS 

Tin, LCS 

Strontium, LCS 

Thallium, LCS 

Uranium, LCS 

Vanadium, LCS 

Zinc, LCS 

LCS1 0600086-LC1 Mercury, LCS 


INORGANICS LABORATORY CONTROL STANDARDS REPORT 06108106 

CLIENT: TNUHANPORD RC-047 K0303 LVL LOT 4: 0604L904 

WORK ORDER: 11343-606-001-9999-00 

SPIKED SPIKED 

SAMPLE AMOUNT UNITS 4RECOV 

49.2 50.0 MG/KG 98.4 

446 500 MG/KO 89.3 

972 1000 MG/KG 97.2 

487 500 MG/KG 97.4 

493 500 MG/KG 98.6 

23.7 25.0 MG/KG 94.8 

487 500 MG/KG 97.4 

2530 2500 MG/KG 101.3 

24.9 25.0 MG/KG 99.6 

247 250 MG/KG 99.0 

50.3 50.0 MG/KG 100.6 

114 125 MG/KG 91.4 

499 500 MG/KG 99.8 

2330 2500 MG/KG 93.2 

512 500 MG/KG 102.4 

2470 2500 MG/KG 99.0 

76.7 75.0 MG/KG 102.3 

508 500 MG/KG 101.5 

2360 2500 MG/KG 94.2 

200 200 MG/KG 100.2 

445 500 MG/KG 89.1 

248 250 MG/KG 99.3 

294 300 MG/KG 98.1 

92B 1000 MG/KG 92.8 

342 500 MG/KG 69.6 

505 500 MG/KG 101.0 

492 500 MG/KG 99.5 

995 1000 MG/KG 99.5 

251 250 MG/KG 100.4 

249 250 MG/KG 99.5 

98.1 100 MG/KG 98.1 

6.5 6.2 MG/KG 104.6 

000000043

Lionville Laboratory Use Only 

Eat. Final Prof. Sampl ing Date 

Project 

Project ContocWhone N 

Lionville Laboratory Project Manager 

` 

QC _ S^CG _ Del ^( a. -.._ TAT 

Date Rec'd 

LL 

U(, Dale Due 

u 

S/J b^: /^ b.' 

MATRIX 

CODES: 

S . SON 

SE - Sediment 

SO - Solid 

SL- Sludge 

W - Weber 

O . Oil 

A- 

Ale 

DS- Drum 

Sales 

DL. Drum 

Liquids 

L - E%lCLP 

Leaclrete 

Wl - Wipe 

x - Other 

F - Fish 

Lab 

ID 

W 

J 11 KX8 

1w 

Custody Transfer Record/Lab Work Request Page 1 of a Vil VLI 

LC^^^ } FIELD PERSONNEL: COMPLETE ONLY SHADED AREAS 

C li 

ent IDIDescdpson 

a,- 

Special lm truetlow -Vt-CV.-I, ljF_,b.Ur^ - 

i`001 

Î jwo c'Ld^s^ a. ,bc", r A o 

nleduls, pus, 5 %/« 

-Suv-,^ 060 - 0015-Vil, 4JLLJ 

M e,A-oJf> PCB, P-ra+ r SOYL . 

ReNngWshed Remind 

by i by 

Dole TNrla 

Ki.t J (^/, 

Rel 

ReMgerelar X 

•/Type Container 

Volume 

Prese rvatives 

ANALYSES 

REQUESTED 

Liquid 

Sold 

Liquid 

Solid 

Malrlx 

OC 

Clen as 

V) 

Malrbr 

Date Time 

Collected Collect 

_wAha^^m 

sMM®N 

one 

DNS: ,/ 

i. 

z. 

3. 

a. 

S. 

8. 

Recohrod 

Raw"wehad- Received 

Data Tunis 

Irl W 

by 

W AS TEN 

CveB SRC v 

i 

two Time 

m 

G 

ne 

ON 

M n

Lionville Laboratory Use On ly 

Custody Transfer Record /Lab Work Request Page moo► -;L 

FIELD PERSONNEL: COMPLETE ONLY SHADED REAS 

Client! J C 

Retrlgeraux # 

Eat Final Prol, Sampling Date 

Project # 

Proje 

aQ 

#/Type Container 

Liqu b 

sous 

U uia 

ct 

ContacttPtlone # Volume 

Lionville Laborato ry Prole 

OC Del 

ensger 

TAT 

Pretereellves 

Solid 

ORGANIC I NORG 

Date Recd Dale Due 

ANALYSES 

REQUESTED 

Is- Q 

p 

< 

to 

a P 

= 

1i 

- '^ 

V 

MATRIX 

j Lbmllle Laboratory Use Only j 

CODES: 

a- soil 

Sediment 

SO • Solid oot 

SL- Sludge 

W .Water. 

0- ON 

Db 

Client ID/Description 

MsMs 

OC 

Chosen 

V1 

MS IMSD 

Mad" 

Date Time 

Colleeled Collected 

y^ 

O 

o 

O U 

A. Air a 

l7s- Drum 

Solids 

DL- Drum 

oZ^ 

^/ 

.X 

^j J 

Liquids I J1 L a3 13^b .::.: - X X 

[L 

- x 

L - EP/TCLP 

LaMiats 5 a - X j^ . . X 

w,- YApe 

X. Mer 015 Jt1 S-2 v lom 

ofS X xi X X 

F- Fish 

Special Instruc tions: 

DATE/REVISIONS: 

J7,(^ a. 

Re6nb bhsd Received 

Dais 

RNingalshed Received 

Time 

Dole Time 

Res shed Received 

by by by by by 

x a3 

2. 

4. 

6. 

6. 

Deb Time 

'Kan, 

a 

m

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047 259 Pain -I of 1 

Collector 


Company ContactTelenhone No, 



KESSNER, IH Price Code 9N Data Turna round 

Atr Qwlaty q 

45 Days m 

rolect DesianaHon Sanmlina Locat ion SAF No. 

100 & 300 Area Component of the RCBRA S ediment and Ti 600-132/600-190 OFFAL RC-047 9 

Ice Chat No. Field Loaboolc No. COA Method of Shioment m 

EL-159S BESRAS6520 FED EX m 

Shipp Offsik Proaeriv No. ? 

Bi 

®^J 

ll of Lad in stAir Bi ll No. 

QLAERLINE SERVICES LIONVILLE _ ^^^ SEE OSPC 

POSSIBLE SAMPLE RAZARDS/REMARJSS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-266 

Collector 

TILLER, B. rA KLIN 

lest Deslanation 

100 k 300 Ana Component of the RCBRA Sediment and T1 

Ice Chi N%yc p 

PirG C-Q2- Qr 

Comaanr Contact 

JOAN KESSNER 

Samolioa location 

JBB4H-24 OFFAL Ili O 7-112 

Fltl k No. 

EL- 1595 

Teleabone No. 

375.4688 

COA 

BESRAS6520 

Pags 1 of 1 


KESSNER, JH Price Code g]v Data Turnaround IT 

IT 

,a 

45 Days 6 


Air Quality E] m 

RC-M7 


FED EX 

Slijinago To Oaaile Prooertv No. q^6 D ^ d Bi ll of LdindAlr Bill No, 

EBER . IN ERVIC[Sy LIONVILLE 

/7 SEEOSPC 

POS E HAZARDSWMARKS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-267 Pw 1 of I 

Collector Com pa ny Conta ct 

TILLER, B. TN KLINCKMAN JOAN KFESSNER 

Telephone No, 

375-4688 

Pro ieet Coordirulor 

KESSNER, IH Price Code 9N Data T7lrnarsund00 

It 

Protect factiona lism 

100 & 300 Ara Compooeul of the RCBRA Sediment and Ti 

Stmmline Locaflon 

110-N-3 OFFAL 



Air Quality q 45 Days m 

0 

Ice Chat No. Field Logbook No. COA Method of SWnmeat 

î ^^-- ." -'IjOJT EL, 1595 BESRAS6520 FED EX m 

Shin Olraite Property No. 

/J /l 

of Lad hWAtr Bi ll • ERI.iNE SERVICES LIONVILLE O^v 6K13 6) 

No. 

SEE OSPC 

POSSIBLE SAMPLE AAZARDS(REMARKS 

POTENTIAL RADIOACTIVE k;'"I" 

Bill 

AG G/P G/P eG aG aG 

1 

I B a 0 0 

250g log 155 505 mg 50g 

Seek—Win Seeite-Ml- SeehenMi. PCB.- 31182 Pw& _ SmaFVOA- 

Spaiol Sp..:, Spnial 1011 9270A(7CLI 

humwkau Iwrrmum. me,sener, , 

-.";_ _ 

J71KL6 OTHER SOLID APR 01 1006 IVLCJ Al X x 

,.»+s `1:s` ,,, "f-`*"^'`^ a.t.:^'un 1`'' ,s, â4 _'^' ti':,' - ^` t'`3--" 

CHAIN OF POSSESSION Si6n/Prinl Names SPECIAL INSTRUC`nONS 

Matrix • 

8tquidcd By/Removed Tom rose NOTE: Rwrlfim- ^^ 

vamo paWTIimr 

perfam Genera Spec Nee vaaship bottle to 1]otrville Labs, if p ossible maintain 4 C 

EAS LOCKED STOR GE •Y- °" 

Got++* cooling. n& LAWnille: pmferm secants, this is surykis available. Canon Joan 

s6seAnmt 

Kessler upon receipt. _ a^J 

' s A Aw Dawelriroe iwd By/Stored In 

V Flo 

d B lRenloved t Dame Remived B r/Slarxd 

N 

t*iA 04 

DoaelFnrtr 

tr 

D! 

me 

; 

(1)Gao nnSpec-(Full 

Us t) l Anrcm io241, Aveissmy-127, Be Beryllium-7, 7, Cesium- 134, Cesium 137. 

Cobak-60.Erro0uml52,EmoO 154, Ewapiw 155,Pa sim 40, RaAium226. Radium?g, 

- Ru1hmmmlo6, Uranium2i5. Urariwn2381 

l'-)SaaMm iu89,90--To 

msaw, 

0'a 

ta .— 

B 

b 

emgved Rpn I)aieTmr Reccived 5 din 

/, 

7 /i I^.UO F^l^ 

b 

ime 

l Sr Isotopic lnon lThm m t2321: Isatlpit Utiure m l Urary um233f274, 

Unoin235. m L4 n 2381; Is otopic nonlinu 

Month 

Ma - 6010 (Full Lisa) I Aluminum num Antimony. A rsenic, Ba rium, Beryl 

os.d,..s,s,a. 

m.o,.eLws : 

T•T 

li 

X 

nonli 

(3) ICP 

um, Bistauk Boron 

Cadmi CadmiumCalcium Calcium Llnmium. 

Cobal4 Coypuron 

Manganese. 

. I I:ad, lithium Magnesiumq Mangaae. 

Molybdenum Nickel, Phosphorus. Pa sion Se lenium Silicon. Silver. So di she y/R Flop O+te/fitrc Received 

x 3 

Dote?inc 

um Strontium Thallium 

T^&Llmnium Vandium7iml:Mem y-7471-(CV) 

x"a 

Relirpuishe y/Renpved From Da¢Tnx ived By/Swr4i TA Dale/rine 

LABORATORY Received By Tide Date/rime 

SECTION 

FINALSAMPLE Disposal Method Disposed By Daterrine 

DISPOSiTiON 

BHI-EE-011 (08/2912005)

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-271 Pa9F 1 -I 

olledor Company Ca rrie d Telephone No. Prulact Coord in ator 

TILLER, B. TR KLINC JOAN KESSNER 375-4688 KESSNER, IH 

rolect Desienation Serenade Location SAF No. 

100 & 300 Am Component of the RCBRA Sediment and n 1607-D2:1 OFFAL RC-047 

[ce Cheat Na. r e- DI '^ No. 

Fk EL-1595 

S 

Offshe Property No. ADG DJ rI[/ 

BESRAS6520 

BN of Ladhie/Alr Bill No. 

ERIJNE SERVIC LIONVBLB JJ SEE OSPC 

POSSIBLE SAMPLE HAZARDS MEMARKS 

POTEMTIALRADIOACTIVE

WashlnRton Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047473 J PW 3 err 3 

Follecter 

TILLER, B. TA KLINCKNIAN 

Co mwr Contact 

JOAN KESSNER 

Telrobooe No. 

375-4688 

Pro kct Coordinator 

KESSNER. B-1 

rice Cods 9N 

Data Ttu-narotl Iect Dada nation 

100 & 300 Area Component of the RCBRA Sediment and Ts 

Samullm Loca tion 

BORROW PH' 24 OFFAL 



Air Quality q 45 Daym 

IceChesiNo. p _ Field Loebook No. 

EL-1595 

COA 

BESRAS6520 

MetLadorShbm 

FED EX 

t 

m 

9 

Shi Odsite Prooertr No. BIB of Ladh»/Air BIB No. 

ERLME SERVK;ES LIONVILLE /-'^fDO 0 SEE OSPC 



v 

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-274 J PAV 1 °f J 

Collector 

TILLER, B. 

Tfl KLINCKMAN 

Protect Dasimation 

100 & 300 Area Component of the RCB RA Sediment and Ti 

Ice Chest No. 

- 4"e-O2 

Cmulpsuy Contact Telephone No. 

JOAN KBSSNER 375J688 

Sammlissa Location 

YAKIMA RIDGE II OFFAL 

Field Loabook No. 

EL, 1595 

COA 

BESRAS6520 

Protect Cootdinalor 

KESSN8R, 1H 

SAF Na 


Price Code Data 9N TutnRrotuo-+ 

In 

45 Da m 

Alr Quality El 

m 

Method of Shipment 0] 

FED ETC 

m 

Shi Oftalte Properly No. QO /D Big LLSt^dAlr Bill No. 

T 

RERLINE SERVICES LIONVIILE H 

POSSIBLE SAMPLE IIAZARDSIREMAIM 

0 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-275 J NF L of L 

TILLER, B. TR KIINCKAtAN 

C JOAN ESSNER 

T o 

375-4688 KESSNEA, Hlpator Price Code 9N Data TurnaroupdN 

roleet Ded imation Sampling Location SAF No. Air Quality E] 

100 & 300 Area Compon ent of the RCBRA Sediment and Ti VERKITA UPRIVER ON SOUTH SIDE OFFAL RC-047 

In 

45 Days (m 

Ice Cheat No. /^ /^ ^±^ Field Logbook No. COA 

m 

Metkod of Shipment 

4 T C' 612 ',7 a' `r FL- 1595 BESRAS6520 FED FX m 

9 

S OtTsite Proxrly No. Bie of LadhadAir Bill No. 

_ RERIAI@SERVICPS^ pNVIIAE Ôdo 33 o SEEOSPC 

POSSIBLE SAM I 7.A REMARKS 

POTEN7ALR4010ACTIVE


Collector 

TILLER, B. TR KUNCKMAN 

roieet Desho stlose 

100 & 300 Area Component of The RCBRA Sediment and Tie 

Ice Chest No.Â 

G — OZ -Sz s - 

S EBE L o S .R LIONVRJE 

POSSIBLE SAMPLE nAZARDS IR MARKS 


LOAN KESSNER 375-4688 

Safrplloa Loca tion 

McOEE RANCH OFFAL 

Fi el d Logbook No. 

EL-1595 

OHsile Property No. 

POTENTIAL RADIOACTIVE 

_ 

Washington Closure Hanford CHAIN OF CUSTOIJIMAMPLE ANALYSIS REQUEST RC"047.277 I NP L of L 

Reclor _ 

Comoaor Contact Telmhone No. Protect Coordinator 

9N 

Price 

Data Tutnarousut 

TILLER, B. 11 KUNCKMAM - JOAN KESSNER 775-4688 KESSNER, 7H 

In 

rolectDeslanation Sa urnslinaLoealim SAFNo. 

AI[ 45 DaySm 

Quality q 

100 &300 Am Component of the RCBRA Sediment and Ti SADDLE MOUNTAIN OFFAL RC-017 m 

0 

Ice Chest No. o 

Field Loaboolc No. COA Melhad of SWm Sent 

m 

r/C c- Q.z-'lUs 

EL-1595 BESRA56520 FED EX m 

ShalooedTo - OBslle Property No. Bill Ladina/A ir Bi ll No. 

BE L.AIESERVIC LIONVILLE 1 406 b 3 3 D 1 EEOSPC 



Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-322 Page L of I 

Collector 

TILLER, B. TN KLINCKMAN 


JOAN KFSSNER 

Telephone No. 

375-4688 


KESSNER, lH Pria Cow 9N Data 7•aswrou 

In 

Air Quality p 45 Days% 

Protect Designation Sampline Location SAF No. 

100 & 300 Area Component of the RCBRA Sediment and Ti 1(10-DO8:2 OFFAL RC-047 m 

lee Chen( No. r Field Logbook No. COA Method of Shipment 

EL-1595 BEESSRAS6520 FED EX 

ShjRocdTo O(LSile Property No. 0 / ^ 

E RLM LIONVILLE g O (/ 

POSSIBLE SAMPLE H AZARDS/REMARKS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-323 Pea 1 of I 

cotledcor 


Prolect Dafenallo p 

100 & 300 Area Cam ent of the RCBRA Sediment and Ti 

I" Chest No. 

. 

y^ 

g j^C-01 '„rdf 

Company Canted Telephone No. 


SamolWa Loaaon 

100-D-492 OFFAL 


KESSNER, )H 

SAFNo. 


FirW Loahaok No. 

COA 

Method of Shfomepl 

Shipp ed To 

EI. 1595 

ORsite Property No.yy^^ G 

/'>'Qlo6?.3 

BFSRAS6520 

FED EX 

Bi ll ER ESERVIC LIONVRtE 

of Ladipe/Air Bill No, 

EE OSPC 

POSSIBLE SAMPLE HAZARDS(REMARKS 


Washington Closure Hanford " CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-328 gR 1 of I 

Collector Company Contact Telephone No. Proled Coordinator 

Price Code 9N Data Turnamm 

TILLER, B. TR KLINCKMAN JOAN KESSNER 375-4688 - KESSNER, IH in 

Protect Designation Samoan Loca 

Air Quality q 45 Days% 

ti on SAF No. 

100 & 300 Area Compon en t of the RCBRA Sediment and Ti 116-DR-I.DR-2/100-D-22 OFFAL RC-047 m 

Ice Chest No.n Feld Logbook No. COA Method of Shiomeal m 

O/c C— 0.2 '4rQ.r El: 1595 - BFSRAS6520 FED EX m 

Shi 'o Offaite Properly No. ^D 

Bill of LadiaWAir Bill No. 

OERLINE SERVICES LIONVILLE SEE OSPC 

POSSIBLE SAMPLE HAZARDS/REMARES 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE -ANALYSIS REQUEST RC-047-330 [Ng- 

Collector 

TILLER, B. 

TB KLINCKMAN 

Protect Dealenadon 


Ice Cheat No . yy ^ 

/Lxe e2 -„s175 

Sh' 

ComOauv Contact Telephone No, 

JOAN KESSNER 375.4688 

Saco olina L. scaflon 


Field Loabs6ok No. 

EI.- is93 

Off lte Properly No. 

^ 

COA 

BESRAS6520 - 


KPSSNER, III 

2 Big of LadilldAir Bill No. 

B FJ2LINESERVICPS LK)NVILLE 

4Os%s3t^ SEE OSPC 

1s SSIBLE SAMPLE IIAZARD.MU MARKS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC447-332 jPw I ar i 

Collector Company Contact Telephone No. Protect Coordinator 

TILLER, B. TR KLINCKMAN JOAN KESSNP,R 3754688 KESSNF.R, JH Prim Code 9N Data Turnaround; 

diem Desiapaaon Samptina Lorstim SAF No. 

100 & 300 Area Component on of the RCBRA Scdimml and Ti 600-131 OFFAL RC-047 

Method 

lee Chest No. FiE 1595ookNo. 

aFjCC-0,2-tvs, BESRAS6520 

FED EX 

SAipped To 

ESERVI /LIONVILIE 

Ofbite Property No. ^/^n/ Q p 

/lf/Y/U33o 

Bill of Ladlae,/Alr Bill No. 

SEE OSPC 

POSSIBLE SAMPLE 11AZARDSMEMARKS 

POTEA77AL RADIOACTIVE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-343 P 3 d 1 

Collector 


Coolant, Contact 

JOAN KESSNER 

Telephone No. 

375.4688 

Protect Coordina tor 

KESSNER, IH 

Price Cade 9N Data Turparou11a9 

w 

Protect Designa tion 

100 & 300 Ar a Co entof the RCBRA Sedim 

Samplingtion Loca SAF No. 

AIC Quality C] 

45 Days 

m 

e 

en t and Ti CENTRAL PLATEAU SHRUB STEPPE OFFAL RC-047 m 

Ina Chest No. 

4ce e^"U 2- 

Field Logbook No. COA Method of Shipment mm 

—,D,% ELLI595 BESRAS6520 FED EX m 

Sh ORstle Property No 

Air BW No. 

_ BERLBdE SERVICE LIONVILE 14 0 6 033D 

B ll E OSPC 

POSSIBL PLEHAZARDSIREMARKS 

PO7'EA77AL RADIOACTIVE



CLIENT: __Tt U 1aRr^ c^ Date: 

e Order / Pmjact# 1 

SAFN / W# / Release #: RC ^^^ 

v Batch #: r I n T I Sample Custodian: 

1. Samples Hand Delivered QLShipped 



3. Outside of coolers or shipping containe rs are 


4. All expected papetworkreceived (roc and 

other client specific information) sealed in 


5. Samples Mcciv4 cool r ambient? Z Q 

6. Custody seals on sample containe rs intact. 



S. Sample containers are intact? 







SR-001-11 

13. VOA, TOC, TOX free of headspaoe? 


client? 


Po licy? (Identify all bottles not within 


16. Project Manager c=bwtedconcetactg 

discrepancies? namedate (or samples 

outside crite ria) 

vLI 

?4rs 

1/O 

7 

O No 

Yes O No 

Wes O No 

TTemp '7 3 °C 

¢(Yes O No O No Sells 

.r 

es 13 No 

0 Yes O No 

(L^Ya O No 

Yet q No 

)dYa 

O No 

Yes 

Jd O No 

0 Yu 

O Yes 

O Yes 

i7Yes 

q No ,ey NIA 

q No /C^4A 

O NO 

a7 a S 05 '7 

Airbill# 7 Cf 

O No Sells Comments 

Cooler# SAuDS—\b---3 

O No 

Dis r zodn 

000000061


BNA ANALYTICAL DATA PACKAGE FOR 


DATE RECEIVED: 04/28/06 LVL LOT # :0 E 

N 

r 

MME i 

3V` 24 

CLIENT ID LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS 

J11KKB 001 SO 06LE0457 04/05/06 06/02/06 06/29/06 

J11KKB 001 MS SO 06LE0457 04/05/06 06/02/06 06/29/06 

J11KK8 001 MSD SO 06LE0457 04/05/06 06/02/06 06/29/06 

J11KL5 002 SO 06LE0457 04/05/06 06/02/06 07/02/06 

JIIKL6 003 SO 06LE0457 04/03/06 06/02/06 06/30/06 

J11KMO 004 SO 06LE0457 04/05/06 06/02/06 06/30/06 

J11KM2 005 SO 06LE0457 04/03/06 06/02/06 06/30/06 

J11KM3 006 SO 06LE0457 04/03/06 06/02/06 06/30/06 

J11KM4 007 SO 06LE04S7 04/03/06 06/02/06 06/30/06 

J11KM5 008 SO 06LE0457 - 04/03/06 06/02/06 06/30/06 

J11KM6 009 SO 06LE0457 04/03/06 06/02/06 06/30/06 

J11KV1 010 SO 06LE0457 04/05/06 06/02/06 06/30/06 

J11KV2 011 SO 06LE0457 04/05/06 06/02/06 06/30/06 

J11L21 012 SO 06LE0457 04/03/06 06/02/06 06/30/06 

JllL23 013 SO 06LE0457 04/03/06 06/02/06 06/30/06 

0111,25 014 SO 06LE0457 04/05/06 06/02/06 06/30/06 

JIIL36 015 SO 06LE0457 04/03/06 06/02/06 06/30/06 

LAB QC: 

SBLKZH MB1 S 06LE0457 N/A 06/02/06 07/02/06 

SBLKZH MB1 BS S 06LE0457 N/A 06/02/06 07/02/06 

000000001


Client: TNU-HANFORD RC-047 W.O. #: 11343-606-001-9999-00 

LVL #: 06041,904 Date Received: 04-28-2006 


SEMIVOLATILE 

Fifteen (15) soil (mice) samples were collected on 04-03,05-2006. 

The samples and their associated QC samples were extracted according to Lionville Laboratory 

SOPs based on SW 846 method 3540C on 06-02-2006 and analyzed according to criteria set forth 

in Lionville Laboratory SOPS based on SW 846 Method 8270C for TCL Semivolatile target 

compounds on 06-29,30-2006 and 07-02-2006. 




acceptance policy with the exception of some discrepancies, which were documented on the 

Sample Receipt Checklist. 

2. All samples were stored in a refrigerator (ID# R003) that malfunctioned and failed to 

maintain the required sample storing temperature (4°C +/- 2°C) on 05-10-2006. A copy of 

the Sample Discrepancy Report (SDR) has been enclosed. 

3. Samples were extracted outside required holding time. A copy of the Sample Discrepancy 

Report (SDR) has been enclosed. 

4. Due to the nature of the sample matrix, approximately 2g initial sample volume for the 

extraction and reduced final volume was used for the analysis. A copy of the Sample 

Extraction Record has been enclosed for detail information. 

5. All sample results were reported on a wet-weight basis. 

6. Non-target compounds were detected in the samples. 

7. Seventy-seven (77) of one hundred fourteen (114) surrogate recoveries were outside 

acceptance criteria. A copy of the Sample Discrepancy Report (SDR) has been enclosed. 

The results presented in this report relate only to the analytical testing and conditions of the samples at receipt and during storage. All pages of this report are integral parts of 

the analytical data. Therefore, this report should only be reproduced in its entirety of 5 3 pages. 


4(30.tVLi6(Cf4iL•

8. One hundred twenty-two (122) of one hundred twenty-eight (128) matrix spike recoveries 

were outside acceptance criteria. A copy of the Sample Discrepancy Report (SDR) has 

been enclosed. 

9. Sixty-three (63) of sixty-four (64) blank spike recoveries were outside acceptance criteria. 

A copy of the Sample Discrepancy Report (SDR) has been enclosed. 

10. The method blank contained the common laboratory contaminant Bis (2-Ethylhexyl) 

phthalate at a level less than the CRQL. 

11. Internal standard area criteria were not met for sample JllKK8 MSD. The analysis of 

associated matrix spike sample fulfills the reanalysis requirement. 

12. Manual integrations are performed according to SOP QA-125 to produce quality data with 

the utmost integrity. All manual integrations are required to be technically valid and 

properly documented. Appropriate technical flags are defined in the Glossary ("Technical 

Flags For Manual Integration"). 



analytes/methods, please contact your Project Manager. 

14. I certify, that this sample data package is in compliance with SOW requirements, both 


data, contained in this hard-copy data package, has been authorized, by the Laboratory 


am 

`l 

Iai aniel 

La ratory Manager 


som\gomp\data\bna\mu-hanford\0604-904.doa 


ate 

V 

•raasuswxat4u

_WrrvurV r..duvrdtory -)ampie 

Initiator. Orlette Johnson Batch: ^ 

Date: §117106 Samples: 

Client: dQt Method: 

RCoLi7 


ncy Keport (ZwK) 111 - ' to o rr 

Parameter: 

Matrix: i] A 

Prep Batch: 

a. COC Disc repancy , Tech P rofile Error Client Request Sampler Error on C-O-C 

Transc ri ption Error _ Wrong Test Code _ Other 


Missing Sample/Extract _ Container B roken Wrong Sample Pulled _ Label ID's Illegible 

Hold Time Exceeded Insufficient Sample Preserva ti on Wrong _ Received Past Hold 

_ Imp roper Bottle Type _ Not Amenable to Analysis X Other 

Note`: Verified by (Logan] or [Prep Group] (circle) ... signaturelcI ta: 

c. Problem (Include all relevant spe cific results; attach data if necessa ry) 

On 5/10106 sample storage refrigerator ID# R003 malfunctioned and was not holding the required sample storage 

temperature of 4°C +/- 2°C 

2. Known or P robable Causes(s) 

B ro ken motor 

3-Discussion and Proposed Action Other Desc ri ptions 

_ Re-log At the time of malfur ^tion R003 was used for storage of samples received 

_ En tire Batch for extractable organics, metals and wet chemist ry (except TOG) analyses. 

Following Samples: All samples we re removed from R003 to another refrigerator on 5110/06. 

_ Re-leach R003 was tagged out on 5/10106, repaired on 5112/06, and we have 

_ Re-extractcertified fiat R003 is maintaining the required sample storage temperatu re. 

_ Re-digest 

Revise EDD 

_ Change Test Code to 


4. Project Manager Instructions ... signaturerdate: 

Concur with Proposed Ac ti on 

ag ree with Proposed Action; See Instruc ti on 

nclude In Case Narrative 

Client Conta ^'' 

Date/Person t3 G`40 

_ Add 

Cancel 

5. Final Action ... s4nature/dau Other Explanation: 

_ VoRed rei4][leach][e ][digest][ n lysisJ clil 

eluded in Case Narrative 


Elect ro nic COC Revised 

_ EDD Cor rections Completed 

When Final Action has been recorded, forward original to QA Specialist for distribution and filing. 

Route Distribu ti on of Completed SDR Route Distribution of Completed SDR 

X Ini ti ator_ Metals: Welsh 

X Lab Manager. I. Dan' _ _ Inorganic: Perrone 

X P roject Mgr. Ston ohnso GC/LC: Kiger 

_ Data Management MS: Schnsider/Beley C6t r0(C rL 

_ Sample P rep: Beegle/Kiger — _— Login: Per ry 

b, 

Admin: 

O ther. 

c `^r6^`' 

QA-105-A-0805 

13 00000004

Lionville Laborato ry Sample Discrepancy Report (SDR) SDR #: 06PM002 

Initiator: Orlette Johnson Batch: 06d6l,gM Parameter. G6 2S14 

Date: 6/21/06 Samples: Matrix: 'td 

... 

Client: 1W 4vii6d A Q2_ Method: cAm1cLPr Prep Batch: 


a. COC Discrepancy _ Tech P rofile Error Client Request Sampler Error on C-O-C 

Transcription Error _ Wrong Test Code _ O ther 

b. General Discrepancy . 

_ Missing Sample/Extract _ Container B roken _ Wrong Sample Pulled _ Label ID's Illegible 

X Hold Time Exceeded Insufficient Sample _ Preservation Wrong _ Received Past Hold 


Note: Vented by [Log4ril or (Prep Group) (drde)...algnatureddate: 

c. Problem (In clude all relevant specific results; attach data if necessa ry) 

Sample(s) waslwe re extracted 4^ days beyond the hold time 

Sa* rt o4d to 4 js kw/ku?'^V6 &J1t.1A6 

Z Known or P robable Causes(s) due to a temporary glassware shortage created by a malfunc tioning d rying kiln I.e, 

much of our glassware was lost when one of the kilns overheated. We made eve ry effort to replace glassware as soon as 

possible but our needs exceeded on-the-shelf vendor stocks of certain c ritical Items. This problem was exacerbated by an 

unusually high number of samples received du ring this period of time for organics extraction. 

3. Discussion and P roposed Action Other Description: 

_ Re-log 

_ Entire Batch 

Following Samples: We have replenished glasswa re stocks to higher levels than those 

_ Re-leach in-house before the kiln malfunction. We have also replaced the kiln. 

_ Re-extract 

_ Re-digest 

_ Revise EDD 


_ Place O rdTake Off Hold (circle) 

4. P roject Manager Instructions ... smnature/date: 

_ Concur with Proposed Action 

Disagree with P roposed Action; See Instruction 

X Include in Case Narra ti 

ve 


Date/Person 

_ Add 

Cancel 

S. Final Action ... synatureidate: Other Explana ti 

on: 

Ve rified re-[log][leach][ digest][analysr ] ( rcle) 

X Included in Case Narrative 




When Final Action has been recorded, forward original to OA Specialist for distribution and filing. 

Route Distribution of Completed SDR 

X Ini 


ti 

ator 

X Lab Genera[ Man I. anrels 

X P roject Mgr. Ston o' son 

X Data Management 

_ Sample Prep: I(iger 

— 

_ Metals: Welsh 


GC/LC: Kiger 

'L `^ MS: Schne[de arclen 

_ _ Log-in: Per ry 

Admin: 


oA-ios-A-osos 

096000605

Lionville Laborato ry Sample Discrepancy Repo rt (SDR) SDR #: aarjrZZ? 

Initiator: Batch: L Parameter: 06WH 

Date: Samples: _ _ Matrix: 

Client: Method: wwi Prep Batch: 


a. CDC Discrepancy _ Tech P rofile Er ror Client RequestSampler Er ro r on C-0-C 

Transcription Er ro r _ Wrong Test Code _ Other 


_ Missing SampletExtract^ . _ Container B roken _ Wrong Sample Pulled _ Label ID's Illegible 

Hold Time Exceeded _ Insufficient Sample _ Preserva ti 

on Wrong _ Received Past Hold 

_ Improper Bo ttle Type _ Not Amenable to Analysis 

Note: Ve rified by [Log-Ini or [Prep Groupl (drde) ... aignatumWate: 

c. Problem (Include all relevant specific results; attach data If necessary) 

m 

4f 5-P6 IV FA" FCi^ntsV Gk l/hfrS 

2. Known or Probable Causes(s) ,,,, q, , ,^^ ^ _1 _ 4 _ ^,/^ eye `, 

Y"..'"' 

wlûGc aMr^ 

1&4) c*,,rp' 

3. Discussion and Proposed Action Other Description,`^"^v 

_ Re-log 

_ En ti 

re Batch 


Re-leach 

Re-extract 

_ Re-digest 

_ Revise EDD 


_ Place Onrrake Off Hold (circle) 

4. Pp6ject Manager Instructions ... signaturerd 

V Concur with P ro posed Action 

_ Disagree with P roposed Action; See Instruction 

_ Include in Case Narrative 


DatelPerson 

_ Add 

Cancel 

5. Final Action ... signatu re/date: 

_WVenilled re-[bg](leach)[e digest][analysisj ( 

Other Explanation: 

ci 

"ncluded in Case Narrative 

_ Hard Copy CDC Revised 


_ EDD Correc 

rcle) 

ti 

ons Completed 

When Final Action has been recorded, forward original to QA Specialist for dist ribution and filing. 


X Initiator 

X Lab General Manager aylor 

X P roject Mgr. Ston ohnson 

_ Data Management: 

_ Sample Prep: BeeglelKger 

_ 


— Beegle 


GC/LC: Kiger 

f MS: Rychl aley 

_ Log-in: Perarr 

_ _Admin: 


oA- 1 05-A-pep5 

000000006


GLOSSARY 

U = Compound was analyzed for but not detected. The associated numerical value is the 

estimated sample quantitation limit which is included and corrected for dilution and percent 

moisture. 

J = Indicates an estimated value. This flag is used under the following circumstances: l) when 

estimating a concentration for tentatively identified compounds (TICS) where a l:I 

response is assumed; or 2) when the mass spectral data indicate the presence of acompound 

that meets the identification criteria but the result is less than the specified detection limit 

but greater than zero. For example, if the limit of detection is 10 ug/L and a concentration 

of 3 ug/L is calculated, it is reported as 3J. 

B = This flag is used when the analyte is found in the associated blank as well as in the sample. 

It indicates possible/probable blank contamination. This flag is also used for a TIC as well 

as for a positively identified TCL compound. 

E = Indicates that the compound was detected beyond the calibration range and was 

subsequently analyzed at a dilution. 

D = Identifies all compounds identified in an analysis at a secondary dilution factor. 


NQ = Result qualitatively confirmed but not able to quantify. 

N = Indicates presumptive evidence of a compound. This flag is only used for tentatively 

identified compounds (TICs), where the identification is based on a mass spectral library 

search. It is applied to all TIC results, For generic characterization of a TIC, such as 

chlorinated hydrocarbon, the N code is not used. 

X = This flag is used for a TIC compound which is quantified relative to a response factor 

generated from a daily calibration standard (rather than quantified relative to the closes 

internal standard). 

Y = Additional qualifiers used as required are explained in the case narrative. 

sb\10-01gloss.doc

ABBREVIATIONS 

GLOSSARY 

BS — Indicates blank spike in which reagent grade water is spiked with the CLP matrix spike 

solutions and carried through all the steps in the method. Spike recoveries are repo rted. 


MS = Indicates matrix spike. 

MSD = Indicates matrix spike duplicate. 

DL Suffix added to sample number to indicate that results are from a diluted analysis. 


DF = Dilution Factor. 

NR Not Required. 

SP, Z = Indicates Spiked Compound. 

sb\I0-03\g1oss.dm 

r1 

L_^ 

000000008

TECHNICAL FLAGS FOR MANUAL INTEGRATION 

Manual quan modifications or integrations are performed routinely to improve the data quality 

for a variety of technical reasons. Documentation of these modifications should be clear and 

concise. The following `flags' are used to indicate the technical reasons for quan modifications: 

MP - Missed Peak: Manually added peak not found by automatic quan 

program. 

PA - Peak Assignment: Quan report was changed to reflect correct peak 

assignment. 

RI - Routine Integration: Routine integrations are performed for some 

analytes that are consistently integrated improperly by the automatic 

integration programs. Examples are the Dichlorobenzene isomers on the 

VOA packed column and Benzo (b) fluoranthene /Benzo (k) fluoranthene 

which are poorly resolve on the BNA column. 

SP - Split Peak: The automatic integration improperly split the peak; a manual 

integration was performed to get the correct area. 

CB - Co-elution/ Background: Peak was manually integrated to eliminate 

contribution from co-eluting compounds, background signal, or other 

interference. 

PI - Proper Integration: A peak with poor or inconsistent integration (i.e., 

excessive tail) was properly integrated manually. 

LV -21-21-035/AZM 

909099009

uivuviaio ueuaaa.n wa.]i, aau. 

Semivolatiles by GC/MS, HSL List Report Date: 07/13/06 13:42 

RFW Batch Number: 06041,904 Client: TNUHANFORD RC-047 K0303 Work Order: 11343606001 Pane, la 

Cust ID: JllKKS J11KK8 J11KK8 J11KL5 J11KL6 1T11KM0 

Sample RFW#: 001 001 MS 001 MSD 002 003 004 


D.F.: 0.800 0.800 0.800 0.800 0.800 0.800 

Units: ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg 

Nitrobenzene-d5 0 * % 11 * t 

Surrogate 2-Fluorobiphenyl 6 * % 13 * t 

Recovery Terphenyl-d14 17 * % 16 * % 

Phenol-d5 2 * % 12 * 

2-Fluorophenol 1 * % 10 * 

2,4,6-Tribromophenol 15 * t 17 * 

Phenol 4000 U 14 * t 

bis(2-Chloroethyl)ether 4000 U 12 * 

2-Chlorophenol 4000 U 13 * °s 

1,3-Dichlorobenzene 4000 U 11 * jr 

1,4-Dichlorobenzene 4000 U 11 * % 

1,2-Dichlorobenzene 4000 U 11 * t 

2-Methylphenol 4000 U 14 * 

2,2'-oxybis(1-Chloropropane) 4000 U 12 * 

4-Methylphenol 4000 U 15 * t 

N- Nitroso-di-n-propylamine 4000 U 15 * t 

Hexachloroethane 4000 U 10 * % 

Nitrobenzene 4000 U 12 * % 

Isophorone 4000 U 13 * t 

2-Nitrophenol 4000 U 13 * t 

2,4-Dimethylphenol 4000 U 15 * t 

bis(2-Chloroethoxy)methane 4000 U 13 * t 

2,4-Dichlorophenol 4000 U 14 * 

1,2,4-Trichlorobenzene 4000 U 12 * t 

Naphthalene 4000 U 12 * t 

4- Chloroaniline 4000 U 13 * % 

Hexachlorobutadiene 4000 U 14 * 

4- Chloro-3-methylphenol 4000 U 14 * 

2-Methylnaphthalene 4000 U 14 * 

Hexachlorocyclopentadiene 4000 U 7 * t 

2,4,6-Trichlorophenol 4000 U 15 

2,4,5-Trichlorophenol 9900 U 14 * 

*= Outside of EPA CLP QC limits. 

24 t 14 * 0 7 * % 17 * % 

30 % 25 * % 14 * t 21 * t 

37 % 31 1 22 % 31 % 

25 21 * 1 13 * % 21 * t 

21 * % 14 * t 7 * t 16.* % 

42 % 30 21 % 26 t 

29 * % 540 J 3700 U 640 J 

26 * % 3700 U 3700 U 3400 U 

28 * % 3700 U 3700 U 3400 U 

24 *s 3700 U 3700 U 3400 U 

24 * 3700 U 3700 U 3400 U 

25 * % 3700 U 3700 U 3400 U 

28 * t 3700 U 3700 U 3400 U 

25 * t 3700 U 3700 U 3400 U 

32 * t 230 J 3700 U 3400 U 

31 * % 3700 U 3700 U 3400 U 

22 * t 3700 U 3700 U 3400 U 

26 * t 3700 U 3700 U 3400 U 

29 * t 3700 U 3700 U 3400 U 

29 * % 3700 U 3700 U 3400 U 

31 * % 3700 U 3700 U 3400 U 

29 * t 3700 U 3700 U 3400 U 

30 * % 3700 U 3700 U 3400 U 

27 * % 3700 U 3700 U 3400 U 

27 * % 3700 U 3700 U 3400 U 

26 t 3700 U 3700 U 3400 U 

30 * t 3700 U 3700 U 3400 U 

28 * % 3700 U 3700 U 3400 U 

29 * % 3700 U 3700 U 3400 U 

24 t 3700 U 3700 U 3400 U 

32 t 3700 U 3700 U 3400 U 

30 * t 9200 U 9200 U 8600 U 

m 

m

RNW batcn NUmoer: u0U4L9u4 1.11C1LU: lAUu rVAW A^-Vzi nua-V. wUlx V1uCl: llJ%ODuOVV1 roue: lU 

Cust ID: J11KKS J11KK8 J11KK8 J11KL5 J11KL6 J11KM0 

RFW#: 001 001 MS 001 MSD 002 003 004 

2-Chloronaphthalene 4000 U 13 * % 30 * % 3700 U 3700 U 3400 U 

2-Nitroaniline 9900 U 14 * % 29 * % 9200 U 9200 U 8600 U 

Dimethylphthalate 4000 U 15 * % 34 * % 3700 U 3700 U 3400 U 

Acenaphthylene 4000 U 14 * % 30 * % 3700 U 3700 U 3400 U 

2,6-Dinitrotoluene 4000 U 14 * % 32 * % 3700 U 3700 U 3400 U 


Acenaphthene 4000 U 13 * % 30 * % 3700 U 3700 U 3400 U 

2,4-Dinitrophenol 9900 U 7 * % 25 9200 U 9200 U 8600 U 

4-Nitrophenol 9900 U 1 * %; 1 * °s 9200 U 9200 U 8600 U 

Dibenzofuran 4000 U 14 * % 30 * °s 3700 U 3700 U 3400 U 

2,4-Dinitrotoluene 4000 U 15 * % 29 * t 3700 U 3700 U 3400 U 

Diethylphthalate 4000 U 15 * % 33 * % 3700 U 3700 U 3400 U 

4-Chlorophenyl-phenylether 4000 U 14 * % 31 * % 3700 U 3700 U 3400 U 

Fluorene 4000 U 14 * % 30 * % 3700 U 3700 U 3400 U 


4,6-Dinitro-2-methylphenol 9900 U 15 * % 38 * % 9200 U 9200 U 8600 U 

N-Nitrosodiphenylamine (1) 4000 U 13 * % 31 * % 3700 U 3700 U 3400 U 

4-Bromophenyl-phenylether 4000 U 15 * % 36 * % 3700 U 3700 U 3400 U 

Hexachlorobenzene 4000 U 18 * % 42 * % 3700 U 3700 U 3400 U 

Pentachlorophenol 9900 U 1 * % 32 % 9200 U 9200 U 8600 U 

Phenanthrene 4000 U 16 * % 43 * % 3700 U 3700 U 3400 U 

Anthracene 4000 U 15 * % 31 * % 3700 U 3700 U 3400 U 

Carbazole 4000 U 15 * % 36 * % 3700 U 3700 U 3400 U 

Di-n-butylphthalate 4000 U 15 * % 33 * % 3700 U 3700 U 3400 U 

Fluoranthene 4000 U 15 * % 39 * % 3700 U 3700 U 3400 U 

Pyrene 4000 U 16 * % 36 * % 3700 U 3700 U 3400 U 

Butylbenzylphthalate 4000 U 16 * % 33 * % 3700 U 3700 U 3400 U 

3,3 1 -Dichlorobenzidine 4000 U 11 * % 21 %: 3700 U 3700 U 3400 U 

Benzo(a)anthracene 4000 U 15 * % 34 * % 3700 U 3700 U 3400 U 

Chrysene 4000 U 16 * % 32 * % 3700 U 3700 U 3400 U 

bis(2-Ethylhexyl)phthalate 230 JB 16 * % 30 * % 3700 U 3700 U 3400 U 

Di-n-octyl phthalate 4000 U 15 * % 26 * % 3700 U 3700 U 3400 U 

Benzo(b)fluoranthene 4000 U 14 * % 33 * % 3700 U 3700 U 3400 U 

Benzo(k)fluoranthene 4000 U 14 * % 27 * % 3700 U 3700 U 3400 U 

Benzo(a)pyrene 4000 U 14 * % 30 * % 3700 U 3700 U 3400 U 

Indeno(1,2,3-cd)pyrene 4000 U 16 * % 35 * It 3700 U 3700 U 3400 U 

Dibenz(a,h)anthracene 4000 U 16 * % 35 * % 3700 U 3700 U 3400 U 

Benzo(g,h,i)perylene 4000 U 16 * % 33 * % 3700 U 3700 U 3400 U 

(1) - Cannot be separated from Diphenylamine. *= Outside Of EPA CLP QC limits_ 

m

--------- ----------- r-.-- 


RFW Batch Number: 0604L904 Client: TNUHANFORD RC-047 K0303 Work Order, 11343606001 Paae: 2a 

Cust ID: J11KM2 J11KM3 J11KM4 J11KM5 J11KM6 J11KV1 

Sample RFW#: 005 006 007 008 009 010 


D.F.: 0.800 0.800 0.800 0.800 0.800 0.800 

Units: ug/Kg ug/Kg ug/Kg ug/Kg ug /Kg ug/Kg 

Nitrobenzene-d5 17 * % 17 * % 11 * % 28 0 19 * % 16 * 

Surrogate 2-Fluorobiphenyl 20 * % 19 * % 13 * % 33 % 21 * 19 * 

Recovery Terphenyl-d14 29 % 26 1 19 % 42 % 29 % 25 

Phenol-d5 19 * % 18 * % 12 * % 32 % 20 * % 15 * 

2-Fluorophenol 15 * % 15 * % 10 * 1 27 % 18 * % 13 * °s 

2,4,6-Tribromophenol 24 % 24 % 18 * % 39 % 27 % 20 % 

f1=====__===== f1===== __=====fl°==== __==== =f1 

Phenol 260 J 240 J 3200 U 660 J 300 J 540 J 

bis(2-Chloroethyl)ether 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

2-Chlorophenol 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

1,3-Dichlorobenzene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 



2-Methylphenol 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

2,2'-oxybis(1-Chloropropane) 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

4-Methylphenol 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

N-Nitroso-di-n-propylamine 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Hexachloroethane 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Nitrobenzene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Isophorone 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

2-Nitrophenol 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

2,4-Dimethylphenol 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

bis(2-Chloroethoxy)methane 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

2,4-Dichlorophenol 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

1,2,4-Trichlorobenzene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Naphthalene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

4-Chlorcaniline 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Hexachlorobutadiene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

4-Chloro-3-methylphenol 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

2-Methylnaphthalene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Hexachlorocyclopentadiene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

2,4,6-Trichlorophenol 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

2,4,5-Trichlorophenol 8300 U 8400 U 8000 U 8100 U 7400 U 9200 U 


N 

.r 

m 

CD 

G 

W

0 

RFW BatCn Number- UbU4L5U4 Ellen ' 17xyn"ryj%y xl-"/ Ava w rvorx Uraer • IIJYJOVOUVI rave• zo 

Cust ID: J11KM2 J11KM3 J11KM4 J11KM5 J11KM6 J11KV1 

RFW#: 005 006 007 008 009 010 

2-Chloronaphthalene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

2-Nitroaniline 8300 U 8400 U 8000 U 8100 U 7400 U 9200 U 

Dimethylphthalate 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Acenaphthylene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

2,6-Dinitrotoluene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 


Acenaphthene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

2,4-Dinitrophenol 8300 U 8400 U 8000 U 8100 U 7400 U 9200 U 

4-Nitrophenol 8300 U 8400 U 8000 U 8100 U 7400 U 9200 U 

Dibenzofuran 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

2,4-Dinitrotoluene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Diethylphthalate 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

4-Chlorophenyl-phenylether 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Fluorene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 


4,6-Dinitro-2-methylphenol 8300 U 8400 U 8000 U 8100 U 7400 U 9200 U 

N- Nitrosodiphenylamine (1) 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

4-Bromophenyl-phenylether 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Hexachlorobenzene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Pentachlorophenol 8300 U 8400 U 8000 U 8100 U 7400 U 9200 U 

Phenanthrene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Anthracene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Carbazole 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Di-n-butylphthalate 3300 U 3400 U 3200 U 2200 J 3000 U 3700 U 

Fluoranthene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Pyrene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Butylbenzylphthalate 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

3,3 1 - Dichlorobenzidine 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Benzo(a)anthracene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Chrysene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

bis(2-Ethylhexyl)phthalate 3300 U 250 JB 3200 U 3200 U 190 JB 3700 U 

Di-n-octyl phthalate 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Benzo(b)fluoranthene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Benzo(k)fluoranthene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Benzo(a)pyrene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Indeno(1,2,3-cd)pyrene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Dibenz(a,h)anthracene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

Benzo(g,h,i)perylene 3300 U 3400 U 3200 U 3200 U 3000 U 3700 U 

(1) - Cannot be separated from Diphenylamine. *= Outside of EPA CLP QC limits. 

M 

m


RFW Batch Number: 06041,904 Client: TNUHANFORD RC-047 K0303 Work Order: 11343606001 Pape: 3a 

Cust ID: J11KV2 J111,21 JIIL23 JlIL25 J11L36 SHLKZH 

Sample RFW#: 011 012 013 014 015 06LE0457-MB1 

Information Matrix: SOLID SOLID SOLID SOLID SOLID SOIL 

D.F.: 0.800 0.800 0.800 0.800 0.800 0.800 

Units: ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg 

Nitrobenzene-d5 2 * % 13 * % 16 * % 20 * % 14 * % 26 a 

Surrogate 2-Fluorobiphenyl 8 * % 16 * % 20 * % 22 * % 16 * % 27 * % 

Recovery Terphenyl-d14 21 e 19 % 21 % 24 0 21 % 45 % 

Phenol-d5 6 * % 15 * % 17 * % 19 * % 14 * % 29 % 

2-Fluorophenol 3 * % 13 * °s 16 * % 20 * % 14 * % 26 % 

2,4,6-Tribromophenol 15 * % 12 * % 18 * % 20 % 14 * % 33 

----------------------------------------===== 

--------------------------- f1=====__===== f1=====__=====fl=====__===== fl=====__===== f1===== __=====fl 

Phenol 4000 U 280 J 160 J 220 J 260 J 270 U 

bis(2-Chloroethyl)ether 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

2- Chlorcphenol 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

1,3-Dichlorobenzene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 



2-Methylphenol 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

2,2'-oxybis(i-Chloropropane) 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

4-Methylphenol 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

N-Nitroso-di-n-propylamine 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Hexachloroethane 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Nitrobenzene 

Isophorone 

4000 

4000 

U 

U 

2900 

2900 

U 

U 

2800 

2800 

U 

U 

3200 

3200 

U 

U 

3700 

3700 

U 

U 

270 

270 

U 

U 

2-Nitrophenol 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

2,4-Dimethylphenol 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

bis(2-Chloroethoxy)methane 

2,4-Dichlorophenol 

1,2,4-Trichlorobenzene 

Naphthalene 

4-Chloroaniline 

Hexachlorobutadiene 

4-Chloro-3-methylphenol 

2-Methylnaphthalene 

Hexachlorocyclopentadiene 

2,4,6-Trichlorophenol 

2,4,5-Trichlorophenol 


4000 

4000 

4000 

4000 

4000 

4000 

4000 

4000 

4000 

4000 

9900 

U 

U 

U 

U 

U 

U 

U 

U 

U 

U 

U 

2900 

2900 

2900 

2900 

2900 

2900 

2900 

2900 

2900 

2900 

7100 

U 

U 

U 

U 

U 

U 

U 

U 

U 

U 

U 

2800 

2800 

2800 

2800 

2800 

2800 

2800 

2800 

2800 

2800 


U 

U 

U 

U 

U 

U 

U 

U 

U 

U 

U 

3200 

3200 

3200 

3200 

3200 

3200. 

3200 

3200 

3200 

3200 


U 

U 

U 

U 

U 

U 

U 

U 

U 

U 

U 

3700 

3700 

3700 

3700 

3700 

3700 

3700 

3700 

3700 

3700 

9200 

U 

U 

U 

U 

U 

U 

U 

U 

U 

U 

U 

270 

270 

270 

270 

270 

270 

270 

270 

270 

270 

670 

U 

U 

U 

U 

U 

U 

U 

U 

U 

U 

U 

a 

m

RFW Batcn Number: UOU4L `JU4 L11C11L: 11IV13 PVR3 n - v ^Vuo n4 

Cust ID: JllKV2 J11 1, 21 JllL23 JlIL25 JllL36 SBLKZH 

RFW#: Oil 012 013 014 015 06LE0457-MB1 

2-Chloronaphthalene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

2-Nitroaniline 9900 U 7100 U 7100 U B100 U 9200 U 670 U 

Dimethylphthalate 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Acenaphthylene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

2,6-Dinitrotoluene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

3-Nitroaniline 9900 U 7100 U 7100 U 8100 U 9200 U 670 U 

Acenaphthene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

2,4-Dinitrophenol 9900 U 7100 U 7100 U 8100 U 9200 U 670 U 

4-Nitrophenol 9900 U 7100 U 7100 U 6100 U 9200 U 670 U 

Dibenzofuran 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

2,4-Dinitrotoluene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Diethylphthalate 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

4-Chlorophenyl-phenylether 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Fluorene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

4-Nitroaniline 9900 U 7100 U 7100 U 8100 U 9200 U 670 U 

4,6-Dinitro-2-methylphenol 9900 U 7100 U 7100 U 8100 U 9200 U 670 U 

N-Nitrosodiphenylamine (1) 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

4-Bromophenyl-phenylether 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Hexachlorobenzene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Pentachlorophenol 9900 U 7100 U 7100 U 8100 U 9200 U 670 U 

Phenanthrene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Anthracene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Carbazole 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Di-n-butylphthalate 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Fluoranthene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Pyrene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Butylbenzylphthalate 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

3,3 1 -Dichlorobenzidine 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Benzo(a)anthracene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Chrysene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

bis(2-Ethylhexyl)phthalate 4000 U 2900 U 2800 U 190 JB 2000 JB 18 J 

Di-n-octyl phthalate 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Benzo(b)fluoranthene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Benzo(k)fluoranthene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Benzc(a)pyrene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Indeno(1,2,3-cd)pyrene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Dibenz(a,h)anthracene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 

Benzo(g,h,i)perylene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U 


N 

M 

m 

G 

m 

M 

CD 

m

RFW Batch Number: 0604L904 


Client: TNUHANFORD RC-047 K0303 Work Order: 11343606001 Page: 4a 

Cust ID: SBLKZH BS - m mCD 

Sample 

Information 

RFW#: 

Matrix: 

D.F.: 

06LE0457-MB1 

SOIL 

0.800 

m 

Units: ug/Kg 

Nitrobenzene-d5 10 * % 

Surrogate 2-Fluorobiphenyl 11 * % 

Recovery Terphenyl-d14 16 *s 

Phenol-d5 9 * % 

2-Fluorophenol 9 * % 

2,4,6-Tribromophenol 14 * 

_____________________________________________ fl=====__===== fl=====__===== fl=====__=====f1=====__=====f1==°==__=====f1 

Phenol 10 * % 

bis(2-Chloroethyl)ether 11 

2-Chlorophenol 11 * % 

1,3-Dichlorobenzene 10 * % 



2-Methylphenol 10 * % 

2,2'-oxybis(i-Chloropropane) 11 * % 

4-Methylphenol 10 * % 

N-Nitroso-di-n-propylamine 12 * % 

Hexachloroethane 10 * 

Nitrobenzene 10 * 

Isophorone 12 * % 

2-Nitrophenol 10 * % 

2,4-Dimethylphenol 7 * % 

bis(2-Chloroethoxy)methane 11 * t 

2,4-Dichlorophenol 10 * % 

1,2,4-Trichlorobenzene 11 * % 

Naphthalene 11 * % 

4-Chloroaniline 11 * % 

Hexachlorobutadiene 11 * % 

4-Chlaro-3-methylphenol 10 * 

2-Methylnaphthalene 12 * 

Hexachlorocyclopentadiene 7 * % 

2,4,6-Trichlorophenol 12 % 

2,4,5-Trichlorophenol 10 * % 


ID

RFw batch Number , Ubu4L90 4 1:11enL: WilunAMOUnL n^ -ULl AU .3V3 WOrx uruer • 113434UbUU1 ease 40 

Cust ID: SBLRZH BS 

RFW#: 06LE0457-MB1 

2-Chloronaphthalene 11 * % 

2-Nitroaniline 11 * % 

Dimethylphthalate 13 

Acenaphthylene 

11 

2,6-Dinitrotoluene 11 * % 

3-Nitroaniline 

12 

Acenaphthene 11 * % 

2,4-Dinitrophenol 0 * % 

4-Nitrophenol 0 

Dibenzofuran 12 * % 

2,4-Dinitrotoluene 12 * % 

Diethylphthalate 13 * % 

4-Chlorophenyl-phenylether 12 * % 

Fluorene 

12 

4-Nitroaniline 10 

4,6-Dinitro-2-methylphenol 10 

N-Nitrosodiphenylamine (1) 12 + % 

4-Bromophenyl-phenylether 12 * 

Hexachlorobenzene 15 * 

Pentachlorophenol 0 * % 

Phenanthrene 13 * % 

Anthracene 12 * % 

Carbazole 13 * % 

Di-n-butylphthalate 13 * % 

Fluoranthene 13 * % 

Pyrene 17 * % 

Butylbenzylphthalate 16 * % 

3,3 1 -Dichlorobenzidine 11 

Benzo(a)anthracene 13 

Chrysene 14 * % 

bis(2-Ethylhexyl)phthalate 15 * % 

Di-n-octyl phthalate 17 * % 

Benzo(b)fluoranthene 14 * % 

Benzo(k)fluoranthene 15 * % 

Benzo(a)pyrene 14 

Indeno(1,2,3-cd)pyrene 14 

Dibenz(a,h)anthracene 11 * % 

Benzo(g,h,i)perylene 12 * % 


h 

m 

m 

Q 

CD

IF CLiENT SAMPLE NO. 

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET 

TENTATIVELY IDENTIFIED COMPOUNDS 

IJ11KKB 

Lab Name: Lionville Labs, Inc. Work Order: 11343606001 

Client: TNUHANFORD RC-047 K0303 

Matrix: (soil/water) SOLID Lab Sample ID: 06041,904-001 

Sample wt/vol: 2.02 (g/mL) Lab File ID: N062914 

Level: (low/med) LOW Date Received: 04/28/06 

%, Moisture: 100 decanted: (Y/N) _ Date Extracted: 06/02/06 

Concentrated Extract Volume: 500(uL) Date Analyzed: 06/29/06 

Injection Volume: 2_0(uL) Dilution Factor: 0.800 

GPC Cleanup: (Y/N) Y pH: 

Number TICS found: .5 

CONCENTRATION UNITS: 

(ug/L or ug/Kg) ua/Kg 

1 

CAS NUMBER 

1 

COMPOUND 

1 1 

NAME RT EST. 

CONC. 

1 

1 

Q 1 

1. 110-82-7 1CYCLOHEXANE 1 3.539 1 70001 JNB 1 

2. JORGANIC ACID 1 21.6241 200001 J 1 

1 3. JUNKNOWN 1 22.7211 400001 J 1 

1 4. UNKNOWN 1 28.5681 30001 J 1 

1 5. 

1 

UNKNOWN 1 34.0861 

I I 

800001 

FORM 1 SV-TIC RFW (v3.3) 

I 

J 1 

000000018 

1

IF CLIENT SAMPLE NO. 



J11KL5 



Matrix: (soil/water) SOLID Lab Sample ID 0604L904-002 

Sample wt/vol: 2.18 (g/mL) G 

Level: (low/med) LOW 

g Moisture: 100 decanted: (Y/N) _, 

Concentrated Extract Volume: 5500(uL) 

Injection Volume: 22. (uL) 


Number TICS found: 5 

CAS NUMBER COMPOUND NAME 

1. 110-82-7 ^CYCLOHEXANE 

2. JORGANIC ACID 

3. JUNKNOWN 


5. JUNKNOWN 

Lab File ID: N070111 

Date Received: 04/28/06 

Date Extracted: Q6/02/06 

Date Analyzed: 07/02/06 

Dilution Factor: 0.800 


(ug/L or ug/Kg) ua/Ka 

RT EST. CONC. Q 

3.419 1 

60001 JNB 

21.5471 600001 J 

22.6351 1000001 J 

1 22.7131 300001 J 

1 33.8201 5000001 J 


000000019

1F 



Lab Name: Lionville Labs Inc. Work Order: 11343606001 


Matrix: (soil/water) SOLID 

Sample wt/vol: 2.17 (9/ML) -Q 


& Moisture: 100 decanted: (Y/N)_ 

Concentrated Extract Volume: 500 (uL) 

Injection Volume: 2_0(uL) 

GPC Cleanup: (YIN) Y pH: 

Number TICS found: 

Lab Sample ID: 

Lab File ID: 

Date Received: 

Date Extracted: 

Date Analyzed: 

Dilution Factor 


(ug/L or ug/Kg) ua/Kd 

CL1liIJ'r SAMPLE NO. 

I 

^J11KL6 

I 

0604 1, 904-003 

N063006 

04/28/06 

06/02/06 

06/30/06 

0.800 

CAS NUMBER COMPOUND NAME RT EST. CONC. Q 

1. JUNKNOWN 1 5.804 1 80001 J 

1 2. JORGANIC ACID 1 21.5911 300001 J 

1 3. JUNKNOWN 1 22.6881 900001 J 

4. JORGANIC ACID 1 22.7661 200001 J 

5. UNKNOWN 1 33.9681 2000001 J 


000000020



TENTATIVELY IDENTIFIED .COMPOUNDS 

J11KMO 


i 


Matrix: (soil/water) SOLID Lab Sample ID: 06041,904-004 

Sample wt/vol: 2.32 (g/ML) Lab File ID: N063007 


Moisture: 100 decanted: (Y/N) _ Date Extracted: 06/02/06 


Injection Volume: 2.0(uL) Dilution Factor: 0.800 




(ug/L or ug/Kg) u K 

I 

CAS NUMBER 

1. 110-82-7 ICYCLOHEXANE 

1 2. JUNKNOWN 

1 3. JORGANIC ACID 

4. JUNKNOWN 

5. JUNKNOWN 

I 

COMPOUND NAME 


3.471 1 10000 JNB 

5.829 1 80001 J 

1 21.5821 200001 J 




000000021

1F CLIENT SP.MPLE NO. 



I J11KM2 

Lab Name: Lionville Labs, Inc. Work Order.: 11343606001 


Matrix: (soil/water) SOLID Lab Sample ID: 0604 1, 904-005 



°s Moisture: 100 decanted: (Y/N) _ 



GPC Cleanup: (Y/N) _y pH: 



1. 110-82-7 ICYCLOHEXANE 

2. (ORGANIC ACID 

1 3. (UNKNOWN 

1 4. JUNKNOWN 

5. 

UNKNOWN 

1 

I 

^ 

Lab File ID: N063008 


Date Extracted: 06/02/06 




(ug/L or u9/Kg) ua/Kq 

_I 


1 3.471 1 100001 JNB I 

21.S901 400001 J 


28.4741 50001 J I 

33.9061 2000001 J 


000000022 

I

1F CLIENT SAMPLE NO. 



J I I KM3 



Matrix: (soil/water) SOLID Lab Sample ID: 0604L904-006 

Sample wt/vol: 2.38 (g/mL) Lab File ID: N063009 


g Moisture: 100 decanted: (YIN)_ Date Extracted: 06/02/06 


injection Volume: 2_0(uL) Dilution Factor: 0.800 



Number TICS found: 5 (ug/L or ug/Kg) u K 


=-^-=a=asses======== ____:» â^:as== 

1. 

JUNKNOWN 


1 3. JUNKNOWN 


5. 

JUNKNOWN 

1 

11 

PT I EST. CONC. Q 

1 5.906 1 100001 J 

1 21.5591 600001 J 1 

22.7051 1000001 J 1 


1 33.9841 4000001 J 


000000023


GPC Cleanup: (Y/N) Y 




TENTATIVELY IDENTIFIED COMPOUNDS I 



1 1 

pH: 



(ug/L or ug/Kg) u cr /Ka 

^JllKM4 


Sample wt/vol: 2.50 (g/mL) G Lab File ID: N063010 


% Moisture: 100 decanted: ( Y/N) _, Date Extracted: 06/02/06 



1. 110-82-7 I CYCLOHEXANE 1 3.473 1 100001 JNB 

1 2. JORGANIC ACID 1 21.6021 500001 J 

1 3. JUNKNOWN 1 22.6991 1000001 J 

4. JORGANIC ACID 122.7681 200001 J 

1 5. JUNKNOWN 1 33.9181 1000001 J 


000000024

IF 





CLIENT SAMPLE NO. 

JJ11KM5 


Sample wt/vol: 2.48 (g/mL) Q Lab File ID: N063011 


t Moisture: 100 decanted: (Y/N) _ Date Extracted: 06/02/06 

Concentrated Extract Volume: 500(UL) Date Analyzed: 06/30/06 

Injection Volume: ,2.0(UL) Dilution Factor: 0.800 


Number TICs found: 5 


(ug/L or ug/Kg) ug/Kg 

CAS NUMBER 

1 

COMPOUND 

I I 1 

NAME RT EST. CONC. Q 

1. 110-82-7 ICYCLOHEXANE 1 3.471 1 100001 JNB 

2. JUNKNOWN 1 5.603 1 80001 J 

1 3. JORGANIC ACID 1 21.6001 500001 J 

4. JUNKNOWN 1 22.6971 1000001 J 

S. JUNKNOWN 1 33.9671 3000001 J 


I 

000000025

IF CLTENT SAMPLE NO. 


TENTATIVELY IDENTIFIED COMPOUNDS 1 

I J11KM6 

Lab Name: Lionville Labs Inc. Work Order: 11343606001 



Sample wt/vol: 2,71 (g/mL) Lab File ID: N063012 

Level: (low/med) LOW_ Date Received: 04/28/06 

% Moisture: 100 decanted: (Y/N) _ Date Extracted: 06/02/06 





1 1 

1 CAS NUMBER 1 COMPOUND NAME 

1====_=..=.=====1========== a_ 

1 1. 110-82-7 1CYCLOHEXANE 

1 2. (ORGANIC ACID 

3. (UNKNOWN 


1 5. JUNKNOWN 

1 1- 



(ug/L or ug/Kg) ua/Kg 

RT 

1 

EST_ CONC. 

3.478 1 200001 JNB 1 


22.6861 700001 J 1 

22.7641 200001 J 1 

33.9481 2000001 J 


1 

Q 

1 

000000026

IF 






I 

^J11KV1 

Matrix: (soil/water) SOLI D Lab Sample ID: 0604 1, 904-010 



s Moisture:100 decanted: (Y/N) 


Injection Volume: 2.0(uL) 











1. (UNKNOWN 


3. JUNKNOWN 


5. JUNKNOWN 


5.862 200001 J 

21.5891 400001 J 

22.6B61 600001 J 

1 22.7641 200001 J 



000000027 

1




^J11KV2 



Matrix: (soil/water) SOLID Lab Sample ID: 0604 1, 904-011 



% Moisture: 100 decanted: (YIN)— 

Concentrated Extract Volume: JU (uL) 





Date - Received: 04/28/06 





( ug/L or ug / Kg) ua/Ka 


1. 110-82-7 I CYCLOHEXANE 1 3.469 1 60001 JNB 

2_ (ORGANIC ACID 1 21.5801 100001 J 

3. JUNKNOWN 1 22.6691 30000 1 J 

4: (UNKNOWN 1 29.1981 80001 J 

5. JUNKNOWN 1 33.9051 2000001 J 


000000028

1F CLIENT SAMPLE NO. 



IJ11L21 



Matrix: (soil/water) SOLID Lab Sample ID: 00 4 1, 904-012 

Sample wt/vol: 2.80 (g/mL) Q 

Level: ( low/med) LOW 

°s Moisture: 100 decanted: (YIN)_ 





1 1 

Lab File ID: D063006 






(ug/L or ug/Kg) ua/Kq 


______________ 

1. 

JUNKNOWN 

----ewe-°===___^___ °___^_____________^_____^ 

1 4.749 1 

50001 J 

2. (UNKNOWN 1 5.171 1 40001 J 

3. JUNKNOWN 1 8.523 1 60001 J 

1 4. JUNKNOWN 1 22.0231 50001 J 

5. JUNKNOWN 1 32.6541 2000001 J 


000000029

IF 




Client: TNUHANFORD RC -047 K0303 

CLIENT SAh]PLE NO. 

I 

IJIIL23 

I 




%^ Moisture: 100 decanted: (Y/N) _ 

Concentrated Extract Volume: 5_QQ(uL) 





1. JUNKNOWN 


3. JUNKNOWN 


1 5. JUNKNOWN 






'ONCENTRATION UNITS: 



4.782 1 90001 J 

1 20.9271 90001 J 

22.0291 200001 J 

1 22.1071 90001 J 


_I 


000000030 

I

1F 



Lab Name: Lionville Labs. Inc. Work Order: 11343606001 



JllL25 

I 




Moisture: 100 decanted: (Y/N) _ 













1. UNKNOWN 1 4.802 1 50001 J 

2. ORGANIC ACID 1 20.9381 300001 J 

3. JUNKNOWN 1 21.0421 50001 J 1 


S. JUNKNOWN 1 32.6811 3000001 J 


000000031

1F 






I 

IJIIL36 


Sample wt/vol: 2.18 (9/ML) Q Lab File ID: D063009 

Level: (low/med) Low Date Received: 04/28/06 

% Moisture: 100 decanted: (Y/N)_ Date Extracted: 06/02/06 


Injection Volume: 2_0(uL) Dilution Factor: 0.800 

GPC Cleanup: (Y/N) Y PH: 

Number TICS found: 




1. JUNKNOWN 1 

13.2161 20001 J 

2. (UNKNOWN 1 21.0211 10001 J 

3. JUNKNOWN 1 21.2111 20001 J 


1 5. 

JUNKNOWN 1 32.6261 2000001 J 

1 


000000032 

I




ISBLKZH 



Matrix: (soil/water) SOIL Lab Sample ID: 06LE0457-MB1 



Moisture: decanted: (YIN) 











(ug/L or ug/Kg) ua/Kq 


1 1. 110-82-7 ICYCLOHEXANE 1 3.421 1 10001 JN 

1 2. JUNKNOWN 1 29.0811 2001 J 

1 3. JUNKNOWN 1 30.6521 2001 J 


1 5. JUNKNOWN 1 37.8811 601 J 


000000033

Lionville Lanoratory, inc. 


Sheet no.: 1 

Extract. Date: 06/02/06 Extraction Batch No: 06LE0457 Analyst: MF Method: **** m mm 

Test: 0625 Cleanup Date: Analyst: Client: TNUHANFORD RC-047 K0303 mm mm 

LIMS Report Date: 07/13/06 Solvent: DCM Adsorbent: 

I 

Sample No: 

Client Name pH Initial Surr. Spike Final Final Split GPC It C/D I 

Client ID WT/VOL Mult. Mult. VOL VOL Mult. Y/N Solids FACTOR I 


001 H J11KK8 2.02 1.0 0.4 1.0 Y 0.00 198.0 

001 HS J11KKB 2.00 1.0 1.0 0.4 1.0 Y 0.00 200.0 

001 HT J11KK8 2.86 1.0 1.0 0.4 1.0 Y 0.00 139.9 

002 H J11KL5 2.18 1.0 0.4 1.0 Y 0.00 183.5 

003 H JllKL6 2.17 1.0 0.4 1.0 Y 0.00 184.3 

004 H J11KM0 2.32 1.0 0.4 1.0 Y 0.00 172.4 

005 H JllKM2 2.42 1.0 0.4 1.0 Y 0.00 165.3 

006 H J11KM3 2.38 1.0 0.4 1.0 Y 0.00 168.1 

007 H J11KM4 2.50 1.0 0.4 1.0 Y 0.00 160.0 

008 H J11KM5 2.48 1.0 0.4 1.0 Y 0.00 161.3 

009 H J11KM6 2.71 1.0 0.4 1.0 Y 0.00 147.6 

010 H J11KV1 2.18 1.0 0.4 1.0 Y 0.00 183.5 

011 H J11KV2 2.02 1.0 0.4 1.0 Y 0.00 198.0 

012 H J11 1, 21 2.80 1.0 0.4 1.0 Y 0.00 142.9 

013 H JlIL23 2.83 1.0 0.4 1.0 Y 0.00 141.3 

014 H JlIL25 2.47 1.0 0.4 1.0 Y 0.00 161.9 

015 H JllL36 2.18 1.0 0.4 1.0 Y 0.00 183.5 

06LE0457-MB1 H SBLKZH 30.0 1.0 0.4 1.0 Y 100.00 13.33 

O6LE0457-MB1 HS SBLKZH 30.0 1.0 1.0 0.4 1.0 Y 100.00 13.33 

Comments: 

Surrogate: 500 UL ESU BNA 89915405 @100-150 UG/ML 

Spike: 750 UL BNA LCS SPIKE 86951017E 

(Extracts Transferred Relinquished By Date Time ( Received By I Date Time I Reason for Transfer 

I I 

I I I I I I 

^ ^. I } 'I 3 Vb 

I I 

M

Extract. Date: 06/02/06 

ieSt: 3625 

LIMS Report Date: 06/29/06 

Sample No: Client ID 


Sheet no.: t 

Extraction Batch No: 06LE0457 Analyst: MF Method: **** S ay'^S.^ J 

Cleanup Late: AL is iy'6t: Client: RC-547 K6363 m m 

Solvent: DCM Adsorbent: m m 

pH Initial Surr. Spike Final Final Split GPC t C/D 

WT/VOL Mult. Mult. VOL VOL Mult. Y/N Solids FACTOR 

. 

0604 1, 904- TNUHANFORD RC-047 K0303 

001 

001 

001 

H 

HS 

HT 

J11KK8 

J11KK8 

J11KK8 

2.024W 

2.00 1.0 1.0 

2.86 1.0 1.0 

0.4 

0.4 

0.4 

0.5 

0.5 

0.5 

Y 

Y 

Y 

0.0 

0.0 

0.0 

99.01 

100.0 

69.93 

002 H J11KL5 2.18 1.0 0.4 0.5 Y 0.0 91.74 

003 H J11KL6 2.17 1.0 0.4 0.5 Y 0.0 92.17 

004 H J11 104 0 2.32 1.0 0.4 0.5 Y 0.0 86.21 

005 H J11KM2 2.42 1.0 0.4 0.5 Y 0.0 82.64 

006 H J11KM3 2.38 1.0 0.4 0.5 Y 0.0 84.03 

007 H J11KM4 2.50 1.0 0.4 0.5 Y 0.0 80.00 

008 H J11KM5 2.48 1.0 0.4 0.5 Y 0.0 80.65 

009 

01 0 

H 

H 

J11KM6 

311KV1 

2.71 

2.18 

1.0 

1.0 

0.4 

0.4 

0.5 

0.5 

Y 

Y 

0.0 

0.0 

73.80 

91.74 

011 

012 

H 

H 

J11KV2 

J111,21 

2.02 

2.80 

1.0 

1.0 

0.4 

0.4 

0.5 

0.5 

Y 

Y 

0.0 

0.0 

99.01 

71.43 

013 

014 

015 

06LE0457-MB1 

06LE0457-MB1 

H 

H 

H 

H 

HS 

711L23 

J11 1,25 

J11L36 

SBLKZH 

SBLKZH 

2.83 

2.47 

2.18 

30.0 

30.0 

1.0 

1.0 

1.0 

1.0 

1.0 1.0 

0.4 

0.4 

0.4 

0.4 

0.4 

0.5 

0.5 

0.5 

0.5 

0.5 

Y 

N 

N 

N 

N 

0.0 

0.0 

0.0 



70.67 

80.97 

91.74 

6.67 

6.67 

Comments: 

Surrogate: 500 UL ESU BNA 89915405 @100-150 UG/ML 

Spike: 750 UL BNA LCS SPIKE 86951017E 

Extracts Transterreo Relinquisned By Date Time Received By Date Time Reason for Transfer 

I I i 

__^/U^ I L 6 c^ j /^, l^rr 

N 

M 

m 

m

Lionville Laboratory Use On ly 

Client T14Lk % e%-CorP RC-047 

Custody Transfer Record/Lab Work Request Page! of a IV= 

Es t. Final Prof. Sampling Date #/Type Cemalner 

/./ ^} 

Project ^^^J^^1 ^4?1^G7' ^n^^-13—do -f 1 

Pro)ect CoMacUPhone A` Volume 

Lionville Laboratory Project 0 

^ Manager 

OC "" Del J! G(._. TAT l ti t G 

/.i 

Date Rec'd H'Uô Date Due S/J t'' 

T'o^ 

FIELD PERSONNEL. COMPLETE ONLY SHADED YEAS 

See SRC M 

m 

Rahgeretor• m 

p reservatives 

ANALYSES 

REQUESTED 

Liq uid 

Send 

U wid 

Sow 

ORGANIC INORG 

< 

O Zm a Q^ = CP M U 

j Llolwllle Laboratory Use only 1 

MATRIX 

CODES: 

Matrix 

SE - Soi 

Oc 

Time 

Lab 

Matrix 

CH 

sedenent ID 

ID/Deacrlpeon 

Chosen 

Colllected 

^l ^~ 

so - Solid 

SL - Sludge 

J 

w- Water 

MS MSD 

V `^C 

O- Oil 

A- Air co, J ► S KKS y'S X 

DS- Drum 

solids 

DL - Drum 

Uquaa ow 

! 

q$-0te 14-20 X I X - 

L• EP/TCLP 

6 x X 

Leadate 

wl - wqm 

X • Other 

F- fish 

cow 

oc 

3i 1 

C;)— 

S 

la 

10 3 

X 

X I X 

X I x 

X 

n 

X 

I X 

X 

OCA J 5 X X 

po° J l YY1 

J1 I KV I 

X X1 

Xi 

1X 

I 

X I- 

K Special Instructions: ruc ?--it -3-M" ttNlS: 

X 

,r , C 

ti 

^ 

-9001 t. f 

^ 

ewe ul.L1s^ 1x4.Da.^ ^W I^.-f'cs+, z. 

(Ylr ls, PC8,SJoL. s. 

Me-`V35 PCB, RrSA- S\10c 

Reanqulehed 

by 

Received 

by 

Dale Tlma 

êa^,aA - rNcTRr ^ K-[ -rP'^r,^, 

4. 

MMrquasbad Rec eived Data 

RNlnqulaMd 

by Tirol 

by by .. 

Received 

W 

^c aYo ^!3 i,;Q POYIip 

WASTEe 

Data Three 

m 

m

Lionville Laborato ry Use Only Custody Transfer Record/Lab Work Request Page^ oj VaW O^ FIELD PERSONNEL: COMPLETE AREAS ONLY f SHADEDr 

M 

6 

Client 1 Z, C- 


Est. Final Pro). Sampling Date orrype Container 

Project # 

G 

Project ContacVPhone # Volume 

Lion ville Laboratory Projectl4imager 

G 

Press. ral Ives 

OC Del TAT 

O NIC INORG 

Date Rec'd Date Due 

ANALYSES _^ 

REQUESTED 

Q 

p 

¢ 

Zm 

â 

y 

a 

^ 

= SJ 

MATRIX 

j /L Lionville 

L ionville Laboratory Use On ly j 

CODES: 

Marta 

S - Soil Lab 

OC Mahler 

Date 

lD/Descdpaon 

Chosen 

Coll 

SE.- S 

ID 

V) 

ec 

Time 

ted Collected 

>(1 C'O ^^ 

SO •solid rd 

^ ^ ^-- 

SL- Sludge 

W. Water O U v 

MS IMSO 

O • Oil 

A • Air 

N C;L 

DS • Drum 

.x:.. 

Solids o I a X /1 

DL. Drum 

` 

1 

Liquids V, L a3 

a . _. 

1 ;:.. ^/ 

X 

L, X 

EP/rCLP 

Lesahate 5 Q X^ 

X- 

«her 016 J \^ o)s X )c X 

F - Fish 

Special Instruc ti 

ons: 

DATEtREYtS ONS: 

i1 r.:rJx r ^^^ ► .I SL, r< ^, fî; t I, ^r? c, (% z. 

Re li 

r 9. 

nquished itacatvad 

Re 

Dale 

linquished Rece 

Time 

iv ed 

by by by by 

A-\m-ki 3 

1. 

5. 

8. 

Liquid 

Sold 

Liquid 

Solid 

Tbrna 

U 

Relinquished Received 

by 

by 

Date Tlma 

m

Washineton Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-259 Page l or i 

Collector 


Conotnmv Contact 

JOAN KPSSNER 

Telephone No. 

375-4688 


KESSNER, IH Pdce Code 9N Data Turnaround Co 

45 Days 

rolect DDesignation esi[ 

Sampling Location SAY Na. 

Air Quality ^ Da y m 100 & 300 Area Component of the RCBRA Sediment and Ti 600-131/600-190 OFFAL RC-047 0 

9 

I ce Clsest Np.yp Field Lo[book No. COA Method of Shipment 

, rC e - a,2 ^fJ^ EL-1595 BESRAS6520 FED EX 0 

Ship ORsito Property No. a Bi ll of Lading/Air Bill No. 

RLINE SERViCEV LIONVILLE J L/ SEE OSPC 



Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-266 Page 3 of I 

Collector Coamapv CORtaet Tdephouse No. Prolect Coordimtor 

TRJER, B. 111 KLINC JOAN KESSNER 375-4688 KESSNER, JH 

roiect Desiemtion Samplina Lismu n 


100 & 300 Ana Component of the RCBRA Sediment and Ti 3894H-3k OFFAL ^G 0 ] />^z 


Ice ChestNo.y - 

tîAOC —^2' D.r 

0 J11KL5 OTHER SOLID 1W6 Z, 

Fie E No. COA Method of Shisma l 

141oe Code 9th Data Turnreravuod m 

U, 

45 Days 9 

Air Quality q m_ 

EL, 1595 BESRAS6520 FED EX m 

Sipmed To Offalte Property No. n^ 6 O y d BIB of LadiodAlr Bi ll No. 

EBERLM LIONVILLE /7 •7 SEE OSPC 

PO HAZARDSMEMARKS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-267 j pxv 1. d I 

Collector 

TILLER, B. TH KLINCKMAN 

C[mmanv Cantact 

JOAN KESSNER 

Teletsbone No. 

375-4688 


KESSNER, JH Price Code 9N 

Protect DesienaGon 

100 & 300 Area Component of the RCBRA Sediment and n 

Ice Chest No.r 

y j^(J -- ^^ 

Satnpbne Location 

1 I6-N-3 OFFAL 


FL-1595 

COA 

BESRAS6520 




FED EX 

Air Quality 

Data Trrrnarourssm 

V 

45 Days m 

CD 

m— 

m 

m 

CD 

Ship 

L•RLINE SERVICES LIONVILLE _ 

ORsile Pronety No. / p 

Q(/Q J^L/ 

Bib of Ladlisit/A ir BIB No. 

SEEOSPC 

POSSIBLE SAMPLE HAZARD6/ItEMARKS 

POTENTIAL RADIOACTIVE eDOTUMITS 

Special Handling and/or Storage 



S ^, 41 

Presevauon 


No. of Contalaer(s) 

Volume 

Iw ® 3 

Sample No. Max Matrix • 

Sam Date Sample Time 

J11KL6 OTHER SOLID APR 0 3 2006 Wo k 

Coal Node Cu l 4C Goes 4C eu4C m Cu,d4C 

aG 

GIP G/P aG aG aG 

1 I 0 0 0 0 

25% log 158 30s 508 508 

Seeias(11n Seeinn(21in 

Speid Spew 

Seelam(3)in 

speew 

Porn-tion Peabides. 

anal 

SeriVOA- 

IMA (TCL) 

Ihharahfom Inamnbna I.urununa. 

_ r r 

k x 

r` £ 

CHAIN OF POSSESSION Sign/Print Name SPECIAL INSTRUCTIONS 

Matrix' 

Re6nryished By/Remond From /K smc 

EAS LOCKED STOR ts^ ey'°,.^ 

Dalefrime 

- 

NOTE: Ebalme. Perform Gaorna Spec *am baa+hp book I01Jomil le Labs, if possib le maintain 4 C 

Gong. ofi L'omil le.Pulorm me ta Nk/V DalHnme 

NOW 

7h C) 

ell uis d B /Rmnuved F s Daemme 

aq 

Rtttî ved By/5[aed In 

! 

r". 

Received B Y/Sward N 

Date/rime 

IeT^ 

Z 

ls, FCBXEST,SVOC in order as simp le is avai lable. Contract Coact Joan 

Kessocr salon macipa. _ 

(1) Gamma Spa-(Full lisp lAmencima:fl, Anrirraay-125. Be rylinm7, Cesitmn134-Cesium137, 

Cobalt-60. Europiuml52. Europium-154, Etaopiam155, P erassiu -40, Radium22 ( , Radlam226. 

•sa 

f^s E.s 4ma 

so-ASw 

sksh hs. 

W. W. 

OcO 1 

A.A. 

O/ RurlcniumlOO.Unoium235,Uracium23s) Relic 'hed e F DotNrmle 

X Yt^ ^! 6 OG ^G 17/7 

eGuquishe By/R Hued From Dame 

x 

4linqui 5hc y/Removedroom Daerfacc 

T*TA 

Received /S din 

D^— 

rived 

Received By/Stonfl 14 

_ 

b 

)me 

DdeTme 

Durerring 

l^ (2) ShootinmB9.90--Tarsi Sr. lsaopk Tho ium(Tnaiwsr23?); Isotopic U ranium l Uranium-233834, 

Uranium235,Unomm238);lsouocPlalonium 

(3) ICP Meala-60101Fu11 IJsq lAlurhiaam Antieay.rse n Anic• Barium 8cryllium Bismank aca B. 

Cadmium Ca lcium, Chromium Cabal, Copper, bra, lead. IAtdum Magnesium Manganese, 

Molybdenum L ybdenum Nickel. Phosphdos, Po pnium Seleainm Silicon. Silver, Sodium Strontium Thallium 

Uranium. Vanadium Zinc ): Mercu ry - 7471 - (CV) 

uM 

sK.o, &" 

a.ne.,,ugy 

T.Ta.. 

wr.w^l. 

'd 

z.alh. 

LAAORATORY Received By TitleDateTme 

`^+VS 

SECTION 

FINAL SAMPLE Disposal Method Disposed By D+INfime 

UISPOtiI'I'ION 

SHI-EE-011 (08/29/2005)

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-271 j Pw I of I 

Collector 

rnLLER, B. TR KLINC 

Compam Contact 

JOAN KESSNER 

Telephone No. 

375-4688 

Pro ject Coordinator 

KESSNER, Bit 

Price Code 9N Data TurOaro .. 

oiect Desianation 


Samdina Location 

1607-13 2:1 OFFAL 



Air Quality q 

Ice Chest No.///tea 

/y i[ (^- ^1 ^^ 

Field Loabo rk No. 

EL-1595 

COA 

DESRAS6520 

Method of Shlomept 

FED EX 

(S) 

m 

Offxtle Pum1v No. ,y06D q?^ B 

Sh' ro 

BI of Ladmv/Air Bi ll No. 

ERLBVE SERVICE LIONVILLE •73 SEE OSPC 

POSSIBLE SAMPLE HAZARDSJREMARKS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-273 Nse t el 1 

011ecLE TILLER, TI B. TR KLINCKMAN 

CompanyContact 

T 

375-4689 

o 

KFSiSNER. III 

Price Code 9N Data Turtaarouî 

Proled Designation 

100 & 300 Area Component of the RCHRA Sediment and Ti - 

Samp ling Location 




Air Quality q 45 Day% 

m 

Ice Cheat No. 

eree- e2 -/j Q r 

Field Loabook No. COA Method of Shipment h9 

_ 

EL 1595 BESRAS6520 FED EX 

Shipp OBbite Property No. Bi ll 

of LadipdAir Bi ll 

No. 

HERLINESRVICES LIONVILLE SEE OSPC 

POSSIBLE SAMPLE IIAZA RDSfREMARKS 

POTENTIAL RADIOAC77VE eOOTLIMITS 

Special Handlingand/or Storage 



S.^[. -afA 

Praeryatlon 


No. of Contaicer(s) 

Volume 

^ 3 G1 ^ 

Caa 4C none caul ac Caul 4C Cad 4C Qad 4C 

'Cs 

Gm GOP aG- aG aG 

I 1 0 0 0 0 

2508 log 15g SOB 509 50g 

Ses h.01n Scit.(2)a Seeionn P)ia PCns- M2 Paua _ Sbaivm. 

3P." S Pcdel Slaid tol l 8270A(7CL! 

lows+ Inu.iutm Invnlcl{pay 

Sample No. Matrix • Sample Date Samp le Tune c. may,,, =r .^.- -, w 

J1IHM2 

SOLID 

OTHER 

0 3 2570 /1( X x ^( 

CHAIN OF POSSESSION 

Re linquished ByliemovWPsom 

^/ 

EAS L 

_qqu lRe rant,r:_jy 

IrLL 

Relinquished ey moved Fars 

Relingni B e ved Fran 

Relinquished By/Rerr oved Fran 

Y-/° -"` 

/ 3 e' 

Dale/Time 

/fp0 

Irate/time 

WidrMac 

DmcRi"n 

SigNPrint Names 

R i B din 

S 

Re caiv y/Staed to 

—ica 

4r— 

Hecehed By In 

H 8 In 

ived By S cd In 

SPECIAL INSTRUCTIONS 

DucTme 

NOTE: Bberire- perfpm Gardens Spec Men tranship bode to Lionville tabs, Possible smintain 4C 

cook IS. Lionvil le: pertinent net W. PCB.PBSTSVOC in this order as tample is availab le. Canaan Joan 

7p Kesster",etxipt. 

_ 

DgaRme 

(I) Gammn Spec-(FAN tin) IAnerieiaawUl. Aninuny425, BeryIUum7,Caium134,Cesiam132, 

Cobek-60, Fnmpiuml5?, rwaopium154, Cvopiurth-155, PMassium40, Rahanm22ti, Radium?^8. 

Out _)(^ 

,"^n/e 

Rulhnium106, Urnrium235, Undum23 11 I 

Z Vp V (2) Suaninm89.90 ._ Total Sr hoopic Thorium ITho ium2321: Isaapk Umnism iUmni m233/734. 

DatelTinac 

Unudhms235, Unnihms2381: Isaopic Plutonium 

(3) ICP Meta ls - 6010 (FUN List) IAkmdnum Asainmy, A rsenic, Ba rium Berylliu m Bismuth, Boron, 

'UL 0 âo Cadndum Gkium Chromium Cabe a. Copper, Imn, lead, Lithium Ma Magnesium Manganese, 

Da1c/lise Molybdenum Nickel, Phosphorus, Potassium Se lenium Silicon, Silver. Sodium Stradium T1ml lium, 

Trn, Umnium Vanadium Lncl: Mercury- 7471 - (CV) 

Matrix *' 

Ma 

aFiawae 

p.Sl 

`.w°tl 

nàl 

py us 

T•Twr•wxv 

n'^ 

x.01- 

Relinquished By/Removed frown nafe/flne Received By/Srored in Date/fime 

S'4-A I(^j 3 C) 7) 

LABORATORY Received By Tide Date/1-mw 

SECTION 

FINAL SAMPLE Disposal Me thod Disposed By Dne?'me 

DISPOSITION 

BHI-EE-011 (08128!2005)

Washington Closu re Hanford CHAIN OF CUSTODYISAMPLE ANALYSIS REQUEST RC-047-274 >,^ i w t 

Collector 

Company Contact Tekphone No. Pro tect Coordinator 


JOAN KPSSNER 375-4688 KESSNER. JH 

^^ Code 9N Data 7Lrnerouda 

rrolect Desirnaaon - Sarnuline Lanaon SAFNe. 

100 & 300 Area Compon Component of the RCBRA Sedisnau and Ti YAKIPAA RIDGE IF OFFAL RC-047 0 

Ice Chest No. ! FIeELA 595ook No. Method^Shiproeot 

FSRAS6520 

Slri J 

ORsite Prow"v No. Ô^ O 2 ? Bill of Ladinv/Air Bill No. 

BERLfNESERVICFS LIONVR.LE 

JJ SEE OSPC 



Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-275 I pw J of 1 

Collect" 


roiect Desienatioa 

100 & 300 Arcs Component of the RCBRA Sediment and Tt 

Ice Chat No.p n 

/L TC " DZ -,dS 

Shi 

BERLINESERVICES ONVIL)E 

POSSIBLE SAM PUETFAZARDSJREMARILS 

POTENTIALRADIOAMV£

Washington Closu re Hanford CHAIN OF CUSTOIJIMAMPLE ANALYSIS REQUEST RC-047-276 Page 2 of L 

Collector 

TILLER, B- TR KLINCKMAN 

Protect Destination 

100 & 300 Arm Component of the RCBRA Sediment and Ti 

fee Chest No. p^ 

plc C — Oz -5,D,57— 

Sh 

ERE LI ESER LIONVILLE 


POTENTIAL RADIOACTIVE 3 D 3 


KESSNER, JH price Code 9N Data Turnarounlll 

V 

SAP No. 


43 Days m 

Air Quality El y m 0 

COA Method orShioment m 

ESRAS6520 

FED EX 

m 

2qBE 

Z2603 d0- 

of 

BS E 

SO PC 

BRI No. 

Cue14C name Ceu14C C.1 4C C.1 4C I C-14C 

aG GIP GIP aG aG MG 

( 1 0 0 0 0 

1509 log 158 508 50g 508 

Sae imr(1)n Seeaann(2)ia Smkan Min iCB,.Wl P

Washin>;ton Closure Hanford CHAIN OF CUSTODYISAMPLE ANALYSIS REQUEST RC-047-277 ^^ L or 5 

Ilect" _ 

TILLER. B. R KLINCKMAII 

Comoanr Contact 

JOAN KESSNER 

Telephone No. 

375-4688 

Praiecl Coordinator 

ICESSNER, ]H Price code 

roiect Desirnndan 

100 & 300 Area Component of the RCBRA Sediment and Tt 

Sanoline Location 

SADDLE MOUNTAIN OFFAL 


RC-007 

9N 

Air Quality 

Data Turstarmumn 

a 

45 Da ^' sm m 

9 

Ice Chest No. y^^ _ Oz Field L.oebook No, COA Merlwd of Shimomt m 

C ÛS 

Et, 1595 BESRAS6520 FED EX m 

Sld ed To - Offske Properly No. BID of Ah• BID No, 

BERLINE SFBVIC LIONVILLE ff J SEE OSPC 

POSSIBLE SAMPLE IIAZARDS /REMARKS 

POTEN77AL RADIOACTIVE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REOUEST RC-047-322 J PW I of I 

Collector 


Costwapy Contact Telephone No. 



KESSNER, JH 

Price Code 9N 

Data Tsrnarour^ 

45 Days9 

'ralect 1)esienation Samalirs¢ Lo cation SAF No. 

Air Quality 

IM) & 300 Area Component of the RCBRA Sediment and 71 100-DAS:2 OFFAL RC-047 m 

Ice Chest No. r 

Field Loebook Na. COA Method of SWonant - m 

-JrO156-m 

C -Q.Z EL_ 1595 BFSRAS6520 FED EX 

MPO^SJBLF _= SAMPLE 

LIONVILLE 

HAZARDSIREMARKS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS RE UEST RC-047-323 I Pate I Of I 

Collector 


Protect Desknotion 



JOAN KESSNER 

Samulina Loca ti on 

100-0.49:2 OFFAL 

Telephone No. 

375-4688 

Pro ieet Coordinator 

KESSNER, III 

SAP No. 


Price Code 9N 

Air Quality p 

pale Tururg0 naro 

m 

45 Day m 

(g 

m 

ICE Chest No. Field Logbook No. 

EL- 1595 

COA 

BESRAS6520 

Method of Shipmmtt 

FED EX 

m 

,^D,6oa33o 

S - ped'ra Olfsile Property No. 

Bill of Lading/Air Bill No. 

ER 04ESERVI 1LIONVILLE SEEOSPC 

POSSIBLE SAMPLE HAZARDWREMARKS 

POTENTIALRADIOACnVE

Washington Closure Hanford ' CHAIN OF CUSTODY/SAMPLE"ANALYSIS REQUEST RC-047-328 Paso 1 of 1 

Collector 

TILLER, B. TR KLINCKMAN - 


JOAN KESSNER 

Telephone No. 

375-4688 

Proisd Coordinator 

KESSNER, JH Price Code 9N Date 

It u, 

roket Destenalion 

100 & 300 Area Comp.mest of the RCBRA Seditrseot and Ti 

Ice Chest No. y-N 

Pi le C' 0.2 - 3rO,S 

So sogna Locadat 

116-DR-I,DR-7JI00-D-22 OFFAL 

Field Lenbook No, 

Et.-1595 

COA 

BFSRAS6520 




FED EX 

Air Quality Qy q 

5 Days% 

%m 

tD 

Ship 

D ERLINESERVICES LIONVILLE 


POTENTIAL RADIOACTIVE.

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-330 [ P -P 1 « 1 

Collector 

TILLER, B. 

TR KLINCKMAN 

'rolat Designation 

100 & 300 Atha Component of the RCBRA Sediment and Ti 

lee Chest No.pp 

2 see e.2 -,sly Jam' 

Company Contact Te lephone No. 


Samp ling Loca ti on 


Field Losbook No. 

EL-1595 

A06033a 

COA 

BESRAS6520 

Sh OfEdtc Properly No. 

Bi ll of Ladins/Air Bill No. 

EBERLINESERVICES LIONVILLE SEE OSPC 

POSSIBLE SAMPLE HAZARDMU MARKS 

POTENTIAL RADIOACTIVE Tne ,04 

EM LOCJ(ED STORAG E 

R^li vep^ y ^^^ 

s 

m b-4eH Dakrtirm 

/ ^(/aU 

U {^ bG ^.S-O p 

elirquis 8 eoved m Fmm Dak?nz 

SigulPrint Names 

fn :^^ 

eceived BylStded In 

^(' ,d Cx 

Received B n 


Dn^me 

NOTE: aeffee-perform Gamma Spec 0sentranshipbottle toUm•ilk Labs, ifpossible rtsinaio4C 

caa ft limrilk: perform an PCB.PEST,SVOC in this 0 as sa yk is anilable. Cod t loan 

y0 (J 

R 

ICesnrr upm receipt. 

Datemme 

(1) Omani Spec - (Full Liso 1 Americium241, Andmany-13. Bnyllium7, Cesium134. Ceaium137. 

Cobdt-60, FLmpitn.152, Euopium154, BvWium155, Pomsiu1r1d0. Radii 226, Radior 228, 

'Dal ^'m 1^ Rudica u e, 106. Urmhm-235, Undom2381 

Relin sbedd c Fmm a Unt 

t1A 9, 

Received B In Iku 

(n 

me 

s/U (2) Stmndu n39.90- Toad Sr. holopie T hmium I Thork m2321: 

IsdWk Urtmsm l Uranimu233/r_34, 

Umniom235. Uamimt-2381: hdapie P lutonium 

Reli quisle y/Re ed From 

Relinquished BY/Remmed Fwn, 

De nse 

Datefftme 

Recei B 

Received BY 

InDndfine 

A ck 0730 

d In Outeflihm 

^Gûl (E^ 50-t. 

LABORATORY Received By Tit leDate?rte 

SECTION 

FINAL SAMPLE Dispmal Method Disposed By Dale/rim 

DISPOSITION 

13 HI-EE-011 (08/2912005) 

Matrix 

s . 

soaeta 

sasaw. 

W. W. 

°'O^ 

'yp A. e+ w 

1a.a t.q. n 

T-Tiwe 

4LpuY 

v"vga°n. 

xon 

-

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047.332 Page I of L 

Collector 

TILLER, B. 

TH KLINCKMAN 

Conmur Contact 

JOAN KESSNER 

Telephone No, 

375-4688 

Protect Designation - Sampling Location SAF Na 

100 & 300 Area Component of the RCBRA Sediment and Ti 600.131 OFFAL RC-047 

Protect Coord inator 

KESSNER, JH Price Code 9N Data Turnarour^ 

Air Quality p 

45 Day ,'. 'n 

Ice Chat No.////â Field Loahook No. COA Method of Shipment 

lee— m 

EL.- 1595 BESRAS6520 FED EX m 

Shinned To Offaile Property No. Atr Bill m 

^ 

os^ Na 

- INESERV / LIONVILLE 

SEE 



Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-343 I NVe i of i 

collector - Company Contact Telephone No. Prolecl Coordinator 

TILLER, B. TR KLINCKIAAN JOAN KESSNER 375-4688 KESSNER,IH 

Price Code 9N 

Data Tnrstarousq^ 

45 Daysm 

oiect Desiauation SampRne Location 

SAF No, Air Quality E] 

100 & 300 Ar a Component of the RCBRA Sedimeat and Ts CF14TRAL PLATEAU SHRUB STEPPE OFFAL RC-047 em_ 

Ice Chest No. Fleld Na 

EL, 1595 

Slg C. 

OfrAle Property No 

HERLINE SERVIC LIONVILLE 

POSSIBLE XE HAZA RW/REMARKS 

POTEATIALRADIOAC71VE

^\ 

CLIENT: —Y-VW 

Lionvi ll 

e Laboratory Incorporated 

SAMPLE RECEIPT CRECKLIST (SRC) 

( 

r 

Yurchsê Order / Project# / C y 

/ W# / Release #: R 

n 

\iCiN-J- t3^ Date: 

Batch # : ?^ , 1 • Sample Custodian: 

1. Samples Hand De livered w Shipped 



NOTE: 

3. Outside of coolers or shipping containe rs are 


4. All expected paperwork received (coo and 

other c lient speci fic information) sealed in 

plastic bag and easily access ible? 

5. Samples receiv cool ambient? yQ 

6. Custody seals on sample containers intact 



8_ Sample containers are inta ct? 



10. Ali 

label information matches coc? 




SR-002-11 



client? 


Policy? (Identify a ll bottles not within 

policy. See reverse side for policy) 


discrepancies? nameldste (or samples 


vLl 

N ALL DISCREPk 

-e. so 

/ 

l 4" O Ne 

P 

TT7 

Yes O No 

a O No 

emp —j-'J °C 

Yes O No 

ra 

Ya 

Y 

/ es 

I9(Yes 

)dyes 

Yes 

O Ya 

O Ycs 

O Yes 

6]"Yes 

O No 

ONO 

O No 

O No 

0 No 

O No 

ONO 

Airb ill# 701 27 

O No Seals Comments 

o15O'J 7 

Cooler# SANS-\^3 

O No Seals 

^N/A 

ONO n,(/A 

ONo 

44 

P.= 3 

0 N No 

Discrepancies 

000000053

w EBERLINE 

VSERVICES 

May 30, 2006 

Ms. Joan Kessner 


3190 George Washington Way 

MSIN H9-02 


Reference: P.O. #630 

Eberline Se rvices R6-04-093-7420, SDG K0303 


-12a 

\^,ÔZ6l•8^ 

Enclosed is the data report for sixteen solid (other solid) samples designated under SAF No. 

RC-047. The samples were received at Ebertine Se rvices on Ap ril 12, 2006. The samples were 

analyzed according to the accompanying chain-of-custody documents. 

Please call if you have any questions conce rn ing this report. 

Sincerely, 

Melissa C. Mannion 

Senior Program Manager 

MCM/njv 

Enclosure: Data Package 

,Zr 

Z 

w 

^^9^^^^' 

Analytical Services 

2030 Wright Avenue 

P.O. Box 4040 

Richmond, California 94804-0040 

(510) 235-2633 Fax (510) 235.0438 

Toll Free (800) 841-5487 

www.eberlineservices.com

Eberline Services Washington Closure Hanford 

W.O. No. R6-04-093-7420 SDG K0303 

Case Narrative Page 1 of 1 

1.0 GENERAL 

Washington Closure Hanford (WCH) Sample Delivery Group K0303 was composed of 

sixteen solid (other solid) samples designated under SAF No. RC-047 with a Project 

Designation of: 100 & 300 Area Component of the RCBRA Sediment and Ti. 

The samples were received as stated on the Chain-of-Custody documents. Any 

discrepancies are noted on the Ebertine Services Sample Receipt Checklist. All results 

were transmitted to WCH via e-mail on May 25, 2006. 

2.0 ANALYSIS NOTES 

2.1 Total Strontium Analysis 

No problems were encountered during the course of the analyses. 

2.2 Isotopic Thorium Analysis 


2.3 Isotopic Uranium Analysis 


2.4 Isotopic Plutonium Analysis 


2.4 Gamma Spectroscopy 


Case Narrative Certification Statement 

"I certify that this data package is In compliance with the SOW, both technically 

and for completeness, for other than the conditions detailed above. Release of the 

data obtained in this hard copy data package has been authorized by the 

Laboratory Manager or a designee, as verified by the following signature." 

Melissa C. Mannion Date 

Senior Program Manager

E B E R L I N E S E R V I C E S/ R I C H M O N D 

SAMPLE DELIVERY GROUP K0303 

SDG 7420 Client Hanford 

Contact Melissa C. Mannion Contract No. 630 

Case no SDG K0303 

S U M M A R Y D A T A S E C T I O N 

T A B L E O F C O N T E N T S 

About this section 1 

Sample Summaries 3 

Prep Batch Summary 5 

Work Summary 6 

Method Blanks 10 

Lab Control Samples 12 

Duplicates 13 

Data Sheets 15 

Method Summaries 31 

Report Guides 41 

End of Section 55 

Lab id EBRLNE 

Prepared by Protocol Hanford 

Version Ver 1.0 

Form DVD-TOC 

Version 3.06 

Reviewed by Report date 05/25/06

EBERLINE SERVI CES / RI CHMOND 

SAMPLE DELIVERY GROUP X0303 


Contact Melissa C. Mannion R E P O R T G U I D E Contract No. 630 


ABOUT THE DATA SUMMARY SECTION 

The Data Summary Section of a Data Package has all data, in several 

useful orders, necessary for first level, routine review of the data 

package for a Sample Delivery Group (SDG). This section follows the 

Data Package Narrative, which has an overview of the data package and a 

discussion of special problems. It is followed by the Raw Data Section, 

which has full details. 

The Data Summary Section has several groups of reports: 

SAMPLE SUMMARIES 

The Sample and QC Summary Reports show all samples, including QC 

samples, reported in one SDG. These reports cross-reference client and 

lab sample identifiers. 

PREPARATION BATCH SUMMARY 

The Preparation Batch Summary Report shows all preparation batches 

(lab groupings reflecting how work was organized) relevant to the 

reported SDG with information necessary to check the completeness and 

consistency of the SDG. 

WORK SUMMARY 

The Work Summary Report shows all samples and work done on them 

relevant to the reported SDG. 

METHOD BLANKS 

The Method Blank Reports, one for each Method Blank relevant to the 

SDG, show all results and primary supporting information for the blanks. 

LAB CONTROL SAMPLES 

The Lab Control Sample Reports, one for each Lab Control Sample relevant 

to the SDG, show all results, recoveries and primary supporting 

information for these QC samples. 

Lab id EBRLNE 

Protocol Hanford 

REPORT GUIDES Version Ver 1.0 

Page 1 Form DVD-RG 

SUMMARY DATA SECTION Version 3.06 

Page 1 Report date 05/25/06

E B ERLINE SERVICES/RICHMOND 



Contact Melissa C. Mannion G U I D E, C O n t Contract No. 630 


DUPLICATES 

A BOUT T HE DATA SUMMARY SECTION 

The Duplicate Reports, one for each Duplicate and Original sample pair 

relevant to the SDG, show all results, differences and primary 

supporting information for these QC samples. 

MATRIX SPIKES 

The Matrix Spike Reports, one for each Spiked and Original sample pair 

relevant to the SDG, show all results, recoveries and primary supporting 

information for these QC samples. 

DATA SHEETS 

The Data Sheet Reports, one for each client sample in the SDG, show all 

results and primary supporting information for these samples. 

METHOD SUMMARIES 

The Method Summary Reports, one for each test used in the SDG, show all 

results, QC and method performance data for one analyte on one or two 

pages. (A test is a short code for the method used to do certain work 

to the client's specification.) 

REPORT GUIDES 

The Report Guides, one for each of the above groups of reports, have 

documentation on how to read the associated reports. 

Lab id EBRLNE 




SUbDIARY DATA SECTION Version 3.06 


CLIENT SAMPLE ID 

J11KK8 

JllKL5 

JllKL6 

J11KM0 

JllKM2 

Jll KM3 

Jll KM4 

J11KM5 

JllKM6 

J11KT0 

J11KV1 

J11KV2 

JIIL21 

JIIL23 

JIIL25 

JllL36 

SIG 7420 

Contact Melissa C. Mannion 

Method Blank 

Lab Control Sample 

Duplicate (R604093-06) 

SAMPLE SUMMARY 

Page 1 

SUMMARY DATA SECTION 

Page 3 

EBERLINE SERVICES/RICHMOND 



LAB CHAIN OF 

Client Hanford 

Contract No. 630 

Case no SOO X0303 

LOCATION MATRIX LEVEL SAMPLE ID SAP NO CUSTODY COLLECTED 

600-132/600-190 OFFAL SOLID R604093-02 RC-047 RC047-259 04/05/06 09:19 

1607-H2 OFFAL SOLID R604093-03 RC-047 RC047-266 04/05/06 08:12 

116-N-3 OFFAL SOLID R604093-04 RC-047 RC047-267 04/03/06 14:20 

1607-D2:1 OFFAL SOLID R604093-05 RC-047 RC047-271 04/05/06 07:52 

BORROW PIT 24 OFFAL SOLID R604093-06 RC-047 RC047-273 04/03/06 12:56 

YAKIMA RIDGE II OFFAL SOLID R604093-07 RC-047 RC047-274 04/03/06 12:30 

VERNITA UPRV S.SIDE OFFL SOLID R604093-08 RC-047 RC047-275 04/03/06 10:43 

MCGEE RANCH OFFAL SOLID R604093-09 RC-047 RC047-276 04/03/06 09:45 

SADDLE MOUNTAIN OFFAL SOLID R604093-10 RC-047 RC047-277 04/03/06 09:00 

116-N-3 INVERTEBRATES SOLID 8604093-01 RC-047 RC047-311 04/D3/06 06:57 

100-D-48:2 OFFAL SOLID R604093-11 RC-047 RC047-322 04/05/06 06:55 

100-D-49:2 OFFAL SOLID R604093-12 RC-047 RC047-323 04/05/06 07:20 

116DR1,DR-2/100-D-22 OFL SOLID R604093-13 RC-047 RC047-328 04/03/06 13:56 

BORROW PIT 23 OFFAL SOLID R6D4093-14 RC-047 RC047-330 04/03/06 13:20 

600-131 OFFAL SOLID R604093-15 RC-047 RC047-332 04/05/06 08:48 

CENT.PL.AT .SHRUB STEP.OFL SOLID R604093-16 RC-047 RC047-343 04/03/06 10:15 

SOLID 8604093-18 RC-047 

SOLID R604093-17 RC-047 

BORROW PIT 24 OFFAL SOLID R604093-19 RC-047 04/03/06 12:56 

Lab id EBRLNE 



Form DVD-CS 

Version 3.06 

Report date 05/25/06




/^ 


4 C SUMMARY Contract No. 630 


CHAIN OF t SAMPLE BASIS DAYS SINCE LAB DEPARTMENT 

QC BATCH CUSTODY CLIENT SAMPLE ID MATRIX SOLIDS AMOUNT AMOUNT RECEIVED COIL SAMPLE ID SAMPLE ID 

7420 RC047-259 J11KK8 SOLID 100.0 77.8 g 04/12/06 7 R604093-02 7420-002 

RC047-266 JllKL5 SOLID 100.0 69.6 g 04/12/06 7 R604093-03 7420-003 

RC047-267 J11KL6 SOLID 100.0 74.5 g 04/12/06 9 R604093-04 7420-004 

RC047-271 JllKM0 SOLID 100.0 86.8 g 04/12/ 06 7 R604093 -05 7420-005 

RC047-273 J11KM2 SOLID 100.0 88.7 g 04/12/06 9 R604093-06 7420-006 



RC047-276 J11KM5 SOLID 100.0 65.9 g 04/12/06 9 R604093-09 -7420-009 


RC047-311 JllKT0 SOLID 100.0 2.21 g 04/12/06 9 R604093-01 7420-001 

RC047-322 J11KV1 SOLID 100.0 71.2 g 04/12/06 7 R604093-11 7420-011 

RC047-323 JllKV2 SOLID 100.0 67.6 g 04/12/06 7 R604093-12 7420-012 

RC047-328 JIIL21 SOLID 100.0 64.7 g 04/12/06 9 R604093-13 7420-013 

RC047-330 JIIL23 SOLID 100.0 71.4 g 04/12/06 9 R604093-14 7420-014 

RC047-332 J11 1,25 SOLID 100.0 80.8 g 04/12/06 7 R604093-15 7420-015 

RC047-343 J11 1,36 SOLID 100.0 71.5 g 04/12/06 9 R604093-16 7420-016 

Method Blank 

Lab Control Sample 

Duplicate (R604093-06) 

SOLID 

SOLID 

SOLID 100.0 88.7 g 04/12/06 9 

R604093-18 

R604093-17 

R604093-19 

7420-018 

7420-017 

7420-019 

Lab id EBRLNE 


QC SUMMARY Version Ver 1.0 

Page 1 Form DVD-OS 






Contact Melissa C. Manion PREP BATC:H SUMMARY Contract No. 630 

Case no SDG X0303 

PREPARATION ERROR PLANCHETS ANALYZED QUALI- 

TEST MATRIX METHOD BATCH 20 % CLIENT MORE RE BLANK LCS DUP/ORIG MS/ORIG PIERS 

Alpha Spectroscopy 

PU SOLID Plutonium, Isotopic in Solids 7161-066 5.0 15 1 1 1/1 

TH SOLID Thorium, Isotopic in Solids 7181-066 5.0 15 1 1 1/1 

U SOLID Uranium, Isotopic in Solids 7181-066 5.0 15 1 1 1/1 

Beta Counting 

SR SOLID Total Strontium in Solids 7181-066 10.0 16 1 1 1/1 

Gamma Spectroscopy 

GAM SOLID Gamma Scan 7181-066 15.0 15 1 1 1/1 

Duplicates and Matrix Spikes are those with original (Client) sample in this Sample Delivery Group. 

Blank and LCS planchets are those in the same preparation batch as some Client, Duplicate or Spike sample 

Lab id EBRLNE 


PREP BATCH SUMMARY Version Ver 1.0 

Page 1 Form DVD-PBS 






Contact Melissa C. Mannion WORK SUMMARY Contract No. 630 

CLIENT SAMPLE ID LAB SAMPLE ID 

LOCATION MATRIX COLLECTED SUF- 

CUSTODY SAF NO RECEIVED PLANCHET TEST FIX ANALYZED REVIEWED BY METHOD 

Case no BIG K0303 

J11KK8 R604093-02 7420-002 GAM 04/19/06 04/25/06 MWT Gamma Scan 

600-132/600-190 OFFAL SOLID 04/05/06 7420-002 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 

RC047-259 RC-047 04/12/06 7420-002 SR 05/09/06 05/16/06 MWT Total Strontium in Solids 

7420-002 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids 

7420-002 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids 

JllKL5 R604093-03 7420-003 GAM 04/19/06 04/25/06 MWT Gamma Scan 

1607-H2 OFFAL SOLID 04/05/06 7420-003 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 

RC047-266 RC-047 04/12/06 7420-003 SR - 05/09/06 05/16/06 MWT Total Strontium in Solids 



J11KL6 R604093-04 7420-004 GAM 04/20/06 04/25/06 MWT Gamma Scan 

116-N-3 OFFAL SOLID 04/03/06 7420-004 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 




JIlKM0 R604093-05 7420-005 GAM 04/21/06 04/25/06 MWT Gamma Scan 

1607-D2:1 OFFAL SOLID 04/05/06 7420-005 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 




JllKM2 R604093-06 7420-006 GAM 04/19/06 04/25/06 MWT Gamma Scan 

BORROW PIT 24 OFFAL SOLID 04/03/06 7420-006 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 




J11K43 R604093-07 7420-007 GAM 04/21/06 04/25/06 MWT Gamma Scan 

YAKIMA RIDGE II OFFAL SOLID 04/03/06 7420-007 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 




Lab id EBRLNE 


WORK SUMMARY Version Ver 1.0 

Page 1 Form DVD-CWS 

SUM4AARY DATA SECTION Version 3.06 


ESERLINE SERVICES/RICHMOND 



Contact Melissa C. Mannion WORK SUMMARY, C oI1t. Contract No. 630 


LOCATION MATRIX COLLECTED SUP- 

CUSTODY SAF No RECEIVED PLANCRET TEST FIX ANALYZED REVIEWED BY METHOD 


JllKM4 R604093-08 7420-008 GAM 04/21/06 04/25/06 MWT Gamma Scan 

VERNITA UPRV S.SIDE OFFL SOLID 04/03/06 7420-008 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 




JllXM5 R604093-09 7420-009 GAM 04/21/06 04/25/06 MWT Gamma Scan 

McGEE RANCH OFFAL SOLID 04/03/06 7420-009 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 




J11KM6 R604093-10 7420-010 GAM 04/21/06 04/25/06 MWT Gamma Scan 

SADDLE MOUNTAIN OFFAL SOLID 04/03/06 7420-010 PU 05/22/06 05/23/06 MWT Plutonium, Isotopic in Solids 



7420-010 D 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids 

J11KTO R604093-01 7420-001 SR 05/09/06 05/16/06 MWT Total Strontium in Solids 

116-N-3 INVERTEBRATES SOLID 04/03/06 

RC047-311 RC-047 04/12/06 

J11KV1 R604093-11 7420-011 GAM 04/21/06 04/25/06 MWT Gamma Scan 

100-D-48:2 OFFAL SOLID 04/05/06 7420-011 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 




J11XV2 8604093-12 7420-012 GAM 04/22/06 04/25/06 MWT Gamma Scan 

100-D-49:2 OFFAL SOLID 04/05/06 7420-012 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 

RC047-323 RC-047 04/12/06 7420-012- SR 05/10/06 05/16/06 MWT Total Strontium in Solids 



J111,21 R604093-13 7420-013 GAM 04/22/06 04/25/06 MWT Gamma Scan 

116DR1,DR-2/100-D-22 OFL SOLID 04/03/06 7420-013 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 




Lab id REPINE 


WORK SUMMARY Version Ver 1.0 

Page 2 Form DVD-CWS 



SDG 7420 




Contact Melissa C. Mamion WORK SUMMARY, cont. Contract No. 630 


LOCATION MATRIX COLLECTED SUF- 

CUSTODY SAF No RECEIVED PLANCHET TEST FIX ANALYZED REVIEWED BY METHOD 


J111,23 R604093-14 7420-014 GAM 04/22/06 04/25/06 MWT Gamma Scan 





J11L25 R604093-15 7420-015 GAM 04/22/06 04/25/06 MWT Gart Scan 

600-131 OFFAL SOLID 04/05/06 7420-015 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 




JIIL36 R604093-16 7420-016 GAM 04/22/06 04/25/06 MWT Gamma Scan 

CENT.PLAT.SHRUR STEP.OFL SOLID 04/03/06 7420-016 PO 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 



7420-016 q 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids 

Method Blank R604093-18 7420-018 GAM 04/20/06 04/25/06 MWT Gamma Scan 

SOLID 7420-018 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 

RC-047 7420-018 SR 05/09/06 05/16/06 MWT Total Strontium in Solids 



Lab Control Sample R604093-17 7420-017 GAM 04/20/06 04/25/06 MWT Gamma Scan 

SOLID 7420-017 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids 

RC-047 7420-017 SR 05/10/06 05/16/06 MWT Total Strontium in Solids 



Duplicate (R604093-06) R604093-19 7420-019 GAM 04/21/06 04/25/06 MWT Gamma Scan 


WORK SUMMARY 

Page 3 

RC-047 04/12/06 7420-019 SR 05/09/06 05/16/06 MWT Total Strontium in Solids 


7420-019 q 05/17/06 05/22/06 MET Uranium, Isotopic in Solids 

Lab id EBRLNE 



Form DVD-CWS 


Page 8 


SDG 7420 



Contact Melissa C. Mannion WORK SUMMARY, cont. 

TEST SAP No 

METHOD 

COUNTS OF 

TESTS BY 

REFERENCE 



Case no SOO X0303 

SAMPLE TYPE 

CLIENT MORE RE BLANX ICE CUP SPIKE TOTAL 

GAM RC-047 Gamma Scan GAFAtA_GS 15 1 1 1 18 

PU RC-047 Plutonium, Isotopic in Solids PUISO_PLATE_AEA 15 1 1 1 18 

SR RC-047 Total Strontium in Solids SRTOT_SEP_PRECIP_GPC 16 1 1 1 19 

TH RC-047 Thorium, Isotopic in Solids THISO_IE_PLATE_AEA 15 1 1 1 18 

U RC-047 Uranium, Isotopic in Solids UISO_PLATE_AEA 15 1 1 1 18 

TOTALS 76 5 5 5 91 

WORK SUMMARY 

Page 4 

Lab id EBRLNE 



Form DVD-CWS 

S^Y DATA SECTION Version 3.06 




R604093-18 Method Blank 

METHOD BLANK 

SDG 7420 


Lab sample id R604093-18 

Dept sample id 7420-018 

ANALYTE CAS NO 

Client/Case no Hanford SDG K0303 


Client sample id Method Blank 

Material/Matrix SOLID 

SAF No RC-047 

RESULT 

PCi/g 

2a ERR 

(COUNT) 

MDA 

pCi/g 

RDL 

pci/g 

QUALI- 

PIERS TEST 

Total Strontium SR-RAD 0.023 0.18 0.32 1.0 U SR 

Thorium 228 14274-82-9 -0.087 0.35 0.84 1.0 U TH 

Thorium 230 14269-63-7 0.261 0.35 0.67 1.0 U TH 

Thorium 232 TH-232 0 0.17 0.67 1.0 U TH 

Uranium 233/234 U-233/234 0 0.052 0.20 1.0 U U 

Uranium 235 15117-96-1 0 0.063 0.24 1.0 U U 

Uranium 238 U-238 0 0.052 0.20 1.0 U U 

Plutonium 238 13981-16-3 0 0.071 0.27 1.0 U PU 

Plutonium 239/240 PU-239/240 0 0.071 0.27 1.0 U PU 

Potassium 40 13966-00-2 U 3.1 U GAM 

Cobalt 60 10198-40-0 U 0.14 0.050 U GAM 

Cesium 137 10045-97-3 U 0.20 0.10 U GAM 

Radium 226 13982-63-3 U 0.23 0.10 U GAM 

Radium 228 15262-20-1 U 0.50 0.20 U GAM 

Europium 152 14683-23-9 U 0.26 0.10 U GAM 



Thorium 228 14274-82-9 U 0.13 U GAM 

Thorium 232 TH-232 U 0.50 U GAM 

Uranium 235 15117-96-1 U 0.37 U GAM 

Uranium 238 U-238 U 13 U GAM 

Americium 241 14596-10-2 U 0.33 U GAM 

Beryllium 7 13966-02-4 U 0.68 U GAM 

Ruthenium 106 13967-48-1 U 0.84 U GAM 

Antimony 125 14234-35-6 U 0.23 U GAM 

Cesium 134 13967-70-9 U 0.14 U GAM 

100&300Area Compnt RCBRA Sediment&Ti 

Lab id EBRLNE 


METHOD BLANKS Version Ver 1.0 

Page 1 Form DVD-DS 



EBERLINE SERVICES / RICHMOND 


R604093-18 Method Blank 

BLANK, con t. 

SDG 7420 




QC-BLANK #56758 



Client sample id Method Blank 

Material/Matrix SOLID 


Lab id EBRLNE 


METHOD BLANKS Version Ver 1.0 






R604093-17 Lab Control Sample 

LAB CONTROL SAMPLE 

SIG 7420 Client/Case no Hanford SDG K0303 


Lab sample id R604093-17 Client sample id Lab Control Sample 

Dept sample id 7420-017 Material/Matrix SOLID 

ANAL YTE 

RESULT 

pCi/g 

2a ERR 

(COUNT) 

MDA 

pCi/g 

RDL 

pCi/g 

QUALI- 

FIRM TEST 


ADDED 

pCi/g 

2s ERR 

pCi/g 

REC 

g 

30 IMPS 

(TOTAL) 

PROTOCOL 

Total Strontium 10.9 0.52 0.18 1.0 SR 10.8 0.43 101 B2-118 80-120 

Thorium 230 38.6 5.0 0.43 1.0 TH 44.4 1.8 87 81-119 80-120 

Uranium 233/234 19.8 2.0 0.88 1.0 U 19.3 0.77 103 82-118 80-120 

Uranium 235 16.6 1.8 0.19 1.0 U 15.7 0.63 106 80-120 80-120 

Uranium 238 20.0 2.0 0.85 1.0 U 21.0 0.84 95 83-117 80-120 

Plutonium 238 24.7 2.4 0.20 1.0 PU 26.2 1.0 94 B4-116 80-120 

Plutonium 239/240 26.9 2.5 0.20 1.0 PU 29.0 1.2 93 84-116 80-120 

Cobalt 60 4.47 0.34 0.16 0.050 GAM 4.47 0.18 100 74-126 80-120 

Cesium 137 4.84 0.31 0.25 0.10 GAM 4.61 0.18 105 74-126 80-120 

100&300Area Compnt RCERA Sediment&Ti 

QC-LCS #56757 

Lab id EBRLNE 


LAB CONTROL SAMPLES Version Ver 1.0 

Page 1 Form DVD-LCS 


Page 12 Report date 05/25/06 

LIMITS

SDG 7420 


DUPLICATE 



ANALYTE 

6 solids 100.0 



R604093-19 J11KM2 

DUPLICATE 

DUPLICATE 

pCi/g 

20 ERR 

(COUNT) 

ORIGINAL 



MDA 

pCi/g 

Received 04/12/06 

t solids 100.0 

ML 

pCi/g 

QUALI- 

PIERS TEST 



Client sample id S11KM2 

Location/Matrix BORROW PIT 24 OFFAL SOLID 

Collected/Weight 04/03/06 12:56 8B.7 q 

Custody/SAF No RC047-273 RC-047 

ORIGINAL 

Total Strontium 0.386 0.15 0.22 1.0 SR 0.505 0.16 0.22 27 77 1.0 

Thorium 228 -0.053 0.11 0.41 1.0 U TH 0 0.10 0.39 U - 0.7 

Thorium 230 -0.158 0.11 0.40 1.0 U TH 0.051 0.31 0.49 U - 1.3 

Thorium 232 0 0.11 0.40 1.0 U TH -0.051 0.10 0.39 U - 0.7 

Uranium 233/234 0 0.054 0.21 1.0 U U 0.032 0.065 0.25 U - 0.8 

Uranium 235 0 0.065 0.25 1.0 U U 0 0.078 0.30 U - 0 

Uranium 238 0.054 0.054 0.21 1.0 U U 0 0.065 0.25 U - 1.3 

Plutonium 238 0 0.075 0.29 1.0 U PU 0 0.045 0.17 U - 0 

Plutonium 239/240 0 0.075 0.29 1.0 U PU 0 0.045 0.17 U - 0 

Potassium 40 2.65 0.99 0.60 GAM 3.28 1.0 0.55 21 78 0.8 

Cobalt 60 U 0.063 0.050 U GAM U 0.068 U - 0.1 

Cesium 137 U 0.064 0.10 U GAM U 0.066 U - 0 

Radium 226 U 0.11 0.10 U GAM U 0.12 U - 0.1 

Radium 228 U 0.25 0.20 U GAM U 0.30 U - 0.3 

Europium 152 U 0.15 0.10 U GAM U 0.15 U - 0 

Europium 154 U 0.21 0.10 U GAM U 0.21 U - 0 

Europium 155 U 0.14 0.10 U GAM U 0.15 U - 0.1 

Thorium 228 U 0.090 U GAM U 0.095 U - 0.1 

Thorium 232 U 0.25 U GAM U 0.30 U - 0.3 

Uranium 235 U 0.24 U GAM U 0.26 U - 0.1 

Uranium 238 U 8.2 U GAM U 9.7 U - 012 

Americium 241 U 0.25 U GAM U 0.28 U - 0.2 

Beryllium 7 U 0.53 U GAM U 0.58 U - 0.1 

Ruthenium 106 U 0.55 U GAM U 0.59 U - 0.1 

Antimony 125 U 0.15 U GAM U 0.16 U - 0.1 

Cesium 134 U 0.072 U GAM U 0.079 U - 0.1 

1006300Area Compnt RCBRA Sediment&T1 

pCi/g 

20 ERR 

(COUNT) 

MDA 

pCi/g 

QUALI- 

PIERS 

RPD 

t 

30 

TOT 

Lab id EBRLNE 


DUPLICATES Version Ver 1.0 

Page 1 Form DVD-DUP 


Page 13 Report date 05/25/06 

DER 

a

R604093-19 

SDG 7420 


DUPLICATE 



4 solids 100.0 

QC-OUP#6 56759 

DUPLICATES 

Page 2 

SUMMARY DATA SECTION 

Page 14 



DUPLICATE, cont. 

ORIGINAL 







Client sample id J11KM2 

Jll1 

Location/Matrix BORROW PIT 24 OFFAL SOLID 

Collected/Weight 04/03/06 12:56 88.7 a 

Custody/SAF NO RC047-273 RC-047 

Lab id EBRLNE 



Form DVD-DUP 

Version 3.06 




R604093-02 J11XK8 

DATA SHEET 

SDG 7420 Client/Case no Hanford SDG K0303 


Lab sample id R604093-02 Client sample id JllKK8 

Dept sample id 7420-002 Location/Matrix 600-132/600-190 OFFAL SOLID 

Received 04/12/06 Collected/Weight 04/05/06 09:19 77.8 a 

% solids 100.0 Custody/SAF No RC047-259 RC-047 


RESULT 

pCi/g 

20 ERR 

(COUNT) 

MDA 

pCi/g 

ROL 

pCi/g 

QUALI- 

PIERS TEST 


Thorium 228 14274-82-9 0.069 0.14 0.53 1.0 U TH 

Thorium 230 14269-63-7 0.137 0.41 0.66 1.0 U TH 

Thorium 232 TH-232 0.069 0.14 0.53 1.0 U TH 

Uranium 233/234 U-233/234 0.423 0.20 0.19 1.0 U 

Uranium 235 15117-96-1 0 0.060 0.23 1.0 U U 

Uranium 238 U-238 0.597 0.25 0.19 1.0 U 

Plutonium 238 13981-16-3 0.031 0.13 0.24 1.0 U PU 

Plutonium 239/240 PU-239/240 0.157 0.13 0.24 1.0 U PU 


Cobalt 60 10198-40-0 U 0.13 0.050 U GAM 


Radium 226 13982-63-3 U 0.25 0.10 U GAM 

Radium 228 15262-20-1 U 0.53 0.20 U GAM 




Thorium 228 14274-82-9 U 0.15 U GAM 


Uranium 235 15117-96-1 U 0.41 U GAM 






Cesium 134 13967-70-9 U 0.12 U GAM 


Lab id EBRLNE 


DATA SHEETS Version Ver 1.0 






R604093-03 J11KL5 

DATA SHEET 

SDG 7420 





W solids 100.0 

ANALYTH CAS NO 



Client sample id J11KL5 

Location/Matrix 1607-H2 OFFAL SOLID 



RESULT 

pci/g 

2a ERR 

(COUNT) 

MDA 

pCi/g 

RDL 

pCi/g 

QUALI- 

PIERS TEST 


Thorium 228 14274-82-9 0 0.087 0.33 1.0 U TH 

Thorium 230 14269-63-7 0.044 0.26 0.42 1.0 U TH 

Thorium 232 TH-232 0 0.087 0.33 1.0 U TH 

Uranium 233/234 U-233/234 0.020 0.040 0.15 1.0 U U 

Uranium 235 15117-96-1 0 0.049 0.19 1.0 U U 

Uranium 238 U-238 0 0.040 0.15 1.0 U U 

Plutonium 238 13981-16-3 -0.053 0.053 0.25 1.0 U PU 



Cobalt 60 10198-40-0 U 0.14 0.050 U GAM 


Radium 226 13982-63-3 U 0.22 0.10 U GAM 

Radium 228 15262-20-1 U 0.48 0.20 U GAM 




Thorium 228 14274-82-9 U 0.13 U GAM 


Uranium 235 15117-96-1 U 0.35 U GAM 






Cesium 134 13967-70-9 U 0.14 U GAM 


Lab id EBRLNE 






EBERLINE SER V ICES / RICHMOND 


R604093-04 J11KL6 

DATA SHEET 

SDG 7420 





* solids 100.0 




Client sample id J11KL6 

Location/Matrix 116-N-3 OFFAL SOLID 

Collected/Weight 04/03/06 14:20 74.5 q 


RESULT 

PCi/g 

2a ERR 

(COUNT) 

MDA 

pCi/g 

RDL 

pCi/g 

QUALI- 

FIERS TEST 


Thorium 228 14274-82-9 0.162 0.33 0.62 1.0 U TH 

Thorium 230 14269-63-7 0.243 0.33 0.62 1.0 U TH 

Thorium 232 TH-232 0 0.16 0.62 1.0 U TH 

Uranium 233/234 U-233/234 0.024 0.048 0.18 1.0 U U 

Uranium 235 15117-96-1 0 0.058 0.22 1.0 U U 

Uranium 238 U-238 0.024 0.048 0.18 1.0 U U 

Plutonium 238 13981-16-3 0 0.052 0.20 1.0 U PU 



Cobalt 60 10198-40-0 U 0.11 0.050 U GAM 


Radium 226 13982-63-3 U 0.24 0.10 U GAM 

Radium 228 15262-20-1 U 0.52 0.20 U GAM 




Thorium 228 14274-82-9 U 0.15 U GAM 


Uranium 235 15117-96-1 U 0.41 U GAM 






Cesium 134 13967-70-9 U 0.12 U GAM 

100&30OArea Compnt RCBRA Sediment&Ti 

Lab id EBRLNE 






EBER L INE SER V ICES / RICHMOND 


R604093-05 J11XM0 

DATA SHEET 

SDG 7420 





* solids 100.0 




Client sample id JllKM0 

Location/Matrix 1607-D2:1 OFFAL SOLID 



RESULT 

pCi/g 

2a ERR 

(COUNT) 

MDA 

pCi/g 

RDL 

pCi/g 

QUALI- 

PIERS TEST 


Thorium 228 14274-82-9 0 0.15 0.56 1.0 U TH 

Thorium 230 14269-63-7 0.147 0.30 0.56 1.0 U TH 

Thorium 232 TH-232 0 0.15 0.56 1.0 U TH 

Uranium 233/234 U-233/234 0 0.070 0.27 1.0 U U 

Uranium 235 15117-96-1 0 0.084 0.32 1.0 U U 

Uranium 238 U-238 0 0.070 0.27 1.0 U U 

Plutonium 238 13981-16-3 0 0.11 0.26 1.0 U PU 

Plutonium 239/240 PU-239/240 -0.027 0.055 0.21 1.0 U PU 


Cobalt 60 10198-40-0 U 0.10 0.050 U GAM 


Radium 226 13982-63-3 U 0.21 0.10 U GAM 

Radium 228 15262-20-1 U 0.46 0.20 U GAM 




Thorium 228 14274-82-9 U 0.13 U GAM 


Uranium 235 15117-96-1 U 0.36 U GAM 






Cesium 134 13967-70-9 U 0.11 U GAM 


Lab id EBRLNE 






EBERLI N E SE RVIC ES /RICHMOND 


R604093-06 J11KM2 

DATA SHEET 



Lab sample id R604093-06 Client sample id J11KM2 

Dept sample id 7420-006 Location/Matrix BORROW PIT 24 OFFAL SOLID 

Received 04/12/06 Collected/Weight 04/03/06 12:56 88.7 ca 

V solids 100.0 Custody/SAF No RC047-273 RC-047 


RESULT 

pCi/g 

2a ERR 

(COUNT) 

MDA 

pCi/g 

RDL 

pCi/g 

QUALI- 

FIERS TEST 

Total Strontium SR-RAD 0.505 0.16 0.22 1.0 SR 

Thorium 228 14274-82-9 0 0.10 0.39 1.0 U TH 

Thorium 230 14269-63-7 0.051 0.31 0.49 1.0 U TH 

Thorium 232 TH-232 -0.051 0.10 0.39 1.0 U TH 

Uranium 233/234 U-233/234 0.032 0.065 0.25 1.0 U U 

Uranium 235 15117-96-1 0 0.078 0.30 1.0 U U 

Uranium 238 U-238 0 0.065 0.25 1.0 U U 

Plutonium 238 13981-16-3 0 0.045 0.17 1.0 U PU 


Potassium 40 13966-00-2 3.28 1.0 0.55 GAM 

Cobalt 60 10198-40-0 U 0.068 0.050 U GAM 


Radium 226 13982-63-3 U 0.12 0.10 U GAM 

Radium 228 15262-20-1 U 0.30 0.20 U GAM 




Thorium 228 14274-82-9 U 0.095 U GAM 


Uranium 235 15117-96-1 U 0.26 U GAM 

Uranium 238 U-238 U 9.7 U GAM 





Cesium 134 13967-70-9 U 0.079 U GAM 


Lab id EBRLNE 








R604093-07 JlIKM3 

DATA SHEET 

SDG 7420 










Location/Matrix YAKIMA RIDGE II OFFAL SOLID 



RESULT 

pCi/g 

20 ERR 

(COUNT) 

MDA 

pCi/g 

ROL 

pCi/g 

QUALI- 

FIERS TEST 


Thorium 228 14274-82-9 0 0.12 0.46 1.0 U TH 

Thorium 230 14269-63-7 0.178 0.36 0.45 1.0 U TH 

Thorium 232 TH-232 0 0.12 0.45 1.0 U TH 

Uranium 233/234 U-233/234 0 0.056 0.22 1.0 U U 

Uranium 235 15117-96-1 0 0.068 0.26 1.0 U U 

Uranium 238 U-238 0 0.056 0.22 1.0 U U 

Plutonium 238 13981-16-3 0.036 0.036 0.14 1.0 U PU 



Cobalt 60 10198-40-0 U 0.11 0.050 U GAM 


Radium 226 13982-63-3 U 0.18 0.10 U GAM 

Radium 228 15262-20-1 U 0.39 0.20 U GAM 




Thorium 228 14274-82-9 U 0.11 U GAM 


Uranium 235 15117-96-1 U 0.29 U GAM 






Cesium 134 13967-70-9 U 0.096 U GAM 


Lab id EBRLNE 








R604093-08 J11XM4 

DATA SHEET 

SDG 7420 





% solids 100.0 





Location/Matrix VERNITA UPRV S.SIDE OFFL SOLID 



RESULT 

pCi/g 

20 ERR 

(COUNT) 

MDA 

pci/g 

RDL 

pci/g 

QUALI- 

PIERS TEST 


Thorium 228 14274-82-9 -0.112 0.11 0.54 1.0 U TH 

Thorium 230 14269-63-7 0.112 0.22 0.43 1.0 U TH 

Thorium 232 TH-232 0 0.11 0.43 1.0 U TH 

Uranium 233/234 U-233/234 0 0.048 0.18 1.0 U U 

Uranium 235 15117-96-1 0 0.056 0.22 1.0 U U 

Uranium 238 U-238 0.024 0.048 0.18 1.0 U U 

Plutonium 238 13981-16-3 0.032 0.13 0.25 1.0 U PU 

Plutonium 239/240 PU-239/240 -0.032 0.065 0.25 1.0 U PU 

Potassium 40 13966-00-2 2.74 0.77 0.46 GAM 

Cobalt 60 10198-40-0 U 0.060 0.050 U GAM 


Radium 226 13982-63-3 U 0.11 0.10 U GAM 

Radium 228 15262-20-1 U 0.25 0.20 U GAM 




Thorium 228 14274-82-9 U 0.071 U GAM 


Uranium 235 15117-96-1 U 0.17 U GAM 






Cesium 134 13967-70-9 U 0.061 U GAM 


Lab id EBRLNE 








R604093-09 J11KM5 

DATA SHEET 

SDG 7420 










Location/Matrix McGEE RANCH OFFAL SOLID 

Collected/Weight 04/03/06 09:45 65.9 g 


RESULT 

PCi/g 

2a ERR 

(COUNT) 

MDA 

pCi/g 

RDL 

pCi/g 

QUALI- 

FIERS TEST 


Thorium 228 14274-82-9 0.064 0.26 0.49 1.0 U TH 

Thorium 230 14269-63-7 0.064 0.26 0.49 1.0 U TH 

Thorium 232 TH-232 0 0.13 0.49 1.0 U TH 

Uranium 233/234 U-233/234 0.024 0.048 0.18 1.0 U U 

Uranium 235 15117-96-1 0 0.058 0.22 1.0 U U 

Uranium 238 U-238 0 0.048 0.18 1.0 U U 

Plutonium 238 13981-16-3 -0.036 0.14 0.35 1.0 U PU 


Potassium 40 13966-00-2 2.37 1.1 0.66 GAM 

Cobalt 60 10198-40-0 U 0.061 0.050 U GAM 


Radium 226 13982-63-3 U 0.11 0.10 U GAM 

Radium 228 15262-20-1 U 0.26 0.20 U GAM 




Thorium 228 14274-82-9 U 0.084 U GAM 


Uranium 235 15117-96-1 U 0.23 U GAM 






Cesium 134 13967-70-9 U 0.071 U GAM 


Lab id EBRLNE 






EBERLINE SER V ICES / RICHMOND 


R604093-10 J11XM6 

DATA SHEET 

SDG 7420 










Location/Matrix SADDLE MOUNTAIN OFFAL SOLID 



RESULT 

pCi/g 

2a ERR 

(COUNT) 

MDA 

pCi/g 

RDL 

pci/g 

QUALI- 

FIERS TEST 

Total Strontium SR-RAD -0.082 0.12 0.27 1.0 U SR 

Thorium 228 14274-82-9 0 0.14 0.53 1.0 U TH 

Thorium 230 14269-63-7 0.139 0.28 0.53 1.0 U TH 

Thorium 232 TH-232 0 0.14 0.53 1.0 U TH 

Uranium 233/234 U-233/234 0 0.053 0.20 1.0 U U 

Uranium 235 15117-96-1 0 0.065 0.25 1.0 U U 

Uranium 238 U-238 0 0.053 0.20 1.0 U U 

Plutonium 238 13981-16-3 0.051 0.10 0.39 1.0 U PU 



Cobalt 60 10198-40-0 U 0.12 0.050 U GAM 


Radium 226 13982-63-3 U 0.18 0.10 U GAM 

Radium 228 15262-20-1 U 0.39 0.20 U GAM 




Thorium 228 14274-82-9 U 0.11 U GAM 


Uranium 235 15117-96-1 U 0.30 U GAM 






Cesium 134 13967-70-9 U 0.20 U GAM 


Lab id EBRLNE 






EBER L INE S E R V I C E S / R I C H M O N D 


R604093-01 J11KTO 

DATA SHEET 



Lab sample id R604093-01 Client sample id J11KTO 

Dept sample id 7420-001 Location/Matrix 116-N-3 INVERTEBRATES SOLID 


solids 100.0 Custody/SAF No RC047-311 RC-047 

RESULT 20 ERR MDA RDL QUALI- 

ANALYTE CAS NO pCi/g (COUNT) pCi/g pci/g FIERS TEST 



Lab id EBRLNE 








R604093-11 J11XV1 

DATA SHEET 

SDG 7420 









Client sample id J11KV1 

Location/Matrix 100-D-48:2 OFFAL SOLID 



RESULT 

pCi/g 

2a ERR 

(COUNT) 

MDA 

pCi/g 

RDL 

pCi/g 

QUALI- 

PIERS TEST 


Thorium 228 14274-82-9 0.110 0.33 0.68 1.0 U TH 

Thorium 230 14269-63-7 0.165 0.33 0.42 1.0 U TH 

Thorium 232 TH-232 0 0.11 0.42 1.0 U TH 

Uranium 233/234 U-233/234 0.040 0.080 0.30 1.0 U U 

Uranium 235 15117-96-1 0 0.096 0.37 1.0 U U 

Uranium 238 U-238 0 0.080 0.30 1.0 U U 

Plutonium 238 13981-16-3 -0.084 0.17 0.46 1.0 U PU 



Cobalt 60 10198-40-0 U 0.087 0.050 U GAM 


Radium 226 13982-63-3 U 0.14 0.10 U GAM 

Radium 228 15262-20-1 U 0.32 0.20 U GAM 



Europium 155 ,14391-16-3 U 0.16 0.10 U GAM 

Thorium 228 14274-82-9 U 0.088 U GAM 


Uranium 235 15117-96-1 U 0.23 U GAM 






Cesium 134 13967-70-9 U 0.087 U GAM 


Lab id EBRLNE 






EBE RL INE SERVICES /R ICHMOND 


R604093-12 J11KV2 

DATA SHEET 

SDG 7420 









Client sample id 711KV2 

Location/Matrix 100-D-49:2 OFFAL SOLID 



RESULT 

pCi/g 

2a ERR 

(COUNT) 

MDA 

pCi/g 

RDL 

pci/g 

QUALI- 

FIERS TEST 


Thorium 228 14274-82-9 0.282 0.38 0.63 1.0 U TH 

Thorium 230 14269-63-7 0.141 0.28 0.36, 1.0 U TH 

Thorium 232 TH-232 0 0.094 0.36 1.0 U TH 

Uranium 233/234 U-233/234 0 0.080 0.31 1.0 U U 

Uranium 235 15117-96-1 0.048 0.097 0.37 1.0 U U 

Uranium 238 U-238 0 0.080 0.31 1.0 U U 

Plutonium 238 13961-16-3 0.034 0.14 0.33 1.0 U PU 



Cobalt 60 10198-40-0 U 0.21 0.050 U GAM 


Radium 226 13982-63-3 U 0.22 0.10 U GAM 

Radium 228 15262-20-1 U 0.50 0.20 U GAM 




Thorium 228 14274-82-9 U 0.14 U GAM 


Uranium 235 15117-96-1 U 0.35 U GAM 






Cesium 134 13967-70-9 U 0.14 U GAM 


Lab id EBRLNE 








R604093-13 JIIL21 

DATA SHEET 

SDG 7420 









Client sample id J11L21 

Location/Matrix 116DR1,DR-2/100-D-22 OFL SOLID 



RESULT 

pCi/g 

2a ERR 

(COUNT) 

MDA 

pCi/g 

RDL 

pCi/g 

QUALI- 

FIERS TEST 


Thorium 228 14274-82-9 0.060 0.24 0.46 1.0 U TH 

Thorium 230 14269-63-7 0.180 0.36 0.46 1.0 U TH 

Thorium 232 TH-232 0 0.12 0.46 1.0 U TH 

Uranium 233/234 U-233/234 0 0.055 0.21 1.0 U U 

Uranium 235 15117-96-1 0 0.066 0.25 1.0 U U 

Uranium 238 U-238 0 0.055 0.21 1.0 U U 

Plutonium 238 13981-16-3 0 0.12 0.29 1.0 U PU 


Potassium 40 13966-00-2 3.02 1.4 1.0 GAM 

Cobalt 60 10198-40-0 U 0.099 0.050 U GAM 


Radium 226 13982-63-3 U 0.20 0.10 U GAM 

Radium 228 15262-20-1 U 0.52 0.20 U GAM 




Thorium 228 14274-82-9 U 0.20 U GAM 


Uranium 235 15117-96-1 U 0.36 U GAM 






Cesium 134 13967-70-9 U 0.12 U GAM 


Lab id EBRLNE 






EBERLINE SERVICES/RICHMON D 


R604093-14 J11L23 

D ATA SHEET 



Lab sample id R604093-14 Client sample id J11L23 

Dept sample id 7420-014 Location/Matrix BORROW PIT 23 OFFAL SOLID 


t solids 100.0 Custody/SAF No RC047-330 RC-047 


RESULT 

pCi/g 

2a ERR 

(COUNT) 

MDA 

pci/g 

RDL 

pCi/g 

QUALI- 

FIERS TEST 

Total Strontium SR-RAD 0.406 0.15 0.21 1.0 SR 

Thorium 228 14274-82-9 -0.038 0.15 0.42 1.0 U TH 

Thorium 230 14269-63-7 0 0.15 0.29 1.0 U TH 

Thorium 232 TH-232 -0.037 0.075 0.29 1.0 U TH 

Uranium 233/234 U-233/234 0.054 0.11 0.21 1.0 U U 

Uranium 235 15117-96-1 0 0.065 0.25 1.0 U U 

Uranium 238 U-238 0.081 0.11 0.21 1.0 U U 

Plutonium 238 13981-16-3 0.043 0.086 0.33 1.0 U PU 



Cobalt 60 10198-40-0 U 0.062 0.050 U GAM 


Radium 226 13982-63-3 U 0.13 0.10 U GAM 

Radium 228 15262-20-1 U 0.34 0.20 U GAM 




Thorium 228 14274-82-9 U 0.11 U GAM 


Uranium 235 15117-96-1 U 0.30 U GAM 






Cesium 134 13967-70-9 U 0.088 U GAM 


Lab id EBRLNE 








R604093-15 JllL25 

DATA SHEET 



Lab sample id R604093-15 Client sample id JllL25 

Dept sample id 7420-015 Location/Matrix 600-131 OFFAL SOLID 


% solids 100.0 Custody/SAF No RC047-332 RC-047 


RESULT 

pCi/g 

2a ERR 

(COUNT) 

MDA 

pCi/g 

RDL 

pCi/g 

QUALI- 

FIERS TEST 


Thorium 228 14274-82-9 -0.066 0.13 0.51 1.0 U TH 

Thorium 230 14269-63-7 -0.132 0.13 0.51 1.0 U TH 

Thorium 232 TH-232 0 0.13 0.51 1.0 U TH 

Uranium 233/234 U-233/234 0 0.071 0.27 1.0 U U 

Uranium 235 15117-96-1 0 0.086 0.33 1.0 U U 

Uranium 238 U-238 0.035 0.071 0.27 1.0 U U 

Plutonium 238 13981-16-3 -0.038 0.076 0.29 1.0 U PU 


Potassium 40 13966-00-2 2.64 0.64 0.32 GAM 

Cobalt 60 10198-40-0 U 0.034 0.050 U GAM 


Radium 226 13982-63-3 U 0.060 0.10 U GAM 

Radium 228 15262-20-1 U 0.15 0.20 U GAM 




Thorium 228 14274-82-9 U 0.046 U GAM 


Uranium 235 15117-96-1 U 0.11 U GAM 






Cesium 134 13967-70-9 U 0.039 U GAM 


Lab id EBRLNE 








R604093-16 JllL36 

DATA SHEET 

SDG 7420 






ANALYTR CAS NO 



Client sample id J11L36 

Location/Matrix CENT.PLAT.SHRUB STEP.OFL SOLID 

Collected/Weight 04/03/06 10:15 71.5 4 


RESULT 

pCi/g 

2a ERR 

(COUNT) 

MDA 

pCi/g 

RDL 

pCi/g 

QUALI- 

FIERS TEST 


Thorium 228 14274-82-9 0.100 0.20 0.48 1.0 U TH 

Thorium 230 14269-63-7 0.250 0.30 0.38 1.0 U TH 

Thorium 232 TH-232 0 0.10 0.38 1.0 U TH 

Uranium 233/234 U-233/234 0 0.054 0.21 1.0 U U 

Uranium 235 15117-96-1 0 0.065 0.25 1.0 U U 

Uranium 238 U-238 -0.027 0.054 0.21 1.0 U U 

Plutonium 238 13981-16-3 0 0.085 0.33 1.0 U PU 


Potassium 40 13966-00-2 2.95 0.78 0.34 GAM 

Cobalt 60 10198-40-0 U 0.032 0.050 U GAM 


Radium 226 13982-63-3 U 0.055 0.10 U GAM 

Radium 228 15262-20-1 U 0.13 0.20 U GAM 




Thorium 228 14274-82-9 U 0.090 U GAM 


Uranium 235 15117-96-1 U 0.12 U GAM 






Cesium 134 13967-70-9 U 0.034 U GAM 


Lab id EBRLNE 








Test PU Matrix SOLID Client Hanford 

SDG 7420 METHOD SUMMARY Contract No. 630 

Contact Melissa C. Mannion PLUTONIUM, ISOTOPIC IN SOLIDS Contract SDG K0303 

RESULTS 

ALPHA SPECTROSCOPY 

LAB RAW SUF- Plutonium Plutonium 

CLIENT SAMPLE ID SAMPLE ID TEST FIX PLANCHET 238 239/240 

Preparation batch 7181-066 

J11KK8 R604093-02 7420-002 U U 

J11KL5 R604093-03 7420-003 U U 

Jll KL6 R604093-04 7420-004 U U 

J11KM0 R604093-05 7420-005 U U 

JllKM2 R604093-06 7420-006 U U 

Jll KM3 R604093-07 7420-007 U U 

Jll KM4 R604093-OB 7420-008 U U 

J1lKM5 R604093-09 7420-009 U U 

J11KM6 R604093-10 7420-010 U U 

J11KV1 R604093-11 7420-011 U U 

J11KV2 R604093-12 7420-012 U U 

JIIL21 R604093-13 7420-013 U U 

JIIL23 R604093-14 7420-014 U U 

JlIL25 R604093-15 7420-015 U U 

JlIL36 R604093-16 7420-016 U U 

Method Blank R604093-18 7420-018 U U 

Lab Control Sample 8604093-17 7420-017 Ok Ok 

Duplicate (R604093-06) R604093-19 7420-019 - U - U 

Nominal values and limits from method RDLS (pCi/g) 1.0 1.0 

100&300Area Compnt RCBRA Sediment6Ti 

Lab id EBRLNE 


METHOD SODAfARIES Version Ver 1.0 

Page 1 Form DVD-CMS 





Test PU Matrix SOLID Client Hanford 


Contact Melissa C. Mannion PLUTONIUM, ISOTOPIC IN SOLIDS Contract SDO K0303 

METHOD PERFORMANCE 


LAB RAW SUF- MAX MDA ALIQ PREP DILU- YIELD EFF COUNT FWHM DRIFT DAYS ANAL- 

CLIENT SAMPLE ID SAMPLE ID TEST FIX pci/g g PAC TION k % min keV KeV HELD PREPARED YZED DETECTOR 

Preparation batch 7181-066 2a prep error 5.0 % Reference Lab Notebook 7181 pg. 66 

J11KK8 R604093-02 0.24 0.500 49 172 

J11KL5 R604093-03 0.25 0.500 55 172 

J11KL6 R604093-04 0.20 0.500 58 173 

J11KMO R604093-05 0.26 0.500 56 173 

J11KM2 R604093-06 0.17 0.500 68 173 

J11KM3 R604093-07 0.14 0.500 82 173 

JIIKM4 R604093-08 0.25 0.500 49 173 

JllKM5 R604093-09 0.35 0.500 44 144 

J11KM6 R604093-10 0.39 0.500 '59 103 

J11KV1 R604093-11 0.46 0.500 37 144 

J11KV2 R604093-12 0.33 0.500 45 144 

J111,21 R604093-13 0.29 0.500 61 144 

J111,23 R604093-14 0.33 0.500 48 145 

J11L25 R604093-15 0.29 0.500 60 114 

JlIL36 R604093-16 0.33 0.500 55 114 

Method Blank R604093-18 0.27 0.500 68 114 

Lab Control Sample R604093-17 0.20 0.500 90 114 

Duplicate (R604093-06) R604093-19 0.29 0.500 69 113 

Nominal values and limits from method 1.0 0.500 20-105 100 100 180 

PROCEDURES REFERENCE PUISO_PLATE_AEA 

CP-071 Soil Dissolution, > 1.Og Aliquot, rev 5 

CP-941 Plutonium in Water and Dissolved Samples by 

Extraction Chromatography, rev 3 

CP-008 Heavy Element Electroplating, rev 9 

42 05/17/06 05/17 SS-027 

42 05/17/06 05/17 SS-028 

44 05/17/06 05/17 SS-029 

42 05/17/06 05/17 SS-031 

44 05/17/06 05/17 SS-032 

44 05/17/06 05/17 SS-033 

44 05/17/06 05/17 SS-034 

44 05/17/06 05/17 SS-035 

49 05/17/06 05/22 SS-040 

42 05/17/06 05/17 SS-036 

42 05/17/06 05/17 SS-038 

44 05/17/06 05/17 SS-039 

44 05/17/06 05/17 SS-040 

42 05/17/06 05/17 SS-055 

44 05/17/06 05/17 SS-056 

05/17/06 05/17 SS-058 

05/17/06 05/17 SS-057 

44 05/17/06 05/17 SS-059 

AVERAGES t 2 SO M)A 0.28 3 0.16 

FOR 18 SAMPLES YIELD 58 ; 27 

Lab id EBRLNE 


METHOD SUMMARIES Version Ver 1.0 






Test TH Matrix SOLID Client Hanford 


Contact Melissa C. Manion THORIUM, ISOTOPIC IN SOLIDS Contract BIG K0303 

RESULTS 

LAB RAW SUF- 


CLIENT SAMPLE ID SAMPLE ID TEST FIX PLANCHET Thorium 230 


J11KKB R604093-02 7420-002 U 

J11KL5 R604093-03 7420-003 U 

J11KL6 R604093-04 7420-004 U 

J11KM0 R604093-05 7420-005 U 

JllKM2 R604093-06 7420-006 U 

J111043 R604093-07 7420-007 U 

Jll KM4 R604093-08 7420-008 U 

JIIKMS R604093-09 7420-009 U 

1T11KM6 R604093-10 7420-010 U 

JI1KV1 R604093-11 7420-011 U 

J11KV2 R604093-12 7420-012 U 

JIIL21 R604093-13 7420-013 U 

JIIL23 R604093-14 7420-014 U 

JIIL25 R604093-15 7420-015 U 

J111,36 R604093-16 7420-016 U 

Method Blank R604093-18 7420-018 U 

Lab Control Sample R604093-17 7420-017 ok 

Duplicate (R604093-06) R604093-19 7420-019 - U 

Nominal values and limits from method RDLS (pCi/g) 1.0 

1006300Area Compnt RCBRA Sediment&Ti 

Lab id EBRLNE 






Test TH Matrix SOLID 


SAMPLE DELIVERY DROOP K0303 

SDG 7420 METHOD SUMMARY 

Contact Melissa C. Manion THORIUM, ISOTOPIC IN SOLIDS 





Contract SDG K0303 

LAB RAW SUF- MAX MDA ALIQ PREP DILU-.YIELD EFF COUNT FWHM DRIFT DAYS ANAL- 

CLIENT SAMPLE ID SAMPLE ID TEST FIX pCi/g g PAC TION % It min keV XeV HELD PREPARED YZED DETECTOR 

Preparation batch 7181-066 2a prep error 5.0 } Reference Lab Notebook 7181 pg. 66 

J11KKB 8604093-02 0.66 0.250 50 160 

J11KL5 R604093-03 0.42 0.250 77 160 

J11KL6 R604093-04 0.62 0.250 42 160 

J11KM0 R604093-05 0.56 0.250 51 160 

J11XM2 R604093-06 0.49 0.250 66 160 

J11KM3 R604093-07 0.46 0.250 54 160 

J11KM4 R604093-08 0.54 0.250 56 160 

J1IKM5 R604093-09 0.49 0.250 51 160 

JIIKM6 R604093-10 0.53 0.250 47 161 

J11KV1 R604093-11 0.68 0.250 50 167 

J11XV2 R604093-12 0.63 0.250 57 168 

JIIL21 R604093-13 0.46 0.250 45 168 

JllL23 R604093-14 0.42 0.250 70 168 

JIIL25 R604093-15 0.51 0.250 55 169 

JIIL36 R604093-16 0.48 0.250 65 169 

Method Blank R604093-18 0.84 0.250 36 160 

Lab Control Sample R604093-17 0.43 0.250 59 159 

Duplicate (R604093-06) 8604093-19 0.41 0.250 62 160 

Nominal values and limits from method 1.0 0.250 20-105 150 

PROCEDURES REFERENCE THISO_IE_ PLATE _AEA 

SPP-073 Soil Leaching 10-200 g Aliquot, rev 0 

CP-900 Thorium in Water and Dissolved Solid Samples by 



38 05/13/06 05/13 SS-060 

38 05/13/06 05/13 SS-061 

40 05/13/06 05/13 SS-062 

38 05/13/06 05/13 SS-063 

40 05/13/06 05/13 SS-064 

40 05/13/06 05/13 SS-027 

40 05/13/06 05/13 SS-028 

40 05/13/06 05/13 SS-029 

40 05/13/06 05/13 SS-031 

38 05/13/06 05/13 SS-035 

38 05/13/06 05/13 SS-036 

40 05/13/06 05/13 SS-037 

40 05/13/06 05/13 SS-038 

38 05/13/06 05/13 SS-040 

40 05/13/06 05/13 SS-042 

05/13/06 05116 SS-028 

05/13/06 05/16 SS-027 

43 05/13/06 05/16 SS-029 

180 

AVERAGES } 2 SD MDA 0.54 f 0.23 

POR 18 SAMPLES YIELD 55 3 20 

Lab id EBRLNE 








Test U Matrix SOLID Client Hanford 


Contact Melissa C. Mannion URANIUM, ISOTOPIC IN SOLIDS Contract SDG K0303 

RESULTS 


LAB RAW SUP- 1: Uranium 2: Uranium 3: Uranium RESULT RATIOS M 

CLIENT SAMPLE ID SAMPLE ID TEST FIX PLANCRET 233/234 235 238 1a3 2s 2.3 20 


JllKK8 R604093-02 7420-002 0.423 U 0.597 71 45 0 10 

JllKL5 R604093-03 7420-003 U U U 

J11KL6 R604093-04 7420-004 U U U 

J11KM0 R604093-05 7420-005 U U U 

J11KM2 R604093-06 7420-006 U U U 

J11KM3 R604093-07 7420-007 U U U 

J11KM4 R604093-08 7420-008 U U U 

J11KM5 R604093-09 7420-009 U U U 

J11KM6 R604093-10 '7420-010 U U U 

J11KV1 R604093-11 7420-011 U U U 

JllKV2 R604093-12 7420-012 U U U 

J111,21 R604093-13 7420-013 U U U 

J111,23 R604093-14 7420-014 U U U 

J11L25 R604093-15 7420-015 q U U 

J111,36 R604093-16 7420-016 U U U 

Method Blank R604093-18 7420-018 q U U 

Lab Control Sample R604093-17 7420-017 ok ok ok 

Duplicate (R604093-06) R604093-19 7420-019 - U - U - U 

Nominal Values and limits from method RDLS (pCi/g) 1.0 1.0 1.0 100 4 

1006300Area Compnt RCBRA SedimentETi Averages 71 0 

Lab id EBRLNE 








Test U Matrix SOLID Client Hanford 


Contact Melissa C. Mannion URANIUM, ISOTOPIC IN SOLIDS Contract SDG K0303 


CLIENT SAMPLE ID 

LAB RAW SUF- 

SAMPLE ID TEST FIX 

MAX MDA 

pCi/g 


ALIQ 

g 

PREP DILO- YIELD EFF 

FAC TION % t 

Preparation batch 7181-066 20 prep error 5.0 t Reference Lab Notebook 7181 pg. 66 

COUNT FWHM DRIFT DAYS 

min keV KeV HELD PREPARED 

ANAL- 

YZED DETECTOR 

J11KK8 R604093-02 0.23 0.500 63 145 41 05/15/06 05/16 SS-037 

J11KL5 R604093-03 0.19 0.500 76 145 41 05/15/06 05/16 SS-038 

JllKL6 R604093-04 0.22 0.500 76 145 43 05/15/06 05/16 SS-039 

JllKM0 8604093-05 0.32 0.500 59 146 41 05/15/06 05/16 SS-040 

J11KM2 8604093-06 0.30 0.500 56 146 43 05/15/06 05/16 SS-042 

J11KM3 R604093-07 0.26 0.500 66 138 43 05/15/06 05/16 SS-055 

J111044 R604093-08 0.22 0.500 81 138 43 05/15/06 05/16 SS-056 

J11KM5 R604093-09 0.22 0.500 79 139 43 05/15/06 05/16 SS-057 

J11KM6 R604093-10 0.25 0.500 74 139 43 05/15/06 05/16 SS-058 

J11KV1 R604093-11 0.37 0.500 54 136 41 05/15/06 05/16 SS-059 

J11KV2 R604093-12 0.37 0.500 52 137 41 05/15/06 05/16 SS-060 

JIIL21 R604093-13 0.25 0.500 73 137 43 05/15/06 05/16 SS-061 

JlIL23 R604093-14 0.25 0.500 72 137 43 05/15/06 05/16 SS-062 

JlIL25 R604093-15 0.33 0.500 65 137 41 05/15/06 05/16 SS-063 

Jll L36 R604093-16 0.25 0.500 72 137 43 05/15/06 05/16 SS-064 

Method Blank R604093-18 0.24 0.500 79 137 05/15/06 05/16 SS-066 

Lab Control Sample R604093-17 0.88 0.500 96 137 05/15/06 05/16 SS-065 

Duplicate (R604093-06) R604093-19 0.25 0.500 68 145 44 05/15/06 05/17 SS-042 

Nominal values and limits from method 1.0 0.500 20-105 100 100 180 

PROCEDURES REFERENCE UISO_PLATE AEA 

CP-073 Soil Leaching, 10 - 200 g Aliquot, rev 3 

CP-921 Uranium in Water and Dissolved Samples by 



AVERAGES ; 2 SO MDA 0.30 ; 0.31 

FOR 18 SAMPLES YIELD 70 3 22 

Lab id EBRLNE 








Test SR Matrix SOLID Client Hanford 


Contact Melissa C. Mannion TOTAL STRONTIUM IN SOLIDS Contract SOO K0303 

BETA COUNTING 

RESULTS 

LAB RAW SUF- Total 

CLIENT SAMPLE ID SAMPLE IO TEST FIX PLANCRET Strontium 


JllKK8 R604093-02 7420-002 U 

J11KL5 R604093-03 7420-003 U 

1711KL6 8604093-04 7420-004 U 

J11KM0 R604093-05 7420-005 U 

J11KM2 R604093-06 7420-006 0.505 

J111043 R604093-07 7420-007 U 

J1IKM4 8604093-08 7420-008 U 

1711 RM5 R604093-09 7420-009 U 

J11KM6 R604093-10 7420-010 U 

J11KT0 R604093-01 7420-001 U 

JllKV1 R604093-11 7420-011 U 

J11KV2 R604093-12 7420-012 U 

JIIL21 R604093-13 7420-013 U 

JlIL23 R604093-14 7420-014 0.406 

JIIL25 R604093-15 7420-015 U 

JllL36 R604093-16 7420-016 U 

Method Blank 8604093-18 7420-018 U 

Lab Control Sample 8604093-17 7420-017 ok 

Duplicate (R604093-06) R604093-19 7420-019 ok 

Nominal values and limits from method RDLS (pCi/g) 1.0 


Lab id EBRLNE 








Test SR Matrix SOLID Client Hanford 


Contact Melissa C. Mannion TOTAL STRONTIUM IN SOLIDS Contract SDG K0303 


BETA COUNTING 

LAB RAW SUP- MDA ALIQ PREP DILU- YIELD EFF COUNT FWHM DRIFT DAYS ANAL- 

CLIENT SAMPLE ID SAMPLE ID TEST FIX pCi/g g FAC TION % % in keV KeV HELD PREPARED Y2ED DETECTOR 

Preparation batch 7181-066 2s prep error 10.0 k Reference Lab Notebook 7181 pg. 66 

J11KK8 R604093-02 0.26 1.00 94 100 34 05/09/06 05/09 GRB-227 

J11KL5 R604093-03 0.27 1.00 94 100 34 05109106 05/09 GRB-229 

J11KL6 R604093-04 0.27 1.00 94 100 36 05/09/06 05/09 GRB-204 

J11KMO R604093-05 0.26 1.00 89 100 34 05/09/06 05/09 GRB-222 

J11KM2 R604093-06 0.22 1.00 94 100 36 05/09/06 05/09 GRB-227 




J11XM6 8604093-10 0.27 1.00 93 100 37 05/09/06 05/10 GRB-231 

J11KTO R604093-01 0.59 0.500 95 100 36 05/09/06 05/09 GRB-222 

J11KV1 8604093-11 0.22 1.00 94 100 35 05/09/06 05/10 GRB-220 

J11KV2 R604093-12 0.24 1.00 90 100 35 05/09/06 05/10 GRB-221 

JIIL21 R604093-13 0.22 1.00 92 100 37 05/09/06 05/10 GRB-222 

JIIL23 R604093-14 0.21 1.00 94 100 37 05/09/06 05/10 GRB-231 

JIIL25 R604093-15 0.22 1.00 94 120 35 05/09/06 05/10 GRB-201 

JIIL36 R604093-16 0.21 1.00 90 120 37 05/09/06 05/10 GRB-202 

Method Blank R604093-18 0.32 1.00 94 100 05/09/06 05/09 GRB-226 

Lab Control Sample R604093-17 0.18 1.00 96 100 05/09/06 05/10 GRB-222 

Duplicate (R604093-06) R604093-19 0.22 1.00 95 100 36 05/09/06 05/09 GRB-219 

Nominal values and limits from method 1.0 1.00 30-105 100 180 

PROCEDURES REFERENCE SRTOT_SEP_PRECIP_GPC 

CP-071 Soil Dissolution, > 1.Og Aliquot, rev 5 

CP-383 Strontium in Dissolved Solid of < S.Og Aliquot, 

rev 1 

AVERAGES 3 2 SO MDA 0.26 S 0.17 

FOR 19 SAMPLES YIELD 93 3 4 

Lab id EBRLNE 








Test GAM Matrix SOLID 

SOO 7420 METHOD SUMMARY 

Contact Melissa C. Manion GAMMA SCAN 

RESULTS 

LAB RAN SUF- 

GAMMA SPECTROSCOPY 

CLIENT SAMPLE ID SAMPLE ID TEST FIX PLANCEET Cobalt 60 Cesium 137 


JllKK8 R604093-02 

JllKL5 R604093-03 

J11KL6 R604093-04 

JllKM0 R604093-05 

J11KM2 R604093-06 

Jll KM3 R604093-07 

Jll KM4 R604093-08 

J11KM5 R604093-09 

JllKM6 R604093-10 

J11KV1 R604093-11 

J11KV2 R604093-12 

JIIL21 R604093-13 

JlIL23 R604093-14 

J11L25 R604093-15 

JIIL36 R604093-16 

Method Blank R604093-18 

Lab Control Sample R604093-17 

Duplicate (R604093-06) R604093-19 

Nominal values and limits from method 

100E300Aiea Compnt RCBRA Sediment&Ti 

7420-002 U U 

7420-003 U U 

7420-004 U U 

7420-005 U U 

7420-006 U U 

7420-007 U U 

7420-GOB U U 

7420-009 U U 

7420-010 U U 

7420-011 U U 

7420-012 U U 

7420-013 U U 

7420-014 U U 

7420-015 U U 

7420-016 U U 

7420-018 U U 

7420-017 ok ok 

7420-019 - U - 

RDLS (PCi/g) 0.050 0.10 

U 



Contract SDG K0303 

Lab id EBRLNE 








Test GAM Matrix SOLID Client Hanford 

SIG 7420 METHOD SUMMARY Contract No. 630 

Contact Melissa C. Manion GAMM SCAN Contract SIG K0303 

GAPM SPECTROSCOPY 


LAB RAW SUF- MDA ALIQ PREP DILU- YIELD EFF COUNT FWHM DRIFT DAYS ANAL- 

CLIENT SAMPLE ID SAMPLE ID TEST FIX pCi/g g PAC TION % } min keV KeV HELD PREPARED YZED DETECTOR 

Preparation batch 7181-066 2a prep error 15.0 t Reference Lab Notebook 7181 pg. 66 

J11KK8 R604093-02 24 77.8 354. 14 04/17/06 04/19 JR,02,00 

J11KL5 R604093-03 27 69.6 354 14 04/17/06 04/19 JR, 08, 00 

J11KL6 R604093-04 24 74.5 379 17 04/17/06 04/20 JR,02,00 

J11KM0 R604093-05 20 86.8 405 16 04/17/06 04/21 JR,02,00 

J11KM2 R604093-06 17 88.7 354 16 04/17/06 04/19 JR,05,00 

J11KM3 R604093-07 21 81.0 405 18 04/17/06 04/21 JR, 08, 00 

J11KM4 R604093-08 12 91.5 817 18 04/17/06 04/21 JR,03,00 

J11KM5 R604093-09 15 65.9 829 18 04/17/06 04/21 JR,05,00 

J11KM6 R604093-10 17 69.1 829 1S 04/17/06 04/21 JR, 02, 00 

J11KV1 8604093-11 17 71.2 829 16 04/17/06 04/21 JR,08,00 

J11KV2 R604093-12 27 67.6 425 17 04/17/06 04/22 JR,08,00 

J111,21 R604093-13 25 64.7 413 19 04/17/06 04/22 JR,03,00 

JIIL23 R604093-14 20 71.4 413 19 04/17/06 04/22 JR, 05, 00 

J11L25 R604093-15 8.1 80.8 2455 17 04/17/06 04/22 JR, 03, 00 

J111,36 R604093-16 7.8 71.5 2455 19 04/17/06 04/22 JR,05,00 

Method Blank R604093-18 29 64.0 379 04/17/06 04/20 JR,08,00 

Lab Control Sample 8604093-17 0.16 64.0 353 04/17/06 04/20 JR,03,00 

Duplicate (R604093-06) R604093-19 16 88.7 405 18 04/17/06 04/21 JR, 05, 00 

Nominal values and limits from method 0.050 64.0 100 180 

PROCEDURES REFERENCE GAMMA_GS 

SPP-100 Ge(Li) Preparation for Commercial Samples, rev 7 

AVERAGES t 2 SO MDA 18 f 15 

FOR 18 SAMPLES YIELD f 

Lab id EBRLNE 


METHOD SUM44ARIES Version Ver 1.0 


SUM2UZY DATA SECTION Version 3.06 








The Sample and QC Summary Reports show all samples, including QC 

samples, reported in one Sample Delivery Group (SDG). 

The Sample Summary Report fully identifies client samples and gives the 

corresponding lab sample identification. The QC Summary Report shows at 

the sample level how the lab organized the samples into batches and 

generated QC samples. The Preparation Batch and Method Summary Reports 

show this at the analysis level. 

The following notes apply to these reports: 

• LAB SAMPLE ID is the lab's primary identification for a sample. 

• DEPARTMENT SAMPLE ID is an alternate lab id, for example one 

assigned by a radiochemistry department in a lab. 

• CLIENT SAMPLE ID is the client's primary identification for a 

sample. It includes any sample preparation done by the client 

that is necessary to identify the sample. 

• QC BATCH is a lab assigned code that groups samples to be 

processed and QCed together. These samples should have similar 

matrices. 

QC BATCH is not necessarily the same as SDG, which reflects 

samples received and reported together. 

* All Lab Control Samples, Method Blanks, Duplicates and Matrix 

Spikes are shown that QC any of the samples. Due to possible 

reanalyses, not all results for all these QC samples may be 

relevant to the SDG. The Lab Control Sample, Method Blank, 

Duplicate, Matrix Spike and Method Summary Reports detail these 

relationships. 

Lab id EBRLNE 






EBER L INE SERVI CES / RI CHMOND 





PREPARATION BATCH SUMMARY 

The Preparation Batch Summary Report shows all preparation batches in 

one Sample Delivery Group (SDG) with information necessary to check the 

completeness and consistency of the SDG. 

The following notes apply to this report: 

• The preparation batches are shown in the same order as the 

Method Summary Reports are printed. 

• only analyses of planchets relevant to the SDG are included. 

• Each preparation batch should have at least one Method Blank 

and LCS in it to validate client sample results. 

* The QUALIFIERS shown are all qualifiers other than U, J, B, L 

and H that occur on any analysis in the preparation batch. The 

Method Summary Report has these qualifiers on a per sample 

basis. 

These qualifiers should be reviewed as follows 

X Some data has been manually entered or modified. 

Transcription errors are possible. 

P One or more results are 'preliminary'. The data is not 

ready for final reporting. 

2 There were two or more results for one analyte on one 

planchet imported at one time. The results in DVD may 

not be the same as on the raw data sheets. 

Other lab defined qualifiers may occur. In general, these 

should be addressed in the SDG narrative. 

Lab id EBRLNE 











WORK SUMMARY 

The Work Summary Report shows all samples, including QC samples, and all 

relevant analyses in one Sample Delivery Group (SDG). This report is 

often useful as supporting documentation for an invoice. 


* TEST is a code for the method used to measure associated 

analytes. Results and related information for each analyte 

are on the Data Sheet Report. In special cases, a test code 

used in the summary data section is not the same as in 

associated raw data. In this case, both codes are shown on the 

Work Summary. 

* SUFFIX is the lab's code to distinguish multiple analyses 

(recounts, reworks, reanalyses) of a fraction of the sample. 

The suffix indicates which result is being reported. An empty 

suffix normally identifies the first attempt to analyze the 

sample. 

* The LAB SAMPLE ID, TEST and SUFFIX uniquely identify all 

supporting data for a result. The Method Summary Report for 

each TEST has method performance data, such as yield, for each 

lab sample id and suffix and procedures used in the method. 

* PLANCHET is an alternate lab identifier for work done for one 

test. It, combined with the TEST and SUFFIX, may be the best 

link to raw data. 

* For QC samples, only analyses that directly QC some regular 

sample are shown. The Lab Control Sample, Method Blank, 

Duplicate, Matrix Spike and Method Summary Reports detail these 

relationships. 

* The SAS (Special Analytical Services) Number is a client or lab 

assigned code that reflects special processing for samples, such 

as rapid turn around. Counts of tests done are lists by SAS 

number since it is likely to affect prices. 

Lab id EBRLNE 






EBERLINE SERVI CES / RI C HM O ND 





DATA SHEET 

The Data Sheet Report shows all results and primary supporting 

information for one client sample or Method Blank. This report 

corresponds to both the CLP Inorganics and Organics Data Sheet. 


* TEST is a code for the method used to measure an analyte. If 

the TEST is empty, no data is available; the analyte was not 

analyzed for. 

* The LAB SAMPLE ID and TEST uniquely identify work within the 

Summary Data Section of a Data Package. The Work Summary and 

Method Summary Reports further identify raw data that underlies 

this work. 

The Method Summary Report for each TEST has method performance 

data, such as yield, for each Lab Sample ID and a list of 

procedures used in the method. 

* ERRORs can be labeled TOTAL or COUNT. TOTAL implies a 

preparation (non-counting method) error has been added, as 

square root of sum of squares, to the counting error denoted by 

COUNT. The preparation errors, which may vary by preparation 

batch, are shown on the Method Summary Report. 

* A RESULT can be 'N.R.' (Not Reported). This means the lab did 

this work but chooses not to report it now, possibly because it 

was reported at another time. 

* When reporting a Method Blank, a RESULT can be 'N.A.' (Not 

Applicable). This means there is no reported client sample work 

in the same preparation batch as the Blank's result. This is 

likely to occur when the Method Blank is associated with 

reanalyses of selected work for a few samples in the SDG. 

The following qualifiers are defined by the DVD system: 

U The RESULT is less than the MDA (Minimum Detectable Activity). 

Lab id EBRLNE 



Page 4 

Form DVD-RG 






Contact Melissa C. Mannion G U I D E, C o n t Contract No. 630 


DATA SHEET 

If the MDA is blank, the ERROR is used as the limit. 

J The RESULT is less than the RDL (Required Detection Limit) and 

no U qualifier is assigned. 

B A Method Blank associated with this sample had a result without 

a U flag and, after correcting for possibly different aliquots, 

that result is greater than or equal to the MDA for this sample. 

Normally, B is not assigned if U is. When method blank 

subtraction is shown on this report, B flags are assigned based 

on the unsubtracted values while U's are assigned based on the 

subtracted ones. Both flags can be assigned in this case. 

For each sample result, all Method Blank results in the same 

preparation batch are compared. The Method Summary Report 

documents this and other QC relationships. 

L Some Lab Control Sample that QC's this sample had a low 

recovery. The lab can disable assignment of this qualifier. 

H Similar to 'L' except the recovery was high. 

P The RESULT is 'preliminary'. 

X Some data necessary to compute the RESULT, ERROR or MDA was 

manually entered or modified. 

2 There were two or more results available for this analyte. The 

reported result may not be the same as in the raw data. 

Other qualifiers are lab defined. Definitions should be in the 

SDG narrative. 

The following values are underlined to indicate possible problems: 

* An MDA is underlined if it is bigger than its RDL. 

Lab id EBRLNE 






EBE RLIN E SER V ICES / RICHMOND 





DATA SHEET 

* An ERROR is underlined if the 1.645 sigma counting error is 

bigger than both the MDA and the RESULT, implying that the MDA 

may not be a good estimate of the 'real' minimum detectable 

activity. 

* A negative RESULT is underlined if it is less than the negative 

of its 2 sigma counting ERROR. 

* When reporting a Method Blank, a RESULT is underlined if 

greater than its MDA. If the MDA is blank, the 2 sigma counting 

error is used in the comparison. 

Lab id EBRLNE 






EBERLINE SERVI CES / RI CHMOND 

SANPLB DELIVERY GROUP K0303 




LAB CONTROL SAMPLE 

The Lab Control Sample Report shows all results, recoveries and primary 

supporting information for one Lab Control Sample. 


• All fields in common with the Data Sheet Report have similar 

usage. Refer to its Report Guide for details. 

• An amount ADDED is the lab's value for the actual amount spiked 

into this sample with its ERROR an estimate of the error of this 

amount. 

An amount added is underlined if its ratio to the corresponding 

RDL is outside protocol specified limits. 

* REC (Recovery) is RESULT divided by ADDED expressed as a 

percent. 

* The first, computed limits for the recovery reflect: 

1. The error of RESULT, including that introduced by 

rounding the result prior to printing. 

If the limits are labeled (TOTAL), they include 

preparation error in the result. If labeled (COUNT), 

they do not. 

2. The error of ADDED. 

3. A lab specified, per analyte bias. The bias changes the 

center of the computed limits. 

* The second limits are protocol defined upper and lower QC limits 

for the recovery. 

* The recovery is underlined if it is outside either of these 

ranges. 

Lab id EBRLNE 




SUMKARY DATA SECTION Version 3.06 


EBERLINE SERVI CES /RI CHMOND 





DUPLICATE 

The Duplicate Report shows all results, differences and primary 

supporting information for one Duplicate and associated Original sample. 


* All fields in common with the Data Sheet Report have similar 

usage. This applies both to the Duplicate and Original sample 

data. Refer to the Data Sheet Report Guide for details. 

If the Duplicate has data for a TEST and the lab did not do this 

test to the Original, the Original's RESULTS are underlined. 

* The RPD (Relative Percent Difference) is the absolute value of 

the difference of the RESULTS divided by their average expressed 

as a percent. 

If both RESULTS are less than their MDAs, no RPD is computed and 

a '-' is printed. 

For an analyte, if the lab did work for both samples but has 

data for only one, the MDA from the sample with data is used as 

the other's result in the RPD. 

* The first, computed limit is the sum, as square root of sum of 

squares, of the errors of the results divided by the average 

result as a percent, hence the relative error of the difference 

rather than the error of the relative difference. The errors 

include those introduced by rounding the RESULTS prior to 

printing. 

If this limit is labeled TOT, it includes the preparation error 

in the RESULTS. If labeled CNT, it does not. 

This value reported for this limit is at most 999. 

* The second limit for the RPD is the larger of: 

1. A fixed percentage specified in the protocol. 

Lab id EBRLNE 











DUPLICATE 

2. A protocol factor (typically 2) times the average MDA as 

a percent of the average result. This limit applies 

when the results are close to the MDAs. 

* The RPD is underlined if it is,greater than either limit. 

* If specified by the lab, the second limit column is replaced by 

the Difference Error Ratio (DER), which is the absolute value 

of the difference of the results divided by the quadratic sum of 

their one sigma errors, the same errors as used in the first 

limit. 

Except for differences due to rounding, the DER is the 

same as the RPD divided by the first RPD limit with the 

limit scaled to 1 sigma. 

* The DER is underlined if it is greater than the sigma factor, 

typically 2 or 3, shown in the header for the first RPD limit. 

Lab id EBRLNE 






EBER L INE SERVI CES / RI CHMOND 

SAMPLE DBLIVERY GROUP K0303 




MATRIX SPIKE 

The Matrix Spike Report shows all results, recoveries and primary 

supporting information for one Matrix Spike and associated Original 

sample. 


* All fields in common with the Data Sheet Report have similar 

usage. This applies both to the Spiked and Original sample 

data. Refer to the Data Sheet Report Guide for details. 

If the Spike has data for a TEST and the lab did not do this 

test to the Original, the Original's RESULTS are underlined. 

* An amount ADDED is the lab's value for the actual amount spiked 

into the Spike sample with its ERROR an estimate of the error of 

this amount. 

An amount is underlined if its ratio to the corresponding RDL is 

outside protocol specified limits. 

* REC (Recovery) is the Spike RESULT minus the original RESULT 

divided by ADDED expressed as a percent. 

* The first, computed limits for the recovery reflect: 

1. The errors of the two RESULTs, including those 

introduced by rounding them prior to printing. 

If the limits are labeled (TOTAL), they include 

preparation error in the result. If labeled (COUNT), 

they do not. 

2. The error of ADDED. 

3. A lab specified, per analyte bias. The bias changes the 

center of the computed limits. 

* The second limits are protocol defined upper and lower QC limits 

Lab id EBRLNE 






EBER L INE SER V ICES / RICHMOND 



Contact Melissa C. Mannion G U I D E, C O 11 t Contract No. 630 


for the recovery. 

MATRIX SPIKE 

These limits are left blank if the Original RESULT is more than 

a protocol defined factor (typically 4) times ADDED. This is a 

way of accounting for that when the spike is small compared to 

the amount in the original sample, the recovery is unreliable. 

* The recovery is underlined (out of spec) if it is outside either 

of these ranges. 

Lab id EBRLNE 






EBERLINE SE RV I CES /RI CHMOND 





METHOD SUMMARY 

The Method Summary Report has two tables. One shows up to five results 

measured using one method. The other has performance data for the 

method. There is one report for each TEST, as used on the Data Sheet 

Report. 


* Each table is subdivided into sections, one for each preparation 

batch. A preparation batch is a group of aliquots prepared at 

roughly the same time in one work area of the lab using the same 

method. 

There should be Lab Control Sample and Method Blank results in 

each preparation batch since this close correspondence makes the 

QC meaningful. Depending on lab policy, Duplicates need not 

occur in each batch since they QC sample dependencies such as 

matrix effects. 

* The RAW TEST column shows the test code used in the raw data to 

identify a particular analysis if it is different than the test 

code in the header of the report. This occurs in special cases 

due to method specific details about how the lab labels work. 

The Lab Sample or Planchet ID combined with the (Raw) Test Code 

and Suffix uniquely identify the raw data for each analysis. 

* If a result is less than both its MDA and RDL, it is replaced by 

just 'U' on this report. If it is greater than or equal to the 

RDL but less than the MDA, the result is shown with a 'U' flag. 

The J and X flags are as on the data sheet. 

* Non-U results for Method Blanks are underlined to indicate 

possible contamination of other samples in the preparation 

batch. The Method Blank Report has supporting data. 

* Lab Control Sample and Matrix Spike results are shown as: ok, No 

data, LOW or HIGH, with the last two underlined. 'No data' 

Lab id EBRLNE 




SU14K&RY DATA SECTION Version 3.06 








means no amount ADDED was specified. 'LOW' and 'HIGH' 

correspond to when the recovery is underlined on the Lab Control 

Sample or Matrix .Spike Report. See these reports for supporting 

data. 

* Duplicate sample results are shown as: ok, No data, or OUT, with 

the last two underlined. 'No data' means there was no original 

sample data found for this duplicate. 'OUT' corresponds to when 

the RPD is underlined on the Duplicate Report. See this report 

for supporting data. 

* If the MDA column is labeled 'MAX MDA', there was more than one 

result measured by the reported method and the MDA shown is the 

largest MDA. If not all these results have the same RDL, the 

MAX MDA reflects only those results with RDL equal to the 

smallest one. 

MDAs are underlined if greater than the printed RDL. 

* Aliquots are underlined if less than the nominal value specified 

for the method. 

* Prepareation factors are underlined if greater than the nominal 

value specified for the method. 

* Dilution factors are underlined if greater than the nominal 

value specified for the method. 

* Residues are underlined if outside the range specified for the 

method. Residues are not printed if yields are. 

* Yields, which may be gravimetric, radiometric or some type of 

recovery depending on the method, are underlined if outside the 

range specified for the method. 

* Efficiencies are underlined if outside the range specified for 

the method. Efficiencies are detector and geometry dependent so 

this test is only approximate. 

Lab id EBRLNE 






EBERLINE SE RV ICES/RICHMOND 

SAMPLB DELIVERY GROUP K0303 


Contact Melissa C. Mannion G U I D E, c O n t Contract No. 630 



• Count times are underlined if less than the nominal value 

specified for the method. 

• Resolutions (as FWHM; Full Width at Half Max) are underlined if 

greater than the method specified limit. 

• Tracer drifts are underlined if their absolute values are 

greater than the method specified limit. Tracer drifts are 

not printed if percent moistures are. 

• Days Held are underlined if greater than the holding time 

specified in the protocol. 

• Analysis dates are underlined if before their planchet's 

preparation date or, if a limit is specified, too far after 

it. 

For some methods, ratios as percentages and error estimates for them are 

computed for pairs of results. A ratio column header like 1 1+3' means 

the ratio of the first result column and the third result column. 

Ratios are not computed for Lab Control Sample, Method Blank or 

Matrix Spike results since their matrices are not necessarily 

similar to client samples'. 

The error estimate for a ratio of results from one planchet reflects 

only counting errors since other errors should be correlated. For a 

ratio involving different planchets, if QC limits are computed based on 

total errors, the error for the ratio allows for the preparation errors 

for the planchets. 

The ratio is underlined (out of spec) if the absolute value of its 

difference from the nominal value is greater than its error estimate. 

If no nominal value is specified, this test is not done. 

For Gross Alpha or Gross Beta results, there may be a column showing the 

sum of other Alpha or Beta emitters. This sum includes all relevant 

Lab id EBRLNE 


REPORT GUIDES version Ver 1.0 







Contact Melissa C. Mannion G U I D E, C o n t Contract No. 630 



results in the DVD database, whether reported or not. Results in the 

sum are weighted by a particles/decay value specified by the lab for 

each relevant analyte. Results less than their MDA are not included. 

No sums are computed for Lab Control, Method Blank or Matrix Spike 

samples since their various planchets may not be physically related. 

If a ratio of total isotopic to Gross Alpha or Beta is shown, the error 

for the ratio reflects both the error in the Gross result and the sum, 

as square root of sum of squares, of the errors in the isotopic results. 

For total elemental uranium or thorium results, there may be a column 

showing the total weight computed from associated isotopic results. 

Ignoring results less than their MDAs, this is a weighted sum of the 

isotopic results. The weights depend on the molecular weight and 

half-life of each isotope so as to convert activities (decays) to weight 

(atoms). 

If a ratio of total computed to measured elemental uranium or thorium is 

shown, the error for the ratio reflects the errors in all the 

measurements. 

Lab id EBRLNE 






Washin0on Closure Hatiford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-311 Page J of 1 

Collector 


TN KLINCKN 

project Coordinator 

TILLER, B. JOAN KESSNER 375-4688 KESSNER, 1H Price Code 9N Data Turnaround 

oiect Destenation 

S=vline Loca 

100 

ti on [Ô D 9 /7^.y -\ SAF No. 

& 300 Area Component of the RCBRA Sediment and Ti 116-N-3 INVERTEBRATES ) 3[I J / I0 RC-047 


Field Loebook No. COA Method of Shipment 

^P 6 -02 -SD5- 


Shin Offsite Proverty No. ^/ 7 Bi ll of LadbWAir Bi ll No. 

C BE INESERVIC LIONVILE 19*0330 SEE OSPC 

PO LE HAZARDS/REMARKS 

covi_ 4C 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-259 Page I of 1 

Collector 

Company Contact Telephone No Proiect Coordinator 


JOAN KESSNER 375-4688 KESSNER, IH 

roiect Desdmnsdton 


Sampline Location 

600-1321600-190 OFFAL 

ff^ 2 /)1 2 

/' 3 v3 

7 LIw SAF No. 


Ice Chest No, _ OZ 

Field No. 

Method Shipment 

ELL 95^k 

BESRAS6520 FED 

Ô,S 

(:Fj RUNE SERRVICES LIONVILLE 


POTENTIALRADIOACTlVE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-266 Page 1 of j 

Collector 

TILLER, B. TR KLINCK 

oiect Designation 


Ice Chest NoX C_ _ O r 

Ae Q 7 

Comnanv Contact Telephone No. 

JOAN KESSNER 

Saamline Loca tion 

.199-Fh94 OFFAL 

375-4688 

7 —/74.z /^030-3 (7 yin 

Ft gL-1595 

k No. 

BESRAS6520 


KESSNER, JH price Code 9th Data Turnaround 



EXShipmenl 

FED 

S ' To G 

Offsitc Proverty No. 2 

AO 6 O ^„7 O 

Bi La 

ll 

EBERLPIE LIONVBIR 

of diWA r B ill No. 

SEE OSPC 

POS E HAZARDS/REMARKS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-267 Page I of I 

Collector 

TALLER, B. TR KLINCKMAN 

Protect Desiena tion 


Ice Chest No. 

r 

7îeC ^' .^' t7 d 3^ 

Companv Contact Telephone No. 


Sampling Loca tion 

l lti-N -3 OFFAL /%0,30,3(7^2.D 

Field Loabook No. 

EL-1595 

Ship o Offsite Property No, 

ERLINESERVICES LIONVILLE ('Jf/ J C/ 




Collector 

TR.LER, B. TR KLINCKMAN 



Ice Chest No. n^- D^ 

Field 

EL-15955 

No. 

Sid 

BERLINE SERVVICÊS LIONVI LE 


POTENTIAL RADIOACTIVE 7, Cesium-134, Cesium137, 

Cobalt-60, Epium152, uro Etucpium154, Europi155, um Poassium-40, Radium226, Radi228, um 

RutMnium106, Umsuum235, Umruum2381 

(2) Strontium-89,90 -- Total Sr; Is ot opic Tho rium lThorium2321; Isotopic Uranium lUramum-233234, 

Unnium235, Umniom2381; Isotopic Plutonium 

(3) ICP Metals -6010 (Full List) lAlumnum Antimony, Arsenic, Ba rium Beryl lium BismuW, Boron, 

Cadmium Cakium Chromium Cobalt, Copper, I ron, Lead, Litbium Magnesium Manga ne Relinquished By/Removed Prom Dale,Time 

A LOCKED STORAGE 

& 

se, 

Molybdenum Nickel, Phosphorus. Poussium Se lenium Silicon, Silver, Sodium Strontium Thallium 

Tin, Uranium Vanadium Zi nc 1; Mercury - 7471 - (CV) 

n /^ 

e^lyed ored In , 

/ F 

Date/Ti. 

e- // 1840 

R.hi,iqme Received By/Stored In 

D tte/rinn 

Î OO -^- /SO O ^^^ 

Relinquished B 

Relinquished B 

ved F om 

ermved From 

Date/I'irrc 

DateM. 

Received B /St 

emived B St 

U 

d In 

D 

1Da 

?ime 

0 

D ite/rime 

- 1 

^Y^ 

Relinquished By/Rerroved From Date/Time Received By/Stoed In Datelrime 

Relinquished By/Removed From Date/Tir ne received By/Stored In Date/Time 

LABORATORY 

SECTION 

Received By Tine DateTnx 

FINAL SAMPLE Disposal Meth d Disposed By Date/I'ime 

DISPOSITION 

BHI-EE-011 (08/29/2005) 

Mat ri x 

s_ i 

^sy; 

ode 

si=amre 

o-o,WyQ 

ns=o,ma s+m 

nuDmm Liam: 

r=ruu< 

Vqa d 

[ 

v=v,t,nn 

x=0m.,

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-273 Page 1 of I 

Company Contact Telephone No. Proiect Coordinator 

Collector 


JOAN KESSNER 375-4688 KESSNER, III 

rotect Desienation Sampline Location /,[/ ? Î 

0 Q 


100 & 300 Area Component of the RCBRA Sediment and Ti BORROW PIT 24 OFFAL /' OJ 

7 —1 W RC-047 

Ice Cheat No. Q_QC --,J 

rG e,?. Qs_ 

Field Loe ll ook No. COA Method of Shipment 


Shipped To Offshe Property No. ,l / Bi ll 

of LadiwJAir Bi ll 

No. 

BERLINE SERVICES LIONVILLE ^vIOO ,?j0 SEE OSPC 




Collector 

Comnanv Contact Telephone No. Proiect Coordinator 


JOAN KFSSNER 33775-4688 KESSNER, JH Price Code 9N Data Turnaround 

roiect Desiena tion Stranding Location /a ? IR 

100 & 300 Area Component of the RCBRA Sediment and Ti YAKIMA RIDGE II OFFAL 03(ly /' 

lee Chest No.^^ FieELLo9book 

No. 

7/JÔ 

S -^ZS^ BESRAS6520 


FED EXShioment 

M 

Slq Offsite Propertv No. Bill of Air B il l No 

BER INE SERVICES LIONV B.LE /7 SEE OSPC 




Collector Comaanv Contact Telephone No. Proieel Coordinator 

TILLER, B. TR KLINCKMAN JOAN KESSNER 375-4688 KESSNER, IH pr Price Co de 9N Data Turnaround 

roiect Desih aa tiun Samulin r Loca tion ^L 7°/2J SAF No. 

100 & 300 A rea Component of the RCBRA Sediment and Ti VERNrrA UPRIVER ON SOUTH S JD 6PFAL RC-047 

Ice Chest No.^-7 

Field Loe llook No. COA Method of Stdoment 

4^C - QZ ",7 r' S EL-1595 BESRAS6520 FED EX 

S ' o Offsite Pronerty No. Bi ll of Ladine/Air B ill No. 

BERLINE SERVICES IONVILLE fro6o 33 o SEE OSPC 

POSSIBLE SAMMIMARDSIREMARKS 

POTENTIAL RADIOACTIVE 

Kessner upon receipt. 

sr=wummi 

s WW 

Datelrime Ri=-o cl By/Stored In DateTtne 

(1)Gamma Spec-(Fu1Ws0 l Amencium-341, Antimony-125, Beryllium-7. Cesium- 134, Cesiu137, 

stis lud, 

W=W,or 

Relinquished7eeaved From Date?ime e, ed By/S red I " 

tt 

Dotell'ime 

Cobalt-60, Europium152, Europium154, Europium-155, Potassium-40, Radium 226,Radium228, 

Ruthenium-106, Uranium235. Uraniurrf381 

(2) S trontium-89,90 -- To cel Sr; Iso topic Thonum I Thonum-2321; Is 

a-ei 

Ds=Dwm sa i m 

ot opic Umnium 1Umnium-233234, Dt_D—L,r.d: 

Relinquished B emoved From Date/Ti. eceive By/Stored In Datell'ime 

Uranium-235, U ranium-2381; Isotopic Plu tonium 

(3) ICP Metals - 6010 (Full List) IAluminum Anumony, Arsenic, Banton Beryllium Bismuth, Boron 

Cadmium Calcium Chromium, Cobal t. Copper, Iron, Lead, Lithium Magnesium Manganese, 

Molybdenum Nickel, Phosphorus, Potassium Selenium Silicon Silver, Sodium S 

v w ^ 

tr on ti Re um Thallium 

V,e 

earn m 

xmmR 

li nquished By/Removed From Datelflme Received By/Stored In Date?ime 

Tin, Uranium Va nadium Zinc 1; Memory - 7471 - (CV) 

Relinquished By/Renroved From DateMnic Received By/Stored In Darellime 

LABORATORY 

SECTION 

Received By Title Daterrime 

FINAL SAMPLE Disposal Method Disposed By Da re/Time 

DISPOSITION 

SHI-EE-011 (08/29/2005)


Collector 



100 & 300 Arcs Component of the RCBRA Sediment and Ti 

Ice Chest No. p^ 

Pifc C'0 

S EBE LINE SERV LIONVI.L.E 


POTENTIAL RADIOACTIVE . •sM ât ^ 

7 'e _ 7/-z) /_fva 

R et d / W In DativTime 

flN ra" 

^GV f 

Received By/Stotxd In 

DateTre s 

p rice Code 

9N 

Air Quality L] 

Data Turnaround 

45 Days 

11.7Mat 

rix 

NOTE: Eberine- perform Gamma Spec then tranship bottle to Lionville Labs, if possible maintain 4 C 

cooling. Lionville: perform metals, PCB,PEST,SVOC in this order as sample is available. Contact loan 

Kess ner upon receipt. 

(1) Gamma Spec - (Full Ust) ( Amenaum- 24 1, Andmony-M, Be ryllium7, Cesium 134, Cesium 137, 

Cobalt-60, Europium 152, Europium 154, Europium 155, Potassium40, Radium?26, Radium228. 

RusheNum 106, Urarum235, Uanium238) 

(2) Svondum89,90 - - Total Sr; Isotopic Tho rium ITho rium2321; Isotopic U ra nium (Uanium2331134, 

Uaniom235, Unniu238); m Isotopic Plu tonium 

(3) ICP Metals -6010 (Full Lisp (Aluminum, Antimony, Arsemq Barium, Be ry l lium Bismuth, Boron , 

Cadmium Calcium Chromium. Cobalt, Copper, Iron, Lead, Lithium Mag nesium Manganese. 

Molybdenum Nickel, Phospho rus, Potassium Selenium Si li Relinquished emoved Fro Date?ime 

^ 

Received B St In Da 

6d 1 1 

'1rê 

Vlo 

r „ ,2 

/(ô 

Relinquished y/Removed R6 Date/Time Received B Stored In Da /Time 

Relinquished By/Remrved From Dat con, Silver, Sodium S trontium ThalBum 

Tin, Uranium, Vanadium Zinc It Mercury - 7471 - (CV) 

efr'°e Received By/Stored In DateMme 

Relinquished By/Removed From Date/Time received By/Stored In DateMme 

LABORATORY 

SECTION 

Received By Title Date?true 

FINAL SAMPLE Disposal Method Disposed By Date/Lime 

DISPOSITION 

BHI-EE-011 (08/29/2005) 

s=s,.t 

srrswmmt 

so=sate 

st=sim^ 

w=w"a 

0-0.1 

os=D,^m sd^m 

DL.=onm t ,d, 

T=T °'° 

M-.., 

mL,amd 

v=vsgnwnn 

x=aha

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-277 Page J of J 

ollector_ 

TILLER, B. R KLINCKMAN 

Project Destination 



JOAN KESSNER 

Telephone No. 

375-4688 

Samolina Location r/ y g 

SADDLE MOUNTA IN OFFAL /) xo,3 7w 


KESSNER, JH price Code 9N Data Turnaround 



Ice Chest No. fin _ Oz 

Field No. Method SIdpment 


S ed To Fi h 

LINE SERVIC LIONVB.LE 




Collector 

TIII R, B. TR KLINCKMAN 

Companv Contact 

JOAN KESSNER 

Telephone No. 

375-4688 


KESSNER,JH Rice Code 9th Data Turnaround 

oicet Dedenation 


SamuliLocation 

100-D-48:2 OFFAL 

^,/ 

/ 



Air Quality E] 45 Days 

o 303 7 

Ice Chest No. + nG _ —r0 

Field Logbook No. COA Method of Shipment 

Li F^ S EL-1595 RESRAS6520 FED EX 

SlijMwd,To Offsite Pronertv No. 

RO / E ERLINE RVI LIONVILLE O U (f^(^ 

BIB of Lading/Air Bill No. 

SEE OSPC 

POSSIBLE SAMPLE RAZARDS/REMARES 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-323 jPw J of 1 

Collector 


Protect Designation 


Ice Chest No. 

—IrlleC — z 1 '&-675— 

Shinned To 

B RLINE SERVICE ILIONVILLE 


POTEIVTIALRADIOAC77VE

i 

Washington Closure Hanford ' CHAIN OF CUSTODY/SAMPLYNNALYSIS REQUEST I RC-047-328 Page J of I 

Collector Companv Contact Telephone No. Project Coordinator 

TILLER, B. TR KLINCKMAN JOAN KESSNER 375-4688 KESSNER, IH Price Code 9N Data Turnaround 

roiect Desienation Sampline Location 2Q 

SAF No 

100 & 300 Area Component of the RCBRA Sediment and Ti 116-DR-I,DR-21100-D-22 OFFAL 11 0303 ^^ 


Ice Chest No. yn Field Loehook No. COA Method of Shipment 

Ift C-02 'ro,- EL-1595 BESRAS6520 FED EX 

Ship o Offsite Property No. Bill of Bi ll 

BERLINE SERVICES LIONVILLE 


/O 

f7 (O6) 

atAir 

SEE OSPC 


Washington Closure Hanford ` 'CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-330 INge " 

1 of 

Collector 

Company Contact Tele rthane No. Project Coordinator 


JOAN KESSNER 375-4688 KESSNER, lH 

!^0 303 7Ì 

Pro j ect Designa tion Samp ling Loca tion 


100 & 300 Area Component of the RCBRA Sediment and Ti BURROW PIT 23 OFFAL 2D 


Ice Chest No. . 

/Z^C e^'.2 '-5"D sj 



Price Code 9N Data Ttt 

Air Quality q 

S Offsite Property No. Bill of Lactim Av BBI No. 

EBERLWESERVICES LIONVILLE /T SEE - 



. 

pa 

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALI YSIS REQUEST RC-047-332 ge L of L 

Collector 


Project Designation 


Com oanv Contact Telephone No. 


Sampline Location `' 

600-131 OFFAL IrC 3 - D-3 71.zo 


KESSNER, JH Price Code 9N Data Turnaround 

SAY No. 


Ice Chest No. Ft dpment 

Method St 

0,2 r^ 0 OS 

EL- 1595 

No. 

BCESRAS6520 


45 Days 

Shi ed To /L 

Of isite Property No. n / ^J 2 g 

Bill#JAir pp 

Bill No. 

'INE SERVIC /LIONVILLE // OIpV 3r7 v 

SEE OSPC 

_ 



Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REOUEST RC-047-343 Page J of 1 

Collector Comi)anv Contact Telephone No. Proiecl Coordinator 

TILLER, B. iH KLINCKMAN JOAN KESSNER 375-4688 KESSNER, JH 

roiect Desienation SampBne Loca tion A030 

100 & 300 Area Component of the RCBRA Sediment and Ti CENTRAL PLATEAU SHRUB STEPPE OFFAL 


Ice Chest No. Field Loebook No. COA Method of Shipment 

are, —aZ^,JO ,J EL-1595 BESRAS6520 FED EX 

Shi Offsite Properly No , ,l a 

EBERLP]E SERVICES LIONVR.LE 

POSSIBLE LE HAZARDS/REMARKS 


iIL7 

I-lien- 

tC, Il ri t"T-u ^`y 

RicHM6NII. LA I-A'aaRA-ra RY 

SAMPLE RECEFT CHECKL:S7 

Gity I" 'CP ^^rv^ S3^ "" 

u e Sit 2, , "-7,271 Z73 -7 r 274 >--7S z76 

No ^'^^ / 277 , 3Zy r 313 1 hzB 1 33 a 1332 

GareTime received fLIO^° 

I(^^^^Gor 

Gorrainer 1. â . N g C ^^ Z ^"" !;epunsted79 (Days) P.O. Received Yes [ J No [ 

1 

q 

^. 

E_ 

7 . 

e 

g . 

1D. 

11. 

73. 

t3. 

14. 

15. 

INSP°_C I-ION 

CLlstony seals on shippin g container Inract' Yes NO( j N1 I'tj • ) 

/ gstnty seats on srnoptno comarner rated & sinned" Y es j No j j IQ /F. j 

Gusmay seats on sample conramers rl4aCt? Yes 

/ j WO j j iv/,=. 

CUMDay seats on sample comamen; raced & stone d? Yes J No j j N//- j 

Packing matenal is -. r /Wet ( 1 Li ^ yj 

Number or samples in snipping ccmarner. Sample MET x qj* 1 n-- gOUD 

Number of comamers per sam ple (Or see Go-- 

L-^— 

Samples are In correct cor Amer Yes jV j No j j 

Paperwork, agrees with samotes? Yes ^< j No ( j 

Samples nav e -. i ape j j Hazard tabets j-) Pad tabets j ) Approonate sample iaoeis'-'4' j 

Samptes are -. In 000d condition (A Leaking [ j BrOKen Gomamer j j Missing [ j 

Samptes are. Preserved j J Not p reserved j j pH Pr°SanratlVE 

Describe any anoma lies. 

Was P.M. notified of any anomattes^ Yes ( j No j J Data 

1 . 

tnspecred by Dare: Q ^Y 7rm:: 7 ' 

Cusmmer I I 

Sample NO. 

Ism 

I I Lusromer Samoee I f I 

mRrm Wipe No. rpm f mRlnr mree 

I I I I I 

I I ^ I I I' 

I I I I 

I I I I I I 

I I I f I I 

i I i I I I I 

I 

ion Chamber Ser. No Calibaion dal 

Ainna McTer Ser. No. Calibnmon cal 

Bem/Gamma Mazer Ser, No. Cajibznnn raL. 

Form 5 P-01. , D1-_ Oz 

j 

I 

over55 yeas D; Duajjry nucjearsermces" 

t

Joan Kessner 

WC-Hanford 

3190 Washington Way 

MSIN H9-03 


Subject: Analytical Data Package 


Enclosed are the hard copy analytical repo rts for the batch number/fraction indicated 

(marked X) in the following table: 

LvLI Batch .f.. j 0604L750 

................ DG..# ...............................-.K0303_.... 

Date ..... Received 1 4/12/06 

. . . . . ... . . . . . . . . . .... - . . -. 

.. .. ............. .. 

Samples.............................. .......... ....^.5........... 

. 

. . . . . . . . . . . . . . . . . . . . . . . . . . . Mat\nx . . . . .. . . . . . . . .. . . . _ . . . . . . . . . . . . . Other Solid 

Volatiles ..................................................................... 

Semivolatiles I 

PAH 

Herbicides 

........... . ... . . . . . . ... . . . . . . . ........... I. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 

Metals i X 

The electronic data deliverable (EDD) will be emailed sho rtly. If you have any 

qqestions, please don't hesitate to contact me at (610) 280-3012. 

cerely, 

iville L Incorporated 

Orlette S. Johnson 

Project Manager 

r:\group\pm\orle tte\tnu-hanford\data\b_ltrs.doc 

208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-3000 • Fax (610) 280-3041

DATE RECEIVED: 04/12/06 

CLIENT ID LVL # 

J11KR2 Oil 

LAB QC: 

PBLKGG MBl 

PBLKGG MB1 BS 

^ G4 

ca ^^`' 2C 

Lionville Laboratory, Inc. e Nt.: 

PEST/PCB ANALYTICAL DATA PACKAGE FOR 

TNUHANFORD RC-047 K0303 \4cx 

LVL LOT # :0 2 WVS6 

r ^ 

MTX PREP # COLLECTION EXTR/PREP ANALYSIS 

SO 06LE0112 04/03/06 04/23/06 05/07/06 

S 06LE0312 N/A 04/23/06 05/03/06 

S 06LE0312 N/A 04/23/06 05/03/06 

tll 

000000001 

N


Client: TNU-HANFORD RC-047 W.O. #: 11343-606-001-9999-00 

LVL #: 0604L750 Date Received: 04-12-2006 


CHLORINATED PESTICIDES 

One (1) solid samples was collected on 04-03-2006. 

The sample and it's associated QC samples were extracted on 04-23-2006 and analyzed according 

to Lionville Laboratory SOPS based on SW846, 3rd Edition procedures on 05-03,07-2006. The 

extraction procedure was based on method 3540C and the extracts were analyzed based on method 

8081. All soil samples are reported on a dry weight base unless requested by the client, required by 

the method or noted otherwise. 



1. The sample was analyzed within required holding time. 

2. The sample was extracted 20 days outside of recommended hold time. A copy of the 

Sample Discrepancy Report has been enclosed. 

The sample and it's associated QC samples received Copper-Sulfur cleanups according to 

Lionville Laboratory SOPS based on SW846 methods 3660A respectively. 


Two (2) of six (6) surrogate recoveries were outside acceptance criteria. A copy of the 


6. The blank spike recoveries were within acceptance criteria. 

7. Matrix spike analyses are associated with LvLi lot 0604L748. 

8. The results for soil samples were reported on a wet-weight basis. 

9. The sample 011 required a 4-fold instrument dilutions due to matrix. Reporting limits have 

been adjusted to reflect the necessary dilutions. 


The results presented in this report relate only to the analytical testing and wnditiona of the samples at receipt mid dining storage. All pages of this report are integral pans of 

the analytical data. Therefore, flus report should only be reproduced in its entirety of 42 7 pages. 


MGMG88Z

11. The continuing calibration standards analyzed prior to sample extracts were within 

acceptance criteria. 




13. I certify that this sample data package is in compliance with SOW requirements, both 




Laboratory Manager 


Idmtr:\VoupWata\pest\mu ha,ifotd\0604-750.pst 

vLl 

,-511(10P 

Date

Lionville Laboratory Sample Discrepancy Repo rt (SDR) SDR#: 6YGC. 1447 

Initiator. Batch: arm. N-»âParameter. 

Date: c Samples.. ^J Matrix: 

Client: gW Prep Batch: 

^^ 


a. CDC Discrepancy _ Tech Profile Er ror Client RequestSampler E rror on C-O-C 

Transcription Error _ Wrong Test Code _ Other 


_ Missing Sample/Extract _ Container B roken — Wrong Sample Pulled _ Label ID's Illegible 

Hold Time Exceeded Insufficient Sample _ Preservation Wrong _ Received Past Hold 


Note": Vwffled by Rmg-ln] or [Prep Grout) (drde) ... slgnaturerdate: 

c. Problem (Include all relevant speci fic raspdata if necessary) 


^(4p 

3. Discussion and Proposed Action Other Description: 

_ R 

_ En ti re Batch 


_ Re-leach 

_ Re-extract 

_ Re-digest 

_ Revise EDD 



4. Project Manager Instructions ... slpnatwddate: 

_ Concur with P roposed Ac tion 

_ Disagree wi th Proposed Action; See Instruc ti on 

_ In clude in Case Narrative 


Date/Person 

_ Add 

Cancel 

cet.7 ^(s+-^- CY -fie 4--- F-N-r-..ô^^ 

5. Final Action... algnaturardate: Other Explanation: 

Verified re-[logJ[IeaehJ[extractJ[dig ysr5 (d te) 

7.X ad In Case Narrathre 


Elect ro nic COC Revised 


When Final Ac ti on has been recorded, forward original to QA Specialist for distribution and filing. 

Route Distribution of Completed SDR Route Distribu ti on of Completed SDR 

X Initiator _ Metals: Beegle 

X Lab General Manager. M. Taylor _ Inorganic: Perrone 

X P roject Mgr: Stone/Johnson _ _ _ GC/LC: IGger 

Data Management: Stilwell _ MS: Rychlak/Daley 

_ Sample P rep: Beeglel4ger _ _ Log-in: Per ry 

_ _Admin: 


OA-1 05-A-0805 

A

VLY=LM=1W 

DATA OUALIF'IERS 



sample (not the method detection ]unit) is reported with the U (e.g., I Op. 

J = Indicates an estimated value. This flag is used in cases where a target analyte is detected at a level 

less than the lower quantification level.. If the limit of quantification is 10 ug/L and a concentration 

of 3 ug/L is calculated, it is reported as 33. 

B = This flag is used when the analyte is found in the associated blank as well as in the sample. It 

indicates possible/probable blank comemination. 

E 


Indicates that the compound was detected beyond the calibration range and was subsequently 

analyzed at a dilution. 

1 = Indicates an interference on one analytical column only. Result is reported from remaining analytical 

column. 

ABBREVIATIONS 

BS = Indicates blank sprite in which reagent grade water is spiked with the CLP matrix spiking solutions 

and carried through all the steps in the method. Spike recoveries are reported. 


MS = Indicates matrix spike. 

MSD = 

Indicates matrix spike duplicate. 

DL = indicates that recoveries wen not obtained because the extract had to be diluted for analysis. 


DF 

Dilution Factor. 

NR Not Required. 

NS = Not Spiked. 

SP Indicates Spiked Compound. 

P = This flag is used for an PESTTCIDE/PCB target analyte when there is greater than 25% 

difference for detected concentrations between the two GC columns (see Form X). The 

Iowa of the two values is reported on Form I and flagged with a'P'. 

D Ibis flag identifies all compounds identified in an analysis at a secondary dilution factor. 

C This flag applies to a compound that has been confirmed by GOMS. 

NPM = No patient match for mull-component target analytes. 

000000005

.....,.. +i.a ua Vlaw+:y, XK&C. 


RFW Batch Number: 0604L750 Client, TNUHANPORD RC-047 K0303 Work Order: 11343606001 Page: 1 

Cust ID: J11KR2 PBLKGG PBLKGG BS 

Sample RFW#: 011 06LE0312 -NB1 06LE0312-NB1 

Information Matrix: SOLID SOIL SOIL 

D.F.: 4.00 1.00 1.00 

Units: UG/KG UG/KG UG/KG 

Surrogate: Tetrachloro-m-xylene 177 * t 106 t 117 

Decachlorobiphenyl 173 * t 88 % 96 t 

____'________________________________________ fl=====__=====f1=====__===== f1=====__=====f1=====__=====f1=====___====£1 

Alpha-BHC 40 U 0.33 U 100 

gamma-BHC (Lindane) 40 U 0.33 U 97 t 

Beta-BHC 40 U 0.33 U 100 t 

Heptachlor 40 U 0.33 U 92 t 

Delta-BHC 40 U 0.33 U 89 t 

Aldrin 40 U 0.33 U 78 % 

Heptachlor epoxide 40 U 0.33 U 90 

gamma-Chlordane 40 U 0.33 U 90 % 

Endosulfan I 40 U 0.33 U 90 % 

alpha-Chlordane 220 .I 0.33 U 89 t 

4,4'-DDE 40 U 0.33 U 92 % 

Dieldrin 40 U 0.33 U 92 % 

Endrin 40 U 0.33 U 96 % 

4,4'-DDD 40 U 0.33 U 96 t 

Endosulfan II 40 U 0.33 U 89 % 

4,4'-DDT 40 U 0.33 U 87 % 

Endrin aldehyde 40 U 0.33 U 85 % 

Endosulfan sulfate 40 U 0.33 U 86 % 

Methoxychlor 40 U 0.33 U 90 t 

Endrin ketone 40 U 0.33 U 87 % 

Toxaphene 400 U 3.3 U 3.3 U 

U= Analyzed, not detected. J= Present below detection limit. B= Present in blank. NR= Not reported. NS= Not spiked. 

%= Percent recovery. D= Diluted out. I= Interference. NA= Not Applicable. *= Outside of EPA CLP QC 

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Collector TR KLINCKMAN -- Conaamr Contact Telephone No. Proiect Coordinator 

TRIER, B. JOAN KFSSNER 375-4688 KESSNER, JH 

Protect Deehpation Samo [iae Location SAF No- 

[DO & 300 Area Component of the RCBRA Sediment and Ti 100-D482 INVERTEBRATES RC-047 

, 

Price Code 9N 

Air Quality L] 

pain Turnarow^' 

45 Days co 

Ice Chat No - 0a 7 Field Leabook No. COA Method of Shinuuut 

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POSSIBLESAMCLEHAZA BKS 

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ce Chest No, r ev -- 

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POSSIBLE SAMPLE HAZSRDVRERAM 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047.311 a c °( —I 

Collector 

Comoaay ContactTdeohone No. Proicet Coordinator 

TTLIL+R B. TR KLINCKMAN 

JOAN KESSNER 3754688 KESSNER, JH Price Code yr( 

Data Turnaround 

3 Days 

project Designation Samollae Location SAF No. 

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fee Cheat N%g // Field I"book No. COA - Method of Shiomcnt 

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D 

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Bi ll EBFRIJt4E SERVICES ONVR.iB 

of Ladine/Air Bill No. 

SEE OSPC 

POSSIBLE SAMPLE HAZARDS/RFMAM --- __ -- 

t 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-315 t'a ` L u. 1 

°!lector KLINCKMAN Company Contact Telephone No. Proiect Coordinator 

TIU,FR, B. JOAN KESSNER 375-4688 KESSNER. JH 

Oxl:s'rprnuround 

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roleet Deatamtion Sampling Lo 

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O 

ca tion SAF No. 

100 A 300 Area Component of the RCBRA Sediment and Ti 1607-1)2:1 INWRTEBRATPS RC-047 l9 1 

Ice Chat No. Field luabook No. COA Method of Shipment (9 

^^C mil — 07 EG1595 BESRAS6520 FED EX m 

Skipped To Olraile Property Na ^/ 

' 

Bi ll 

EBERLINESERVICE3 ONVELE ^G!%O.^3r 

of Ladine/Air Bt tl No. 

SEE OSPC 

POSSIBLE SAMPLE HAZARDS/REMAR KS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-317 Pna I or J 

Ilectar 

IR KLINCKMAN Commnr Contact T elenhem No. Proiect Coordinator 

TILLER, B. JOAN KESSNER 375-4688 KESSNER, M 

Price Code 9N Data TornarumtdM 

Iect Designation S=WRM LonUOn SAF No. 

Air Quality C, 

45 Days m 

100 A 300 A Compenl of the RCBRA Sedinte at an rea oo d Ti BORROW PIT 24 INVERTEBRATES RC-047 9 

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1595 BFSRAS652A FED EX m 

C't^.2' Q EL- 

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Bi ll 

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SEE OSPC 

POSSIBLE SAMPLE HAZARDS/REMARKS — -. 

PO7ENTIALRADIOACTIVE


ector TR KUNUMAN Company Contact Telephone No. Protect Coordinator 

MIER, B. JOAN KESSNER 375-4688 KESSNER, JH 

1',Itie 

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11JB 

Olfoite Prel ertr No. 

^(O /, 

B Bill No. 

SEE OS^dAir 

m 

POSSIBLE SAMPLE HAZARDS/REMARKS t/ 

-- -- --- — — — 

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usaueueuaa^- ^^1 

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CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-31 9robe i 

! 

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! 

Collector 

TILLER, B. -o:. WMAN 

- 

Compsav Contact 

JOAN KESSNER 

Telephone No. 

375-4688 


KESSNER, )H Price Cudc 9N Data Turuarowid^ 

rolect Deslenalbn SamnBM Locadatl SAF No. 

45 

Air Quality L] Days m 

100 & 300 Arcs Component of she RCBRA Sedhnent and Ti VERNITA UPR IVER ON SOUTH SIDE INVERTEBRATES RC-047 0 I 

Ice Chest No. 

neld Laebook No. COA Method of Shipment m 

It ^G-^l — ELI1595 BBSRAS6520 FED ER m 

Sldoped To Ottalle Property No. Bi ll of LadhWAir Bill No. m 

EBERLNE SERVICES LIONVIIE Ao6 d . SEE OSPC 

POSSIBLE SAMPLE AZ HARDS/R®lARKS 

POT&MALRADIOACME .

Washinxton Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-320 1 'aµ ! n ! 

ôneclor THRINCKMAN '- V- Company Centael Teleutione No. Proiect Coordinator 

T61ER, B. JOAN KESSNER 375-4688 KESSNER, IH Price Code Data Turnaround D 

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100& 30D Area Component of the RCBRA Sediment and Ti McGEE RANCH INVERTEBRA TES 


G 

ice C6eet No Field Lpakook No. COA Method of Shimncot 

m 

07 EL- 1595 BESRAS6520 FED EX m 

Shipped To Ofbik Properly No. /1O6 Q 2s-/ Bill of LadindAir Bill No- 

EBERLESERVIC IN 

LIONVILIE ' .7 ^" SEE OSPC 

POSSIBLE SAMPLE IiA RSS -- .-- --- --- 

PO7ENTIALRADJOACJ7VE

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REOUFST RC-047-321 

° TR KLIflf:KMAN Company Contact Telephone No. Proiect Courduwtelr 

TILLER, B. JOAN KE.SSNER' 375.4688 KESSNER, Ili Ptice Code 9N 

Oatu'1'un::n-mtudp. 

Proleet Dedamillon Samodua Location SAF No. 

Air Qttality q YJ Days 

100 & 300 Am Compoment of the RCBRA Sediment and Ti SADDLE MOUNTA 

0 ' 

IN INVERTEBRATES RC-047 m 

Ice Cheat No, Field Loahuok No. COA Method of Shipment 

0 7 EI. 1595 BESRAS6520 FED EX 

Shipped To, 

EBERLINESERVIC ONVRIE 

Othite Property No. 

Ao60 3tS 

Bi ll of Ladine/Air Bill No. 

SEE OSPC 


POTENTJAL RAD/OAC77VE

Washinoton Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-31 a 1'a e 

olleetar . CommarContact 

T eleohone 

TR KLINCKMAN 

No. Proiect Coordinator 

TILLER, B. ^ 

JOAN KESSNER 375-4668 KESSNER, JH Yricc Code t DaL•r 7lornaruuud 

00 

. rolectIlleslumitton SamoBne LOUfdoB 160;9jf^^ SAF No. 

t00&300Arn Con Component of the RCBRA Sediment and Ti 74VERTEBRATM 

m 

RC-047 19 

)N 

Air Quality 0 4 5 Days 

let Chest No. 

Fld No, COA Method of Shioneat W 

, ! Re e2 ` ff'O 7 EL- 1595 BESRAS6520 FED EX m 

S Eyed To SERVICES ONVBllr 

Offsite Ptnoerts No. NO^ ^^ O 

f1 

BiB of Ladioa/Air Bill No. 

SEEOSPC 

m 

POSSIBLE SAMPLE HAZARD.S/AEMAR ICS 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-303 ?-1e'c = n( 

Collector - Comoany Contact Teleohone No. Protect Coordinator 

TRIER, B. XM Xi wrKMAN JOAN KESSNER 375-4688 KESSNER, JH Price Code 9N Win Turnaround 

olecl Desfanaaon Saaaoli=Lo ti= SAF No. Alr Quality 45 Days m 

100 & 300 Am Component of the RCBRA Sediment and Ti 6M132/WD-190 INVERTEBRATES RC-(M7 

O 

0 

Ice Chat No. n Field Loahook No. COA Method of SI»ometst m 

7 641595 BESRAS6520 FED EX m 

Shinned To 

EBERLINESERVICPS uONVn.in 

POSSIBLE SAMPLE HAZARWRF.MARKS 

I 

Offaite Pronerp No '/ 

603^^ 

BID of Ladin2/Air BRI No. 

SEE OSPC 

POTEWML RADIOACTIVE

-i 

Washington C osure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-345 1•:,g,. w 

Collector 

TILLER, B. TR KLIKKKAN 

Commany Contact Telephone No. 

JOAN KFSSNER 375-4688 

Proiecl Coordinator 

KESSNER, JH Price Code 9N Data Turnaround 

m 

Air Quality I,_f 4^ B2 

y' 

i (V 

9 

Protect Deshmation Sampling Lo cation SAF No. 

LBO & 300 Area Component of the RCBRA Sedim cat and Ti CENTRAL PLATEAU SHRUB STEPPE INVERTEBRATES RC-047 6 

Ice Chtat No. // -+. 

y07 

Fleld Logbook No. COA Method FEDEXSItioment 

EL- 1595 BESRAS6520 

Shipped To 

EBERLINE SERVICESONVUlE 

ORgite ProDWO No. 

060 

Bill of Ladinp/Air Bi ll No. 

SEE OSPC 

POSSIBLE SAMPLE HAZARDS/REMARKS ------ - _. --. - - - - 

POTENTIALRADIOACTJVE

s - 

Washington Closure Hanford CHAIN OF CUST01Y/SAMPLE ANALYSIS REQUEST RC-047-342 ,'ng i n 

ector 

Coany mp Cemtact Telephone No. 


TR KLINCKMAN 

JOAN 

MCC Cade 9N a)ata'1'unm ruwuh 

TILLER, B. KESSNER 375-4688 KESSNER, JH 

T^ N 

ieel Deslenalion Sampling Location SAF No. 

45 D"-Ys 

Air Quality 

m '. 

100 & 300 Area Compm cut of the RCBRA Sediment and n 600-131 INVERTEBRATES RC-047 q 

m 


/y .QC-Ol 0 

Field Loebook No. COA Method of Sldument 

-7 EL-1595 BESRAS6520 FED EX m 

m 

Shioced To Onsite Property No. ^y Bill of Ladiae/Air Bi ll No. 

EBERLINE SERVICES VB1E SEE OSPC 

POSSIBLE SAMPLE HAMAIJ) /REMARES -- -- 


Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047.340 l'agc ! ar ! 

Collector 

TR KUNCKMAN 

Company Contact Telephone No. Proicet Coordinator 

TILLER, B. - JOAN KPSSNER 375-4688 Price Code yN Data Turrarotuw,N 

KESSNER, IH 

a 

Protect et IJel[mtlon 

SampWU lg Load" tl 


Days 

Ail• Quality ^_l`'3"m 

100 A 300 Arm Coripaoenl of the RCBRA Sediment and Ti BORROW PIT 23 INVERTEBRATES RC-047 m 

Ice Chat No. 

ArieG ^Q,7 - O' 

Field Loeb" No. 

1141595 

COA Method of Shipment m 

BESRAS6520 FED EX 

m— 

m 

Shipped To Offaita Property No. .2 q Bill of Ladine/Air Bill No. 

EBERLINE SERVICESell SEEOSPC 

POSSIBLE SAMPLE HAZA RKS 


Washington Closu re Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047.335 ;Ace ! u 

Collector 

- Comanv Contact Telephone No. Proiect Coordinator 

T11.1-11R, B. AR JOAN KESSNER 375-4688 KESSNER, JH Price Code 9N llxta -furn:u•owsd 

M 

Protect Desienat)on Sanmllne Location SAF No. 

45 D 

Air Quality q 

a V S N 

9 

100 A 300 Ara Compoteot of the RCBRA Sedisneat and Ti 116-DR-i, DR-Tl1lK1-0.22 INVP.RTEBRATES RC-047 m 

Ice Chat No. Xwe — 

Fi el d Umbook No. COA Method of Shioment m 

EI- 1395 BESRAS6520 FED EX m 

Shipped To O/fdhe Property No. nom/ Bill of Ladine/Air Bi ll No. m 

EBERLINE SERVICES llONVn 7F " C23^ SEE OSPC 

POSSIBLE SAMPLE HAZA RKS 


1_ Samples Hand Delivered orhippe 


SAMTLE RECEIPT CHECKLIST (SRC) 

CLIENT:-T ISU VA4r-,Coe- P Date: 4- la• d- 

P chase Order/ Project# / R C.O+-4'7 

CAF#' SOW#/Release#: 

LvLI Batch 9 : h ` 1 —7 ^ Sample Custodian: 

2. Custody seals on coole rs or shipping 


l 1 t n f Y^L I GJIJ 

NOTE: EXPLAIN ALL DISCREPANCIES / 

3. Outside of coolers or shipping containers are 





5. Samples receiver ambient? 

6. Custody seals on sample containers intact, 




9. All samples on coc received? AL samples 




12. Samples received within bold times? 


a-M-B 



client? 


Po licy? (Identify all bottles cot within 

policy. See reverse side for policy) 


discrepancies? nameldate (or samples 


^Lr 

Airbili# —IgD3 169-11 -)- 1-q 

G(Yes ONO O No Seals Comments 

VYes ONO 

IXYes O No 

Temp ^.8 OC Cooler # F—K4 'Oa • 4




1234ss) 

^ N ti^ N 

^Pyw 

DATE RECEIVED: 04/12/06 LVL LOT # :0604L Ôl 816 


J11KV5 


SILVER, TOTAL 001 REP SO 06L0284 04 /03/06 05/09/06 05/09/06 


ALUMINUM, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/12/06 


ARSENIC, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06 


BORON, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 


BARIUM, TOTAL 001 REP SO 06L0284 04 /03/06 05/09/06 05/09/06 


BERYLLIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 


BISMUTH, TOTAL REP 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 


CALCIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 


CADMIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 


COBALT, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06 

CHROMIUM, TOTAL _ 001 SO 06LO284 04/03/06 05/09/06 05/09/06 

CHROMIUM, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06 


COPPER, TOTAL 001 REP SO 06L0264 04/03/06 05/09/06 05/09/06 

IRON, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/09/06 

IRON, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 


MERCURY, TOTAL 001 REP SO 0600080 04 /03/06 04/27/06 04/27/06 

MERCURY, TOTAL 001 MS SO 0600080 04/03/06 04/27/06 04/27/06 


POTASSIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 

LITHIUM, TOTAL 001 SO 06L0284 04/03/06 05/09/06 .05/09/06 

LITHIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 


MAGNESIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 

000000001






MANGANESE,.TOTAL 001 SO 06LO284 04/03/06 05/09/06 - 05/09/06 

MANGANESE, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 


MOLYBDENUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 


SODIUM, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06 


NICKEL, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06 


PHOSPHORUS, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/12/06 


LEAD, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 


ANTIMONY, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06 


SELENIUM, TOTAL 001 REP SO 06-LO284 04/03/06 05/09/06 05/09/06 


SILICON, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06 

TIN, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06 

TIN, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06 


STRONTIUM, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06 


THALLIUM, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06. 


URANIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 


VANADIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 

ZINC, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/09/06 

ZINC, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06 

ZIRCONIUM, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/12/06 

ZIRCONIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/12/06 

J11KV6 


SILVER, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06 


000000002






ALUMINUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/12/06 


ARSENIC, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06 


BORON, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06 


BARIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06 


BERYLLIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06 


BISMUTH, TOTAL SPIKE 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 


CALCIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 


CADMIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06 


COBALT, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 


CHROMIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 


COPPER, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 

IRON, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06 

IRON, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06 

MERCURY, TOTAL 002 SO 0600080 04/03/06 04/27/06 04-/27/06 


POTASSIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06 


LITHIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 


MAGNESIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 


MANGANESE, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 


MOLYBDENUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 


SODIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 


NICKEL, TOTAL. 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 

000000003







PHOSPHORUS, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/12/06 

LEAD, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06 

LEAD, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 


ANTIMONY, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 


SELENIUM, TOTAL 002 MS SO 06L0264 04/03/06 05/09/06 05/09/06 


SILICON, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 

TIN, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06 

TIN, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 


STRONTIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 


THALLIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06 


URANIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06 


VANADIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06 

ZINC, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06 

ZINC, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06 

ZIRCONIUM, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/12/06 

ZIRCONIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/12/06 

J11KT0 







BISMUTH, TOTAL 003 S0 06LO284 04/03/06 05/09/06 05/09/06 





000000004







IRON, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06 










LEAD, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06 




TIN, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06 





ZINC, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06 


J11KT4 













IRON, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06 

000000005













NICKEL, TOTAL 004 SO 06LO284 04/03/06 05/09/06 0,5/09/06 


LEAD, TOTAL 004 SO 06L0264 04/03/06 05/09/06 05/09/06 




TIN, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06 


THALLIUM, TOTAL 004 SO 061,02B4 04/03/06 05/09/06 05/09/06 



ZINC, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06 


J11KT6 








CALCIUM, TOTAL 005 $O 06L0284 04/03/06 05/09/06 05/09/06 








000000006













LEAD, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/09/06 




TIN, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06 





ZINC, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/09/06 


J11KT7 













IRON, TOTAL, 006 SO 06LO284 04/03/06 05/09/06 05/09/06 

MERCURY, TOTAL 006 50 0600080 04/03/06 04/27/06 04/27/06 

POTASSIUM, TOTAL 006 SO 06L02B4 04/03/06 05/09/06 05/09/06 



000000007















TIN, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06 





ZINC, TOTAL 006 SO 06L0284 04/03/06 05/09/06 05/09/06 


J11KT8 













IRON, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06 







000000008


INORGANIC ANALYTICAL DATA PACKAGE.FOR 








ANTIMONY, TOTAL 007 SO 06L0284 - 04/03/06 05/09/06 05/09/06 



TIN, TOTAL 007 SO 06LO284 04/03/06 05/09/06 05/09/06 







J11KT9 

SILVER, TOTAL 008 SO 06L0284 . 04/03/06 05/09/06 05/09/06 












IRON, TOTAL 008 SO 0610284 04/03/06 05/09/06 05/09/06 









000000009







LEAD, TOTAL 008 SO 06L0284 04/03/06 05/09/06 05/09/06 




TIN, TOTAL 008 SO 06L0284 04/03/06 05/09/06 05/09/06 







J11KVO 







BISMUTH, TOTAL - 009 SO 06L0284 04/03/06 05/09/06 05/09/06 

















000000010









TIN, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06 





ZINC, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06 


J11KR9 













IRON, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06 










LEAD, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06 



000000011







TIN, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06 





ZINC, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06 


J11KR2 


ALUMINUM, TOTAL O11 SO 06L0284 04/03/06 05/09/06 05/12/06 

ARSENIC, TOTAL O11 SO 06L0284 04/03/06 05/09/06 05/09/06 

BORON, TOTAL O11 SO 06L0284 04/03/06 05/09/06 05/09/06 


BERYLLIUM, TOTAL O11 SO 06L0284 04/03/06 05/09/06 05/09/06 




COBALT, TOTAL O11 SO 06L0284 04/03/06 05/09/06 05/09/06 


COPPER, TOTAL O11 SO 06L0284 04/03/06 05/09/06 05/09/06 

IRON, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06 










LEAD, TOTAL Oil SO 06L0284 04/03/06 05/09/06 05/09/06 




TIN, TOTAL Oil SO 06L0284 04/03/06 05/09/06 05/09/06 

000000012










ZINC, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06 


JllL38 













IRON, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06 










LEAD, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06 




TIN, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06 



000000013










JlIL35 











CHROMIUM, TOTAL 013 $O 06L0284 04/03/06 05/09/06 05/09/06 


IRON, TOTAL 013 SO 06L0284 04/03/06 05/09/06 05/09/06 














TIN, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06 





000000014








JIIL33 













IRON, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06 










LEAD, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06 




TIN, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06 







000000015






J11L31 























LEAD, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06 




TIN, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06 





ZINC, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06 


LAB QC: 

SILVER LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06 

000000016






SILVER, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

ALUMINUM LABORTORY LC1 BE S 06LO284 N/A 05/09/06 05/12/06 

ALUMINUM, TOTAL MB1 S 06L0284 N/A 05/09/06 05/12/06 

ARSENIC LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06 

ARSENIC, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

BORON LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06 

BORON, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

BARIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06. 05/09/06 

BARIUM, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

BERYLLIUM LABORATORY LC1 BE S 06L0284 N/A 05/09/06 05/09/06 

BERYLLIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

BISMUTH, LCS LC1 BE S 06L0284 N/A 05/09/06 05/09/06 

BISMUTH, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

CALCIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06 

CALCIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

CADMIUM LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06 

CADMIUM, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

COBALT LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06 

COBALT, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

CHROMIUM LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06 

CHROMIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

COPPER LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06 

COPPER, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

IRON LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06 

IRON, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

MERCURY LABORATORY LC1 BS S 0600080 N/A 04/27/06 04/27/06 

MERCURY, TOTAL MB1 S 06C0080 N/A 04/27/06 04/27/06 

POTASSIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06 

POTASSIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

LITHIUM LABORATORY LC1 BE S 06LO284 N/A 05/09/06 05/09/06 

LITHIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

MAGNESIUM LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06 

MAGNESIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

MANGANESE LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06 

MANGANESE, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

MOLYBDENUM LABORATOR LC1 BS S 06L0284 N/A 05/09/06 05/09/06 

MOLYBDENUM, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

SODIUM LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06 

000000017





CLIENT ID /ANALYSIS LVL # MTX PREP #1 COLLECTION EXTR/PREP ANALYSIS 

SODIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

NICKEL LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06 

NICKEL, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

PHOSPHORUS LCS LC1 BS S 06L0284 N/A 05/09/06 05/12/06 

PHOSPHORUS, TOTAL MB1 S 06L0284 N/A 05/09/06 05/12/06 

LEAD LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06 

LEAD, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

ANTIMONY LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06 

ANTIMONY, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

SELENIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06 

SELENIUM, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

SILICON LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06 

SILICON, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

TIN LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06 

TIN, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06 

STRONTIUM LCS STANDA LC1 BS S 06L0284 N/A 05/09/06 05/09/06 

STRONTIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

THALLIUM LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06 

THALLIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

URANIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06 

URANIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

VANADIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06 

VANADIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

ZINC LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06 

ZINC, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06 

ZIRCONIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/12/06 

ZIRCONIUM, TOTAL MB1 S 06L0284 N/A 05/09/06 05/12/06 

000000018

Client: TNU-HANFORD RC-047 W.O.#: 11343-606-001-9999-00 

LVL#: 0604L750 Date Received: 04-12-06 

SDG/SAF#: K1428/RC-047 

METALS CASE NARRATIVE 

The following is a summary of the QC results accompanying the sample results. Lionville 

Laboratory (LvLI) certifies that all test results meet the requirements of NELAC except as noted 

below. 

All soil samples are reported on a dry weight basis unless requested by the client, required by the 

method, or noted otherwise. 

1. This narrative covers the analyses of 15 solid samples. 

2. The samples were prepared and analyzed in accordance with methods checked on the attached 

glossary. The samples are reported on a wet weight, ` as received' b asis. 

In file HG042701 for Mercury, sample J11KT6 read 2.07 µg2 in the digestate, followed by 

sample J11KT7, which read -0.728 µg/L in the digestate. These 2 samples were rerun in file 

HG050401 (3 days p ast hold) to confirm the results. Initially, J11KT6 read 4.48 µg/L, and 

J11KT7 read -2.73 µg/L. The CCB following these samples dropped to -0.226 gg/L. The 

instrument was recalibrated, and these 2 samples rerun once again, with 5-fold dilutions, and 

each followed by a blank. In this file, HG050402, both read between -0.1 and 0.1 µg/L. 

Results from HG042701 were reported, which were within the hold time for Mercu ry . 

3. All analyses were performed within the required holding times. 

4. All Initial and Continuing Calibration Verifications (ICV/CCVs) were within the 90-110% 

control limits (80-120% for Mercury). 

5. All Initial and Continuing Calibration Blanks (ICB/CCBs) were within control limits (less 

than the PQL). 

6. All preparation/method blanks (MB) were within method crite ria {less than the Practical 

Quantitation Limit (3X the IDL), or samples greater than 20X MB value). Refer to the 

Inorganics Method Blank Data Summary . 

7. All ICP Interference Check Standards were within control limits. 

The re su lt 

s presented in this report relate only to the analy tical testing and conditions ofthe samples at receipt and during storage. All pages ofthis report are 

integral parts of the analytical data The refo re , this re port should only be reproduced in its entirety of (pO pages. 


44?R€'ir'!^#41 t?f

8. All laboratory control samples (LCS) were within the 80-120% control limits with the 

exception of Silicon at 31.2%. Refer to the Inorganics Laboratory Control Standards Report. 

Associated sample results may be biased low. 

9. The matrix spike (MS) recoveries for 4 analytes were outside the 75-125% control limits. 

Refer to the Inorganics Accuracy Report. 

10. For analytes where the ICP MS is out-of-control, a post-digestion MS (PDS) and serial 

dilution are performed. A PDS was not performed for Zinc. A PDS was prepared at 

meaningful concentration level for the following analytes: 

PDS PDS 

Sample ID Element Concentration (onb) % Recovery 

J11KV6 Iron 22,000 101.9 

Phosphorous 4,000 110.5 

Zirconium 200 100.4 

11. The duplicate analyses for 8 analytes were outside the 201/6 Relative Percent Difference 

(RPD) control limits. Refer to the Inorganics Precision Report. 

12. For the purposes of this report, the data has been reported to the Instrument Detection Limit 

(IDL). Values between the IDL and the Practical Quantitation Limit (PQL) are acquired in a 

region of less-certain quantification. 




14. I certify that this sample data package is in compliance with SOW requirements, both 

technically and for completeness, other than the conditions detailed above. Release of the data 

contained in this hard-copy data package has been authorized by the Laboratory Manager or a 

designee, as verified by the following signature. 

aniel 

rrrr Laboratory Manager 


jjw/m04750 

vLl 

4u 

Date

METALS METHOD GLOSSAR Y 

The following methods are used as'reference for the digestion and analysis of samples contained within f 

Lot#: pbo y L^5-v s 

Leaching Procedure: _1310 _1311 _1312 _Other: 

CLP Metals _Digestion and _ Analysis Methods: 

"03.0 _ILMO4.0 

Metals Digestion Methods: _3005A _3010A _3015 _3020A Zo3050B _3051 _200.7 _SS17 


Aluminum 

Antimony 

Arsenic 

Ba 

SW846 

-)C 601 OR 

)c601 0B _7041' 

^C 601 OR `7060A 

ri Metals Analysis Methods 

EPA 

um 

Beryllium 

Bismuth 

Boron 

Cadmium 

Calcium 

Chromium 

Cobalt 

Copper 

Iron 

Lead 

Lithium 

Magnesium 

Manganese 

Mercury 

Molybdenum 

Nickel 

Potassium 

Rare Earths 

Selenium 

Silicon 

Silica 

Silver 

Sodium 

Stron tium 

Thallium 

Tin 

Titanium 

Uranium 

Vanadium 

Zinc 

Zirconium 

EPA STD MTD 

_200.7 

_200.7 204.2 

200.7 206.2 311313 

-f- 601 OR _200.7 

*C6010B _200.7 

Y-6010B' _200.7' 

6010B _200.7 

16010B _7131A' _200.7 _213.2 

7r-6010B _200,9 

^C6010B _7191' 200.7 218.2 

--ewlw _200.7 

r 6010 _7211' _200.7 _220.2 

r6010B 

200.7 

35601013 _7421' _200.7 _239.2 3113B 

^J6010B _7430' 200;7 

Zc6OIOB 

200.7 

-f-6010B 

::200.7 

7470A'r-7471 245.1 '_245.5 2 

-jC 6010B _200.7 

f- 601 

_200.7 

ÊWJOB _7610' _200.7 _258.1' 

_601013 ' 

200.7 1 

6010B _7740' 200.7 270.2 3113B 

1601 OR 

200.7 

_6010B _200.7 

601013 _7761 _200.7 _272.2 

601013 _7770' _200.7 273.14 

^601 OR 

200.7 

•,f6010B _7841' 200.7!279.2_200.9 

JG60IOB _200.7 

_601 OR _200.7 

5&OlOB' 

200.7' 

6010B -200,7 

601013 

200.7 

^6010B' 200,7' 

OSWR 

_1620 

_1620 

_1620 

_1620 

_1620 

_1620 

_1620 

USATHAMA 

99 

_99 

99 

99 

99 

_SS17 

_99 

_99 

_99 

_99 

_99 

-^• 

_99 

_99 

99 

99 

_99 

99 

99 

99 

99 

99 

99 

99 

99 

-^ 

99 

99 

99 

99 

Other: p Method• 4moQ 4m, . 

000000021

METHOD REFERENCES AND DATA QUALIFIERS 

U = Indicates that the parameter was not detected at or above the reported limit. The 

associated numerical value is the sample detection limit. 

+ = Indicates that the original sample result is greater than 4x the spike amount added. 

MB = Method or Preparation Blank. 

MS = Matrix-Spike. 

MSD = Matrix Spike Duplicate. 

REP - Sample Replicate 

LCS = Laboratory Control Sample.. 

NC — Not calculated. 

1. Not included in the method element list. 

2. Modified Hg: Hgl and Hg2 require less total volume of digestate due to the 

autosampler analysis. Sample volumes and reagents for mercury determinations 

in water and soil have been proportionately scaled down to adapt to this semiautomated 

technique. The sample volume used for water analysis is 33 mL. For 

soils, approximately 0.3 grams of sample is taken to a final volume of 50 ml, 

(including all reagents). 

3. Flame AA. 

4. Graphite Furnace AA. 

L-WI-033/N-04/98 

000000022

CLIENT: TNURANPORD RC-047 X0303 

WORK ORDER: 11343-606-001-9999-00 


-001 011KV5 Silver, Total 



Boron, Total 

Barium, Total 





Cobalt, Total 


Copper, Total 

I., Total 




Magnavium, Total 



Sodium, Total 

Nickel, Total 


Lead, Total 




Tin, Total 





Zinc, Total 

Zirconium, Total 



LVL LOT #: 0604L750 



0.1 MG/KG 0.07 1.0 

30.2 MG/KG 2.3 1.0 

0.95 MG/KG 0.59 1.0 

619 MG/KG 0.23 1.0 

2.1 MO/KG 0.02 1.0 

0.02 u MG/KG 0.02 1.0 

0.50 u MG/KG 0.50 1.0 

511 MG/KG 1.6 1.0 

0.07 MG/KG 0.07 1.0 

0.14 u MG/KG 0.14 1.0 

0.42 MG/KG 0.13 1.0 

6.5 MG/KG 0.12 1.0 

94.8 MG/KG 3.4 1.0 

0.02 u MG/KG 0.02 1.0 

2600 MG/KG 2.2 1.0 

0.08 MG/KG 0.03 1.0 

826 MG/KG 0.94 1.0 

7.5 MG/KG 0.03 1.0 

0.53 MG/KG 0.28 1.0 

446 MG/KG 0.74 1.0 

0.23 u MG/KG 0.23 1.0 

2840 MG/KG 0.87 1.0 

0.30 u MG/KG 0.30 1.0 

D.43 u MG/KG 0.43 1.0 

D.56 MO/ICG 0.46 1.0 

47.2 MG/KG 2.2 1.0 

1.0 a MG/KG 1.0 1.0 

6.3 MG/KG 0.01 1.0 

0.68 u MG/KG 0.68 1.0 

0.85 u MG/KG 0.65 110 

D.15 MG/KG 0.09 1.D 

6015 MG/KG 0.16 1.0 

1.0 u MG/KG 1.0 1.0 

000000023

CLIENT: TNUHANFORD RC-047 X0303 

WORK ORDER: 11343-606-001-9999-00 


-002 311KV6 Silver, Total 



Boron, Total 

Barium, Total 





Cobalt, Total 


Copper, Total 

Iron, Total 




Magnsaium, Total 



Sodium, Total 

Nickel, Total 


Lead, Total 




Tin, Total 





Zinc, Total 




LVL LOT #: 06041,750 

RRPORTING DILUTION 


........ ...... 

........ 

0.07 

MG/KG 

.......... 

0.07 

110 

$2.3 MG/KG 2.3 1.0 

0.85 MG/KG 0.59 1.0 

S.9 MG/KG 0.23 1.0 

2.1 MG/KG 0.02 1.0 

0.02 u MG/KG 0.02 1.0 

0.49 u MG/KG 0.49 1.0 

346 MG/RG 1.6 1.0 

0.07 u MG/1(G 0.07 1.0 

0.13 u MG/KG 0.13 1.0 

0.31 MG/KG 0.12 1.0 

6.5 MG/KG 0.12 1.0 

211 MG/KG 3.4 1.0 

0.01 U MG/KG 0.01 1.0 

2540 MG/KG 2.2 1.0 

0.11 MG/KG 0.03 1.0 

828 MG/KG '0.93 1.0 

9.2 MG/KG 0.03 1.0 

0.54 MG/KG 0.28 1.0 

491 MG/KG 0.73 1.0 

0.35 MG/KG 0.23 110 

2590 MG/KC 0.86 1.0 

0.30 u MG/KG 0.30 1.0 

0.42 U MG/KG 0.42 1.0 

0.45 u MG/KG 0.45 1.0 

57.1 MG/KG 2.2 1.0 

1.0 U MG/KG 1.0 1.0 

5.5 MG/KG 0.01 1.0 

0.67 u MG/KG 0.67 1.0 

0.6S u MG/KG 0.65 1.0 

0.46 MG/KG 0.09 1.0 

51.9 MG/KG 0.15 1.0 

1.0 u MG/KG 1.0 1.0 

000000024



CLIENT: TNUAANPORD RC-047 X0303 LVL LOT 4: 0604L75O 

WORK ORDER: 11343-606-001-9999-00 


SAMPLE SITS ID ANALYTB RESULT UNITS LIMIT FACTOR 

....... ........ ........ 

-003 1T11KT0 Silver, Total 0.07 U MG/KG 0.07 1.0 


Arsenic, Total 1.4 MG/KG 0.50 1.0 



Beryllium, Total 0.02 U MG/KG 0.02 1.0 

Bismuth, Total 0.49 u MG/KG D.49 1.0 


Cadmium, Total 0.09 MG/KG 0.07 1.0 

Cobalt. Total 0.14 MG/KG 0.13 1.0 




Mercury, Total 0.01 U MG/KG 0.01 1.0 

Potasoium, Total 2560 MG/KG 2.2 1.0 


Magnaaium, Total 613 MG/KG 0.92 1.0 


Molybdenum, Total 0.79 MG/KG 0.20 1.0 








Tin, Total 1.0 u MG/KG 1.0 1.0 

Strontium, Total 5.2 MG/KG 0-01 1.0 

Thallium, Total 0.67 u MG/KO 0.67 1.0 

Uranium, Total 0.84 u MO/KG 0.04 1.0 



Zirconium, Total 1.0 U MG/KG 1.0 1.0 

000000025

CLIENT: TNUHANPORD RC-047 K0303 

WORK ORDER: 11343-606-001-9999-00 


-004 J11KT4 Silver, Total 



Boron, Total 

Barium, Total 





Cobalt, Total 


Copper, Total 

Iron, Total 







Sodium, Total 

Nickel, Total 

phosphorus, Total 

Lead, Total 




Tin, Total 





Zinc, Total 




LVL LOT M: D604L750 



0.07 u MG/KG 0.07 110 

34.3 MG/KG 2.3 1.0 

0.85 MG/KG 0.60 1.0 

3.7 MG/KG 0.24 1.0 

1.3 MG/KG 0.02 1.0 

0.02 u MG/KG 0.02 1.0 

0.50 u MG/KG 0.50 1.0 

414 MG/KG 1.6 1.0 

0.07 u MG/KG 0.07 1.0 

0.14 MG/KG 0.14 1.0 

0.22 MG/KG 0.13 1.0 

6.6 MG/1CG 0.12 1.0 

120 MG/KG 3.4 1.0 

0.02 u MG/KG 0.02 1.0 

2670 MG/KG 2.2 1.0 

0.10 MG/KG 0.03 1.0 

678 MG/KG 0.95 1.0 

7.2 MG/KG 0.03 1.0 

0.62 MG/KG 0.28 1.0 

461 MG/KG 0.74 1.0 

0.24 u MG/KG 0.24 1.0 

2520 MG/KG 0.88 1.0 

0.30 u MG/KG 0.30 1.0 

0.43 u MG/KG 0.43 1.0 

0.64 MG/KG 0.46 1.0 

48.3 MG/KG 2.2 1.0 

1.0 u MG/KG 1.0 1.0 

4.2 MG/KG 0.01 1.0 

0.69 u MG/KG 0.69 1.0 

0.86 u MG/KG 0.86 1.0 

0.15 MG/KG 0.09 1.0 

45.1 MG/KG 0.16 1.0 

1.0 u MG/KG 1.0 1.0 

000000026

CLIENT: TNUHANFORD RC-047 K03D3 

NORK ORDER: 11343-606-001-9999-00 


005 JIIKT6 

ANALYTE 

Silver, Total 



Boron, Total 

Barium, Total 





Cobalt, Total 


Copper, Total 

Iron, Total 







Sodium, Total 

Nickel, Total 


Lead, Total 




Tin, Total 





Zinc, Total 




LVL LOT p: 0604L750 

REPORTING 

RESULT UNITS LIMIT 

0.12 MG/KG 0.08 

19.2 MG/KG 2.6 

0.81 MG/KG 0.68 

4.0 MG/KG 0.27 

3.3 MG/KG 0.02 

0.02 a MG/KG 0.02 

0.57 u MG/KG 0.57 

327 MG/KG 1.8 

0.08 u MG/KG 0.08 

0.16 u MG/KG 0.16 

0.20 MG/KG 0.14 

6.4 MG/KG 0.13 

76.3 MG/KG 3.9 

0.36 MG/KG 0.02 

2530 MG/KG 2.5 

0.05 MG/KG 0.03 

697 MG/KG 1.1 

5.0 MG/KG 0.03 

0.57 MG/KG 0.32 

542 MG/KG 0.84 

0.27 u MG/KG 0.27 

2500 MG/KG 1.0 

0.34 u MG/KG 0.34 

0.49 u MG/KG 0.49 

0.53 MG/KG 0.52 

45.6 MG/KG 2.5 

1.2 u MG/KG 1.2 

3.3 MG/KG 0.01 

0.78 u MG/KG 0.78 

0.98 u NG/KG 0.98 

0.1 u MG/RG 0.1 

36.8 MG/KO 0.19 

1.2 u MG/KG 1.2 

DILUTION 

FACTOR 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

1.0 

990069027

CLIENT: TNUHAN17ORD RC-047 K0303 

WORK ORDER: 11343-606-001-9999-00 


-006 aI1KT7 Silver, Total 



Boron, Total 

Barium, Total 





Cobalt, Total 


Copper, Total 

Iron, Total 







Sodium, Total 

Nickel, Total 


Lead, Total 




Tin, Total 





Zinc, Total 


Lion Ville Laboratory, Inc. 


LVL LOT #: 06041,750 



0.07 MG/KG 0.07 1.0 

29.9 MG/KG 2.3 1.0 

0.86 MG/KG O.S9 1.0 

3.2 MG/KG 0.23 1.0 

1.8 MG/KG 0.02 1.0 

0.02 a MG/KG 0.02 1.0 

0.50 u MG/KG O.SO 1.0 

714, MG/KG 1.6 1.0 

0.07 MG/KG 0.07 1.0 

0.16 MG/KG 0.14 1.0 

0.13 u MG/KG 0.11 1.0 

611 MG/KG 0.12 1.0 

81.9 MG/KG 3.4 1.0 

0.01 u MG/KG 0.01 1.0 

2370 MG/KG 2.2 1.0 

0.06 MG/KG 0.03 1.0 

496 MG/KG 0.94 1.0 

8.4 MG/KG 0.03 1.0 

0.48 MG/KG 0.28 1.0 

432 MG/KG 0.74 1.0 

0.23 u MG/KG 0.23 1.0 

2040 MG/KG 0.87 1.0 

0.30 u MG/KG 0.30 1.0 

0.43 u MG/KG 0.43 1.0 

0.46 u MG/KG 0.46 1.0 

39.6 MG/KG 2.2 1.0 

1.0 u MG/KG 1.0 1.0 

6.2 MG/KG 0.01 1.0 

0.68 u MG/KG 0.68 1.0 

D.85 u MG/KG 0.85 1.0 

0.19 MG/KG 0.09 1.0 

30.5 MG/KG 0.16 1.0 

1.0 u MG/KG 1.0 1.0 

999090028

CLIENT: TNUNANPORD RC-047 X0303 

WORK ORDER: 11343-606-001-9999-00 

SAMPLE SITE ID ANALYTR 

-007 J11KTS Silver, Total 



Boron, Total 

Barium, Total 





Cobalt, Total 


Copper, Total 

Iron, Total 







Sodium, Total 

Nickel, Total 


Lead, Total 




Tin, Total 





Zinc, Total 




LVL LOT A: O6041,750 



.....: .. ...... 

........ 

0.07 u 

MG/KG 

.......... 

0.07 

1.0 

11.6 MG/KG 2.2 1.0 

0.59 MG/KG 0.58 1.0 

2.1 MG/KG 0.23 1.0 

1.2 MG/KG 0.02 1.0 

0.02 u MG/KG 0.02 1.0 

0.46 u MG/KG 0.48 1.0 

222 MG/XG 1.5 1.0 

0.07 u MG/KG 0.07 1.0 

-0.13 u MG/KG 0.13 1.0 

0.16 MG/KG 0.12 1.0 

4.6 MG/KG D_11 1.0 

61.0 MG/KG 3.3 1.0 

0.01 u MG/KG 0.01 1.0 

2310 MG/KG 2.1 1.0 

0.03 MG/KG 0.03 1.0 

700 MG/KG 0.91 1.0 

3.7 MG/KG 0.03 1.0 

0.48 MG/KG 0.27 1.0 

389 MG/KG 0.72 1.0 

0.23 u MG/KG 0.23 1.0 

7340 MG/KG 0.85 1.0 

0.29 u MG/KG 0.29 1.0 

0.41 u MG/KG 0.41 1.0 

0.44 u MG/KG 0.44 1.0 

31.3 MG/KG 2.1 1.0 

1.0 u MG/KG 1.0 1.0 

2.5 MG/KG 0.009 1.0 

0.66 u MG/KG 0.66 1.0 

0.83 u MG/KG 0.83 1.0 

0.08 u MG/KG 0.06 1.0 

29.1 MG/KG 0.15 1.0 

1.0 u MG/KG 1.0 1.0 

000000029

Lionville Laboratory. Inc. 

INORGANICS DATA SUMMARY REPORT O5/25/D6 

CLIENT: TNUHAUPORD RC-047 K03O3 LVL LOT #: 06041,750 

ifORK ORDER: 11343-606-001-9999-00 


SAMPLE SITE ID ANALYTS RESULT UNITS LIMIT FACTOR 

..c o ee .................... -.................... 

-0c8 J13KT9 Silver, Total 0.07 u MG/KG 0.07 1.0 









Cobalt, Total 0.17 MG/KG 0.13 1.0 

Chromium, Total 0.12 u MG/KG 0.12 1.0 






Magnesium, Total 522 MG/KG 0.93 - 1.0 

- Manganese, Total 5.5 MG/KG 0.03 1.0 















Zirconium, Total 1.0 u MG/KG 1-0 1.0 

000000030



CLIENT: TNUNANFORD RC-047 X0303 LVL LOT #: O604L750 

WORK ORDER: 11343-606-001-9999-00 


SAMPLE SITS ID ANALYTE RESULT UNITS LIMIT FACTOR 

-009 331KV0 Silver, Total 0.07 U MG/KG 0.07 1.0 







Calcium, Total 223 MG/KG 1,6 1.0 



Chromium, Total 0.16 MG/KG 0.12 110 






Magnesium. Total 760 MG/KG 0.93 1.0 


Molybdenum, Total 0.46 MG/XG 0.28 110 


Nickel, Total 0.23 u MG/XG 0.23 1.0 



Antimony, Total 0.42 V MG/KG 0.42 1.0 




Strontium, Total 2.0 MG/KG 0.01 110 





Zirconium, Total 1.0 u MG/KG 1.0 1.0 

000000031

CLIENT: TNURANPORD RC-047 K0303 

WORK ORDER: 11343-606-001-9999-00 


....... .................... ... 

-010 J11KI9 Silver, Total 



Boron, Total 

Barium, Total 





Cobalt, Total 


Copper, Total 

Iron, Total 







Sodium, Total 

Nickel, Total 


Lead, Total 




Tin, Total 





Zinc, Total 



IMORGANICS DATA SUMMARY REPORT 05/25/06 

LVL LOT #: O6O4L75O 



0.07 u MG/KG- 0.07 1.0 

36.0 MG/KG 2.3 1.0 

1.5 MG/KG 0.59 1.0 

5.4 MG/KG 0.23 1.0 

1.4 MG/KG 0.02 1.0 

0.02 u MG/KG 0.02 1.0 

0.50 u MG/KG 0.50 1.0 

264 MG/KG 1.6 1.0 

0.07 u MG/KG 0.07 1.0 

0.14 u MG/KG 0.14 1.D 

0.16 MG/KG 0.13 1.0 

6.0 MG/KG 0.12 1.0 

110 MG/KG 3.4 1.0 

0.01 u MG/KG D.01 1.0 

2370 MG/KG 2.2 1.0 

0.05 MG/KG 0.03 1.0 

710 MG/KG 0.94 3.0 

4.8 MG/KG - 0.03 1.0 

0.74 MG/KG 0.25 1.0 

446 MG/KG 0.74 1.0 

0.33 u MG/KG 0.23 1.0 

2640 MG/KG 0.87 1.0 

0.30 u MG/KG 0.30 1.0 

0.43 u MG/KG 0.43 1.0 

0.46 u MG/KG 0.46 1.0 

54.5 MG/KG 2-2 1.0 

1.0 u MG/KG 1.0 1.0 

3.6 MG/KG 0.03 1.0 

0.68 u MO/KG 0.69 1.0 

0.85 u MG/KG 0.85 1.0 

0.14 MG/KG 0.09 1.0 

36.1 MG/KG 0.16 1.0 

1.0 u MG/KG 1.0 1.0 

000000032

CLIENT; TNURANFORD RC-047 X0303 

WORK ORDER: 11343-606-001-9999-00 

SAMPLE SITE ID ANALYT6 

-011 J11XR2 Silver, Total 


Arsenic. Total 

Moron, Total 

Barium, Total 


Biemuth, Total 



Cobalt, Total 


Copper, Total 

Iron, Total 


Pataesium, Total 





Sodium, Total 

Nickel, Total 


Lead, Total 




Tin, Total 





Zinc, Total 


Lionville Laboratory, Inc- 


LVL LOOT #! 0604L750 



........ ...... 

........ 

0.07 u 

MG/KG 

.......... 

0.07 

1.0 

38.1 MG/KG 2.3 1.0 

0.59 u MO/KG 0.59 1.0 

2.6 MG/KG 0.23 1.0 

1.3 MG/KG 0.02 1.0 

0.02 u MG/KG 0.02 1.0 

0.50 U MG/XG 0.50 1.0 

511 MG/KG 1.6 1.0 

0.07 u MG/KG 0.07 1.0 

0.14 U MG/KG 0.14 1.0 

0.57 MG/KG 0.13 1.0 

7.8 MG/KG 0.12 1.0 

121 MG/KG 3.4 1.0 

0.02 u MG/KG 0.02 1.0 

2640 MG/KG 2.2 1.D 

0.06 MG/KO 0.03 1.0 

739 MG/KG 0.94 1.0 

6.6 MG/KG 0.03 1.0 

0.52 MG/KG D.28 1.0 

524 MG/KG 0.74 1.0 

0.30 MG/KG 0.23 1.0 

2710 MG/KG 0.87 1.0 

0.30 u MG/KG 0.30 1.0 

0.43 u MG/KG 0.43 1.0 

0.46 u MG/KG 0.46 1.0 

53.5 MG/KG 2.2 1.0 

1.0 u MG/KG 1.0 1.0 

3.4 MG/KG 0.01 1.0 

0.68 u MG/RG 0.68 1.0 

D.85 u MG/KO 0.85 1.0 

0.15 MG/KG 0.09 1.0 

38.7 MG/KG 0.16 1.0 

1.0 u MG/KG 1.0 1.0 

000000033



CLIENT: TNUKANFORD RC-047 K0303 LVL LOT 1!: 06041,750 

WORK ORDER: 11341-606-001-9999-00 


SAMPLE SITE ID ANALYTE RESULT UNITS LIMIT FACTOR 

.................... 

------' 

-012 J31L38 Silvar, Total 0.07 u MG/KG 0.07 1.0 

Aluminum, Total 2S.2 MG/KG 2.3 1.0 





Biamuth, Total 0.49 u MG/KG 0.49 1.0 



Cobalt, Total 0.13 u MG/XG 0.13 1.0 




Mercury, Total 0.01 u MO/KG 0.01 1.0 



Magnesium, Total 927 MG/1(G 0.93 1.0 





Phosphoruo, Total 2400 MG/KG 0.86 1.0 



Selenium, Total - 0.48 MG/KG 0.45 1.0 

Silicon, Total 4S.4 MG/KG 2.2 1.0 

Tin, Total 1.0 u MG/KG 1.0 - 1.0 



uranium, Total 0.65 u MG/KG 0.95 1.0 



Zirconium, Total 1.0 u MG/KG 1.0 1.0 

000000034

CLIENT: TNUNANFORD RC-047 KD302 

MORIC ORDER: 11343-606-001-9999-00 


-013 Tl2L35 Silver, Total 



Boron, Total 

Barium, Total 





Cobalt, Total 

Chromium, Total. 

Copper, Total 

Iron, Total 







sodium, Total 

Nickel, Total 


Lead, Total 




Tin. Total 





Zinc, Total 



INDRGAMICS DATA SUMMARY REPORT 05/25/06 

LVL LOT k: 06041,750 



........ ...... 

........ 

0.07 u 

MG/KG 

.......... 

0.07 

1.0 

23.7 MG/KG 2.2 1.0 

0.93 MG/KG 0.58 1.0 

2.5 MO/KG 0.23 1.0 

0.97 MG/KG 0.02 1.0 

0.02 u MG/KG 0.02 1.0 

0.49 u MG/KG 0.49 1.0 

392 MG/KG 1.6 1.0 

0.07 u MG/KG 0.07 110 

0.13 u MG/KG 0.13 3.0 

0.17 MG/KG 0.12 1.0 

7.3 MG/KG 0.11 110 

66.9 MG/KG 3.3 1.0 

0.02 V MG/KG 0.02 1.0 

2240 MG/KG 2.2 1.0 

0.03 MG/KG 0.03 1.0 

579 MG/KG 0.92 1.0 

5.1 MG/KG 0.03 1.0 

0.45 MG/KG 0.28 1.0 

499 MG/KG 0.72 1.0 

0.27 MG/KG 0.23 1.0 

2110 MG/KG - 0.86 1.0 

0.30 u MG/KG 0.30 1.0 

0.42 u MG/KG 0.42 1.0 

0.45 u MG/KG 0.45 1.0 

44.6 MG/KG 2.2 1.0 

1.0 u MG/KG 1.0 1.0 

3.1 MG/KG 0.01 1.0 

0.67 u MG/KG 0.67 1.0 

0.64 u MG/KG 0.64 1.0 

0.1 MG/KG 0.09 1.0 

30.1 MG/KG 0.15 1.0 

1.0 u MG/KG 1.0 1.0 

000000035

CLIENT: TNVNANFORD RC-047 X0303 

WORK ORDER: 11343-606-DO1-9999-00 





Boron, Total 

Barium, Total 

Baryllium, Total 




Cobalt, Total 


Copper, Total 

Iron, Total 







Sodium, Total 

Nickel, Total 


Load, Total 




Tin, Total 





Zinc, Total 




LVL LOT #: 06041,750 



0.07 MG/KG 0.07 1.0 

24.6 MG/KG 2.2 1.0 

0.58 u MG/KG 0.56 1.0 

311 MG/KG 0.23 1.0 

1.6 MG/KG 0.02 1.0 

0.02 u MG/XG 0.02 1.0 

0.49 u MG/KG 0.49 1.0 

354 MG/KG 1.6 1.0 

0107 MG/KG 0.07 1.0 

0.13 u MG/XG 0.13 1.0 

0.21 MG/KG 0.12 1.0 

5.1 MG/XG 0.11 1.0 

76.2 MG/KG 3.3 110 

0.01 u MG/KG 0.01 1.0 

2600 MG/KG 2.2 1.0 

0.03 MG/KG 0.03 1.0 

690 MG/KG 0.92 1.0 

5.9 MG/KG 0.03 1.0 

0.49 MG/KG 0.28 1.0 

432 MG/KG 0.72 1.0 

0.23 U MG/KG 0.23 1.D 

2560 MG/KG 0.86 1.0 

0.30 U MG/KG 0.30 1.0 

0.42 u MG/KG 0.42 1.0 

0.45 u MG/KG 0.45 1.0 

50.1 MG/KG 2.2 1.0 

1.0 u MG/KG 1.0 1.0 

3.9 MG/KG 0.01 1.0 

0.67 u MG/KG 0.67 1.0 

0.84 u MG/KG 0.84 1.0 

0.14 MG/KG 0.09 1.0 

30.9 MG/KG 0.15 1.0 

1.0 u MG/KG 1.0 1.0 

000000036

CLIENT: TNOMANFORD RC-047 K0303 

WORK ORDER: 11343-606-001-9999-00 


....... .................... ............. 

-015 JLIL31 Silver, Total 



Boron, Total 

barium, Total 





Cobalt, Total 


Copper, Total 

Iron, Total 







Sodium, Total 

Nickel, Total 


Lead, Total 




Tin, Total 




vanadium. Total 

Zinc, Total 




LVL LOT S: 0604LISO 



0.07 U MG/KG 0.07 1.0 

57.0 MG/KG 2.3 1.0 

0.59 u MG/KG 0.59 1.0 

3.5 MG/KG 0.23 1.0 

2.4 MG/KG 0.02 1.0 

0.02 U MG/KG 0.02 110 

0.49 u MG/KG 0.49 1.0 

580 MG/KG 1.6 1.0 

0.09 MG/KG 0.07 1.0 

0.18 MG/1(G 0.13 1.0 

0.22 MG/KG 0.12 1.0 

6.1 MG/KG 0.12 1.0 

188 MG/KG 3.4 1.0 

0.01 u MG/KG 0.01 1.0 

2360 MG/KG 2.2 1.0 

0.10 MG/KG 0.03 1.0 

740 MG/KG 0.93 1.0 

7.7 MG/KG 0.03 1.0 

0.61 MG/KG 0.26 1.0 

386 MG/KG 0.73 1.0 

0.23 u MG/KG 0.23 1.0 

2470 MG/KG 0.86 1.0 

0.30 u MG/KG 0.30 1.0 

0.42 u MG/KG 0.42 110 

0.45 u MG/KG 0.45 110 

63.5 MO/KG 2.2 1.0 

1.0 u MG/KG 1.0 1.0 

4.2 MG/KG 0.01 1.0 

0.67 u MG/KG 0.67 1.0 

0.85 u MG/KG 0.85 1.0 

0.29 MG/KG 0.09 1.0 

32.6 MG/KG 0115 1.0 

1.0 u MG/KG 1.0 1.0 

000000037

CLIENT: TNUKANPORD RC-047 X0303 

WORK ORDER: 11343-606-001-9999-00 


BLANKS 04LO284-MB1 Silver, Total 


INORGANICS METHOD BLANK DATA SUMMARY PASS 05/25/06 



Boron, Total 

Barium, Total 





Cobalt, Total 


Copper, Total 

Iron, Total 






Sodium, Total 

Nickel, Total 


Lead, Total 




Tin, Total 





Zinc, Total 


BLANKI 0600080-MB1 Mercury, Total 

LVL LOT #: 06O4L750 



........ ...... 

-------- 

0.07 u 

MG/KG 

.......... 

0.07 

1.0 

2.4 u MG/KG 2.4 1.0 

0.61 u MG/KG 0.61 1.0 

0.24 u MG/KG 0.24 1.0 

0.02 u MG/KG 0.02 1.0 

0.02 U MG/KG 0.02 1.0 

0.51 u MG/KG 0.51 1.0 

2.0 MG/KG 1.6 1.0 

0.07 u MG/KG 0.07 1.0 

0.14 u MG/KG 0.14 1.0 

0.13 u MG/KG 0.13 1.0 

0.12 u MG/KG 0.12 1.0 

3.5 u MG/KG 3.5 1.0 

2.3 U MG/KG 2.3 1.0 

0.03 u MG/KG 0.03 1.0 

0.97 u MG/KG 0.97 1.0 

0.03 u MG/KG 0.03 1.0 

0.29 u MG/KG D.29 1.0 

0.76 u MG/KG 0.76 110 

0.24 u MG/KG 0.24 110 

0.90 u MG/KG 0.90 1.0 

0.31 u MG/KG 0.31 1.0 

.0.44 u MG/KG 0.44 1.0 

0.47 u MG/KG 0.47 1.0 

2.) u MG/KG 2.3 110 

1.1 u MG/KG 1.1 1.0 

0.01 MG/KG 0.01 1.0 

0.70 U MG/KG 0.70 1.0 

0.68 u MG/KG 0.88 1.0 

0.09 u MG/KG 0.09 1.0 

0.16 u MG/KG 0.16 1.0 

1.1 u MG/KG 1.1 1.0 

0.02 u MG/KG 0.02 3.0 

000000038



CLIENT: TNUNANPORD RC-047 K0303 LVL LOT M: 06041,750 

WORK ORDER: 11343-606 -OD1- 9999-00 

SPIKED INITIAL SPIKED 

SAMPLE SITE ID ANALYTE SAMPLE RESULT AMOUNT TREODV 

-001 011KV5 Mercury, Total 0.14 0.02u 0.15 96.6 

DILUTION 

FACTORS PK) 

1.0 

000000039



CLIENT: TNVRANPORD RC-047 X0303 LVL LOT p: 06041,750 

WORK ORDER: 11343-606-001-9999-00 


SAMPLE 

....... 

SITE ID 

.................... 

ANALYTE 

...................... 

SAMPLE 

....... 

RESULT 

....... 

AMOUNT 

...... 

tRSOOV 

....... 

PACTOR(SPK) 

.......... 

-002 JI1KV6 

Silver, Total 

4.5 

0.07 

4.8 

92.3 

Aluminum, Total 202 52.3 192 77.9 1.0 

Arsenic, Total 162 0.85 192 84.1 1.0 

Boron, Total 69.3 5.9 96.1 86.8 1.0 

Barium, Total 173 2.1 192 88.8 1.0 

Beryllium, Total 4.3 0.O2u 4.8 89.6 1.0 

Bismuth, Total 418 O.49u 480 87.0 1.0 

Calcium, Total 2640 346 2400 95.3 1.0 

Cadmium, Total 4.3 O.O7u 4.8 89.6 1.0 

Cobalt, Total 43.6 O.13u 48.0 90.8 1.0 

Chromium, Total 17.8 0.31 19.2 91.1 1.0 

Copper, Total 27.5 6.5 24.0 87.5 1.0 

Iron, Total 224 211 96.1 13.6 1.0 

Potassium, Total 4420 2540 2400 78.4 1.0 

Lithium, Total 94.2 0.11 96.1 97.9 1.0 

Magnesium, Total 3030 828 2400 91.7 1.0 

Manganese, Total 52.3 9.2 48.0 89.8 1.0 

Molybdenum, Total 86.5 0.54 96.1 89.4 1.0 

Sodium, Total 2660 491 2400 90.3 1.0 

Nickel, Total 42.9 0.35 48.0 88.7 1.0 

Phosphorus, Total 2930 2590 480 48.5- 1. 0, 

Lead, Total 42.2 0.30u 48.0 87.9 1.0 

Antimony, Total 39.5 0.42u 48.0 82.3 1.0 

Selenium, Total 156 0.45u 192 82.5 1.0 

Silicon, Total 174 57.1 96.1 121.3 1.0 

Tin, Total 80.9 1.0 u 96.1 84.2 - 1.0 

Strontium, Total 90.7 515 96.1 88.7 1.0 

Thallium, Total 168 O.67u 192 87.4 1.0 

Uranium, Total ,213 O.85u 240 89.9 1.0 

Vanadium, Total 44.9 0.46 48.0 92.6 1.0 

Zinc, Total 134 51.9 48.0 172.1 

Zirconium, Total 320 1.0 u 4S0 66.6 1.0 

1.0 

000000040


INORGANICS PRECISION REPORT 05/25/06 

CLIENT! TNUKANFORD RC-047 K0303 LVL LOT 8: 0604L750 

WORK ORDER: 11343-606-001-9999-00 


SAMPLE SITE ID ANALYTR RESULT REPLICATE RFD FACTOR(REP) 

....: .. ...........................:a.........:.... ........ ...».... ._.:..: ----------- 

-001REP S11KV5 Silver, Total 0.1 0. 07u -No. 1.0 

Aluminum, Total 30 . 2 43.3 35.6 1.0 

Arsenic, Total 0.95 1.1 14.4 1.0 

Boron, Total 6.9 6.1 12.3 1.0 

Barium, Total 2.1 2.3 9.1 1.0 

Beryllium, Total 0 . 02u 0 . 02u NC 1.0 

Bismuth, Total O.SOu 0.49u NC 1.0 

Calcium, Total 511 506 0.88 1.0 

Cadmium, Total 0.07 0.07u .IiC 1.0 

Cobalt, Total 0.14u 0.13u NC 1.0 

Chromium, Total 0.42 0.28 38.2 1.0 

Copper, Total 6.5 6.7 3.0 1.0 

Iron, Total 94,8 159 50.6 1.0 

Mercury , Total 0.02u 0.02U NC 1.0 

Potassium, Total 260D 2420 7.1 1.0 

Lithium, Total 0.08 0.09 4.9 1.0 

Magnesium, Total 826 874 5 .7 1.0 

Manganese, Total 7.5 8.6 13.7 1.0 

Molybdenum, Total 0.53 0.48 10 1.0 

Sodium, Total 446 413 7.8 1.0 

Nickel, Total 0.23u 0.27 -?w 1.0 

Phosphorus, Total 2840 2710 4.7 1.0 

Lead, Total 0.3Du 0.30u NC 1.0 



0.43U 

0.56 

0.42U 

0.45u 

NC 

^/ 

"s- /V " r 

1.0 

1.0 

Silicon, Total 47.2 54.9 15.1 1.0 

Tin, Total 1.0 v 1.0 u NC 1.0 

St ro ntium, Total 6.3 5.8 9.3 1.0' 

Thallium, Total 0,68u 0.67u NC 1.0 

Uranium, Total 0.66u O.BSu NC 1.0 

Vanadium, Total 0.15 0.26 54.9 1 1 0' 

Zinc, Total 60.5 62.7 3.6 1.0 

Zirconium, Total 1.0 u 1.0 u NC 1.0 

`V W 1 

000009041

CLIENT: TNUHA14PORD RC-047 K0303 

WORK ORDER: 11343-606-001-9999-00 


INORGANICS LABORATORY CONTROL STANDARDS REPORT 05/25/06 

SPIKED SPIKED 

LVL LOT $: 0604050 

SAMPLE SITE ID ANALYTE SAMPLE AMOUNT UNITS LRECOV 

LC81 06L0284- LC1$6ìi : Silver, LCS 47.8 50.0 MG/KG 95.6 

Aluminum, Les 458 500 MG/KG 91.6 

Arsenic, LCS 895 1000 MG/KG 89.5 

Boron, LCS 454 500 MG/KG 90.8 

Barium, LCS 468 500 MG/KG 93.5 

Beryllium, LCS 22.9 25.0 MG/KG 91.6 

Bismuth, LCS 455 500 MG/KG 91.1 

Calcium, LCS 2370 2500 MG/KG 94.8 

Cadmium, LCS 2219 25.0 MG/KG 91.6 

Cobalt, LCS 232 250 MG/KG 92.9 

Chromium, LCS 46.7 50,0 MG/KG 93.4 

Copper, LCS 117 125 MG/KG 93.4 

Iron, LCS 477 500 MG/KG 95.5 

Potassium, LCS 2260 2500 NG/KG 91.1 

Lithium, LCS 491 500 MG/KG 98.3 

Magnesium, LCS 2350 2500 MG/KG 94.1 

Manganese, LCS 72.2 75.0 MG/KG 96.3 

Molybdenum, LCS 478 500 MG/KG 95.7 

Sodium, LCS 2310 2500 MG/KG 92.5 

Nickel, LCS 184 200 MG/KG 92.0 

Phosphorus, LCS 466 500 MG/KG 93.5 

Lead, LCS 226 250 MG/KG 91.0 

Antimony, LCS 273 300 MG/KG 91.0 

Selenium, LCS 873 1000 MG/KG 87.3 

Silicon, LCS 156 500 MG/KG 31.2 

Tin, LCS 473 500 WKG 94.6 

Strontium, LCS 476 500 MG/KG 95.2 

Thallium, LCS 924 1000 MG/KG 92.4 

Uranium, LCS 235 250 MG/KG 93.9 

Vanadium, LCS 239 250 MG/KG 95.8 

Zinc, LCS 90,6 100 MG/KG 90.6 

Zirconium, LCS 478 500 MG/KG 95.6 

LCS1 06C0000-LC1 Mercury, LCS 6.6 6.2 MG/KG 106.4 

000000042

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Washington Closure Hanford CHAIN OF CUSTODY/SAWLE ANALYSIS REQUEST RC•047326 ''_` _ nr ! 

Collector TR KLINCKMAN -' Ctamoaev Contact Teleohone Nm Proiect Coordinator 

TILLER, B. JOAN KESSNER 375 4688 KESSNER, IH Price Code 9N 

roicet Desinna tion Samati a Location SAF No. 

100 & 300 Arm Component of the RCBRA Sediment and Ti 100-D-48:2 INVERTEBRATES RC•047 

Air Quality _ ] 

Ice Cheat No OIL+' 7 Field Loahook No. 

COA Method of Shinmcnt 

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1311 1595 DESRAS6520 FED EX 

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EBERLWESERVICES 

POSSIBLE SAMPLE HA 

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No. 

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Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-327 h lea ! or i 

Collector TR KLINCKMAN Companv Contact Telephone No. Pro ject Coordinator 

TILLER, B. JOAN KESSNER 3754688 KI?SSNER, IN 

Protect Desienatlon Sarnwine Loca tion SAP No. 

1 00 & 300 Am Component of the RCBRA Sediment and Ts 100.1149:2 94VERTEBRATES RC-047 

Ice Chest No•^.^ G , O ^^ 

Field Loebaok No. COA Method of Sldomenl 

– 7^7 7 

EL 1595 BESRAS6520 FED EX 

Sli pped To OHsite Property NO Î / Bi ll 

of LaditwJAir Bi ll No. 

EBERLINESERVIC LIONVIIfF /1 Qp D^„r^ SEE OSPC 

Price Code 9N Dala "Curneroura 

Air Quality Lj 45 02'y'S 

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POTEA77ALRADIOACTIVE

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Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS BEQUEST RG4147-311 

Collector 

TILLER. B. TR KLINCKMAN 

feet Desiaoation 

100 & 300 Arca Component of the RCBRA Sediment and Ti 

a Chest No }± // 

6 e-e1 ' T^ 7 

Shiooed To 

EBERLINE SERVICES gioEyZip 

POSSIBLE SAMPLE IIA7. 

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M 

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9 

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Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-315 t'aga 

Collector TR KLINCKMAN Conaaam Contact Telephone No. Proiect Coordinator 

TILLER, B. JOAN KESSNER 375-4688 KESSNER, JH 

iecl Deshma tion Sapplina Location SAFNo, 

100 & 300 Am Component of the RCBRA Sediment and Ti 1607-D2:1 INVERTEBRATES RC-(M7 

Ice Chest No. Field Logbook No. COA Method of Shinme lat 

^G = e. >- ;I 0 7 EL-1595 BFSRAS6520 FED EX 

Sldsroed To 

EBERLINB SERVICES IONVRJ .0 

Of wile Property No. N 

^^dî^ 

Bill 

of Ladina/Air Bill No. 

SBEOSPC 

POSSIBLE SAMPLE HAZARD&TEMARKS 


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6 

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0 

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Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST IZC-047-317 me , of ! 

Collector tR KLINCKMAN Company ContactTelephone No. Project Coordinator 

TILLER, B. JOAN KESSNER 375-4688 KESSNER, III 

olect Desi gna tion Samolhat Loca tion- SAF No. 

100 & 300 Area Component of the RCBRA Sediment and Tt BORROW Prr 24 INVERTEBRATPS RC-047 

lee Chest No. Fleld Loabook No. COA Method of Shiomcnt 

/fie- 02 - a EL-1595 1 BESRAS6520 FED EX 

Shlemed To OffiRe Ptvnertr No . Bill of Ladine/Air Bill No. 

EBERLWESERVICES IONVILLE â6o3(s^ SEE 

OSPC 

Price Code 9N 

Air Quality D 

Datrl Turmnrmmd 

45 `^^^'$ 

POSSIBLE SAMPLE BAZARDS IREMARKS - —^--- 

POTEA77AL RADIOACTIVE eDOTLfMI7S 

Special Handling and/or Storage 

COOL 4 17 MATRIX COMPOSED OF INSECTS" 

Preservation 


Cww 

No. of Container(s) L 

Volume 

P 

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SAMPLE ANALYSIS t^m`rpne 

Sample No. Matrix • Sample Date Sampk Tin* - `' ' s,:' ' `'' .asx.k'•' ,"''y r^-^ X', - - 

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CHAIN OF POSSESSION rint us 

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( I) ICP Metals - 6010 (Full list) IAlmnnum. Amimony, A rsenic. Dativn A ytlium, Uisnwlh, Uoiun, 

Cadmium Ca lcium Cluornaun. Cobak, Copper. Iron, Ltad, Ufluun t, MagMsiunl M:mgw esc, 

MdybdeoanL Nickel, Phmplarus, Potassium Selcniunl Silicon. Silver, Sodium. Strontium, Thulliwn 

Tin. Usioiwn, Vanadium lire l: Mercury -7171-(CV) 

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LABORATORY 

SECTION 

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Washington Closure Hanford CHAIN OF CUSTODYISAMPLE ANALYSIS REQUEST RC -047-3 1. 8 ; --w a: 

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TII ector l FR B. TR KLINCKMAN Company m Contact Tdeohone No. Protect Coordinator 

)DAN KESSNER 375.4688 KESSNER, III 

Protect Designation Samolhsa Location 


100 A 300 Area Component of the RCBRA Sediment and Ti YAKRNA RIDGE B INVERTEBRATES RC-047 

Ice Cheat No, 

Field Field Logbook No. COA Method of Shipment 

, e —^2 — ^v 

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of Lading/Air I1i ll No. 

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Washington zre Mora CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047 -319 I'ase 1 of ! 

Collector 

TILLER, B. - i-INLSMAN 

JOAN KESSNER 375-4688 KESSNER, IH 

Company Contact Telephone No. Proieet Coordinator 

rolect Designa tion Sampling Lo ca tion SAF No. 

100 & 300 Am Component of the RCBRA Sediment and 11 VERNIPA UPRIVER ON SOUTH SIDE INVERTEBRATES RC-047 

Ice Chest No.^r 

4r1Zl ' 7 

Field L.o¢hook No. 

COA Method or Shipment 

EL-1595 BESRAS6520 FED F-X 

Shipped To Offaite Property No./ Bi ll of Ladino/Air Bill No. 

EBERLINE SERVICES UONVMIE fqa, 0 SEE OSPC 

POSSIBLE SAMPLE HAZARDS/REMAR KS 

POTENTIAL RADIOACTIVE ..1 

Relinquished By/Rensoved From Datdrinic Received By/Stared In Datefrime 

Rchnquislsed By/Rentaved From Datr3rim Received By/St ared In Dale rime 

LABORATORY Received BY Title DaWk w 

SECTION 

FINAL SAMPLE Disposal Medtad Disposed By DateRhua 

DISPOSITION 

BHI-EE-011 (08/29/2005)


;onedor M KLINCKMAN 7 ' ^'• 

TILLER, B. 

'roiecl Designation 

100 & 300 Area Component of the RCBRA Sedim 

ce Cheri No. may,ee 7 

!Z oz - o 

Upped To 

EBERLINE SERVICES WONVILIE 

POSSIBLE SAMPLE RKS 

POTEM/AL RADIOACTIVE

CD 

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0 

0 

0 

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Collector TR KLINCKMAN Company Contact Te)ephoneNo. ProiectCoorditator 

TILLER, R. LOAN KESSNER 375-4688 ^ KESSNER, IH Price Code 9N llata T'u nsnrmu:d 

oieet Designation Samoline Leaders SAF Nu. 

100 A 300 Area Component of the RCBRA Sediment and Ti SADDLE MOUNTA IN INVERTEBRATES RC-047 

Ice Chat No. ^+ 

;L RC' ^Z' 


D 7 ELI595 BESRAS6520 FED EX 

Shipped To 

EBERLBVE SERVIC ONVII LE 

Offaite Property No. 060 3S 

BIB of Lading/Air Bill Nu. 

SEE OSPC 

POSSIBLE SAMPLE RAZARDS/REMARKS --^-- 

POTENTIALRADIOACI7VE

0 

CD 

9 

9 

0 

0 

M 

N 

A 

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-3° tEi`'"° °` 

collector 

TR 

Conmaev Coetaet Tdephone No. Proiect Coordinator 

KLiNCKMAN 

TILLER, B. JOAN KPSSNER 375-4688 KESSNER, IH 

protect Deshmation Sampllrsa Loladw 16pmz- SAY No. 

100 & 300 Area Component of the RCBRA Sediment and Ti INVERTER ATM RC-047 

Ice Chest No. ^2` 02 -^D^ 

F' boo No. COA Method of Miloment 

EL-1595 BESRAS6520 EEDEX 

Shinned To Offshe Pronerty No. H Bi ll of Ladine/Air Bill To. 

EBERLINE SERVICES ONVRLE Ôlvo3,f SEEOSPC 

P rice Code 9N 


POSSIBLE SAMPLE HAZARDSMEMARKS - 

POTEN'TIAL RADIOACTIVE

(D 

9 

C9 

9 

0 

0 

0 

Lg 

N 

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-303irae< _ 

Collector Cerny Contact Telephone No. Proieet Coordinator 

TILLER, B. JOAN KESSNER 375-4688 KESSNER, IH Price Code 9N Dact Tunsarowrd 

roieet Designation Sampling Lo ca tion SAF No. 

rea 

100 & 300 A Component of the RCBRA Sediment and Tit 600.132/600-190 INVERTEBRATES RC-047 

Ice Chest No. ^^,_ OZ ,7 Field Lo[hook No. 

COA Method of SWument 

Z EL, 1595 BESRAS6520 1 

FED EX 

Shlolred To OB+1te Properly No. Bill of Ladin¢/Air Bill No. 

EBERLINE SERVICES LK)NVRLE 6D„^.ff^ SEE OSPC 

POSSIBLE SAMPLE HAZARDS/REMARKS' 

POTEN77ALRADIOAC7WE

(D 

0 

0 

9 

9 

CD 

0 

N 

(r 

Washin¢ton Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-345 i'..ge ! cr 

Comoany Contact T el ephone No. Prolect Coordinator 

Collector 

TILLER, B. TN KuNCKMAN 

JOAN-KESSNER 3754688 KESSNER, IH 

Protect Desimatlon - Sunbathes Location - SAF No. 

100 & 380 Apra Component of the RCBRA Sediment and Ti CENTRAL PLATEAU SHRUB STEPPE INVERTEBRATES RC-047 

Ice Chest No. C 

lroe — ^.1 D 7 

Field Leabook No. COA Method of Shimnent 


Puce Code 91sTDmlm'1`. 1711nround 

Air Quality 0 

45 Days 

Shipped To 

EBERLINE SERVICESONV UAE 

Offstte Property No. 

.gO6Q 

Bi ll of Ladine/Air B ill No. 

SEE OSPC 

POSSIBLE SAMPLE HAZARDS/REMARKS E^ 

POTENTIAL RAOIOAC77VE

i9 

9 

m 

CD 

CD 

9 

N 

v 

Washington Closure Hanford CHAIN OF CUSTO USAWLE ANALYSIS REQUEST RC-047.342 Pa; 1 v ! 

Bedor 

Company 

Tfl KUNCKMAN 

Contact Telephone No. Protect Coordinator 

MIER B JOAN KESSNER 375-4688 KESSNER, JH Price Code 9^r a 

roiecl Dedanation Santana Location SAF No. 

100 & 300 Area Component of the RCBRA Sediment and Ti 600-131 INVERTEBRATES RC-047 

Ice Cheat No. 

IF -'ee - p22- 0' 

Field Leabook No. COA Method of Shipment 

EIA595 BESRAS6520 FED EX 

Air Quality q 

nnh: ratan,-uurd 

45 Days 

Shipped To Offsite P ro perty No. ^J Bi ll 

EBERLINE SERVICES ONVBLE /TO^pO S 

of Lading/Air Bill No. 

SEE OSPC 

POSSIBLE SAMPLE HAZARDS/REMARKS - 

i- 


CD 

0 

9 0 

0 

CD 

6 

N 

Ib 

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047-340 1'av I nl 

Collector 

TN KLINCKMAN Connonr Contact Tdeohone Ne. Project Coordinator 

TILLER, B. JOAN KESSNER 375.4688 KESSNER, JH 

roieet DalEnation SamoBata Loca ti on SAF No. 

100 R 300 Area Complmrnt of the RCBRA Sediment and Ti BORROW Pfl' 23 INVBRTEDRA7FS RC-047 

Im Chat No.p 

g lee, -Q? - O 7 

Field Logbook No. COA Method or Shioment 

EIr1595 BFSRAS6520 FED EX 

Price Code 9\ Dp'1'uroorocnd 

[a 

Air Quality [] 

Shinned To Offshe Proper" No. ^r Diu or LadinE/Air Bill No. 

EBERLWE SERVICESONVILLE SEE OSPC 

POSSIBLE SAMPLE RAZARDWOUSURKS ^^ 

POTFJMAL JZADIOAC77VF.

(D 

G 

9 

M 

9 

CD 

0 

N 

•D 

Washington Closure Hanford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST RC-047 -333 

Collector Comuaas ContactTelephone No. - Project Coordinator 

TILLER, B. NCKMAN JOAN KESSNER 375-4688 KESSNER, JH Price Code 9th 

Data Tnrnasrol:nrt 

,,tt 

lecl Destenation Sampling Location SAF No. 

Air Quality [^ `t1 Days 

160 & 300 Ana Component of the RCBRA Sediment and Ti 116-DR-i. DR-2/ 100-D-22 INVERTEBRATES RC-047 

Ice Chest No. Field Loalaoolt No. COA Method of Shiomcut 

"e-e — OZ -- 7 EL- 1595 BESRAS6520 PFD EX 

Shinned To - Offsite Prooetty No. ^J ` Bill of Ladine/Air Bill No. 

EBERLINE SERVICES UONVn rF {y(/(/D,73 SEE OSPC 

POSSIBLE SAMPLE HAZA ARKS --- 


A 


SAlVIP]C E RECEIPT CHECKLIST (SRQ 

CL NT:^" t1 t f VA 0.c-rCo P Date: 

P)^rcbase Order / Project# / R C-CA7 

L* SOW'S/Release#r: 

C(Yes ONO q No Seals Comments 

i 

CVYes a No 

yes q No 

[3 Cs ONO allo Seals 

1 Yes 17 No 

Yes ONO 

Cf 9. All samples on coc received? A Yes ONO 

ll 

samples 

Yes ONO 

rYa q No 

Yes q No 

a Yes a No 94A 

a Yes ONO 94A 

Yes 13 No 

t^^ Ola 

LvLT Batch # : Sample Custodian: 

0(-0 lSO 

NOTE: EXPLA IN ALL DISCREPANCITS 

1. Samples Hand De livered 



3. Outside of coolers or shipping containers are 





5. Samples receivoled r ambient? 

MR. 

6. Custody seals on sample containers intact, 







12. Samples received within hold t imes? 


13. VOA, TOC, TOX free of hesdspaee? 

14. QC stickers placed on bottles.designated by 

client? 


Policy? (Identify all bottles not with in 


16. Proje ct Manager contacted concerning 

discrepancies? aame/date (or samples 


SR-0o2•B 

V^ 

eX 

a Yes ONO ,p No 

/ Discrepaeties 

Airbill# ' 1 ge3 b'1-1 I ")-k 

Temp 1. 8 °C Cooler # EK4 - 63 • 41^17 

ee0eeoo66

SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

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