SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site
SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site
SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site
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<strong>SAF</strong>-<strong>RC</strong>-<strong>047</strong><br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong><br />
<strong>RC</strong>BRA Sediment and Tissues<br />
FINAL DATA PACKAGE<br />
COMPLETE COPY OF DATA PACKAGE TO:<br />
Jill Thomson HO-23 KW 7/19/06<br />
INIT W UDATE<br />
Jeanette Duncan H9-02 KW 7/19/06<br />
INITIAUDATE<br />
COMMENTS:<br />
SDG K0303 <strong>SAF</strong>-<strong>RC</strong>-<strong>047</strong><br />
Rad only Chem only X Rad & Chem<br />
X Complete Partial<br />
Waste <strong>Site</strong>: 600-132/600-190<br />
1607-H2<br />
116-N-3<br />
1607-D2:1<br />
Borrow Pit 24<br />
Yakima Ridge II<br />
Vernita Upriver on South Side<br />
McGee Ranch<br />
Saddle Mountain<br />
Central Plateau Shrub Steppe<br />
r -),:'03SS<br />
AUG 0 7 2006<br />
EDMC<br />
<strong>100</strong>-D-22<br />
Borrow Pit 23<br />
600-131<br />
<strong>100</strong>-D-48:2<br />
<strong>100</strong>-D-49:2<br />
M
4DIVLI<br />
1<br />
Joan Kessner<br />
WC-<strong>Hanford</strong><br />
3190 Washington Way<br />
MSIN H9-03<br />
Richland, WA 99354<br />
Subject: Analytical Data Package<br />
Dear Ms. Kessner:<br />
VdM<br />
\<br />
N V<br />
Enclosed are <strong>the</strong> hard copy analytical reports for <strong>the</strong> batch number/fraction indicated<br />
(marked X) in <strong>the</strong> following table:<br />
LvLIBatch ................._................................._ # . 06041-904<br />
. ..................._... i. . ..._...... . ............._...._K0303.......<br />
<strong>SAF</strong> # <strong>RC</strong>-<strong>047</strong><br />
lte Received<br />
# Samales.._ ..<br />
Volatiles<br />
Semivolatiles<br />
4/28/06<br />
............._...................1.5..............<br />
SOLID<br />
Pest/PCB<br />
PAH<br />
O/KRO/GRO<br />
........._.......__...._...-.-._._<br />
GC Alcohols<br />
Herbicides<br />
Metals<br />
X<br />
The electronic data deliverable (EDD) will be emailed shortly. If you have any<br />
quest Rns, please don't hesitate to contact me at (610) 280-3012.<br />
OrleM S. Johnson<br />
Project Manager<br />
r.\group\pm\orlette\tnu-hanford\data\b_ltrs. doc<br />
208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-<strong>300</strong>0 • Fax (610) 280-3041
Lionville Laboratory, ry, Inc.<br />
PEST/PCB- ANALYTICAL DATA PACKAGE FOR<br />
TNUHANPORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :060<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
06/02/06<br />
1191920--<br />
N RECEIVED<br />
^^` 206<br />
CLIENT ID LVL # MIX PREP # COLLECTION EXTR /PREP ANALYSIS<br />
J11KK8 001 SO 06LE0455 04/05/06<br />
J11KL5 002 SO 06LE0455 04/05/06<br />
Ji1KL6 003 SO 06LE0455 04/03/06<br />
J11KM0 004 SO 06LE0455 04/05/06<br />
J11K 42 005 SO 06LE0455 04/03/06<br />
J11KM3 006 SO 06LE0455 04/03/06<br />
J11KM4 007 SO 06LE0455 04/03/06<br />
J1iKM5 008 SO 06LE0455 04/03/06<br />
J11KM6 009 SO 06LE0455 04/03/06<br />
J11KV1 010 SO 06LE0455 04/05/06<br />
J1lKV2 Oil SO 06LE0455 04/05/06<br />
J11 1,21 012 SO 06LE0455 . 04/03/06<br />
J11L23 013 SO 06LE0455 04/03/06<br />
JlIL25 014 SO 96LE0455 04/05/06<br />
J11L36 015 '50 06LE0455 04/03/06<br />
JIIL36 015 MS ,$0.061:80455 09/03/06<br />
J11 1,36 015 MSD S0 06180455 ' 04/03/06<br />
LAB OC:<br />
PBLKJM MB1 S 06LE0455 N/A<br />
PBLKJM MB1 HS S 06LE0455 N/A<br />
PBLKJM M131 HS _N/A<br />
L<br />
06/23/06<br />
06/23/06<br />
06/23/06<br />
06/23/OE<br />
06/23/06<br />
06/23/06<br />
06/23/OE<br />
06/23/OE<br />
06/23/06<br />
06/23/OE<br />
06/23/OE<br />
06/23/OE<br />
06/23/OE<br />
06/23/OE<br />
06/23/OE<br />
06/23/OE<br />
06/23/OE<br />
06/23/06<br />
07/07/06<br />
06/23/06<br />
000000001
Case Narrative<br />
Client: TNU-F-IANFORD <strong>RC</strong>-<strong>047</strong> W.O. #: 11343-606-001-9999-00<br />
LVL #: 06041-904 Date Received: 04-28-2006<br />
SDG/<strong>SAF</strong> # K(3303/<strong>RC</strong>-<strong>047</strong><br />
CHLORINATED PESTICIDES<br />
Fifteen (15) solid (composed <strong>of</strong> mice) samples were collected on 04-03,05-2006.<br />
The samples and <strong>the</strong>ir associated QC samples were extracted on 06-02-2006 and analyzed<br />
according to Lionville Laboratory SOPS based on SW846, 3rd Edition procedures on 06-23-2006<br />
and 07-06-2006. The extraction procedure was based on method 3540C and <strong>the</strong> extracts were<br />
analyzed based on method 8081A.<br />
The following is a summary <strong>of</strong> <strong>the</strong> QC results accompanying <strong>the</strong> sample results. Lionville<br />
Laboratory Inc (LvLI) certifies that all test results meet <strong>the</strong> requirements <strong>of</strong> NELAC except as<br />
noted below:<br />
1. All results presented in this report are derived from samples that met LvLI's sample<br />
acceptance policy with <strong>the</strong> exception <strong>of</strong> some discrepancies, which were documented on<br />
<strong>the</strong> Sample Receipt Checklist.<br />
2. The sarnples were received outside extraction holding time. Samples were also extracted<br />
outside holding time due to <strong>the</strong> refrigerator (ID # R003) malfunction. A copy <strong>of</strong> <strong>the</strong><br />
Sample Discrepancy Report (SDR) has been enclosed.<br />
3. The soil sample results were reported on a wet-weight basis. All samples were extracted<br />
using reduced sample volume due to <strong>the</strong> nature <strong>of</strong> <strong>the</strong> sample matrix. A copy <strong>of</strong> <strong>the</strong><br />
Sample Extraction Record has been enclosed.<br />
4. All samples and <strong>the</strong>ir associated QC samples received Florisil and Copper-Sulfur cleanups<br />
according to Lionville Laboratory SOPS based on SW846 methods 3620B and 3660A<br />
respectively.<br />
5. The method blank was below <strong>the</strong> reporting limits for all target compounds.<br />
6. Seventeen (17) <strong>of</strong> forty (40) surrogate recoveries were outside acceptance criteria. A copy<br />
<strong>of</strong> <strong>the</strong> Sample Discrepancy Report (SDR) has been enclosed.<br />
The results presented in this report relate only to <strong>the</strong> analytical testing and conditions <strong>of</strong> <strong>the</strong> samples at receipt and during storage. All pages <strong>of</strong> this report are integral parts <strong>of</strong><br />
<strong>the</strong> analytical data. Therefore, Us report should only be reproduced in its entirety <strong>of</strong> 2 g pages.<br />
208 Welsh Pool Road • Exton, PA 19341- 1313 a (610) 280-<strong>300</strong>0 • Fax (610) 280-3041<br />
8laM1
7. Two (2) <strong>of</strong> twenty (20) blank spike recoveries were outside <strong>the</strong> accept ance criteria in <strong>the</strong><br />
pre-Florisil cleanup fraction. Eleven (11) <strong>of</strong> twenty (20) blank spike recove ries were<br />
outside <strong>the</strong> acceptance criteria in <strong>the</strong> Flo risil cleaned fraction due to <strong>the</strong> cleanup procedure.<br />
A copy <strong>of</strong> <strong>the</strong> Sample Discrep ancy Report (SDR) has been enclosed.<br />
8. Eleven (11) <strong>of</strong> for ty (40) matrix spike recoveries were outside accept ance criteria. A copy<br />
<strong>of</strong> <strong>the</strong> S ample Discrep ancy Report (SDR) has been enclosed.<br />
9. All samples required dilution due to <strong>the</strong> nature <strong>of</strong> <strong>the</strong> sample ma trix and high concentration<br />
<strong>of</strong> non-target analytes. The reporting limits were adjusted to reflect <strong>the</strong> necessary dilution.<br />
10. The initial calibrations associated with this data set were within acceptance criteria.<br />
11. The continuing calibration st andards analyzed prior to sample extracts were within<br />
acceptance crite ria.<br />
12. LvLI is NELAP accredited by <strong>the</strong> state <strong>of</strong> Pennsylv ania and holds over 20 additional state<br />
accreditations. For a complete listing <strong>of</strong> accrediting authorities and <strong>the</strong> corresponding<br />
analytes/methods, ple ase contact your Project Manager.<br />
13. I certify that this sample data package is in compli ance with SOW requirements, both<br />
technically and for completeness, o<strong>the</strong>r than <strong>the</strong> conditions detailed above. Release <strong>of</strong> <strong>the</strong><br />
data contained in this hard-copy data package has been authorized by <strong>the</strong> laboratory<br />
Manager or a designee, as verified by <strong>the</strong> following signature.<br />
nt.iel<br />
J ry M an ager<br />
Lionville Laborato ry Incorporated<br />
som4lgoup\daW\put\NU hanford\0604-904s.pst<br />
208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-<strong>300</strong>0 • Fax (610) 280-3041<br />
3 i^lo^<br />
Date<br />
.88.09801 f
Lionville Laboratory Sample Discrepancy Repo rt (SDR) SDR #: ob ec. IA-41<br />
Initiator. Jo ^%. L--0-- Batch: o b O 4 L qa `t Parameter<br />
Date: "1 l • b Samples: Ppss Matrix:<br />
Client: 1-n .. Method: swwdmcAwwcLpt Prep Batch:<br />
Fri. .<br />
n+oYy<br />
1. Reason for SDR<br />
a. CDC Discrepancy _ Tech P r<strong>of</strong>ile Error Client Request Sampler Error on C-O-C<br />
_ Transc ri p ti on Error _ W ro ng Test Code _ O<strong>the</strong>r<br />
b. General Disc repancy .<br />
_ Missing Sample/Extract _ Container B roken _ Wrong Sample Pulled _ Label ID's I ll egible<br />
_ Hold Time Exceeded _ Insufficient Sample _ Preservation Wrong _ Received Past Hold<br />
Improper Bottle Type _ Not Amenable to Analysis<br />
Note* : Verftd by [Logan] or (Prep Group) (drds)...stgnatureldaw<br />
c. Problem (Include all relevant specific results; attach data if necessary)<br />
SPt,.^PtY 3i t r3<br />
S-f•vscl-vs 21c..^K1.<br />
A ►t;a D» t lt^ ic t ^ gS<br />
SPP.PVtt e c CL 1 11 adT rt cY ♦. mo t a Z<br />
2. Known or Probable Causes(s)<br />
3. Discussion and P roposed Action O<strong>the</strong>r Desc ri p ti on:<br />
_ Re-log<br />
_ Entire Batch<br />
Following Samples:<br />
_ Re-leach<br />
_ Re-extract<br />
_ Re-digest<br />
_ Revise EDD<br />
Change Test Code to<br />
_ Place On/Take Off Hold (circle)<br />
4. Pr eat Manager Instructions ... -^<br />
_ Concur Proposed Action<br />
_ Disagree with P roposed Action; See Instruction<br />
_ Include in Case Narra tive<br />
_ Client Contacted:<br />
Date/Person<br />
_ Add<br />
Cancel<br />
(» 1 ! .<br />
S. Final Action ... slgnatunadate: V NEW O<strong>the</strong>r Explana ti on:<br />
verified re-pog][leach]lextmct][digest][an ( e)<br />
/ Included in Case Narrative<br />
_ Hard Copy CDC Revised<br />
Electronic COC Revised<br />
_ EDD Correc ti ons Completed<br />
When Final Action has been recorded, forward original to CIA Specialist for distribution and filing.<br />
Route Distribut ion <strong>of</strong> Completed SDR Route Distribu ti • Ini<br />
on <strong>of</strong> Completed SDR<br />
ti ator<br />
• Lab General Manager. M. Tay lor<br />
X Project Mgr. Stone/Johnson<br />
Data Management S<br />
_<br />
_ _ Metals: Beegle<br />
_ _ Inorganic: Per rone<br />
_ _ GC/LC: IGger<br />
ti lwell<br />
—<br />
_ MS: Rychlak/Daley<br />
Sample Prep: BeegleNger _ _ Log-in: Per ry<br />
_ _Admin:<br />
O<strong>the</strong>r.<br />
GA-105,A-0805<br />
GO MM
"aw"Vurc L-auvrdwly Qdlliplrd LASGrepollGy mepOrr tzoum)<br />
Initiator. Orlette Johnson Batch: Parameter:<br />
Date: !17 06 Samples: Mat ri x:<br />
Client: t Method: swwerlucnwwicLP/ Prep Batch:<br />
1. Reason for SDR<br />
a. COC Discrepancy _ Tech P r<strong>of</strong>ile Er ror Client Request Sampler Error on C-O-C<br />
Transcription Error _ Wrong Test Code _ O<strong>the</strong>r<br />
b. General Discrepancy<br />
_ Missing SampVEx tract _ Container B ro<br />
ken _ Wrong Sample Pulled _ Label ID's Illegible<br />
Hold Time Exceeded<br />
_ Improper Bottle Type<br />
Insufficient Sample<br />
_ Not Amenable to Ana lysis<br />
Preservation Wrong<br />
X O<strong>the</strong>r<br />
— Received Past Hold<br />
Note: Verified by [Log4n] or [Prep Group] (circle)... signature/date:<br />
c. Problem (Include all relevant specific results; attach data if necessa ry)<br />
On 5110!06 sample storage refrigerator ID# R003 malfunctioned and was not holding <strong>the</strong> required sample storage<br />
temperatu re <strong>of</strong> 4°C +/- 2'C<br />
2. Known or Probable Causes(s)<br />
Broken motor<br />
3,. Discussion and P roposed Action O<strong>the</strong>r Description:<br />
_ Re4og At <strong>the</strong> time <strong>of</strong> malfunc tion R003 was used for storage <strong>of</strong> samples received<br />
_ En tire Batch for extractable organics, metals and wet chemist ry (except TOC) analyses.<br />
Following Samples: All samples were removed fr om R003 to ano<strong>the</strong>r refrigerator on 5/<strong>100</strong>6.<br />
_ Re Aeach R003 was tagged out on 5/10/06, repaired on 5/12/06, and we have<br />
_ Re-extract certified that R003 Is maintaining <strong>the</strong> required sample storage temperatu re.<br />
_ Re-digest<br />
Revise EDD<br />
— Change Test Code to<br />
_ Place OnlTake Off Hold (cir cle)<br />
4. Project Manager Instructions ... signature/daw<br />
Concur with Proposed Action<br />
sagree with Proposed Ac ti<br />
on; See Instruction<br />
clude in Case Narrative<br />
Client Conta<br />
Date/Person<br />
_ Add'<br />
Cancel<br />
5. Final Action ... signature/date:<br />
6/^`^^<br />
414110 O<strong>the</strong>r Explana ti _ enfied re-{log][leach][extract][digest][an<br />
Included in Case Narrative<br />
_ Hard Copy COC Revised<br />
Electronic COC Revised<br />
_ EDD Corrections Completed<br />
on:<br />
When Final Action has been recorded, forward original to QA Specialist for distribution and filing.<br />
Route Distribu ti<br />
on <strong>of</strong> Completed SDR Route Distribu ti<br />
X Initiator<br />
X Lab Manager. I. Daniels<br />
X Project Mgr. Stone/Johnson<br />
Data Management: Stilwell<br />
_ Sample Prep: BeegleNger<br />
on <strong>of</strong> Completed SDR<br />
_ _ Metals: Welsh<br />
Inorganic: Perrone<br />
_ GC/LC: Kiger<br />
_ MS: Schneider/Daley<br />
— _ Login: Per ry<br />
Admin:<br />
— O<strong>the</strong>r<br />
NM1 05-A-0805<br />
999000905
vLI<br />
DATA QUALIFIERS<br />
GLOSSARY OF DATA<br />
U = Indicates that <strong>the</strong> compound was analyzed for but not detected. The minimum detection limit for <strong>the</strong><br />
sample (not <strong>the</strong> method detection limit) is reported with <strong>the</strong> U (e.g., l0U).<br />
B<br />
E<br />
= Indicates an estimated value. This flag is used in cases where a target analyte is detected at a level<br />
less than <strong>the</strong> lower quantification level. if <strong>the</strong> limit <strong>of</strong> quantification is 10 ug/L and a concentration<br />
<strong>of</strong> 3 ug/L is calculated, it is reported as 3J.<br />
I = Interference.<br />
I<br />
ABBREVIATIONS<br />
This flag is used when <strong>the</strong> analyte is found in <strong>the</strong> associated blank as well as in <strong>the</strong> sample. It<br />
indicates possiblelprobable blank contamination.<br />
Indicates that <strong>the</strong> compound was detected beyond <strong>the</strong> calibration range and was subsequently<br />
analyzed at a dilution.<br />
Indicates an interference on one analytical column only. Result is reported from remaining analytical<br />
column.<br />
BS = indicates blank spice in which reagent grade water is spiced with <strong>the</strong> CLP matrix spicing solutions<br />
and carried through all <strong>the</strong> steps, in <strong>the</strong> method. Spice recoveries are reported.<br />
BSD = Indicates blank spike duplicate.<br />
MS<br />
MSD =<br />
DL<br />
NA<br />
Indicates matrix spike.<br />
Indicates matrix spice duplicate.<br />
Indicates that recoveries were not obtained because <strong>the</strong> extract had to be diluted for analysis.<br />
Not Applicable.<br />
DF z Dilution Factor.<br />
NR<br />
NS<br />
Not Required.<br />
Not Spired.<br />
SP = Indicates Spiked Compound.<br />
P = This flag is used for an PESTICIDE/PCB target analyte when <strong>the</strong>re is greater than 25%<br />
difference for detected concentrations between <strong>the</strong> two GC columns (see Form JQ. The<br />
lower <strong>of</strong> <strong>the</strong> two values is reported on Form I and flagged with a 'T".<br />
D = T'his flag identifies all compounds identified in an analysis at a secondary dilution factor.<br />
C = This flag applies to a compound that has been confirmed by GUMS.<br />
NPM =<br />
No pattern match for multi-component target analytes.<br />
000000006
uaVU^aaa pYVapYVa7, 11,Y•<br />
Pesticide/PCBs by GC, CLP List Report Date: 07/07/06 15:01<br />
RFW Batch Number: 0604L904 Client• TNURANFORD <strong>RC</strong>-<strong>047</strong> K0303 Work Order: 11343606001 Page: 1<br />
Cust ID: J11KK8 Ji1KL5 J11KL6 J11KM0 J11KM2 J11KM3<br />
Sample RFW#: 001 002 003 004 005 006<br />
Information Matrix: SOLID SOLID SOLID SOLID SOLID SOLID<br />
D.F.: 4.00 4.00 4.00 4.00 4.00 4.00<br />
Units: UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG<br />
Surrogate: Tetrachloro -m-xylene 139 * t 110 t 159 * $ 108 t 153 * t 114 t<br />
Decachlorobiphenyl 124 * t 102 t 138 * t 97 t 125 * 97 t<br />
........... ---------°_______________°_....... fl ........ ====fl= ........ ===fl====—= .... fl.'"==_=`===fl==.=_ ....... f 1<br />
Alpha - BHC 20 U 18 U 16 U 18 U 14 U 18 U<br />
gamma - BHC (Lindane) 20 U 18 U 16 U 8.8 J 14 U 18 U<br />
Beta-BHC 20 J 18 U 20 18 U 14 U 64 I<br />
Heptachlor 19 J 18 U 16 U 18 U 14 U 18 U<br />
Delta-BHC 20 U 18 U 16 U 18 U 18 18 U<br />
Aldrin 16 J 18 U 18 17 J 16 11 J.I<br />
Heptachlor epoxide 20 U 18 U 16 U 18 U 14 U 18 U<br />
gamma-Chlordane 20 U 18 U 16 U. 18 U 14 U 18 U<br />
Endosulfan i 20 U. 18 U 16 U 18 U 14 U 12 J<br />
alpha -Chlordane 20 D . 18 U 16 U 18 U 14 U 18 U<br />
4,4'-DDS 20 U _ 18 U 16 U 18 U 14 U 18 U<br />
Dieldrin 20 U 18 U 16 U 18 U 14 U 18 U<br />
Endrin 20 U 18 U 16 .0 18 U 14 U 18 U<br />
4,4'-DDD 20 U 18 U 16 U 18 U 14 U 18 U<br />
Endosulfan II 20 U 18 U 16 U .18 U 14 U 18 U<br />
4,4'-DDT 20 U 18 U 16 U 18 U 11 J 18 U<br />
Endrin aldehyde 20 U 18 U 16 U 18 U 14 U 18 U<br />
Endosulfan sulfate 20 U 18 U 16 U 18 U 14 U 18 U<br />
Methoxychlor 20 U 18 U 16 U 18 U 14 U 18 U<br />
Endrin ketone 20 U 18 U 16 U 18 U 14 U 18 U<br />
Toxaphene 200 U 180 U 160 U 180 U 140 U 180 U<br />
U= Analyzed, not detected. J- Present below detection limit. B = Present in blank. NR= Not reported. NS. Not spiked.<br />
t= Percent recovery. D. Diluted out. I- Interference. NA= Not Applicable. *= Outside <strong>of</strong> EPA CLP QC<br />
ti<br />
m
A.ionv", a a,auuracury, iuc.<br />
Pesticide/PCBs by GC, CLP List Report Date: 07/07/06 15:01<br />
RFW Batch Number: 0604L904 Client: THURANFORD <strong>RC</strong>-<strong>047</strong> X0303 work Order: 11343606001 Page: 2<br />
Cust ID: J11KM4 J11KN5 J11KM6 JllKV1 JllKV2 J11L21<br />
Sample RFW#: 007 008 009 010 011 012<br />
Information Matrix: SOLID SOLID SOLID SOLID SOLID SOLID<br />
D.F.: 4.00 4.00 4.00 4.00 4.00 4.00<br />
Units: UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG<br />
Surrogate: Tetrachloro-m-xylene 122 * t 104 t 173 * t 177 * t 200 * t 124 * k<br />
Decachlorobiphenyl 101 t 92 t 143 * t 140 * t 155 * t 96 t<br />
---__...... °__ ......... _________ .......... ___f1 ...... _===== f1=====__=====fl=====_...... fl ...........= f1=====__=====f1<br />
Alpha-BHC 20 U 15 U 14 U 18 U 14 U 19 U<br />
gamma-BHC (Lindane) 20 U 15 U 7.3 J 18 U 15 J 19 U<br />
Beta-BHC 46 19 .1 44 51 38 .I 16 J.I<br />
Heptachlor 20 U 15 U 14 U 18 U 14 U 19 U<br />
Delta-BHC 12 J 15 U 14 U 40 14 U 19 U<br />
Aldrin 12 J 15 J 14 U 14 28 19 U<br />
Heptachlor epoxide 20 U 15 U 14 U 18 U 14 U 19 U<br />
gamma-Chlordane 20 U 15 U . 14 D 18 U 14 U 19 U<br />
Endosulfan I 20 U 15 U 14 U 18 U 9.8 J 19 U.<br />
alpha-Chlordane 20 U 15 U 14 U 18 U 14 U 19 II,<br />
4,4'-DDE 20 U 15 U 14 U 12 J 14 U 19 U.<br />
Dieldrin, 20 U i5 II 14 II 18 U 14 U 19 U:<br />
Endrin 20 U 15 U 14 U 18 U 14 U 19 U<br />
4,4'-DDD 20 U 15 II .". 14 II _18 U I 19 U.<br />
Endosulfan II 20 U 15 U 14 U 18 U 14 U 19 U<br />
4,4'=DDT 20 U 10 J 14 U 18 U 19 19 U<br />
Endrin aldehyde 20 U 15 U 14 U 18 U 14 J.I 19 U<br />
Endosulfan sulfate 20 U 15 U 14 U 18 U 14 U 19 U<br />
Methoxychlor 20 U 15 U 14 U 32 14 U 19 U<br />
Endrin ketone 20 U 15 U 14 U 18 U 14 U 19 U<br />
Toxaphene 200 U 150 U 140 U 180 U 140 U 190 U<br />
U- Analyzed, not detected. J. Present below detection limit. B= Present in blank. NR= Not reported. NS= Not spiked.<br />
V- Percent recovery. D- Diluted out. I. interference. NA. Not Applicable. *= Outside <strong>of</strong> EPA CLP QC<br />
4<br />
m<br />
M<br />
M<br />
m
uiuura W ua Wv 06Vcy, auc.<br />
Pesticide/PCBs by GC, CLP List<br />
Report Date: 07/07/06 15:01<br />
RFW Batch Number • 0604L904 Client-, TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303 Work Order- 11343606001 Page-, 3<br />
Sample<br />
Information<br />
Cust ID:<br />
RFW#:<br />
Matrix:<br />
D.F.:<br />
JIIL23<br />
013<br />
SOLID<br />
4.00<br />
JIIL25<br />
014<br />
SOLID<br />
4.00<br />
J11L36<br />
015<br />
SOLID<br />
4.00<br />
J11L36<br />
015 MS<br />
SOLID<br />
4.00<br />
J11L36<br />
015 MSD<br />
SOLID<br />
4.00<br />
PBLKJM<br />
06LE0455 -MIDI<br />
SOIL<br />
1.00<br />
m<br />
mm<br />
m<br />
Units: UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG<br />
Surrogate: Tetrachloro-m-xylene 81 % 133 * $ 116 % 117 $ 149 * $ 113 $<br />
Decachlorobiphenyl 67 $ 109 $ 87 $ 90 $ 135 * $ 97 $<br />
............................................. fl== ---------- fl ..... __=.... fl ... ==__=====fl== = ......... fl ............ fl<br />
Alpha-BHC 16 U 16 U 17 U 76 t 91 $ 0.33 U<br />
gamma-BHC (Lindane) 7.9 J.I 16 U 17 U 91 $ 112 $ 0.33 U<br />
Beta-BHC 46 .I 14 J 17 U 91 % 119 $ 0.33 U<br />
Heptachlor 16 U 16 U 17 U 99 $ 116 $ 0.33 U<br />
Delta-BHC 16 U 16 U 17 U 68 $ 64 $ 0.33 U<br />
Aldrin 16 U 16 U 17 U 90 $ 119 % 0.33 U<br />
Heptachlor epoxide 16 U 16 U 17 U 93 $ 113 $ 0.33 U<br />
gamma-Chlordane 16 U 16 U 17 U 84 $ 119 $ 0.33 U ..<br />
Endosulfan I 16 U 16 U 17 U 94 $ 136 * $ 0.33 U<br />
alpha-Chlordane 16 U 16 U 17, U 94 $ 132 * $ 0.33 U<br />
4,4'-DDE 16 U 16. U 17 U 95 V 141 * $ 0.33 U<br />
Dieldrin 16 U 16 U 17 U 91 $ 132 * % 0.33 T ...<br />
Endrin 16 U 16 U 17 U 111 _ $ 157 * $ 0.33 U<br />
4;4'-DDD 16 U 16 U 17 ,U 102 t 197 *. % 0.33 U<br />
Endosulfan II 16 U 16 U 17 II 94 $ 134 *$ 0.33 U<br />
4,4'-DDT 16 U 16 U 17 U 79 $ 43 $ 0.33 U<br />
Endrin aldehyde 16 U 16 U 17 U 10 * % 5 * $ 0.33 U<br />
Endosulfan sulfate 16 U 16 U 17 U 58 * t 28 * $ 0.33 U<br />
Methoxychlor 16 U 16 U 17 U 107 $ 75 $ 0.33 U<br />
Endrin ketone 16 U 16 U 17 U 79 $ 72 $ 0.33 U<br />
Toxaphene 160 U 160 U 170 U 180 U 180 U 3.3 U<br />
U- Analyzed, not detected. J- Present below detection limit. B- Present in blank. NR. Not reported. NS= Not spiked.<br />
$. Percent recovery. D. Diluted out. I= Interference. NA. Not Applicable. *- Outside <strong>of</strong> EPA CLP QC<br />
m<br />
CD
Pesticide/PCBs by GC, CLP List Report Date: 07/07/06 15:01<br />
RPW Batch Number, 0604L904 Client: TNMLUMORD <strong>RC</strong>-<strong>047</strong> K0303 Work Order- 11343606001 Page r 4<br />
Cust ID: PBLKJM BS PBLKJM BS<br />
Sample RFW#: 06LE04SS -MB1 06LE0455-MB1<br />
Information Matrix: SOIL SOIL<br />
D.P.: 1.00 1.00<br />
Units: UG/KG UG/KG<br />
Surrogate: Tetrachloro-m-xylene 82 $ 94 $<br />
Decachlorobiphenyl 90 t 98 t<br />
.............. ...=...... --- _____________===== fl==........ ..f1-...=__=====fl=====_......fl............ fl .... ........ fl<br />
Alpha-BHC 62 $ 95 $<br />
gamma - BHC ( Lindane) 53 t <strong>100</strong> $<br />
Beta-BHC 25 * $ 106 $<br />
Heptachlor 75 $ 91 %<br />
Delta-BHC 4 * $ 103 t<br />
Aldrin 77 $ 90 $<br />
Heptachlor epoxide 35 * t 95 $<br />
gamma-Chlordane 64 $ 102 $<br />
Endosulfan I 35 * t 106 t<br />
alpha-Chlordane 73 t 99 $<br />
4,4'-DDE 84 t 125 * t<br />
Dieldrin 16 * t 101 t<br />
Endrin 19 * t 101 $<br />
4,4'-DDD 69 $, 142 * t<br />
Endosulfan II 5 * $ 101 t<br />
4,4'-DDT 77 t 141 $<br />
Endrin aldehyde 5 * t 95 t<br />
Endosulfan sulfate 3 * $ 107 %<br />
Methoxychlor 20 * t 165 $<br />
Endrin ketone 4 * t 109 %<br />
Toxaphene 3.3 U 3.3 U<br />
U. Analyzed, not detected. J= Present below detection limit. B. Present in blank. NR= Not reported. NS= Not spiked.<br />
%. Percent recovery. D= Diluted out. I. Interference. NA. Not Applicable. *= Outside <strong>of</strong> EPA CLP QC<br />
P<br />
1^1 ^<br />
m<br />
m
Lionville Laboratory, Inc.<br />
Extract. Date: 06/02/06<br />
Test: 0606<br />
LIMS Report Date: 06/22/06<br />
SAMPLE EXTRACTION RECORD<br />
Extraction Batch No: 06LE0455<br />
Cleanup Date: 06/21/06<br />
Solvent: DCM,HEXANE<br />
Analyst: MF<br />
Analyst: EL<br />
Sheet no.: 1<br />
Method: **** ^' 0^3^0 m M<br />
Client: TNUHANFORD <strong>RC</strong>- <strong>047</strong> K0303 m M<br />
Adsorbent: FLORS m<br />
Client Name Initial Surr. Spike Final Fins bplit uec: a U/u<br />
Sample No: Client ID WT/VOL Mult. Mult. VOL VOL Mult. YIN Solids FACTOR<br />
0604L904- TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
001 H J11KK8 2.0 1.0 10 1.0 N 5000.0<br />
002 H J11KL5 2.20 1.0 10 1.0 N 4545.4<br />
003 H J11KL6 2.56 1.0 10 1.0 N 3906.2<br />
004 H J11KM0 2.17 1.0 10 1.0 N 4608.3<br />
005 H JllKM2 2.86 1.0 10 1.0 N 3496.5<br />
006 H J11KM3 2.18 1.0 10 1.0 N 4587.2<br />
007 H JllKM4 2.00 1.0 10 1.0 N 5000.0<br />
008 H J11KM5 2.67 1.0 10 1.0 N 3745.3<br />
009 H J11KM6 2.86 1.0 10 1.0 N 3496.5<br />
010 H J11KV1 2.19 1.0 10 1.0 N 4566.2<br />
011 H J11KV2 2.86 1.0 10 1. 0 N 3496.5<br />
012 H JlIL21 2.15 1.0 10 1.0 N 4651.2<br />
013 H J11L23 2.52 1.0 10 1 .0 N 3968.2<br />
014 H JlIL25 2.50 1.0 10 1.0 N 4000.0<br />
015 H JllL36 2.30 1.0 10 1.0 N 4347.8.<br />
015 HS J11 1, 36 2.18 1.0 1.0 30 1.0 N 0.0 4587.2<br />
015 HT JlIL36 2.18 1.0 1.0 10 1.0 N 0.0 4587.2<br />
06LE0455-MB1 H PBLKJM 30.0 1.0 10 1.0 N <strong>100</strong>.00 333.3<br />
06LE0455-MB1 HS PBLKJM 30.0 1.0 1.0 10 1.0 N <strong>100</strong>.00 333.3<br />
Comments:<br />
Surrogate: 250 UL OLM PSURR 89915602<br />
Spike: 250 UL FULL LIST PEST SPIKE 89915001B<br />
s Transferred Relinquished By Date Time Received By Date Time Reason for Transfer {
Lionville Laborato ry Use Only<br />
1 p Lci()<br />
Custody Transfer Record/Lab Work Request Page t <strong>of</strong> a 101vLl<br />
FIELD PERSONNEL: COMPLETE ONLY SHADEDYEAS<br />
^1<br />
See S<strong>RC</strong><br />
Client 714Lk 1-6 ey(-0rp gc-o47<br />
Est. Final P ro). Sampling Date<br />
Refrigerator)<br />
I/rype C<br />
- m<br />
on /<br />
Project# /LAG?(^^i^^ ^^'W`7 '^^<br />
Project Contact/Phone #<br />
tainer<br />
Volume<br />
Liquid<br />
L17uld<br />
Bond<br />
arm<br />
m<br />
Lionville Laborato ry Project C 1 ^Manager<br />
QC "^ Del J ,TAT l.c, D<br />
Date Recd Lk ,d 8-0(, Date Dus ^' r" ,^.<br />
Preservatives -^^<br />
ANA LYSES<br />
REQUESTED -^ O<br />
><br />
OR<br />
Q<br />
Z<br />
In<br />
NI<br />
m a<br />
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2<br />
2<br />
-<br />
MATRIX<br />
1 Lionville Laboratory Use Only j<br />
CODES:<br />
Melrla<br />
Date Time<br />
n<br />
S - Son Lab<br />
OC Matrix<br />
Client ID/Description<br />
Chosen<br />
Collected Collected h<br />
SE - Sediment ID<br />
so - Sans<br />
t31<br />
c^ ^^ <<br />
1^<br />
SL. Sludge<br />
CL<br />
W. Water MS I MSD<br />
O<br />
C<br />
0- Oil<br />
Air<br />
A-<br />
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Drum<br />
Salida<br />
DL • Drum<br />
1 y'S' x<br />
V<br />
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L • EFfrC.P<br />
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F. Fish<br />
w<br />
m<br />
a a<br />
la<br />
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x X<br />
X<br />
/^<br />
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X<br />
X<br />
mi<br />
J 5<br />
j t VnLo<br />
^(<br />
X A<br />
X<br />
x X<br />
Special Instruction:<br />
o to J x x x<br />
}C^4.1" D NS:<br />
1 v<br />
^....- n V r -A'00 1. MAI V ca) C<br />
i^ t'1i^1 Ct,o p^,r3^ 0.Y. ^e -^5t, z.<br />
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PCB, PrS4 Sdoc . Kc^'tjJ^/iA7RtX`— n.<br />
Re li nqu ished<br />
by<br />
Roe~<br />
by<br />
Dale Z<br />
Relinquished<br />
by<br />
Received<br />
M<br />
two Time<br />
Relinquishedd<br />
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by<br />
Received<br />
by<br />
Date Time<br />
x<br />
^^ aYo Zrl3 %; r<br />
WASTER<br />
m
I<br />
Lionville Laborato ry Use Only<br />
b<br />
Client I J<br />
Custody Transfer Record/Lab Work Request Page <strong>of</strong> ---;I-<br />
FIELD PERSONNEL: COMPLETE ONLY SHADED AREAS<br />
Refrigerator #<br />
Est. Final P rol. Sampling Date<br />
Project #<br />
Project Contact/Phone #<br />
A<br />
_..<br />
C<br />
NRype Comeiner<br />
Volume<br />
Liquid<br />
Lionville Laborato ry Proj<br />
OC Del<br />
anger A-06<br />
TAT<br />
Prcservetivee<br />
Sd lid<br />
Liquid<br />
I<br />
IVIVLi M<br />
Sad m<br />
ORGANIC INORG<br />
Date Recd Date Due<br />
ANALYSES<br />
REQUESTED —^ p<br />
><br />
Z<br />
CO 0-<br />
p<br />
_<br />
m<br />
Mm<br />
V<br />
Z<br />
j IJemiils laborato ry Use Only 1<br />
MATRIX<br />
CODES:<br />
9 - 505 Lab<br />
SE- Sedime nt 10<br />
SO - So<br />
Client ID/Deacnptlon<br />
Matrix<br />
QC<br />
Chosen<br />
(^<br />
Meolx<br />
Dale Time<br />
Colleted Collected 4'<br />
U)<br />
-^<br />
L',o<br />
^C1<br />
VT<br />
^'<br />
li<br />
d<br />
SL- Sludge<br />
W- Water<br />
D.<br />
% t<br />
Cl-<br />
D5<br />
MS I MSD<br />
O 0<br />
C<br />
A - Air nil, J11y a<br />
DS. Drum<br />
solids<br />
DL- Drum<br />
Liquids<br />
L- EPflCLP<br />
Leaalate<br />
06L ,) I<br />
J1 L 13<br />
s- S0 0<br />
X<br />
X<br />
X "<br />
X X<br />
X- ^<br />
F- Fish<br />
Specia l Instruction:<br />
015 J 11-x(0 ojs X ?^ X<br />
DATEIREVISIONS:<br />
c^° ra y%, '<br />
I ^_• =(^^ RISC-tY^, (^^' ^ r ^ c ^ c<br />
J ) / L^ 3.<br />
RsUnquiehad ReexNad<br />
Ralingtdehad ReaeWitt!<br />
DateTim<br />
Thee<br />
ReUrtqulshod Retxdved<br />
by by by by by by<br />
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e.<br />
5.<br />
6.<br />
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0<br />
9<br />
m
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODYISAMPLE ANALYSIS REQUEST <strong>RC</strong>"<strong>047</strong>-259<br />
Po L or 1<br />
Collector<br />
Company ContactTelephone No. Protect Coordinator<br />
TR NLINCI(MAN<br />
Pelee Code 9]v Data Turnaround<br />
TILLER, B. JOAN KFSSNER 375.4688 KESSNER, JH<br />
Proiect Desianadon Sampling Location <strong>SAF</strong> No. Air Quality q 45 Days<br />
loo & <strong>300</strong> Are <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti 600-13216OD-190 OFFAL <strong>RC</strong>-<strong>047</strong> m<br />
lee Chest No Field Logbook No. COA Method <strong>of</strong> Shipment m<br />
g;ee QZ ^D,J — EL-1595 BESRAS6520 FED ESC l9<br />
Shipp Offsite Property No.2 ^O^,s>, ? BL L g/Air 111111I No.<br />
E .LINE SERVICES LIONVIILE<br />
V.7 J SEE PC<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOAC77VE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-266 PW I <strong>of</strong> 1<br />
Collector Conmany Contact TdeOBone No. Protect Coordinator<br />
fee<br />
TRIER, B. TR KLIN K JOAN KESSNER 375.4688 KESSNER, III<br />
Price Code Data Thrnaund in<br />
9N ro<br />
45 Days m<br />
leer Deshmation<br />
Semolina I.aeaBon<br />
$AF No.<br />
Air Quality<br />
<strong>100</strong> d: <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti IBB^IFdb OFFAL ^G D 7—//Z<br />
<strong>RC</strong>-<strong>047</strong><br />
m<br />
9<br />
No. y^L, Flel k No. COA Method <strong>of</strong> Shipment<br />
m<br />
111.11595 I595 BPSRA56520 FED Px m<br />
SI Oftaite Properly No. ^O^O^ 2Q BI Bill <strong>of</strong> Ladisu/Alr Bill No.<br />
EBEKLINE LIONVI t n ` 7 SEE OSPC<br />
PO EIJAZARDSMEMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>•<strong>047</strong>-267 I PASO I <strong>of</strong> 1<br />
Collector<br />
T[tSER, B. TR KLINCKMAN<br />
Company Contact<br />
LOAN KESSNER<br />
Telephone No.<br />
3 15-1688<br />
Protect Coordio.tor<br />
KESSNER, JH Prim Codt 9N Data 1Lrnatrounl^<br />
Air Quality q 45 Days<br />
lect Designa ti on Sa Hxw Lamson SAY No.<br />
<strong>100</strong> A <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti'. 116-N-3 OFFAL <strong>RC</strong>-<strong>047</strong> m<br />
r<br />
Ice Chest No- Field t.oehook Na COA Method <strong>of</strong> Shiasssml 0<br />
Shipp<br />
ER2 SERVICES LIONVI 1 F<br />
POSSIBLE SAMPLE HAZARDS MFMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-271 j Pw I <strong>of</strong> I<br />
onectar<br />
TR.LER, B. TR NLIN<br />
^rolect Draienaaon<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Ice Cheat No.r<br />
t^,eC'<br />
SI<br />
BEdR ESERV L10NVnJC<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOAC77VE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>473 I NP I at l<br />
Collector<br />
Company Conta<br />
TN KLINCKMAN<br />
ct Tel ep hone No. Protect Coordi nator 00<br />
Price Code 9N Data Turnarm-st<br />
TILLER, Bt JOAN KESSNER 375-MBB KESSNER. IH<br />
rolecl Dex^nW on Sawnslin se Location <strong>SAF</strong> No. Air Quality q 45 Day,<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti BORROW PIT 24 OFFAL <strong>RC</strong>-<strong>047</strong> ,D<br />
Field Loabook No. COA Method <strong>of</strong> Shioment - m<br />
Ice Chest No.<br />
xee- ,Z ',3Q,,f^<br />
El, 1595 BESRAS6520 FED EX m<br />
Shipp Ofls1k Property Na / Bi ll orLadiuWAtr Bill No,<br />
ERUNESERVIM UONVILLE 60 ,3 SEEOSPC<br />
POSSIBLE SAMPLE IiAZARDS/REMARKS<br />
POTEN77ALRADIOACTIVE .DOTIJUITS<br />
Preservation<br />
-<br />
Special handling and/or Storage<br />
Type <strong>of</strong> Container<br />
COOL 4C "MATRIX COMPOSED OF MICE"<br />
No. <strong>of</strong> Conlalner(s)<br />
SAMPLEANALYSIS<br />
Volume<br />
Is_r-164 W 3c 3<br />
Samp le No. Mat ri x • Samp le Date Samp le Time - ,; .. 1,. -.<br />
Coal 4C NO. Car14C Cod IC Cwl4C 0ae14C<br />
aG G/P a? aG aG AG<br />
I 1 0 0 0 0<br />
_2509 109 Ise Sells 509 50g<br />
See ram(1)u Seesm(Dsr Saaon(3)1n PIs-1012 Pwkides . sm-VOAsms<br />
W1W Slacbl ant 9270A rTCL)<br />
Inmanbna Inamlim.<br />
J11KM2 OTHER SOLID Q 3 Z5,& X +X '<br />
18W V<br />
. _ V,_ WW lit_<br />
CHAIN OF POSSESSION<br />
Relinquished By/Remwed from,y<br />
E•as L e/<br />
'nnui i C'icw<br />
Doe/17me<br />
GeV-^i 3o<br />
Date/fine<br />
Sisnmrint Nam es<br />
Ell d In<br />
S<br />
eive y/Srared In<br />
Dat^me<br />
p<br />
Dm^nn<br />
w<br />
SPEC IAL INSTRUCTIONS<br />
NOTE: FLerane- perform Gamlm Spec Wen auubip b attle to tionvilk La bs, if pmsible nainam 4 C<br />
cooky. liowilkt patpmneu4.PCB,PFST,SVOC In this ade'aa rxrpleu avaiYIs Caranct Joan<br />
Kaaaaer upon reeeipl.<br />
Matrix<br />
srnhd<br />
1<br />
su<br />
^+•<br />
Relinquished By snowd From<br />
^1 /,TOO<br />
D ae<br />
^EU<br />
ltcciwd By/Sk n<br />
AA<br />
(1)Ganarw Spw-tpulllisi)IAerericiom241,Animooy-125,Berylaum7,Ccsiuw134,Cesium-137,<br />
CaWlt-60.Emapi IS'IEmvpiam154,Evopinm.ISS,Pdmiurn40,Radmm-224,Radim 329.<br />
W.<br />
m'' w li B e dprom -<br />
-^L<br />
clinquisled By/Rcnvwd From<br />
D"^'ne<br />
DatrJFime<br />
Rec ' B<br />
Received By<br />
In<br />
In<br />
y^U<br />
1 7-y.+10<br />
;7<br />
130 ore<br />
.0`<br />
DotHFbre<br />
RulerdurnlOb. Urasawn- 235. (lanum2391<br />
(2) SUmsiu 89.90 - TOW Sr; hmopic; TbrAan ( T7nr unr232); Isotop ic Unnium I Unnium23323J.<br />
Ummuro-235. U sasft -2391: hmpie o ROroaitan<br />
(3) ICP Mwh -6010 tFUR tm) lAlu ii inum. Animooy. Anenk. Barium Beryl) wm Bisnuolt annual<br />
Cadmium. Cakimlt Owoesimn Cobalt Copper. Ivan. Lcad. fidwaR Magnesium Manganese,<br />
Molybdenum Nickel, Plospborus, Patassiorn Seknlum SWCOW, Silt y, Sodium Swmhmt TMl9u 111.<br />
Ten, Unnis m. Vanadium, Zinc); Mercu ry - 7471 - (CV)<br />
MasprsdW<br />
rat u. Lam,<br />
r•TI.^*<br />
WW'.<br />
ubwa<br />
a.V" .a<br />
X.<br />
Relinquished ByrRemaved From Duerr," Received aylSiomd in Dolarkre<br />
S e^/^ -( )c-G ^' C) 7)<br />
LABORATORY<br />
SECTION<br />
Rceived By Title •l'C<br />
Dale/linx,<br />
FINALSAMPLE Dirpaal McdW Disposed By Dare fine<br />
DISPOS IT ION<br />
SHI-EE-0 11 (08129/2005)
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-274 Par I a L<br />
Rector<br />
TILLER, B. TR KLINCKMAN<br />
Company Contact<br />
JOAN KESSNER<br />
Telephone No.<br />
375-4688<br />
Protect Coordinator<br />
KESSNER. IN Price Code 9N<br />
o+<br />
Data Turaarour^<br />
rolecl Deaianation Samulins Location <strong>SAF</strong> No.<br />
<strong>100</strong> & <strong>300</strong> Am <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti YAKIMA RIDGE 11 OFFAL <strong>RC</strong>-<strong>047</strong><br />
Ice Chest No.<br />
D2:Saf<br />
Air Quality C]<br />
45 Day m<br />
Field Logbook No. COA Method <strong>of</strong> Sldoment m<br />
EL- 1595 BESRAS6520 FEDP.X m<br />
hinned TA OffAtc Property No. OO^O 7 ^ n BID <strong>of</strong> LadindAir BIII No.<br />
BERU NESERVIC LK)NVILE /y 7 v SEE OSPC<br />
POSSIBLE SAMPLE IIAZARDS/REMARKS<br />
POTENTIAL RADIOA C77VE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-275 wp I <strong>of</strong> L<br />
Collector<br />
T ILLER, B. TR KLINCKMAN<br />
roiect Deslanation<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Ice Chest No. p<br />
02 -^ S<br />
S I<br />
BEIdN RESBRViCFS ONVRIE<br />
POSSIBLE SA ZARDS/REMARKS<br />
P07ENTMLRADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-276 I Nse I <strong>of</strong> I<br />
Ilector<br />
TILLER, B. TR KLINCKWIAN<br />
Company Contact Telephone No.<br />
JOAN KESSNER 375-4688<br />
Proled Coordinator<br />
KESSNER, IH Pd«Code 9N Data Turnsroum-'<br />
N<br />
Air Quality q 45 DaySm<br />
sect DeataaaUon Saaoline Lo ca tion <strong>SAF</strong> No.<br />
<strong>100</strong> A <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti MOM RANCH OFPAL <strong>RC</strong>-<strong>047</strong> (fl<br />
Ice Chest No. t^<br />
Field Loehook No. COA Method erShlonnent m m<br />
Pfi G ' O z<br />
EL-1595 BESRAS6520 FED EX<br />
SkglilLd To °ffi Pro<br />
i1e<br />
p erty No.<br />
S LIONVILLE<br />
POSSIBLE SAMPLE HAZARDS/REMA RKS<br />
POTENTIALRADIOAL77VE
Washin gton Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-277 P-P L <strong>of</strong> i<br />
actor<br />
TILLER, B. N KUNCKNIAN<br />
roiect Designation<br />
Company Contact<br />
JOAN KESSNER<br />
Samollo a Loca<br />
Telephone No.<br />
375.4688<br />
Prolect Coordinator<br />
KESSNER, III<br />
price Code 9N<br />
Air Quality El<br />
Data TurnaroualN<br />
N<br />
45 Days@<br />
ti<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
on<br />
SADDLE MOUNTA IN OFFAL<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong> m<br />
tee Clint No.<br />
^^t^ ` Q-z- SV3r<br />
Field Logbook oo No.<br />
COA Metbod orshioml<br />
EL. 1595 BESRAS6520 FED EX<br />
Sh TO Otfsite Property No. BW <strong>of</strong> Ladine/Air BIB No.<br />
BE LINE SERVIC LIONVILLE 14 3 3 D SEEOSPC<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTEN77ALPADIOAC77VE
Washin)Iton Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-322 Poll- 1 <strong>of</strong> I<br />
olleclor<br />
TILLER, U.<br />
TR KLI<strong>RC</strong>KMAN<br />
Coamanv Contact<br />
JOAN xessNER<br />
Telenbone No.<br />
37s-46//<br />
Prefect Coordinator<br />
KESSNER JH<br />
,<br />
p ace Cade<br />
9N<br />
Data TurnarounN<br />
45 Days<br />
Prefect Designation Sampling loca tion <strong>SAF</strong>No.<br />
AirQuty ali El<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti <strong>100</strong>-D-48:2 OFFAL <strong>RC</strong>-<strong>047</strong> m<br />
Ice Cbest No.<br />
Field Logbook No. COA Method <strong>of</strong> Shis nsent<br />
• "C -0,Z E1r1595 BESRAS6520 FED EX<br />
SW To OfhtlePronertrNo. ^D /D ^^/,<br />
g/AirBillNo.<br />
E RIJN LIONVILLE G l/<br />
HISEEOSPC<br />
POSSIBLE SAMPLE HAZARDS.WMARKS<br />
POTENTIALRADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-323 Page 1 <strong>of</strong> 1<br />
Collector<br />
TILLER, B. TR KLINCKMAN<br />
ComwnV Contact<br />
Tdeohone No.<br />
JOAN KESSNER 375-4688<br />
Prulect C serdhudor<br />
KESSNER, JH Price Code 9N Data 7ltrnaroslrN<br />
45 Mpg<br />
Air Quality<br />
y<br />
test Designation Samoiine Location <strong>SAF</strong> No.<br />
<strong>100</strong> & <strong>300</strong> Am <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti [DO-D-49:2 OFFAL <strong>RC</strong>-<strong>047</strong> m<br />
Ice Chml No. Field Loibook No. CIA Method <strong>of</strong> Shlmstent m m<br />
El 1595 BFSRAS6520 FED EX<br />
Sitipped To OffAtc Properly No.<br />
ERLME SERVI / LK)NVILLE<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTEA7MLRADIOAC77VE
Washington Closure <strong>Hanford</strong> " " CHAIN OF CUSTODY/SAMPLE -ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-328 P-P 1 <strong>of</strong> 1<br />
Collector Comoanv Contact Telephone No. Protect Coordinator<br />
TILLER, B. TR KLINCKMAN LOAN KESSNER 375-4688 KESSNER, IH Prim Code Data 9N<br />
Trrn Yausffl<br />
in<br />
roleel Dedenstion Sanmlhan Loca tion <strong>SAF</strong> No.<br />
Air Quality p 45 DayC<br />
<strong>100</strong> R <strong>300</strong> Arta <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sedim ent and Ti 116-DR-I.DR-21<strong>100</strong>-D-22 OFFAL <strong>RC</strong>-<strong>047</strong> M<br />
Ire Chest No. N^3 c ^<br />
ii `(- 0 .2 - i9<br />
Std<br />
ERLBJE SERVICES LIONVILLE<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
Field Leabook No,<br />
EL. 1595<br />
OHsile Property No. V lO6O<br />
COA<br />
BESRAS6520<br />
3v<br />
Method <strong>of</strong> Shi pment<br />
FED EX<br />
Bill <strong>of</strong> Ladina/Alr Bill No.<br />
SEEOSPC<br />
m<br />
m<br />
POTENTIALRADIOACTIVE
Was1iini:lon Closure <strong>Hanford</strong> (CHAIN OF CUSTODY/SAMPLE ATIA LYSIS REQUEST <strong>RC</strong>-<strong>047</strong>.330 Pnta 1 <strong>of</strong> I<br />
Collector<br />
TTLLER, B. TR KLINCKMAN<br />
elect Deslanalion<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Tt<br />
Ice Chest No. A2 -^pSJ<br />
Af kC<br />
Company ContactTelephone No.<br />
JOAN KESSNER 375.4688<br />
SomBline Loca tion<br />
BORROW PIT 23 OFFAL<br />
Field El 1595 is No.<br />
BESRAS6520<br />
Proied Coordinator<br />
KESSNER, III<br />
SAP No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Method Shinment<br />
FED F-X<br />
Price Code 9N<br />
Air Quality q<br />
Data Turnarou"<br />
N<br />
45 Days"<br />
0<br />
m<br />
CD<br />
m<br />
^^ D 3 3 D<br />
SB Offsite Prooertr No. 2 Big Sdi B Air IB No.<br />
EBERLINE SERVICES L.IONVRLE<br />
POSSIBLE SAMPLE IIAZARDB/REMARKS<br />
POTEIIMAL RADIOACTIVE cDOTLIMf1S<br />
Special IIandling and/or Storage<br />
COOL 4C 'MATRIX COMPOSED OF MICE'<br />
SAMPLE ANALYSIS<br />
Preselvotion<br />
Type <strong>of</strong> Container<br />
No. <strong>of</strong> Contain er(s)<br />
Volume<br />
s^Gs^- KA3U'^<br />
Sample No. Matrix • Sample Date Somple Time<br />
cw14c Nan o,w 4C cow 4[ Coot 4C coni 4c<br />
aG GIP GIP aG sG a0<br />
I 1 a o 0 0<br />
250mL log 15S SOS S0g 568<br />
Switun Min Sn Nnm(ne ICPMmuh- PWiidn• PM-1011 Smni-VOA-<br />
SP.M SpmYl 6010(&l Poor 8770A 1T'CU<br />
1<br />
Imnue ont. Imt n Lin);<br />
M__y -<br />
7471 -(M<br />
JIIL23 OTHER SOLID R Q 3 /3frJ X K<br />
CHAIN OF POSSESSION Sign/Print Names SPECIAL INSTRUCTIONS<br />
Matrix<br />
NOTE: FLer6au-p erfm Gump Spec does baml tip boale to Lionville<br />
Relinquished BY/Retnossd<br />
laba, Upon" nisimain 4 C<br />
e•vl<br />
From /^ Daadfirre vy<br />
Dmrjme<br />
In ow—_<br />
coo ling. L2umole: parum mls, ea PCBPS ,PTSVOC in sus urdcr as samplele<br />
EAS LOCKED STO C y -(a'jv aniu Conran Con Jean<br />
O r7<br />
slit d.s<br />
Kusrty upon mgip[. so-sda<br />
us As4elrtored' (,..IeA/ Dame<br />
ReeeisM BY/Smned In Datelrinrc sasu4s<br />
UU<br />
y - G (1) Game Spec- (Full Usti (Americium,241. Aadmony-1 25, BerYl ium7, Cfth m 134, Cesiurrv137, 01<br />
v<br />
Cebali-60, Eaapbu 152, FAt Wk p 154, Eaopium 155, Paarsium-40, Radinm226, Radiumng, wdi<br />
Rclinquis dB etmeed Front DaWI'mx<br />
Recdred By N ^rc<br />
Raheahan106,Unnho 235,Uranium^23 11 ) ^os.pun,r,m,<br />
(2)Sooai.49,90 - Total Sr, lsotopie Thorium JT7wrium-232 1 : Isotopic Ura ni um(Urariltm!33PU, ol.Oam L npw<br />
Dmtda M. Umwum-251 1; hsnayie Pusonium<br />
T•T ..<br />
Rel i d B e eve From<br />
Retzived B d In. none<br />
h ex e$cw*^ y^r^ 6 ^Ei^)<br />
- Fv r.P..<br />
Reli wahe /Re Rpm Datertine B In<br />
^( a^3o<br />
•<br />
Relinquished By/Rennrcd From L1areTime Received By d In 132MMW<br />
^GiuL (^C 3G^<br />
LABORATORY Received By Title DrteMvne<br />
SECTION<br />
FINAL SAMPLE Disposal Method IRspucd By DatelTime<br />
DISPOSITION<br />
RHI-EE-011 (08/29/2005)<br />
% Ono
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>.332 peso -I 1<br />
ollector<br />
TI LER, n. TR KLINCKMAN<br />
roieetDestin ation<br />
<strong>100</strong> lit <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Company Contact<br />
JOAN KESSNER<br />
SamulituLoation<br />
600- 131 OFFAL<br />
Telephone No.<br />
375.4688<br />
Protect Coordinator<br />
-<br />
ID;SSNP.R, JH Prim Code 9N Data Tur tarsti-<br />
<strong>SAF</strong>No.<br />
<strong>RC</strong>-<strong>047</strong><br />
45<br />
Air Quality E] Daysm G)<br />
Ice Cheat No.//^^^a Field Logbook No. COA Method or Shhument m<br />
'Age- ^ (f L7,,,$^ EL-1595 BESRAS6520 FED EX m<br />
Shlnped To OMIte Property No. Bill Ladino/Air Bill No.<br />
INESERV 1LIONVIILE . 06033v SEE OSPC<br />
POSSIBLE SAMPLE IIAZARD6/REMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS RE WEST <strong>RC</strong>-<strong>047</strong>-343 1ka 2 <strong>of</strong> 1<br />
olleclor<br />
TILLER. B. TR KLINCKMAN<br />
Company Contact Telt Rahn No.<br />
JOAN KESSNER 375-4688<br />
Protect Coordinator<br />
KF-SSNER, JH Price Cade 9N<br />
Data Tumamuna0<br />
(y<br />
oiect Desiamtion Samnlna Laration <strong>SAF</strong> No.<br />
Air Quality E]<br />
45 Days m<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> Compon en t <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti CENTRALPL.ATBAU SHRUB STEPPE OFFAL <strong>RC</strong>-<strong>047</strong> m<br />
Ite Chest No.rQ<br />
Field Logbook No- COA Method <strong>of</strong> SWotllmt m<br />
, L EL-1595 BFSRAS6520 FED EX<br />
m<br />
^—QZ -'^,S<br />
5W Offsite Properly No.^^^^jj<br />
14 O<br />
6 D<br />
BERLBJE SERVICES LIONVILLE<br />
POSStIlMNIVERE HAZARDSMEMARKS<br />
33p<br />
Bid <strong>of</strong> Ladina/Air Bill No.<br />
SEE OSPC<br />
POTENTIAL RADIOACTIVE
SR-002-B<br />
13. VOA, TOC, TOX free <strong>of</strong> headspace?<br />
14. QC stickers placed on bottles designated by<br />
client?<br />
15. Shipment meets LYLI Sample Acceptance<br />
Policy? (identify all bottles not within<br />
policy. See reverse side for po licy)<br />
16. Project Manager contacted concerning<br />
discrepancies? name/date (or samples<br />
outside criteria)<br />
vLl<br />
Lionville Laboratory Incorporated<br />
SAMPLE RECEIPT CHECKLIST (S<strong>RC</strong>)<br />
r<br />
CLMNT: 'T^1U. ^r c- Date:<br />
MV,,/Beatch#:<br />
Order / Proj ect# / p<br />
OW# I Release #: R)c - p^^l<br />
C)(<br />
1. Samples Hand Delivered."r Shipped<br />
2. Custody seals on coolers or shipping<br />
container intact, signed and dated?<br />
3. Outside <strong>of</strong> coolers or shipping containers am<br />
free from damage?<br />
4. All expe ct ed paperwork received (coc and<br />
o<strong>the</strong>r client specific information) scaled in<br />
plastic bag and easily acce ssible?<br />
o ^^L^ 1 Sample Custodian:<br />
NOTE: EXPLAIN ALL DISCREPANCIES<br />
S. Samples receiv cool r ambient? Z )<br />
6. Custody seals on sample containers intact.<br />
signed and dated?<br />
7. coc signed and dated?<br />
a. Sample containers are intact?<br />
9. All samples on coc received? A ll samples<br />
received on coc?<br />
10. All sample label information matches cm?<br />
11. Samples properly preserved?<br />
12. Samples received within hold times?<br />
Short holds taken to wet lab?<br />
Sd Yes O No 17 No Seals<br />
res O No<br />
Jd Yes 0 N<br />
/O'-- ONo<br />
t(Yes O No<br />
Yes ONO<br />
lW<br />
J2(Ycs q No<br />
O Yes<br />
O Yes<br />
O Yes<br />
aYes<br />
• No IldN/A<br />
• No CIA<br />
0 N 11<br />
i er^F,.<br />
13 No<br />
Airbill# '7ga7 x565 1"<br />
[YYes O No O No Seals Comments<br />
//4 Yes q No<br />
7<br />
Yes O No<br />
Temp —T - 3 °C Cooler # SA LOS-1b_:^)<br />
ONO<br />
D'+satpaocics<br />
000000029
PBLKJM MB1<br />
PBLKJM MB1 BS<br />
Lionville Laboratory, Inc. 44 2<br />
PCB ANALYTICAL DATA PACKAGE FOR<br />
TNUKANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/26/06 LVL LOT #<br />
CLIENT ID LVL # MTX PREP # COLLECTION EXTR/PREP ANALLYSIS<br />
J11KK8 001 SO 06LE0455 04/05/06 06/02/06 06/22/06<br />
Ji1KL5 002 SO 06LE0455 04/05/06 06/02/06 06/22/06<br />
J11KL6 003 SO 06LE0455 04/03/06 06/02/06 06/22/06<br />
J11KM0 004 SO 06LE0455 04/05/06 06/02/06 06/23/06<br />
J11KM2 005 SO 06LE0455 04/03/06 06/02/06 06/23/06<br />
Ji1KM3 006 SO 06LE0455 04/03/06 06/02/06 06/23/06<br />
JL1KM4 007 SO 06LE0455 04/03/06 06/02/06 06/23/06<br />
J11KM5 008 SO 06LE0455 04/03/06 06/02/06 06/23/06<br />
J11KM6 009 SO 06LE0455 04/03/06 06/02/06 07/06/06<br />
J11KV1 010 SO 06LE0455 04/05/06 06/02/06 06/23/06<br />
J11KV2 011 SO 06LE0455 04/05/06 06/02/06 06/23/06<br />
JlIL21 012 SO 06LE0455 04/03/06 06/02/06 06/23/06<br />
,7111,23 013 SO 06LE0455 04/03/06 06/02/06 06/23/06<br />
JIIL25 014 SO 06LE0455 04/05/06 06/02/06 06/23/06<br />
JlIL36 015 "S0 06LEb455 04/03/06 06/02/06 06/23/06<br />
J111,36 015 MS So 06LE0455 04/03/06 . 06/02/06 06/23/06<br />
JIIL36 015 MSD '96"06LE0455 04/03/06 06/02/06 06/23/06<br />
LAB QC:<br />
N/A<br />
N/A<br />
06/02/06<br />
06/02/06<br />
06/22/06<br />
07/06/06<br />
000000001
Case Narrative<br />
Client: TNU-I IANFORD <strong>RC</strong>-<strong>047</strong> W.O. #: 11343-606-001-9999-00<br />
LVL #: 0604L904 Date Received: 04-28-2006<br />
SDG/<strong>SAF</strong> # K0303/<strong>RC</strong>-<strong>047</strong><br />
PCB<br />
Fifteen (15) solid (composed <strong>of</strong> mice) samples were collected on 04-03,05-2006.<br />
The samples and <strong>the</strong>ir associated QC samples were extracted on 06-02-2006 and analyzed<br />
according to Lionville Laboratory SOPs based on SW846, 3rd Edition procedures on 06-02,23-<br />
2006. The extraction procedure was based on method 3540C and <strong>the</strong> extracts were analyzed based<br />
on method 8082.<br />
The following is a summary <strong>of</strong> QC results accompanying <strong>the</strong> sample results. Lionville Laboratory<br />
Inc (LvLI) certifies that all test results meet <strong>the</strong> requirements <strong>of</strong> NELAC except as noted below:<br />
1. All results presented in this report are derived from samples that met LvLI's sample<br />
acceptance policy with <strong>the</strong> exception <strong>of</strong> some discrepancies, which were documented on<br />
<strong>the</strong> Sample Receipt Checklist.<br />
2. The samples were received outside extraction holding time. All samples were extracted<br />
outside holding time due to <strong>the</strong> refrigerator (ID # R003) malfunction. A copy <strong>of</strong> <strong>the</strong><br />
Sample Discrepancy Report (SDR) has been enclosed.<br />
3. The soil sample results were reported on a wet-weight basis. All samples were extracted<br />
using reduced sample volume due to <strong>the</strong> nature <strong>of</strong> <strong>the</strong> sample matrix. A copy <strong>of</strong> <strong>the</strong><br />
Sample Extraction Record has been enclosed.<br />
4. The method blank was below <strong>the</strong> reporting limits for all target compounds.<br />
5. One (1) <strong>of</strong> thirty-eight (38) surrogate recoveries was outside acceptance criteria. A copy <strong>of</strong><br />
<strong>the</strong> Sample Discrepancy Report (SDR) has been enclosed.<br />
6. All blank spike recoveries were within acceptance criteria.<br />
7. All matrix spike recoveries were within acceptance criteria.<br />
8. The initial calibrations associated with this data set were within acceptance criteria.<br />
The results presented in this report relate only to <strong>the</strong> analytical testing and conditlom <strong>of</strong> <strong>the</strong> samples at receipt and during storage. All pages <strong>of</strong> this report are integral parts <strong>of</strong><br />
<strong>the</strong> analytical data. Therefore, this report should only be reproduced in its entirety <strong>of</strong> 2 7 pages.<br />
208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-<strong>300</strong>0 • Fax (610) 280-3041<br />
nefnneos+r.-r
9. The continuing calibration standards analyzed prior to sample ex tracts were within<br />
acceptance criteria.<br />
10. LvLI is NELAP accredited by <strong>the</strong> state <strong>of</strong> Pennsylvania and holds over 20 additional state<br />
accreditations. For a complete listing <strong>of</strong> accrediting authorities and <strong>the</strong> corresponding<br />
analytes/methods, please contact your Project M anager.<br />
11. I ce rtify that this sample data package is in compliance with SOW requirements, both<br />
technically and for completeness, o<strong>the</strong>r th an <strong>the</strong> conditions detailed above. Release <strong>of</strong> <strong>the</strong><br />
data contained in this hard-copy data package has been authorized by <strong>the</strong> laboratory<br />
Manager or a designee, as verified by <strong>the</strong> following signature.<br />
lain paniels ^<br />
Lab ratory M anager<br />
Lionville Laboratory Incorporated<br />
s m\r:\group\data\pesknu hmford\0604-904.pebs<br />
208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-<strong>300</strong>0 • Fax (610) 280-3041<br />
_)/010 4.<br />
Date<br />
c7
Lionville Laborato ry Sample Discrepancy Report (SDR) SDR#: 8 16 be ' L 4,<br />
Initiator Jo %N. Batch:<br />
Parameter. PY s3 , P UR<br />
Date: 'T1-1 to 6<br />
Sampl Matrix: •. d w t<br />
Client: Ttv.J Metho Prep Batch: nb e o^,^<br />
4-E=e<br />
1. Reason for SDR<br />
a. COC Discrepancy _Tech Pr<strong>of</strong>ile Er ror Client Request — Error on C-O-C<br />
Transcription Error _ Wrong Test Code O<strong>the</strong>r<br />
b. General Discrepancy<br />
Missing Sample/Extract _ Container B roken —Wrong Sample Pulled _ Label ID's Illegible<br />
Hold Time Exceeded _ Insufficient Sample _ Preserva ti on Wrong _ Received Past Hold<br />
_ Improper Bottle Type _ Not Amenable to Analysis<br />
Note * : verified by [Lo In] or [Prep Group] (circle)... signaturaldate:<br />
c. Problem (Include all relevant specific results; attach data if necessa ry )<br />
It<br />
sr%^ tf rf G mot! 11 af'T /'f cJ .....t.^k a Z<br />
2. Known or Probable Causes(s)<br />
3. Discussion and Proposed Action O<strong>the</strong>r Descrip ti on:<br />
_ Re-log<br />
_ En ti re Batch<br />
Following Samples:<br />
_ Re-leach<br />
_ Re-extract<br />
_ Re-digest<br />
_ Revise EDD<br />
Change Test Code to<br />
_ Place On/Take Off Hold (circle)<br />
4. Project Manager Instructions ... signature/date:<br />
Concur with Proposed Action<br />
_ Disagree with P roposed Action; See Ins truction<br />
_ Include in Case Narrative<br />
_ Client Contacted:<br />
Date/Person<br />
_ Add<br />
Cancel<br />
5. Final Ac tion... signature/date:<br />
—<br />
O<strong>the</strong>r Explana tion:<br />
Verified re-[log][leach][extractildigest][an y0sl 016e) e)<br />
_ Included in Case Narrative<br />
_ Hard Copy COG Revised<br />
Electronic COG Revised<br />
_ EDD Corrections Completed<br />
When Final Action has been recorded, forward original to QA Specialist for distribu tion and filing.<br />
Route Distribution <strong>of</strong> Completed SDR Route Dis tribu ti<br />
X Ini<br />
on <strong>of</strong> Completed SDR<br />
ti<br />
ator<br />
X Lab General Manager. M, Taylor<br />
X P roject Mgr. Stone/Johnson<br />
Data Management: S<br />
_<br />
_ _ Metals: Beegle<br />
_ _ Inorganic: Perrone<br />
_ _ GC/LC: IGger<br />
ti<br />
lwell<br />
_ Sample Prep: Beegle/Kiger<br />
_ MS: Rychlak/Daley<br />
_ _ Login: Per ry<br />
Admin:<br />
O<strong>the</strong>r.<br />
QA-105-A-0805<br />
4^u 1<br />
wl^<br />
7/7/6<br />
000000004
Lionville Laboratory Sample Discrepancy Report (SDR) SDR #: 06PM001<br />
Initiator. Odette Johnson Batch: T Parameter: AW AVA, Y°^<br />
Date: /1706 Samples: Mat ri<br />
x:<br />
Client: Method: swaesnacAVVwrcm P rep Batch:<br />
1. Reason for SDR<br />
a. COC Disc repancy _ Tech Pr<strong>of</strong>ile Error _ C li<br />
ent Request Sampler Error on C-O-C<br />
Transcription Error _ Wrwg Test Code _ O<strong>the</strong>r<br />
b. General Discrepancy<br />
_ Missing Sample/Extract _ Container B roken Wrong Sample Pulled _ Label ID's Illegible<br />
Hold Time Exceeded<br />
Improper Bot<br />
Insufficient Sample Preservation Wrong _ Received Past Hold<br />
tl<br />
e Type _ Not Amenable to Analysis X O<strong>the</strong>r<br />
Note: Verified by [Log-In) or [Prep amp[ (drde) ... signeture/daw.<br />
c. Problem (Include all relevant specific results; attach data If necessa ry)<br />
On 5110/06 sample storage refrigerator ID# R003 malfunctioned and was not holding <strong>the</strong> required sample storage<br />
temperature <strong>of</strong> 4'C +/- 2°C<br />
2. Known or P robable Causes(s)<br />
Broken motor<br />
3..Discuss[on and P roposed Action.... O<strong>the</strong>r Description:<br />
_ Re-log At <strong>the</strong> time <strong>of</strong> malfunction R003 was used for storage <strong>of</strong> samples received<br />
_ Entire Batch for extractable organics, metals and wet chemist ry (except TOC) analyses.<br />
Following Samples: All samples were removed from R003 to ano<strong>the</strong>r refrigerator on 5/10/06.<br />
_ f e-Ieach R003 was tagged out on 5/10106, repaired on 5/12/06, and we have<br />
_ Re-extract certified that R003 is maintaining <strong>the</strong> required sample storage temperature.<br />
_ Re-digest<br />
_ Revise EDD<br />
Change Test Code to<br />
_ Place On/Take Off Hold (circle)<br />
4. Project Manager Instructions ... signaturefdate:<br />
Concur with P ro posed Action<br />
gree with Proposed Action; See Instruc<br />
r<br />
ti on<br />
^/ nclude in Case Narrative<br />
Client Conte<br />
Date/Person ^i del l.t^ fGy^D^p<br />
_ Add<br />
Canoel<br />
S. Fine -Acdon..sgnatureaate:<br />
nfied re-[log][leach][extract]<br />
K^Ihcluded in Case Narrative<br />
_ Hard Copy COC Revised<br />
Electronic CDC Revised<br />
_ EDD Co<br />
est)[analysi ] circi )<br />
O<strong>the</strong>r Explanation:<br />
rr ec ti<br />
ons Completed<br />
When Final Action has been recorded, forward original to OA Specialist for dis tribu tion and filing.<br />
Route Distribution <strong>of</strong> Completed SDR Route Distribution <strong>of</strong> Completed SDR<br />
X Initiator _ _ Metals: Welsh<br />
X Lab Manager. I. Daniels Inorganic: Perrone<br />
X Project Mgr. Stone/Johnson _ GC/LC: IQger<br />
Data Management: Stilwell _ MS: Schneider/Daley<br />
_ Sample Prep: BeegleNger _ Log-in: Per ry<br />
Admin:<br />
O<strong>the</strong>r.<br />
oA-105-A-DW5<br />
069960005
19<br />
rNnn1r L10oFAIOF'r /^'<br />
DATA QUALIFIERS<br />
GLOSSARY OF DATA<br />
U = Indicates that <strong>the</strong> compound was analyzed for but not detected. The minimum detection limit for <strong>the</strong><br />
sample (not <strong>the</strong> method detection limit) is reported with <strong>the</strong> U (e.g., IOU).<br />
Indicates an estimated value. This flag is used in cases where a target analyze is dete cted at a level<br />
less than <strong>the</strong> lower quantification level. If <strong>the</strong> limit <strong>of</strong> quanti fication is 10 ug/L and a concentra tion<br />
<strong>of</strong> 3 ug/L is calculated, it is reported as 31.<br />
B = 'Ibis flag is used when <strong>the</strong> analyte is found in <strong>the</strong> associated blank as well as in <strong>the</strong> sample. It<br />
indicates possible/probable blank contamination.<br />
E = Indicates that <strong>the</strong> compound was dete cted beyond <strong>the</strong> calibration range and was subsequen tly<br />
analyzed at a dilu tion.<br />
I = Interference.<br />
I<br />
ABBREVIATIONS<br />
Indicates an interferen ce on one analytical column only. Result is reported from remaining analytical<br />
column.<br />
BS = Indicates blank spike in which reagent grade water is spiked with <strong>the</strong> CLP matr ix spiking solutions<br />
and carried through all <strong>the</strong> steps in <strong>the</strong> method. Spike recoveries are reported.<br />
BSD<br />
Indicates blank spike duplicate.<br />
MS = Indicates matr ix Spike.<br />
MSD = Indicates matrix spike dup li cate.<br />
DL = Indicates that recoveries were not obtained because <strong>the</strong> extract had to be diluted for analysis.<br />
NA = Not Applicable.<br />
DF<br />
Dilu tion Factor.<br />
NR = Not Required.<br />
NS = Not Spiked.<br />
SP = indicates Spiked Compound.<br />
P _ This flag is used for an PEsnCIDE/PCB target analyte when <strong>the</strong>re is greater than 2S°/,<br />
difference for detected concentra ti ons between <strong>the</strong> two GC columns (see Form X). The<br />
lower <strong>of</strong> <strong>the</strong> two values Is reported on Form I and flagged wi th a "P".<br />
D = This flag identifies all compounds identi fied in an analysis at a secondary dilution factor.<br />
C = This flag applies to a compound that has been confirmed by GOMS.<br />
NPM =<br />
No pattern match for multi-component target analytes.<br />
000000006
PCBs by GC,Report Date: 07/10/06 11:35<br />
RFW Batch Number: 0604L904 Client: TNUBANPORD <strong>RC</strong>-<strong>047</strong> K0303 Work Order, 11343606001 Paae • 1<br />
Cust ID: J11KK6 J11KL5 J11KL6 J11KM0 J11KM2 J11KM3<br />
Sample RFW#: 001 002 003 004 005 006<br />
Information Matrix: SOLID SOLID SOLID SOLID SOLID SOLID<br />
D.F.: 1.00 1.00 1.00 1.00 1.00 1.00<br />
Units: UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG<br />
Surrogate: Tetrachloro-m-xylene 93 $ 85 $ 71 t 87 % 78 $ 105 &<br />
Decachlorobiphenyl 102 $ 88 $ 92 % 90 % 97 Ir 104 $<br />
. . ............. . ........... _____________===== f1...... =====-fl===°=_=== ... f1 ..... ___==== £1=====__===== f1=====__='==°fl<br />
Aroclor-1016 200 U 180 U 160 U 180 U 140 U 180 U<br />
Aroclor-1221 200 U 180 U 160 U 180 U 140 U 180 U<br />
Aroclor-1232 200 U 180 U 160 U 180 U 140 U 180 U<br />
Aroclor-1242 200 U 180 U 160 U 180 U 140 U 180 U<br />
Aroclor-1248 200 U 180 U 160 U 180 U 140 U 180 U<br />
Aroclor-1254 200 U 180 U 160 U 180 U 140 U 180 U<br />
Aroclor-1260 200 U 180 U 160 U 180 U 140 U 180 U<br />
Sample<br />
Information.:<br />
Cust ID: J11KM4 JllKM5 J1lmd Ji1KV1 JllKV2 J111,21<br />
RFW#: • 007 006 009 010 011 012<br />
:Matrix: SOLID '.SOLID' SOLID SOLID SOLID SOLID-<br />
D.P.: 1.00 1.00 .1.00 1.00 1.00 1.00<br />
Units: UG/KG UG/KG /KG UG/KG UG/KG UG/KG<br />
Surrogate: Tetrachloro -m-xylene <strong>100</strong> $ 88 % <strong>100</strong> % 120 * $ 105 $ 93 $<br />
Decachlorobiphenyl 97 $ 83 $ 96 $ 116 $ 107 $ 99 $<br />
....... ...................................... fl ...... _=====fl==== ........ fl --- ......... fl............ fl............ fl<br />
Aroclor-1016 200 U 150 U 140 U 180 U 140 U 180 U<br />
Aroclor - 1221 200 U 150 U 140 U 180 U 140 U 180 U<br />
Aroclor-1232 200 U 150 U 140 U 180 U 140 U 180 U<br />
Aroclor-1242 200 U 150 U 140 U 180 U 140 U 180 U<br />
Aroclor-1248 200 U 150 U 140 U 180 U 140 U 180 U<br />
Aroclor - 1254 200 U 150 U 140 U 180 U 140 U 180 U<br />
Aroclor-1260 200 U 150 U 140 U 180 U 140 U 180 U<br />
U= Analyzed, not detected. J- Present below detection limit. B. Present in blank. NR= Not reported. NS= Not spiked.<br />
$= Percent recovery. D= Diluted out. I= Interference. NA= Not Applicable. *• Outside <strong>of</strong> EPA CLP QC U^r<br />
ti<br />
m<br />
m<br />
m<br />
G<br />
m<br />
CD
PCBs by GC Report Date: 07/10/06 11:35<br />
RFW Batch Number: 0604L904 Client: TNQBANFORD <strong>RC</strong> -<strong>047</strong> K0303 Work Order: 11343606001 Paae• 2<br />
Cust ID: JlIL23 J111,25 JlIL36 JIIL36 JlIL36 PBLKJM<br />
Sample RFW#: 013 014 015 015 MS 015 MSD 0GLE0455-MB1<br />
Information Matrix: SOLID SOLID SOLID SOLID SOLID SOIL<br />
D.F.: 1.00 1.00 1.00 1.00 1.00 1.00<br />
Units: UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG<br />
Surrogate: Tetrachloro-m-xylene 93 W 95 8 87 t 103 t <strong>100</strong> %. 82 t<br />
Decachlorobiphenyl 94 t 112 93 %- 108 W 98 t 88 %,<br />
........_____________====fl..===._,..... fl.=..=_.=.... fl............ fl ......... ...fl --- .----- =..fl<br />
Aroclor-1016 160 U 160 U 180 U <strong>100</strong> $ 94 $ 13 U<br />
Aroclor-1221 160 U 160 U 180 U 180 U 180 U 13 U<br />
Aroclor-1232 160 U 160 U 180 U 180 U 180 U 13 U<br />
Aroclor-1242 160 U 160 U 180 U 180 U 180 U 13 U<br />
Aroclor-1248 160 U 160 U ISO U 180 U 180 U 13 U<br />
Aroclor-1254 160 U 160 U 180 U 180 U 180 U 13 U<br />
Aroclor-1260 160 U 160 U :180 U 104 W 96 13 U<br />
Cust ID: PSLKJM BS<br />
Sample RFW#: 0M0455-MB1<br />
Information Matrix: SOIL<br />
D.F.: 1.00<br />
Units: UG/KG<br />
Surrogate: Tetrachloro-m-xylene 94 W<br />
Decachlorobiphenyl 88 %<br />
............................................. fl ... = ........ fl. ....... = .... fl ............ fl=====__=====fl.=.......... fl<br />
Aroclor-1016 80 t<br />
Aroclor-1221 13 U<br />
Aroclor-1232 13 U<br />
Aroclor-1242 13 U<br />
Aroclor-1248 13 U<br />
Aroclor-1254 13 U<br />
Aroclor-1260 81 t<br />
U= Analyzed, not detected. J= Present below detection limit. B. Present in blank. NR= Not reported. NS= Not spiked.<br />
W= Percent recovery. D= Diluted out. I= Interference. NA= Not Applicable. •= Outside <strong>of</strong> EPA CLP QC<br />
1<br />
m<br />
CD<br />
M<br />
G<br />
m
SAMPLE EXTRACTION RECORD<br />
Extract. Date: 06/02/06 Extraction Batch No: 06LE0455 Analyst: MF<br />
766L: 3FCF) Cieaiiup Z, Lc: Ai.alyst: iiF<br />
LIMS Report Date: 07/10/06 Solvent: DCM,HEXANE<br />
Sheet no.: I<br />
Method: **-• m mm<br />
Cl <strong>RC</strong>-,47 K0333<br />
m Adsorbent: FLSLA m Client Name pH Initial surr. Spike Final Final Split GPC % C/D<br />
Sample No: Client ID WT/VOL Mult. Mult. VOL VOL Mult. Y/N Solids FACTOR<br />
0604L904- TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
001 J11KKB 2.0 1.0 10 1.0 N 0.00 5000.0<br />
002 J11KL5 2.20 1.0 10 1.0 N 0.00 4545.4<br />
003 J11KL6 2.56 1.0 10 1.0 N 0.00 3906.2<br />
004 011KMO 2.17 1.0 10 1.0 N 0.00 4608.3<br />
005 J11KM2 2.86 1.0 10 1.0 N 0.00 3496.5<br />
006 J11KM3 2.18 1.0 10 1.0 N 0.00 4587.2<br />
007 J11KM4 2.00 1.0 10 1.0 N 0.00 5000.0<br />
008 J11KM5 2.67 1.0 10 1.0 N 0.00 3745.3<br />
009 J11KM6 2.86 1.0 10 1.0 N 0.00 3496.5<br />
010 J11KV1 2.19 1.0 10 1.0 N 0.00 4566.2<br />
011 JllKV2 2.86 1.0 10 1.0 N 0.00 3496.5<br />
012 JlIL21 2.18 1.0 10 1.0 N 0.00 4587.2<br />
013 Ji1L23 2.52 1.0 10 1.0 N 0.00 3968.2<br />
014 JlIL25 2.50 1.0 10 1.0 N 0.00 4000.0<br />
015 J111,36 2.17 1.0 10 1.0 N 0.00 4608.3<br />
015 -S J111,36 2.17 1.0 1.0 10 1.0 N 0.00 4608.3<br />
015 -T J111,36 2.18 1.10 1.0 10 1.0 N 0.00 4587.2<br />
06LE0455-MB1 PBLKJM 30.0 1.0 10 1.0 N <strong>100</strong>.00 333.3<br />
06LE0455-MB1 -S PBLKJM 30.0 1.0 1.0 10 1.0 N <strong>100</strong>.00 333.3<br />
Comments:<br />
Surrogate: 250 UL OLM PSURR 89915801<br />
Spike: 250 UL AR1660 89915602<br />
(Extracts Transferred I Relinquished By Date Time Received By Date Timei Reason for Transfer<br />
m
Lionville Laborato ry Use Only Custody Transfer Record/Lab Work Request Paget <strong>of</strong> <strong>of</strong> lu^ LI<br />
Est. Final Prol. Sampling Date<br />
Project # !^ l-,yl _^^/^rJ- <strong>of</strong><br />
Project Co rdacUPtwne #<br />
Lionville Laborato ry Project Manager<br />
QC Del ^T d TAT<br />
Date Recd Lk •d s o(, Dale Due .^/J 71 '/rt'-"<br />
MATRIX<br />
CODES:<br />
S- Soli<br />
SE • Sediment<br />
Letr<br />
ID<br />
SO - So li<br />
d<br />
SL • Sludge<br />
w - Wafer<br />
O- oil<br />
A - J it<br />
DS- Drum<br />
Scads<br />
OIL- Drum<br />
Liquids<br />
L- EP/TCLP<br />
Leschele<br />
an • wipe<br />
X • O<strong>the</strong>r<br />
F- Fish<br />
Client ID/DaaMpllon<br />
FIELD PERSONNEL: COMPLETE ONLY SHADED /AREAS<br />
See S<strong>RC</strong><br />
/^ m<br />
u<br />
Refrigerator #<br />
#Mpe Conminer<br />
volume<br />
Preservatives<br />
ANALYSES<br />
REQUESTED<br />
Liquid<br />
So lid<br />
Liquid<br />
So li<br />
d<br />
c<br />
ac<br />
Chosen<br />
d"<br />
Date Time<br />
Col le<br />
cted Collect<br />
10 to lJ1116V 1I 1 1. 4 I'll<br />
Special Instructions: V'VL =CQn', lic"A\¢,L DNS:<br />
^l'^YTL^I p t^L<br />
mC^cy15 , PCQ , Si^OC . *<br />
`l-d^4^ cto.Dw `''`.r3, aY. le.-Pes^^ z.<br />
Me- A-CJS PCB, PCIA, SVOCL . K'<br />
ReanquleMd Roe~<br />
by r by<br />
Onto<br />
Time<br />
1,1<br />
3.<br />
4.<br />
>I a^=lal III<br />
j LloWlis Laboralory U se<br />
X,<br />
r/<br />
Re linquished wed<br />
by by<br />
,.;QMP0.sjJ 0 f<br />
WASTE"<br />
CD<br />
CD<br />
J ^I•^^^ /^Jr<br />
Dale Time
Lionville Laborato ry Use Only<br />
Custody Transfer Record/Lab Work Request Pag e—I.4- <strong>of</strong> ---^l<br />
^V^1<br />
b a ^^o^-<br />
I-<br />
FIELD PERSONNEL: COMPLETE ONLY SHADEDREAS<br />
m<br />
C lient r^ C °" m<br />
Est. Final P ro). Sampling Date X/type Container<br />
liquid<br />
S<br />
m'<br />
m<br />
Project #<br />
Project GontaeVPhone #<br />
^^<br />
(J<br />
vaum.<br />
LigWd<br />
-<br />
m<br />
Lionville Laboratory Pro]<br />
OC Del<br />
- anager<br />
TAT<br />
G<br />
-<br />
Preservatives<br />
Solid<br />
ORGANIC INORG<br />
ANALYSES<br />
Date Recd Date Due<br />
REQUESTED -^ O<br />
><br />
Z<br />
m<br />
Amy<br />
a q I E U<br />
MATRIX<br />
1 LbrMae laboratory Use Only 1<br />
CODES:<br />
matrix<br />
S. SON<br />
SE. Sedent im<br />
SO - Sae<br />
SL- Sludge<br />
W. Water<br />
ob<br />
C lient ID/Descrlptton<br />
OC<br />
Chosen<br />
In<br />
Matrix<br />
Date<br />
Collected<br />
T[ma<br />
Copxlea ^S<br />
:^<br />
V+<br />
O<br />
$<br />
`'<br />
VT<br />
h<br />
Y]<br />
O O- oil<br />
MS I MSD<br />
`a<br />
A - Air<br />
DS- Drum<br />
Solids<br />
DL.<br />
o<br />
NJ<br />
oZ^ - +<br />
L- EP/TC I.<br />
WI Woe<br />
^^ Lai a - , ..:: -x<br />
-.. x -. 'x -K<br />
PLeadwe s so o x t x<br />
X - O<strong>the</strong>r 015 J 1 ^—ZG 015 X x X<br />
F - Fish<br />
Special Instructions:<br />
DATEMEMSIONS:<br />
`SL. "r.J^ 1rL l r j )" f lir 2.<br />
r^^r^^^<br />
J 7 r(L 3.<br />
ReiingWehed Received<br />
Deis Thrre<br />
Refirmpieiled Received<br />
.Data Time<br />
Re li by by by M<br />
nquished<br />
by<br />
Received<br />
by<br />
1 y<br />
4.<br />
5.<br />
8.<br />
Ow 71rM
Washineton Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS RE VEST I <strong>RC</strong>-<strong>047</strong>-259 JPPF I -f 1<br />
Collector<br />
TR KLiNCKMAN<br />
TILLER, B.<br />
Company ContactTelephone No.<br />
JOAN KESSNBR 375-4688<br />
Proleel Coordinator<br />
KESSNFl2, IN<br />
Price Code 9N Data Turnaround<br />
45 Days m<br />
Project Designation<br />
<strong>100</strong> & <strong>300</strong> Arcs <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Sampling Location<br />
600-1321600-190 OFFAL<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Air Qualify [] y m<br />
m<br />
lee Chest No y Field Loebook No. COA Metiaod <strong>of</strong> Shinmeat m<br />
^^_ 133.111595 BESRAS6520 FED EX 0<br />
Sl pv OfTsile Properly No. ^ 7 Bi ll <strong>of</strong> lAdiwJA ir Bill No.<br />
RLINE SERVIC5 LIONVILLE 1-99464!f 7 2 d SEE OSPC<br />
POSSIBLE SAMPLE HAZARDS/BEMARKS<br />
POTEKTIALRADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-266 g F J or s<br />
(lector<br />
TILLER, B. TR KLINC<br />
Company Contact<br />
JOAN KESSNER<br />
Telephone No.<br />
375-4688<br />
Proled Coordinator<br />
KESSNER, JH Price Cade SIN<br />
Dafa Turnaround M<br />
roieel Designation Sampling Loca tion<br />
<strong>SAF</strong> No.<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti .<strong>100</strong>4f-Iii, OFFAL] ^G O ^^}.Z<br />
<strong>RC</strong>-<strong>047</strong><br />
Ice ChatNo-<br />
^Ae / '<br />
Fid No. COA Method <strong>of</strong> Shiosnenl<br />
EL-1595 BESRAS6520 FED EX<br />
SI Ta Oftyite Properly No. Big <strong>of</strong> Lodinx/Air Bill No.<br />
EBERNE LI<br />
LIONVU.F ^906a33 40<br />
SEE<br />
POS E RAZARDSIREMARKS<br />
POTEMIALRADIOACTIVE DOTLIMITS<br />
SpecialIfandlinganNorStorage<br />
COOL 4C "MATRIX COMPOSED OF MICE"<br />
SAMPLE ANALYSLS<br />
Preatrwlion<br />
Type <strong>of</strong> Container<br />
No. <strong>of</strong> Conlailter(s)<br />
Volume<br />
spry koao_3<br />
c v44C None Ce"I/C C °"1K Gautac I C- 1 4C<br />
AG GIP GIP aG aG aG<br />
( ) o a a a<br />
250& log 15g 306 505 50S<br />
Swean( I) in Sxitem(2) k Sw G)m PCBs -1082 Patietlw- Snoi-VOA-<br />
Sprciw Spxid Spaial SRI 9270A(TCL)<br />
1.<strong>100</strong>. I,wwiow. Immnb"s<br />
A.ir QusRty<br />
Sample No. Mat rix Sample Date Sample Time 4 ._,-I - - , ,• r<br />
b<br />
J11KL5 OTHER SOLID APR 0 5 2006 Ci X h<br />
45 Days m<br />
CHAIN OF POSSESSION Sign/Print Names SPECIAL INSTRUCTIONS<br />
NOTE: Fbedi w. peripm Gamto Spec th<br />
Matrix<br />
Relinquished By/Ringd Fiwn Date/(Imev a y/51ap111n /t^ _ Oy DaleJlitee<br />
en m nship hank b Lionville Lahs, if pwsbk rmimin d C<br />
.6l. 'ms's<br />
O<br />
A LOCKED STO AGE y'<br />
io i(3o coding. Lionville: perform acing. PCB,PESTSVOC is Bds order as snopk is available. Contact loan Kessner upon receipt.<br />
>.^<br />
Rhe4 9nn &.e,# Daternnm Received By/Stored In Date/fme<br />
y/<br />
swsgv'<br />
(1)Gamm Spec-(Pollliag lAmericium yAl, Andmany-125, Be W.W.<br />
rylliuna7,Cesium134,Cesiuml37,<br />
Cobalt-6t1.Fjumpivn•15? rsuo pium154.rar*um155,Pdassium4O.Radhw 226,Radhw 221- o'nl<br />
Relinqu ished By/Re fran.J; Dw sce Received By/St o<br />
Ina<br />
q^ Rulhemun- 106, Undmo-235, Unrliuo-2181<br />
apa,pmsoar<br />
r^ as I ' "N (2) Shonimn89,90 -- Total Sr, Isoto pic Thorium I Thmium2J'_): Isotopic Uranium I UmmInt-233P34, p.an.n ewe,<br />
Unnirwa233, Unnom2J g 1: isdopie Pouor:um<br />
T.T.<br />
Retie d By p d IeT<br />
Received ByfSlmd In Da me<br />
ttO<br />
(3) ICP Mpsk 7I - 60101PWI IJsU ( Aluminum Animoily. Anenk, Buiam Beryllium, Bum FPO ph, Koran,<br />
wl.ww<br />
tx ' Gdmium Calcium, Cnorlwuo Coba lt, Copper. Iran, lend, Ulh)um Magnesiwn Man<br />
I}raeao<br />
Ppar,<br />
v.vam,.<br />
Relirq hed tl /Renaved DatNl'ine Reai B d In Date?ime Molybdenum Nicke l. Phosplmus, Porassivm Selenium Sikcoa Silver, Sodium Stmnims Tlullus, x.oue<br />
QC Tin, lhlftii , Vanadium 2'iwl: Mercury - 7471 - (CV)<br />
Relinquished Byl itemoved From DakTne Reaped By d in Date(fine<br />
S'<br />
azV<br />
^Q 30 3<br />
LABORATORY Rea).ed By Tit le UatoTme<br />
SECTION<br />
FINAL SAMPLE Disposal Me th od Disposed By Danrtime<br />
DISPOSITION<br />
BHI-EE-011 (0812912005)<br />
m<br />
m<br />
m
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS RE QUEST <strong>RC</strong>-<strong>047</strong>-267 P+6e L 4t I<br />
Collector -<br />
TILLER, B. iR KLINCKMAN<br />
Comoan Contact<br />
JOAN KESSNER<br />
Telephone No.<br />
375-4668<br />
Protect Coordinator<br />
KESSNER, JH<br />
Code 9N Data Tntvutrouata<br />
lect Deienaaon Swmlim Location <strong>SAF</strong> No-<br />
Air Quality q<br />
45 Days m<br />
<strong>100</strong>A <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti ' 116-N-3 OFFAL <strong>RC</strong>-<strong>047</strong> m<br />
Ice Chest Na Field Loabook No. OA Melted <strong>of</strong> S1Jlrmwl m<br />
EL-1395- BESRAS6520 FED EX<br />
m<br />
Shipa<br />
ERl.B4E SERVICES LIONVIILE<br />
POSSIBLE SAMPLE IIAZARDS/REMAR IIS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODYISAMPLE ANALYSIS REQUEST I <strong>RC</strong>-<strong>047</strong>-271 1 pir 1 <strong>of</strong> I<br />
Collector Company Contact Telephone No. Proled Coordinator uIf77<br />
price Code 9N<br />
Data Turnarons,,.i<br />
TILLER, B. TR BLIN JOAN KESSNER 375 -4685 KESSNER, JH<br />
m<br />
rolect Designation Sawlina Lwalkn <strong>SAF</strong> No.<br />
45<br />
A it Quality q Days<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sedim en t and n 1607.D2:1 OFFAL <strong>RC</strong>-<strong>047</strong><br />
Ice Chest No./^ r<br />
fJ<br />
4r<strong>RC</strong>' eQ -<br />
Field Loabook No. COA Method <strong>of</strong> Shipment m<br />
EL-1595 BESRAS6520 PEDEX m<br />
S1 Offsile Property No. AOIO l 2^ Bill <strong>of</strong> Ladf WAir BBI Na<br />
ERLINESERVICES LK)NVIUE /^ P JJ SEEOSPC<br />
POSSIBLE SAMPLE WARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS RE VEST <strong>RC</strong>-<strong>047</strong>473 Ra t i<br />
Collector<br />
Company Contact Telephone No. Protect Coordinator<br />
TILLER, B. TA KLINCKMAN<br />
JOAN KESSNER 375-4688 KESSNER. JH<br />
Price Code 9N<br />
Data urnarou T^f<br />
Protect Dellenation<br />
<strong>100</strong> &<strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Satnotine Loca tion<br />
BORROW PIT 24 OFFAL<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Air Quality E] 45 Day (OD m<br />
Ice Cheat No. pry<br />
/Z ,C ^-<br />
L ,+<br />
,z ' 3 QJ<br />
Field L.nehook No.<br />
EL-1595<br />
COA<br />
DESRAS6520<br />
Method <strong>of</strong> Shipment<br />
FED EX<br />
-<br />
m<br />
m<br />
Shlu ORsue Property No. O O<br />
B ll OL S A ir BillI N<br />
BERLINE SERVICES LIONVILE /^^^<br />
POSSIBLE SAMPLE IIAZARDS/BEMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>.274 P4a I or 1<br />
Collector<br />
TRIER, B. TR KLINCKMAN<br />
Cotma tv Contact<br />
JOAN KESSNER<br />
Telephone No.<br />
375-4668<br />
Protect Coadb a w<br />
KESSNER, IN Price Code 9N Data Turnarounttoted<br />
Dedenation<br />
<strong>100</strong> & <strong>300</strong> Am <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Sampling Loca tion<br />
YAKIMA RIDGE B OFFAL<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Air Quality q<br />
45 Days%<br />
l9<br />
Ice Chest No. Field Logbook No, COA Method <strong>of</strong> S hIpment m<br />
^^1 ['-02','^^ EL-1595 BESRAS6520 FP.D EX<br />
m<br />
Shl ORslle Property No. Bill <strong>of</strong> Air Bi ll No.<br />
BER ME SERVICES LIONVfILE J ll E OSPC<br />
POSSIBLE SAMPLE IIAZARD&MMARKS<br />
POTENTIAL RADIOACTfVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-275 I Pw 1 <strong>of</strong> J<br />
Collector<br />
Continently Contact T el ephone No. Protect Coordinator<br />
TILLER, B. TR KLINCOAN JOAN K 12SSNER 375-4688 KESSNER, JH Price Data<br />
Pr 9N TssrnaroushhhD M<br />
Protect Deelanasbp Semo lina Location SAP No. 45<br />
Air Quality [] Days 9<br />
Y 0<br />
ICn & <strong>300</strong> Arm Componem <strong>of</strong> <strong>the</strong> <strong>RC</strong>ORA Sediment and Ti VE.RNTTA UPRIVER ON SOUTH S IDE OFFAL <strong>RC</strong>-<strong>047</strong> 0<br />
Ice Chest No. n<br />
4^eC- Field Loebook No, COA<br />
m<br />
Method <strong>of</strong> Shimswlt<br />
e%2<br />
EL, 1595 BESRAS6520 FED EX 0<br />
Si o Offsfle Property No. BIB <strong>of</strong> LadindAir Bill No.<br />
BERLINE SERVICES IONVBLE h'06o 33o SEE OSPC<br />
POSSIBLE SAMPMUZARDSMMARM<br />
POTENTIAL RAVIOAC77VE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-276 P'I2 1 <strong>of</strong> 1<br />
oilector Company Contact<br />
TILLER, R. TR KLINCKMAN JOAN KESSNER<br />
Telephone No.<br />
375-4688<br />
Prolect Coordinator<br />
KFSSNER, JH Fria ce ('ode 9N Data Twuaramaa`<br />
45 Days%<br />
<strong>of</strong>ett Dalana llon<br />
<strong>100</strong> & <strong>300</strong> Arcs, <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Sanmliat Location<br />
McGEE RANCH OFFAL<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Air Quality q<br />
(5J<br />
Ice Chat No.C^<br />
^C'OZ -3-D<br />
Field Logbook No.<br />
EL-1595<br />
COA<br />
DESRAS6520<br />
Method <strong>of</strong> Shipment<br />
PEDEX<br />
m<br />
m<br />
Sh' To Onatle Property No. Bi ll<br />
<strong>of</strong> Ladine/Air Bill ERE L ES VI LIONVILLE 060330<br />
No.<br />
SEE OSPC<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-277 w>R 2 nr 1<br />
olleetor Company ContactT el _<br />
ephone No. Prolect Coordinator<br />
TILLER, B. N KLINCKMAN JOAN KESSNER 375-4688 KFSSNER, III<br />
^,^,nv,^^ v<br />
Prim Code 9N<br />
N<br />
'rolect Deaienmlon Sampling Location <strong>SAF</strong> No.<br />
45 Day s.0<br />
Air Quality q<br />
<strong>100</strong> & <strong>300</strong> Am <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti SADDLE MOUNTA IN OFFAL <strong>RC</strong>-<strong>047</strong> m<br />
Ice Chat No. AeC- e2. sV3<br />
Field Loehook No. COA Method <strong>of</strong> Shipment M<br />
EL 1595 BESRAS6520 FED EX m<br />
ShinuedTo Dil le Property NO. RERLMESERVIC LIONVILLE 3 3 o<br />
BID Lading/Air ill Air No. B<br />
BID <strong>of</strong><br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
PO'FENTUL RADIOACHVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>•<strong>047</strong>422 Paso I <strong>of</strong> I<br />
(lector<br />
TILLER, B. TR KLINCKMAN<br />
Project Dedenatlon<br />
<strong>100</strong> & Me <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Ice Chest No. n ^---^<br />
Coaaanv Contact<br />
JOAN KESSNER<br />
Semolina Location<br />
IWD48:2 OFFAL<br />
Field Logbook No.<br />
Telephone No.<br />
375-4689<br />
-<br />
Project Coordinator<br />
KFSSNER, III<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Price Code 9N<br />
Air Quality q<br />
Data Turoarosu-+<br />
(y<br />
45 Days<br />
m<br />
9—<br />
EL . 1595<br />
COA<br />
BESRAS6520<br />
Method <strong>of</strong> Shipment<br />
FED EX<br />
SI' To Offsile Property No. /^ Z p'l Bill ELa^dAirBBINo.<br />
E RLIN LIONVILL6 /' G c/Jf/<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODUSAMPLE ANALYSIS RE UEST <strong>RC</strong>-<strong>047</strong>-323 Page I <strong>of</strong> I<br />
Collector<br />
TILLER, B. TR KLINCKMAN<br />
Protect Dalenalion<br />
<strong>100</strong> & <strong>300</strong> Ara <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Ice Chase No.<br />
£j^C-01<br />
Sd^<br />
Conmanr Contact<br />
JOAN KESSNER<br />
Samolina Loca tion<br />
<strong>100</strong>-D-49:2 OFFAL<br />
Flekt Loarbook No,<br />
EI. 1595<br />
Teleohom No.<br />
375-4688<br />
COA<br />
BESRAS6520<br />
Proieet Coordinator<br />
KESSNER, IH<br />
SAP No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Method <strong>of</strong> SNoment<br />
FED EX<br />
price Code 911j<br />
Air Quality q<br />
Data TurnarounlV<br />
N<br />
45 Days<br />
m<br />
m-<br />
m<br />
m<br />
SI'ued To<br />
•^R ME SERVO L10NVILIE<br />
Oefatte Property No.<br />
,900033 o<br />
Bill <strong>of</strong> Ladina/Air Bill No.<br />
SEEOSPC<br />
POSSIBLE SAMPLE IIAZARDS/REMARKS<br />
POTENTIAL RAVIOACTNE
Washington Closu re <strong>Hanford</strong> " CHAIN OF CUSTODY/SAMPLE-ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>.328 J or 1<br />
Collector<br />
TILLER, B. TR KLINCKMAN<br />
'roles( Deslewtion<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> rile <strong>RC</strong>BRA Sediment and M<br />
Company Conta ct Telephone No.<br />
JOAN KESSNER 375-4665<br />
Sampling Location<br />
116-DR-1,DR-2/<strong>100</strong>-D-22 OFFAL<br />
Proiect Coordinator<br />
KESSNER,JH<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Price Code 9N Data 7WrnarouWJ<br />
a<br />
Air Quality p 45 Days<br />
m<br />
Ice Chest No. p^r^ r Field Loaboolc No. COA Method <strong>of</strong> Shipment m<br />
AlIC- 0.2 '^7 OJr EGI595 BESRAS6520 FED EX m<br />
Shtp<br />
BERLINE SERVICES LIONVIUB<br />
POSSIBLE SAMPLE RAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong><br />
Collect"<br />
TILLER, B. TR KLINCKMAN<br />
Protect Dalena ion<br />
<strong>100</strong> & <strong>300</strong> Am <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
tee Cheat No. f'r2c^ D2 5a5f<br />
..<br />
OF CUSTODY/SAMPLE -ANALYSIS REOUEST <strong>RC</strong>-<strong>047</strong>-330 J PW 1 -1 t<br />
Company Contact<br />
JOAN KESSNER<br />
Telephone No.<br />
375-4688<br />
Proleet Coordmalor<br />
KESSNER, III Sanitation Lo<br />
Price Code 91V Data Tprnaraucy<br />
N<br />
cati on<br />
BORROW PIT 23 OFFAL<br />
SAP No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Air Quality El<br />
45 Day s%<br />
m<br />
Field Loebook No.<br />
EL-1595<br />
COA<br />
BESRAS6520<br />
Method <strong>of</strong> Shipment<br />
FED EX<br />
0m<br />
m<br />
S Otfa(te Property No. Bill /2 2 Air Bill No.<br />
EBERLINE SERVICES L.IONVILLE<br />
603 3 D<br />
SEE OSPC<br />
POSSIBLE SAMPLE HAZARDSIREMARKS<br />
POTEN77ALRADIOAC17VE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-332 P'2° 1 <strong>of</strong> 1<br />
Collector<br />
Company Contact Telephone No. Prolect Coordinator<br />
TILLER. B. TR KLINCKMAN LOAN KESSNER 375-468R KPSSNBR, JH<br />
Psiee Code 9N Data Tax'oarourU}<br />
Protect Des iena llon Semolina Location <strong>SAF</strong> No. 45 Day .RD<br />
Air Quality q<br />
<strong>100</strong> & <strong>300</strong> Arca <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti 600-131 OFFAL <strong>RC</strong>-<strong>047</strong><br />
Ice Chest No. r^^_D^ Lorlsook No. meow FEDPX shipment<br />
M<br />
—50 ,i ..^ BESRA56520<br />
9—<br />
Shipped To Offshe Property No. ,y O v<br />
Bill <strong>of</strong> LadloNAir Bill No.<br />
E SERVI / LIONVILLE ff'(J 3 SEE OSPC<br />
POSSIBLE SAMPLE IIAZARDSIREMARKS<br />
POTENTIAL RADIOACTIVE ^DOTLIMITS Preservation<br />
Special handling and/or Storage<br />
COOL 4C "MATRIX COMPOSED OF MICE"<br />
SAMPLE ANALYSIS<br />
C-1 IC None c"°I .e eaal4C Caat
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-N7-343 aF i <strong>of</strong> 1<br />
Collector Company Contact Telephone No. Pr<strong>of</strong>ixt Coordinator<br />
«Code Data 9N Turnaromsifl<br />
TILLER, B. Tfl KLINCKMAN JOAN KESSNER 375.4688 KP35NER, IH<br />
led Designation Samsdine Location <strong>SAF</strong> No. Air Quality E) 45 Daysm<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> Cmnponent <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti CENTRAL PLATEAU SHRUB STEPPE OFFAL <strong>RC</strong>-<strong>047</strong> m_<br />
f5]<br />
Ice Chest No.r Field Logbook No. COA Method <strong>of</strong> Shinmml<br />
G c -192- —,Sdj<br />
EL. 1595 BESRAS6520 FED EX<br />
m<br />
S^BERLINE<br />
Offsite Property No.,^0 / Bill Bill<br />
O33D<br />
BI Na.<br />
SERVIC LIONVILLE !^ f7 SEE<br />
POSSIBL LE HAZARDS/REMARKS<br />
POTEAWALSADIOACT/VE fime<br />
SECTION<br />
FINAL SAMPLE Disposal Method Dispo se d By Datemem,<br />
DISPOSITION<br />
SHI-EE-011 (06129/2005)
Lionvi ll<br />
e Laborato ry Incorporated<br />
SAMPLE RECEIPT CHECKLIST (S<strong>RC</strong>)<br />
(<br />
CLIENT: `-NaaRr^ oc,^ Date:`<br />
Order / Project# /<br />
<strong>SAF</strong># w# / Release #: <strong>RC</strong> o' \^<br />
v Batch 9: rl,N ) n ,\,<br />
1. Samples Hand<br />
2. Custody seals on coolers or shipping<br />
container intact, signed and dated?<br />
3. Outside <strong>of</strong> coolers or shipping containers am<br />
free from damage?<br />
4. All expected paperwork received (coc and<br />
o<strong>the</strong>r c li<br />
ent speci fic information) sealed in<br />
plastic bag and easily accessible?<br />
5. Samples receiv cool r ambieut? y Q<br />
6. Custody seals on sample containe rs intact,<br />
signed and dated?<br />
7, coc signed and dated?<br />
8. Sample containers are intact?<br />
9. All samples on coc received? A ll samples<br />
received on coc?<br />
10. All sample label information matches coc?<br />
11. Samples properly preserved?<br />
12. Samples received within hold times?<br />
Short holds taken to wet lab?<br />
SR-002-B<br />
13. VOA, TOC, TOX free <strong>of</strong> headspace?<br />
14. QC stickers placed on bottles designated by<br />
client?<br />
15. Shipment meets LvLI Sample Acceptance<br />
Policy? (Identify all bottles not within<br />
policy. See reverse side for po licy)<br />
16. Project Manager contacted concerning<br />
discrepancies? name/date (or samples<br />
outside criteria)<br />
vLl<br />
EXPLAIN ALL<br />
/<br />
O No<br />
/Q Yes q No<br />
17 3es 0 No<br />
O No Sash Comments<br />
Tetup 7 .3 IC<br />
S<br />
^d Yes O No O No seats<br />
1 93<br />
11 Yes<br />
/^Y4<br />
I(Yea<br />
Yes<br />
Yes<br />
O Yes<br />
Oyes<br />
O Yes<br />
Ye<br />
U Yes<br />
Sample Custodian:<br />
ONO<br />
O No<br />
O No<br />
ONO<br />
O No<br />
O No<br />
O No /^11`NlA<br />
ONO 94 A<br />
ONo<br />
Airbill# '7 q a7 °^ 5 OS<br />
ONo 0 N<br />
Diseeepsoeks<br />
Cooler# SAW - 1a^<br />
000009027
Lionville Laboratory, Inc_<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
N<br />
vd\lE^<br />
N\- ZD<br />
DATE RECEIVED: 04/28/06 LVL LOT # :060 E<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
J11KK8<br />
SILVER, TOTAL . 001 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
SILVER, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06<br />
SILVER, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/30/06<br />
ALUMINUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/30/06<br />
ALUMINUM, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
ARSENIC, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ARSENIC, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06<br />
BORON, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
BORON, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06<br />
BORON, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 001 REP SO 06LO324 0.4/05/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/30/06<br />
BERYLLIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/30/06<br />
BERYLLIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
BISMUTH, TOTAL REP 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06<br />
BISMUTH, TOTAL SPIKE 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 001 REP SO 06L0324 .04/05/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06<br />
COBALT, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
COBALT, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06<br />
COBALT, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06<br />
COPPER, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/30/06<br />
COPPER, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/30/06<br />
000000001
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANPORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :0604L904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
COPPER, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/30/06<br />
IRON, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
IRON, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06<br />
IRON, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 001 SO 0600086 04/05/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
POTASSIUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06<br />
POTASSIUM, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL ,001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 001 SO 66LO324 04/05/06 05/25/06 05/30/06<br />
PHOSPHORUS, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/30/06<br />
PHOSPHORUS, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/31/06<br />
LEAD, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
LEAD, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06<br />
LEAD, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
000000002
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :06041,904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
SILICON, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
SILICON, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06<br />
SILICON, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
TIN, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
TIN, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06<br />
TIN, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 001 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 001 MS SO 06L0324 04/05/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 001 REP SO 06LO324 04/05/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ZINC, TOTAL 001 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ZINC, TOTAL 001 REP SO 06L0324 04/05/06 05/25/06 05/27/06<br />
ZINC, TOTAL 001 MS SO 06LO324 04/05/06 05/25/06 05/27/06<br />
J11KL5<br />
SILVER, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 002 SO 06LO324 04/05/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
BORON, TOTAL 002 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 002 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 002 SO 06LO324 04/05/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 002 SO 06LO324 04/05/06 -05/25/06 05/27/06<br />
COBALT, TOTAL 002 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 002 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
COPPER, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/30/06<br />
IRON, TOTAL 002 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 002 SO 0600086 04/05/06 05/03/06 05/04/06<br />
000000003
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :06041,904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
ME<strong>RC</strong>URY, TOTAL 002 REP SO 0600086 04/05/06 05/03/06 05/04/06<br />
ME<strong>RC</strong>URY, TOTAL 002 MS SO 0600086 04/05/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 002 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/30/06<br />
LEAD, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 002 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
SILICON, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
TIN, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
ZINC, TOTAL 002 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
J11KL6<br />
SILVER, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BORON, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
COBALT, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
COPPER, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
IRON, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 003 SO 0600086 04/03/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
000000004
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :06041,904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
LITHIUM, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
LEAD, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SILICON, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
TIN, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 003 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ZINC, TOTAL 003 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
J11KM0<br />
SILVER, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 004 SO 06L0324 04/05/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
BORON, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 004 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/30/06<br />
BISMUTH,_TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 004 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
COBALT, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 004 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
COPPER, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/30/06<br />
IRON, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 004 SO 06CO086 04/05/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
000000005
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :0604L904<br />
CLIENT ID /ANALYSIS LVL # MIX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
MOLYBDENUM, TOTAL 004 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 004 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 004 SO 06L0324 04/05/06 05/25/06 05/30/06<br />
LEAD, TOTAL 004 SO 061;0324 04/05/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 004 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
SILICON, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
TIN, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 004 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 004 _ SO 06L0324 04/05/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ZINC, TOTAL 004 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
J11KM2<br />
SILVER, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BORON, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
COBALT, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
COPPER, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
IRON, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 005 SO 0600086 04/03/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
000000006
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :0604L904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
PHOSPHORUS, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
LEAD, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
SILICON, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
TIN, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 005 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ZINC, TOTAL 005 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
J11KM3<br />
SILVER, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
BORON, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
COBALT, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
COPPER, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
IRON, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 006 SO 0600086 04/03/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
LEAD, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
000000007
Lionville Laboratory, Inc.<br />
INORGANIC . ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :0604L904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
SELENIUM, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SILICON, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
TIN, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 006 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ZINC, TOTAL 006 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
JllKM4<br />
SILVER, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BORON, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
COBALT, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
COPPER, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
IRON, TOTAL _ 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 007 SO 0600086 04/03/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
LEAD, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SILICON, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
TIN, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
000000008
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :06041,904<br />
CLIENT ID /ANALYSIS LVL # M7% PREP # COLLECTION EXTR/PREP ANALYSIS<br />
STRONTIUM, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 007 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ZINC, TOTAL 007 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
J11KM5<br />
SILVER, TOTAL 008 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
BORON, TOTAL 008 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 008 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 008 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
COBALT, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
COPPER, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
IRON, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 008 SO 06CO086 04/03/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 008 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 008 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 008 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
LEAD, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SILICON, TOTAL 008 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
TIN, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 008 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 008 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 008 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
000000009
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> X0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :0604L904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
VANADIUM, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ZINC, TOTAL 008 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
J11KM6<br />
SILVER, TOTAL 009 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
BORON, TOTAL 009 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 009 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 009 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
COBALT, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 009 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
COPPER, TOTAL 009 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
IRON, TOTAL 009 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 009 SO 0600086 04/03/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 009 SO 06LO324 04/03/06_ 05/25/06 05/27/06<br />
SODIUM, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 009 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
LEAD, TOTAL 009 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SILICON, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
TIN, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 009 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ZINC, TOTAL 009 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
J11KV1<br />
SILVER, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
000000010
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :0604L904<br />
CLIENT ID /ANALYSIS LVL # MIX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
ALUMINUM, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 010 SO 061,0324 04/05/06 05/25/06 05/27/06<br />
BORON, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 010 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 010 SO 06L0324 04/05/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 010 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 010 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
COBALT, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
COPPER, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/30/06<br />
IRON, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 010 SO 0600086 04/05/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 010 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 010 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/30/06<br />
LEAD, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
SILICON, TOTAL 010 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
TIN, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 010 SO 06LO324 04/05/06 05/25/06- 05/27/06<br />
URANIUM, TOTAL 010 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 010 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
ZINC, TOTAL 010 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
S11KV2<br />
SILVER, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
BORON, TOTAL Oil SO 06LO324 04/05/06 05/25/06 05/27/06<br />
000000011
Lionville Laboratory, Inc,<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :06041,904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
BARIUM, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/27/D6<br />
CALCIUM, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
COBALT, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
COPPER, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/30/06<br />
IRON, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 011 SO 0600086 04/05/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/30/06<br />
LEAD, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
SILICON, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
TIN, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL Oil SO 06L0324 04/05/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 011 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
ZINC, TOTAL 011 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
JlIL21<br />
SILVER, TOTAL 012 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 012 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BORON, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 012 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 012 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
000000012
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-04.7 K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :0604L904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
CALCIUM, TOTAL 012 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
COBALT, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 012 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
COPPER, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
IRON, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 012 SO 0600086 04/03/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 012 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/31/06<br />
LEAD, TOTAL 012 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SILICON, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
TIN, TOTAL 012 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 012 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ZINC, TOTAL 012 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
JIIL23<br />
SILVER, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BORON, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
COBALT, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
000000013
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :06041,904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
CHROMIUM, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
COPPER, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
IRON, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 013 SO 0600086 04/03/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/31/06<br />
LEAD, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
SILICON, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
TIN, TOTAL 013 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 013 'SO 06LO324 04/03/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 013 SO 66LO324 04/03/06 05/25/06 05/27/06<br />
ZINC, TOTAL 013 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
JlIL25<br />
SILVER, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 014 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
BORON, TOTAL 014 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 014 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
COBALT, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 014 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
COPPER, TOTAL 014 SO 06LO324 04/05/06 05/25/06 05/30/06<br />
IRON, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
000000014
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :0604L904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
ME<strong>RC</strong>URY, TOTAL 014 SO 06CO086 04/05/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
MAGNESIUM, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 014 - SO 06L0324 04/05/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/30/06<br />
LEAD, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 014 SO 06LO324 04/05/06 05/25/06 05/27/06<br />
SILICON, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
TIN, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
ZINC, TOTAL 014 SO 06L0324 04/05/06 05/25/06 05/27/06<br />
J11L36<br />
SILVER, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ALUMINUM, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
ARSENIC, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
BORON, TOTAL 015 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
BARIUM, TOTAL 015 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
BERYLLIUM, TOTAL 015 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
BISMUTH, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
CALCIUM, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
CADMIUM, TOTAL 015 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
COBALT, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
CHROMIUM, TOTAL 015 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
COPPER, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/30/06<br />
IRON, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
ME<strong>RC</strong>URY, TOTAL 015 SO 0600086 04/03/06 05/03/06 05/04/06<br />
POTASSIUM, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
LITHIUM, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
000000015
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 _ LVL LOT # :0604L904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
MAGNESIUM, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
MANGANESE, TOTAL 015 SO 061,0324 04/03/06 05/25/06 05/27/06<br />
MOLYBDENUM, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
SODIUM, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
NICKEL, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
PHOSPHORUS, TOTAL 015 SO 06LO324 04/03/06 05/25/06 05/30/06<br />
LEAD, TOTAL 015 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ANTIMONY, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
SELENIUM, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
SILICON, TOTAL 015 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
TIN, TOTAL 015 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
STRONTIUM, TOTAL 015 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
THALLIUM, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
URANIUM, TOTAL 015 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
VANADIUM, TOTAL 015 SO 06LO324 04/03/06 05/25/06 05/27/06<br />
ZINC, TOTAL 015 SO 06L0324 04/03/06 05/25/06 05/27/06<br />
LAB QC:<br />
SILVER LABORATORY LC1 BS S 061,0324 N/A 05/25/06 05/26/06<br />
SILVER, TOTAL MBl S 06L0324 N/A 05/25/06 05/26/06<br />
ALUMINUM LABORTORY LC1 BS S 06L0324 N/A 05/25/06 05/30/06<br />
ALUMINUM, TOTAL MB1 S 06LO324 N/A 05/25/06 05/30/06<br />
ARSENIC LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
ARSENIC, TOTAL MBl S 06LO324 N/A 05/25/06 05/26/06<br />
BORON LABORATORY LC1 BS S 06LO324 N/A 05/25/06 05/26/06<br />
BORON, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
BARIUM LABORATORY LC1 BS S 06LO324 N/A 05/25/06 05/26/06<br />
BARIUM, TOTAL MB1 S 06LO324 N/A 05/25/06 05/26/06<br />
BERYLLIUM LABORATORY LC1 BS S 06LO324 N/A 05/25/06 _ 05/30/06<br />
BERYLLIUM, TOTAL MB1 S 06LO324 N/A 05/25/06 05/30/06<br />
BISMUTH, LCS LC1 BS S 06LO324 N/A 05/25/06 05/26/06<br />
BISMUTH, TOTAL MB1 S 06LO324 N/A 05/25/06 05/26/06<br />
CALCIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
CALCIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
CADMIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
CADMIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
COBALT LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
000000016
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :06041,904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
COBALT, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
CHROMIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
CHROMIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
COPPER LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/30/06<br />
COPPER, TOTAL MB1 S 06L0324 N/A 05/25/06 05/30/06<br />
IRON LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
IRON, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
ME<strong>RC</strong>URY LABORATORY LC1 BS S 0600086 N/A 05/03/06 05/04/06<br />
ME<strong>RC</strong>URY, TOTAL MB1 S 0600086 N/A 05/03/06 05/04/06<br />
POTASSIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
POTASSIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
LITHIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
LITHIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
MAGNESIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
MAGNESIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
MANGANESE LABORATORY LCl.BS S 06L0324 N/A 05/25/06 05/26/06<br />
MANGANESE, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
MOLYBDENUM LABORATOR LCl BS S 06L0324 N/A 05/25/06 05/26/06<br />
MOLYBDENUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
SODIUM LABORATORY LC1 BS S 061,0324. N/A 05/25/06 05/26/06<br />
SODIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
NICKEL LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
NICKEL, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
PHOSPHORUS LCS LCl BS S 06L0324 N/A 05/25/06 05/30/06<br />
PHOSPHORUS, TOTAL MB1 S 06L0324 N/A 05/25/06 05/30/06<br />
LEAD LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
LEAD, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
ANTIMONY LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
ANTIMONY, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
SELENIUM LABORATORY LC1 BS S 06LO324 N/A 05/25/06 05/26/06<br />
SELENIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
SILICON LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
SILICON, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
TIN LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
TIN, TOTAL MBl S 06LO324 N/A 05/25/06 05/26/06<br />
STRONTIUM LCS STANDA LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
STRONTIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
THALLIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
000000017
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :06041,904<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
THALLIUM, TOTAL MB1 S 06LO324 N/A 05/25/06 05/26/06<br />
URANIUM LABORATORY LC1 BS S 06LO324 N/A - 05/25/06 05/26/06<br />
URANIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
VANADIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06<br />
VANADIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
ZINC LABORATORY LC1 BS S 06LO324 N/A 05/25/06 05/26/06<br />
ZINC, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06<br />
000000018
Client: TNU-HANFORD <strong>RC</strong>-<strong>047</strong> WON: 11343-606-001-9999-00<br />
LVL#: 0604L904 Date Received: 04-28-06<br />
SDG/<strong>SAF</strong>4: K0303/<strong>RC</strong>-<strong>047</strong><br />
METALS CASE NARRATIVE<br />
The following is a summary <strong>of</strong> <strong>the</strong> QC results accomp anying <strong>the</strong> sample results. Lionville Laborato ry<br />
(LvLI) certi fi<br />
es that all test results meet <strong>the</strong> requirements <strong>of</strong> NELAC except as noted below.<br />
All soil samples are repo rted on a dry weight basis unless requested by <strong>the</strong> client, required by <strong>the</strong> method,<br />
or noted o<strong>the</strong>rwise.<br />
This narrative covers <strong>the</strong> analyses <strong>of</strong> 15 solid samples.<br />
2. The samples were prepared and analyzed in accordance with methods checked on <strong>the</strong> attached<br />
glossary. The samples are reported on a wet weight, `as received' basis.<br />
All samples were rerun for Aluminum, Be ryllium, and Copper, along with <strong>the</strong> Phosphorous<br />
analysis, due to sample matrix. The matrix spike <strong>of</strong> sample J11KK8, and samples J1 1L21 and<br />
J11L23 were rerun for Phosphorous due to high concen trations.<br />
3. All analyses were performed within <strong>the</strong> required holding ti mes.<br />
4. All Ini ti al and Con ti nuing Calibration Verifications (ICV/CCVs) were within <strong>the</strong> 90-110% con trol<br />
limits (80-120% for Mercury).<br />
5. All Ini tial and Continuing Calibration Blanks (ICB/CCBs) were within con trol limits (less than <strong>the</strong><br />
PQL).<br />
6. The preparation/method blanks for 2 analytes were outside method c riteria (less than <strong>the</strong> Prac ti cal<br />
Quantitation Limit (3X <strong>the</strong> IDL), or samples greater than 20X MB value). Refer to <strong>the</strong> Inorganics<br />
Method Blank Data Summary .<br />
a). The MB results for Aluminum and Uranium were greater than <strong>the</strong> Prac ti cal Quantitation Limit<br />
(PQL) (3 x <strong>the</strong> (IDL) Instrument Detection Level) and al l samples read less than 20 ti mes <strong>the</strong> MB<br />
concentration for Aluminum. However, no corrective ac ti on criteria for MBs were provided in<br />
SW846 method 6010B. The sample results were repo rted herein "uncorrected" for <strong>the</strong> levels<br />
found in <strong>the</strong> MB. All samples were below <strong>the</strong> IDL for Uranium.<br />
All ICP Interference Check Standards were within con trol limits.<br />
The re su lts presented in this re port relate only to <strong>the</strong> analytical testing and conditions <strong>of</strong><strong>the</strong> samples at receipt and during storage. All pages <strong>of</strong>this re po rt are<br />
integral pads <strong>of</strong><strong>the</strong> analy tical data The re fo re , this report should only be reproduced in its entirety <strong>of</strong> ^C pages.<br />
208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-<strong>300</strong>0 • Fax (610) 280-3<strong>047</strong>
8. All laboratory control samples (LCS) were within <strong>the</strong> 80-120% control limits with <strong>the</strong> ex cep ti on <strong>of</strong><br />
Silicon at 69.6%. Refer to <strong>the</strong> Inorganics Laborato ry Control Standards Report. Associated<br />
sample results may be bi ased low.<br />
9. The matrix spike (MS) recove ries for 5 analytes were outside <strong>the</strong> 75-125% control limits. Refer to<br />
<strong>the</strong> Inorganics Accuracy Repo rt .<br />
10. For analytes where <strong>the</strong> ICP MS is out-<strong>of</strong>-control, a post-diges tion MS (PDS) and serial dilution are<br />
performed. A PDS w as prepared at meaningful concentration level for <strong>the</strong> following analytes:<br />
Sample ID Element<br />
PDS<br />
Concentra<br />
PDS<br />
ti<br />
on (pob) %Recovery<br />
J11KK8 C al cium 12,000 115.6<br />
Iron 2,000 95.3<br />
Phosphorous 6,000 104.1<br />
Silicon 1,<strong>100</strong> <strong>100</strong>.3<br />
Zinc <strong>100</strong> 117.1<br />
11. The duplicate analyses for 16 analytes were outside <strong>the</strong> 20% Rela ti ve Percent Difference (RPD)<br />
control limits. Refer to <strong>the</strong> Inorg anics Precision Repo rt .<br />
12. For <strong>the</strong> purposes <strong>of</strong> this report, <strong>the</strong> data has been reported to <strong>the</strong> Instrument Detection Limit (IDL).<br />
Values between <strong>the</strong> IDL and <strong>the</strong> Practical Quantitation Limit (PQL) are acquired in a region <strong>of</strong><br />
less-certain quantification.<br />
13. LvLI is NELAP accredited by <strong>the</strong> state <strong>of</strong> Pennsylv ania and holds over 20 addi ti onal state<br />
accreditations. For a complete listing <strong>of</strong> accredi ti ng authorities and <strong>the</strong> corresponding<br />
analytes/methods, ple ase contact your Project M anager.<br />
14. I certify that this sample data package is in compli ance with SOW requirements, both<br />
technically and for completeness, o<strong>the</strong>r than <strong>the</strong> condi ti ons detailed above. Rele ase <strong>of</strong> <strong>the</strong> data<br />
contained in this hard-copy data package h as been autho rized by <strong>the</strong> Laborato ry Manager or a<br />
designee, as verified by <strong>the</strong> following signature.<br />
aniels<br />
I_JL^ovatory Manager<br />
Lionville Laboratory Incorporated<br />
ijw/m04-904<br />
vLl<br />
c, )g1,^<br />
Date<br />
10 4W.
METALS METHOD GLOSSARY<br />
The following methods are used as 'reference for <strong>the</strong> digestion and analysis <strong>of</strong> samples contained within t<br />
Lot#: 66() 4L4aN r<br />
Leaching Procedure: -1310 -1311 -1312 ,_O<strong>the</strong>r:<br />
CLP Metals_ Digestion and _ Analysis Methods: _ILM03 .0 -ILM04.0<br />
Metals Digestion Methods: _<strong>300</strong>5A _3030A 3015 3020A x 3050B 3051 200.7 -SS17<br />
__O<strong>the</strong>r:<br />
Metals Analysis Methods<br />
EPA<br />
SW846 EPA STD MTD OSWR USATHAM ,<br />
Aluminum 46010B _200.7 -99 Antimony<br />
Arsenic<br />
Ba rium<br />
Beryllium<br />
Bismuth<br />
Boron<br />
Cadmium<br />
Calcium<br />
Chromium<br />
Cobalt<br />
Copper<br />
f 6010 -7041' -200.7 -204.2<br />
)oC 6010B -7060A -200.7 _206.2 -3113B<br />
)r, 6010B -200.7<br />
)^- 6010B 200.7<br />
--106010B' _200.7'<br />
)C6010B -200.7<br />
-IC 6010B -7131A' 200.7 213.2<br />
)C6010B -200.7<br />
^6010B _7191' -200.7 218.2<br />
40010B 200.7<br />
6010B -7211<br />
-1620<br />
99<br />
-99<br />
99<br />
99<br />
99<br />
-99<br />
-99<br />
-99<br />
-SSI7<br />
-99<br />
:200.7<br />
Iron<br />
Lead<br />
Lithium<br />
Magnesium<br />
Manganese<br />
Mercu ry<br />
Molybdenum<br />
Nickel<br />
Potassium<br />
Rare Earths<br />
Selenium<br />
Silicon<br />
Silica<br />
Silver<br />
220.2<br />
ZC 6010B _200.7<br />
6010B -7421 5 200.7 -239.2 -3113B<br />
6030$ _7430' _200.7<br />
6010B 200.7<br />
6010B ll 200.7<br />
7470A 3_)(7471A3 -245.1?2455'<br />
-y601 0B -200.7<br />
60101 -200.7<br />
1,60101 -7610' 200.7 _258.1'<br />
_6010B' _200.7'<br />
)C6010B -7740' -200.7 -270-23113B<br />
)L4010B' 200.7<br />
_6010B 200.7<br />
^C 6010B -7761<br />
-1620<br />
-1620<br />
-1620<br />
-1620<br />
-99<br />
-^<br />
-99<br />
99<br />
99.<br />
-99<br />
-99<br />
-99<br />
-99<br />
_99<br />
-99<br />
-99<br />
-99<br />
_99<br />
S Sodium<br />
Strontium<br />
Thallium<br />
Tin<br />
Titanium<br />
Uranium<br />
Vanadium<br />
Zinc<br />
Zirconium<br />
200.7 -272.2<br />
6010B _7770' _200.7 -273.1'<br />
^6010B 200.7<br />
K6010B -7841' 200.7 279.2-200.9<br />
Y 6010B -200.7<br />
6010B 200.7<br />
6010B' 200.7'<br />
6010B _200.7<br />
6010E 200.7<br />
-6010B' 200.7'<br />
-1620<br />
-1620<br />
99<br />
99<br />
-99<br />
99<br />
-99<br />
99<br />
-99<br />
-99<br />
_99<br />
O<strong>the</strong>r. W d<br />
/<br />
Method: 60/06 4m.mws.om .<br />
000000021
METHOD REFERENCES AND DATA QUALIFIERS<br />
U = Indicates that <strong>the</strong> parameter was not detected at or above <strong>the</strong> reported limit. The<br />
associated numerical value is <strong>the</strong> sample detection limit.<br />
" = Indicates that <strong>the</strong> original sample result is greater than 4x <strong>the</strong> spike amount added.<br />
MB = Method or Preparation Blank.<br />
MS = Matrix-Spike.<br />
MSD = Matrix Spike Duplicate.<br />
REP = Sample Replicate<br />
LCS = Laboratory Control Sample.<br />
NC = Not calculated.<br />
Not included in <strong>the</strong> method element list.<br />
2. Modified Hg: Hgl and Hg2 require less total volume <strong>of</strong> digestate due to <strong>the</strong><br />
autosampler analysis. Sample volumes and reagents for mercury determinations<br />
in water and soil have been proportionately scaled down to adapt to this semiautomated<br />
technique. The sample volume used for water analysis is 33 mL. For<br />
soils, approximately 0.3 grams <strong>of</strong> sample is taken to a final volume <strong>of</strong> 50 mL<br />
(including all reagents).<br />
3. Flame AA.<br />
Graphite Furnace AA.<br />
L-W1 -033/N-04/98<br />
000000022
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06/08/06<br />
CLIENT: TNUHANPORD <strong>RC</strong>-<strong>047</strong> K0303 LVL LOT #: 0604L904<br />
WORK ORDER: 11343-606-001-9999-00<br />
REPORTING DILUTION<br />
.SAMPLE SITE ID ANALYTE RESULT UNITS LLMIT FACTOR<br />
: e<br />
-001 J11KK8 Silver, Total 0.07 u MO/KG<br />
0.07 '6i `2.0<br />
Aluminum, Total 26.2 MG/KG 2.2 1.0<br />
Arsenic, Total 0.58 u MG/KG 0.58 1.0<br />
Boron, Total 0.45 MG/KG 0.23 1.0<br />
Barium, Total 4.4 MG/XG 0.02 1.0<br />
Beryllium, Total 0.02 u MG/KG 0.02 1.0<br />
Bismuth, Total 0.49 u MG/KG 0.49 1.0<br />
Calcium, Total 9790 MG/KG 1.6 1.0<br />
Cadmium, Total 0.07 u MG/KG 0.07 1.0<br />
Cobalt, Total 0.13 u MG/KG 0.13 1.0<br />
Chromium, Total 0.41 MG/KG 0.12 1.0<br />
Copper, Total 2.6 MG/KG 0.21 1.0<br />
Iron, Total 94.3 MG/KG 3.3 1.0<br />
Mercury, Total 0.02 u MG/KG 0.02 1.0<br />
Potassium, Total 2680 MG/KG 2.2 1.0<br />
Lithium, Total 0.1 MG/KG 0.03 1.0<br />
Magnesium, Total 471 MG/KG 0.92 1.0<br />
Manganese, Total 3.0 MG/KG 0.03 1.0<br />
Molybdenum, Total 0.28 u MG/KG 0.28 1.0<br />
Sodium, Total 1340 MG/KG 0.72 1.0<br />
Nickel, Total 0.23 u MG/KG 0.23 1.0<br />
Phosphorus, Total 6060 MG/KG 0.86 1.0<br />
Lead, Total 0.30 u MG/KG 0.30 1.0<br />
Antimony, Total 0.42 u MG/KG 0.42 1.0<br />
Selenium, Total D.63 MG/KG 0.46 1.0<br />
silicon, Total 42.9 MG/KG 2.2 1.,0<br />
Tin, Total 1.0 a MG/KG 1.0 1.0<br />
Strontium, Total 10.9 MG/KG 0.01 1.0<br />
Thallium, Total 0.67 a MG/KG 0.67 1.0<br />
Uranium, Total 0.84 u MG/KG 0.84 1.0<br />
Vanadium, Total 0.14 MG/KG 0.09 1.0<br />
Zinc, Total 46.6 MG/KG 0.15 1.0<br />
000000023
SAMPLE SITE ID<br />
002 J11KL5<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06/08/06<br />
CLIENT: TNUMANFORD <strong>RC</strong>-<strong>047</strong> K03O3 LVL LOT M: 0604L9O4<br />
WORK ORDRR: 11343-606-001-9999-00<br />
REPORTING DILUTION<br />
ANALYTR RESULT UNITS LIMIT FACTOR<br />
silver, Total 0.07 u MG/KG 0.07 1.0<br />
Aluminum, Total 76.6 MG/KG 2.2 1.0<br />
Areenic, Total 0.58 U MG/KG 0.5E 1.0<br />
Boron, Total 1.5 MG/KG 0.23 1.0<br />
Barium, Total 3.1 MG/KG 0.02 1.0<br />
Beryllium, Total 0.02 u MG/KG 0.02 1.0<br />
Bismuth, Total 0.49 u MG/KG 0.49 110<br />
Calcium, Total 13500 MG/KG 1.6 1.0<br />
Cadmium, Total 0.07 u MG/KG 0.07 1.0<br />
Cobalt,. Total 0.13 u MG/KG 0.13 1.0<br />
Chromium, Total 0.60 MG/KG 0.12 1.0<br />
Copper, Total 3.3 MG/KG 0.21 1.0<br />
Iron, Total 122 MG/KO 3.3 1.0<br />
Mercury, Total 0.02 u MG/KG 0.02 1.0<br />
Potassium, Total 2910 MG/KG 2.2 1.0<br />
Lithium, Total 0.10 MG/KG 0.03 1.0<br />
Magnesium, Total 641 MG/KG 0.92 1.0<br />
Manganese, Total 6.1 MG/KG 0.03 1.0<br />
Molybdenum, Total 0.28 u MG/KG 0.38 1.0<br />
Sodium, Total 1560 MG/KG 0.12 1.0<br />
Nickel, Total 0.23 a MG/KG 0.23 1.0<br />
Phosphorus, Total 8010 MG/KG 0.86 1.0<br />
Lead, Total 1.5 MG/KG 0.30 1.0<br />
Antimony, Total 0.42 u MG/KG 0.42 1.0<br />
Selenium, Total 0.86 MG/KG 0.45 1.0<br />
Silicon, Total 44.8 MG/RG 2.2 1.0<br />
Tin, Total 1.2 MG/KG 1.0 1.0<br />
Strontium, Total 10.4 MG/[CG 0.01 1.0<br />
Thallium, Total 0.67 u MG/KG 0.67 1.0<br />
Uranium, Total 0.84 u MO/KG 0.84 110<br />
Vanadium, Total 0.16 MG/KG 0.09 1.0<br />
Zinc, Total 83.1 MG/KG 0.15 1.0<br />
606090624
CLIENT: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID ANALYTE<br />
-003 J11KL6 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06/DB/06<br />
LVL LOT 8: 0604L904<br />
REPORTING DILUTION<br />
.RESULT UNITS LIMIT FACTOR<br />
0.07 u MG/KG 0.07 1.0<br />
102 MG/KG 2.3 1.0<br />
0.59 u MO/KG 0.59 1.0<br />
0.55 MG/KG 0.23 1.0'<br />
2.D MG/KG 0,02 1.D<br />
0.02 u MG/KG 0.02 1.D<br />
0.49 u MG/KG 0.49 1.0<br />
9590 MG/KG 1.6 1.0<br />
0.07 u MG/KG 0.07 1.0<br />
0.13 u MG/KG 0.13 1.0<br />
0.45 MG/KO 0-12 1.0<br />
2.7 MG/KG 0.21 1.0<br />
115 MO/KG 3.4 1.0<br />
0.01 u MG/KG 0.01 1.0<br />
2780 MG/KG 2.2 1.0<br />
0.00 MG/KG 0.03 1.0<br />
467 MG/KG 0.93 1.0<br />
5.7 MO/KG 0.03 1.0<br />
0.28 u . MG/KG 0.28 1.0<br />
1310 MG/KG 0.73 1.0<br />
0.27 MG/KO 0.23 1.0<br />
5890 MG/7W 0.86 1.0<br />
2.4 MG/KG 0.30 1.0<br />
0.42 u MG/KG 0.42 1.0<br />
0.81 MO/KG 0.45 1.0<br />
45.3 MG/KG 2.2 110<br />
1.7 MG/KG 1.0 1.0<br />
7.0 MG/KG 0.01 1.0<br />
0.67 u MG/KG 0.67 1.0<br />
0.85 u MG/KG 0.85 1.0<br />
0.14 MG/KO 0.09 1.0<br />
40.5 MG/KG 0.15 1.0<br />
099090625
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06108106<br />
CLIENT: TNDHANFORD <strong>RC</strong>-<strong>047</strong> K0303 LVL LOT #t 0604L904<br />
WORK ORDER: 11343-606-001-9999-00<br />
REPORTING DILUTION<br />
SAMPLE SITE ID ANALYSE RESULT UNITS LIMIT FACTOR<br />
-Fez _zz a ....................... z _<br />
-004 J11KM0 Silver, Total 0.07 u MG/KG 0.07 1.0<br />
Aluminum, Total 39.5 MG/KG 2.3 1.0<br />
Arsenic, Total 0.59 u MG/KG 0.59 1.0<br />
Boron, Total 0.23 u MG/KG 0.23 1.0<br />
Barium, Total 3.2 MG/KG 0.02 1.0<br />
Beryllium, Total 0.02 u MG/KG 0.02 1.0<br />
Bismuth, Total 0.49 u MG/KG 0.49 1.0<br />
Calcium, Total 7900 MG/KG 1.6 1.0<br />
Cadmium, Total 0.07 u MG/KG 0.07 1.0<br />
Cobalt, Total 0.13 u MG/KG 0.13 1.0<br />
Chromium, Total 0.46 MG/KG 0.12 1.0<br />
Copper, Total - 3.6 MG/KG 0.21 1.0<br />
Iron, Total 142 MG/KG 3.4 1.0<br />
Mercury, Total 0.02 u MG/KG 0.02 1.0<br />
Potassium, Total 2730 MG/KG 2.2 1.0<br />
Lithium, Total 0.07 MG/KG .0.03 1.0<br />
Magnanium, Total 583 MG/KG 0.93 1.0<br />
Manganese, Total - 6.6 MG/KG 0.03 1.0<br />
Molybdenum, Total '0.28 u MG/KG 0.28 1.0<br />
Sodium, Total 1200 MG/KG 0.73 1.0<br />
Nickel, Total 0.23 u MG/KG 0.23 1.0<br />
Phouphorue, Total 5590 MG/KG 0.86 1.0<br />
Lead, Total 0.30 u MG/KG 0.30 1.0<br />
Antimony, Total 0.42 u MG/KG 0.42 1.0<br />
Selenium, Total 0.83 MG/KG 0.45 1.0<br />
Silicon, Total 52.6 MG/KG 2.2 1.0<br />
Tin, Total 1.1 MG/KG 1.0 1.0<br />
Strontium, Total 5.2 MG/KG 0.01 1.0<br />
Thallium, Total 0.67 a MG/KG 0.67 1.0<br />
Uranium, Total 0.85 u MG/KG 0.85 1.0<br />
Vanadium, Total 0.15 MG/KG 0.09 1.0<br />
Zinc, Total 98.7 MG/KG 0.15 1.0<br />
000000026
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06/03/06<br />
CLIENT: TNUMANFORD <strong>RC</strong>-<strong>047</strong> K0303 LVL LOT 6: 06D4L904<br />
WORK ORDER: 11343-606-001-9999-00<br />
REPORTING DILUTION<br />
SAMPLE SITE ID ANALYT6 RESULT UNITS LIMIT FACTOR<br />
-005 Ji1KM2 Silver, Total 0.07 u MG/KG 0.07 i 1.0<br />
Aluminum, Total 36.1 MG/KG 2.3 1.0<br />
Arsenic, Total 0.59 u MG/KG 0.59 1.0<br />
Boron, Total 0.30 MG/KG 0.23 1.0<br />
Barium, Total 1.9 MG/KG 0.02 1.0<br />
Beryllium, Total 0.02 u MG/KG 0,02 1.0<br />
Bismuth, Total 0.49 a MG/KG 0.49 1.0<br />
Calcium, Total Salo MG/KG 1.6 1.0<br />
Cadmium, Total 0.07 u MG/KG 0.07 1.0<br />
Cobalt, Total 0.13 u MG/KG 0.13 1.0<br />
Chromium, Total 0.46 MG/KG 0.12 110<br />
Copper, Total 2.9 MG/KG 0.21 1.0<br />
Iron, Total 116 MG/KG 3.4 1.0<br />
Mercury, Total 0.01 u MG/KG 0.01 1.0<br />
Potassium, Total 3060 MG/KG 2.2 1.0<br />
Lithium, Total 0.07 MO/KG 0.03 1.0<br />
Magnesium, Total 354 MG/KG 0.93 1.0<br />
Manganese, Total 3.2 MG/KG 0.03 1.0<br />
Molybdenum, Total 0.28 u MG/KG 0.28 110<br />
Sodium, Total 1430 MG/KG 0.73 1.0<br />
Nickel, Total 0.23 u MG/KG 0.23 1.0<br />
Phosphorus, Total 4350 MG/KG 0.86 1.0<br />
Lead, Total 0.43 MG/KG 0.30 1.0<br />
Antimony, Total 0.42 u MG/KG 0.42 1.0<br />
Selenium, Total 0.86 MG/KG 0.45 1.0<br />
Silicon, Total 44.6 MG/KG 2.2 1.0<br />
Tin, Total 1.3 MG/KG 1.0 1.0<br />
Strontium, Total 3.2 MG/KG 0.01 1.0<br />
Thallium, Total 0.67 u MG/KG 0.67 1.0<br />
Uranium, Total 0.8S u MO/KG 0.85 1.0<br />
Vanadium, Total 0.09 u MG/KG 0.09 1.0<br />
Zinc, Total 59..5 MG/KG 0.15 1.0<br />
996099627
CLIENT: TNURANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID<br />
-006 J11KM3<br />
ANALYTE<br />
Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06/08/06<br />
LVL LOT #: 0604L904<br />
REPORTING<br />
RESULT UNITS LIMIT<br />
0.07 u MG/KG 0.07<br />
45.1 MG/KG 2.3<br />
0.59 u MG/KG 0.59<br />
0.23 u MG/KG 0.23<br />
3.2 MG/KG 0.02<br />
0.02 v MG/KG 0.02<br />
0.49 u MG/KG 0.49<br />
7450 MG/KG 1.6<br />
0.07 u MG/KG 0.07<br />
0.13 u MG/KG 0.13<br />
0.47 MG/KG 0.12<br />
2.5 MG/KG 0.21<br />
192 MG/KG 3.4<br />
0.02 u MG/KG 0.02<br />
2620 MG/KG 2.2<br />
0.09 MG/KG 0.03<br />
394 MG/KG 0.93<br />
4.4 MG/KG 0.03<br />
0.28 u MG/KG 0.29<br />
1450 MG/KG 0.73<br />
0.34 MG/KG 0.23<br />
455D MG/KG 0.86<br />
0.30 u MG/KG 0.30<br />
0.42 u MG/KG 0.42<br />
0.75 MG/KG 0.45<br />
71.5 MG/KG 2.2<br />
1.2 MG/KG 1.0<br />
4.2 MG/1(G 0.01<br />
0.67 u MG/KG 0.67<br />
0.65 u MG/KG 0.85<br />
0.18 MG/KG 0109<br />
46.5 MG/KG 0.15<br />
DILUTION<br />
FACTOR<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.D<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
996999628
Lionville Laboratory, Inc,<br />
INORGANICS DATA SUMMARY REPORT 06108106<br />
CLIENT: TNUHANPORD <strong>RC</strong>-<strong>047</strong> KO303 LVL LOT 41: 06041,904<br />
WORK ORDER: 11343-606-001-9999-00<br />
REPORTING DILUTION<br />
SAMPLE SITS ID ANALYTB RESULT UNITS LIMIT<br />
::<br />
PACTOR<br />
-007 J13KM4 Silver, Total 0.07 u MG/KGx<br />
0.07 "'• 1.0<br />
Aluminum, Total 62.4 MG/KG 2.2 1.0<br />
Arsenic, Total 0.58 u MG/KG 0.58 1.0<br />
Boron, Total 0.23 a MG/KG 0.23 1.0<br />
Barium, Total 3.6 MG/KG 0.02 1.0<br />
Beryllium, Total 0.02 u MG/KG 0.02 1.0<br />
Bismuth, Total 0.49 u MG/KG 0.49 1.0<br />
Calcium, Total 11800 MG/KG 1.6 1.0<br />
Cadmium, Total 0.07 u MO/KG 0.07 1.0<br />
Cobalt, Total 0.13 u MG/KG 0.13 1.0<br />
Chromium, Total 0.45 MG/KG 0.12 1.0<br />
Copper, Total 3.1 MG/KG 0.21 1.0<br />
-- Iron, Total 117 MG/KG 3.3 1.0<br />
Mercury, Total 0.02 u MG/KG 0.02 1.0<br />
Potassium, Total 2980 MG/KG 2.2 1.0<br />
Lithium, Total 0.06 MG/KG 0.03 1.0<br />
Magnesium, Total 549 MG/KG 0.92 1.0<br />
Manganese, Total 4.7 MG/KG 0.03 1.0<br />
Molybdenum, Total 0.28 u MG/KG 0.28 1.0<br />
Sodium, Total 1440 MG/KG 0.72 1.0<br />
Nickel, Total 0.54 MG/KG 0.23 110<br />
Phosphorus, Total 7090 MG/KG 0.86 1.0<br />
Lead, Total 0.30 u MG/KG 0.30 1.0<br />
Antimony, Total 0.42 u MG/KG 0.42 1.0<br />
Selenium, Total 0.62 MG/KG 0.45 1.0<br />
Silicon, Total 43.5 MG/KG 2.2 1.0<br />
Tin, Total 1.5 MG/KG 1.0 1.0<br />
Strontium, Total 5.6 MG/KG 0.01 1.0<br />
Thallium, Total 0.67 a MG/KG 0.67 1.0<br />
Orenium, Total 0.64 u MG/KG 0.84 1.0<br />
Vanadium, Total 0.14 MG/KG 0.09 1.0<br />
Zinc, Total 61.6 MG/KG 0.15 1.0<br />
000000029
CLIENT: TNURANPORD <strong>RC</strong>-<strong>047</strong> K0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID ANALYTE<br />
-008 JIIKMS Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potannium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphoru0, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06108106<br />
LVL LOT 8: 06041,904<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
........ ......<br />
........<br />
0.07 u<br />
MG/KG<br />
..........<br />
0.07<br />
1.0<br />
70.8 MG/KG 2.2 1.0<br />
0.58 u MG/KG 0.69 1.0<br />
0.26 MG/NG 0.23 1.0<br />
4.5 MG/KG 0.02 1.0<br />
0.02 u MG/NG 0.02 1.0<br />
0.46 u MG/KG 0.48 1.0<br />
12800 MG/KG 1.5 1.0<br />
0.07 u MG/KG 0.07 1.0<br />
0.13 u MG/KG 0.13 1.0<br />
0.84 MG/KG 0.12 1.0<br />
3.2 MG/KG 0.21 1.0<br />
233 MG/KG 3.3 1.0<br />
O.D2 u MG/KG 0.02 1.0<br />
2920 MG/KG 2.1 1.0<br />
0.13 MG/KG 0.03 1.0<br />
566 MG/KG 0.91 1.0<br />
7.4 MG/KG 0.03 1.0<br />
0.27 u MG/KG 0.27 1.0<br />
1560 MG/KG 0.72 1.0<br />
0.96 MG/KG 0.23 1.0<br />
7290 MG/KG 0.65 1.0<br />
0.51 MG/KG 0.29 1.0<br />
0.41 u MG/KG 0.41 1.0<br />
0.79 MG/KG 0.44 1.0<br />
91.7 MG/KG 211 1.0<br />
1.1 MG/KG 1.0 1.0<br />
7.2 MG/KG 0.009 1.0<br />
0.66 u MG/KG 0.66 1.0<br />
0.83 u MG/KG 0.83 1.0<br />
0.40 MG/KG 0.08 1.0<br />
61.9 MG/KG 0.15 1.0<br />
000000030
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06/08/06<br />
CLIENT: TNUNANFORD <strong>RC</strong>-<strong>047</strong> K0303 LVL LOT R: 06041,904<br />
WORK ORDER: 11343-606-001-9999-00<br />
REPORTING DILUTION<br />
SAMPLE SITS ID ANALYTR RESULT UNITS LIMIT FACTOR<br />
-009 J11KM6 Silver, Total 0.07 u MG/KG 0.07 1.0<br />
Aluminum, Total 40.9 MG/KG 2.2 1.0<br />
Arsenic, Total O.SB a MG/KG 0.58 1.0<br />
Boron, Total 0.23 u MG/KG 0.23 1.0<br />
Barium, Total 6.6 MG/KG 0.02 1.0<br />
Beryllium, Total 0.02 u MG/KG 0.02 1.0<br />
Bismuth, Total 0.49 u MG/XG 0.49 1.0<br />
Calcium, Total 17900 MG/KG 1.6 110<br />
Cadmium, Total 0.07 u MG/KG 0.07 1.0<br />
Cobalt, Total 0.13 u MG/KG 0.13 1.0<br />
Chromium, Total 0.74 MG/KG 0.12 1.0<br />
Copper, Total 2.7 MG/KG 0.21 1.0<br />
Iron, Total 158 MG/XG 3.3 1.0<br />
Mercury, Total 0'.02 u MG/KG 0.02 1.0<br />
Potassium, Total 2930 MG/XG 2.2 1.0<br />
Lithium, Total 0.1 MG/KG 0.02 1.0<br />
MagneelUM, Total 605 MG/KG 0.92 1.0<br />
Manganese, Total 5.2 MG/KG 0.03 1.0<br />
Molybdenum, Total 0.28 u MG/XG 0.28 1.0<br />
Sodium, Total 1690 MG/KO 0.72 1.0<br />
Nickel, Total 2.9 MG/KG 0.23 1.0<br />
Phosphorus, Total 9490 MG/KG 0.86 1.0<br />
Lead, Total 0.31 MG/XG 0.30 1.0<br />
Antimony, Total 0.42 u MG/KG 0.42 1.0<br />
Selenium, Total 0.64 MG/KG 0.45 1.0<br />
Silicon, Total 74.4 MG/KG 2.3 1.0<br />
Tin, Total 1.3 MG/KG 1.0 1.0<br />
Strontium, Total 10.2 MG/KG 0,01 1.0<br />
ThalliuM, Total 0.67 u MG/KG 0.67 1.0<br />
Uranium, Total 0.94 u MG/KG 0.84 1.0<br />
Vanadium, Total 0.21 MG/KG 0.09 1.0<br />
Zinc, Total 73.0 MG/KG 0.15 1.0<br />
000000031
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06/06/06<br />
CLIENT: TNURANFORD <strong>RC</strong>-<strong>047</strong> X0303 LVL LOT 4: 06O4L904<br />
WORK ORDER: 11343-606-001-9999-00<br />
REPORTING DILUTION<br />
SAMPLE SITE ID ANALYTe RESULT UNITS LIMIT FACTOR<br />
-010 .711XV2 Silver, Total 0.07 u MG/KG 0.07 Lc 1.0<br />
Aluminum, Total 40.3 MG/KG 2.2 1.0<br />
Areenie, Total. 0.56 u MG/RG 0.56 1.0<br />
Boron, Total 0.23 u MG/KG 0.23 1.0<br />
Barium, Total 3.8 MG/KG 0.02 1.0<br />
Beryllium, Total 0.02 u MG/KG 0.02 1.0<br />
Bismuth, Total 0.49 u MG/KG 0.49 1.0<br />
Calcium, Total 6940 MG/KG 1.6 1.0<br />
Cadmium, Total 0.07 u MG/KG 0.07 1.0<br />
Cobalt, Total 0.13 u MG/KG 0.13 1.0<br />
Chromium, Total 0.61 MG/R& 0.12 1.0<br />
Copper, Total 3.0 MG/KG 0.21 110<br />
Iron, Total 164 MG/KG 3.3 1.0<br />
Mercury, Total 0.01 u MG/KG 0.01 1.0<br />
Potassium, Total 2880 MG/KG 2.2 1.0<br />
Lithium, Total 0.07 MG/KG 0.03 1.0<br />
Magnesium, Total 415 MG/KG 0.92 1.0<br />
Manganese, Total 4.5 MG/KG 0.03 110<br />
Molybdenum, Total 0.26 u MG/KG 0.28 1.0<br />
Sodium, Total 1470 MG/KG 0.72 1.0<br />
Nickel, Total 0.24 MG/KG 0.23 1.0<br />
Phosphorus, Total 5270 MG/KG a.86 1.0<br />
Lead, Total 0.33 MG/KG 0.30 1.0<br />
Antimony, Total 0.42 u MG/KG 0.42 1.0<br />
Selenium, Total 0.75 MG/KG 0.45 1.0<br />
Silicon, Total 73.5 MG/KG 2.2 1.0<br />
Tin, Total 1.3 MG/KG 1.0 1.0<br />
Strontium, Total 6.8 MG/ICG 0.01 1.0<br />
Thallium, Total 0.67 u MG/KG 0.67 1.0<br />
Uranium, Total 0.84 u MG/XG 0.84 1.0<br />
Vanadium, Total 0.16 MG/KG 0.09 1.0<br />
Zinc, Total 67.5 MG/1(G 0.15 1.0<br />
000000032
CLIENT: TNUMANPORD <strong>RC</strong>-<strong>047</strong> K0303<br />
MORK ORDER: 11343-606-001-9999-Ob<br />
SAMPLE SITE TO AKALYTS<br />
-011 J11KV2 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06/08/06<br />
LVL LOT #: 0604L904<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
0.07 u MG/KG 0.07 1.0<br />
55.7 MG/KG 2.2 1.0<br />
0.58 u MG/KG 0.58 1.0<br />
0.26 MG/KG 0.23 1.0<br />
4.7 MG/KG 0.02 1.0<br />
0.02 u WKS 0.02 1.0<br />
0.48 u MG/KG 0,48 1.0<br />
17400 MG/KG 1.5 1.0<br />
0.07 u MG/KG 0.07 1.0<br />
0.13 u MG/KG 0.13 1.0<br />
0.61 MG/KG 0.12 1.0<br />
2.8 MG/KG 0.21 1.0<br />
190 MG/KG 3.3 110<br />
0.01 u MG/KG 0.01 1.0<br />
3020 MG/KG 2,1 1.0<br />
0.10 MG/KG 0.03 1.0<br />
727 MG/KG 0.91 1.0<br />
7.0 MG/KG 0.03 1.0<br />
0.27 u MG/KG 0.27 110<br />
1550 MG/KG 0.72 1.0<br />
0.24 MG/KG 0.23 1.0<br />
9420 MG/KG 0.85 1.0<br />
0.46 MG/KG 0.29 1.0<br />
0.41 u MG/KG 0.41 1.0<br />
0.89 MG/KG 0.44 1.0<br />
69.3 MG/KG 2.1 1.0<br />
1.4 MG/KG 1.0 1.0<br />
16.3 MG/KG 0.009 1.0<br />
0.66 u MG/KG 0.66 1.0<br />
0.83 u MG/KG 0.83 1.0<br />
0.25 MG/KG 0.08 1.0<br />
78.6 MG/KG 0.15 1.0<br />
000000033
CLIENT: TNUNAMFORD <strong>RC</strong>-<strong>047</strong> K0202<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID ANALYTB<br />
-012 JIIL21 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Lionvilla Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06/08/06<br />
LVL LOT M! 06041,904<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
0.07 u MG/KG 0.01 1.0<br />
41.9 MG/KG 2.2 1.0<br />
0.56 u MO/KG 0.58 1.0<br />
0.23 u MG/KG 0.23 1.0<br />
5.4 MG/KG 0.02 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
0.49 u MG/KG D.49 1.0<br />
18900 MG/KG 1.6 1.0<br />
0.07 u MG/KG 0.07 1.0<br />
0.13 u MG/KG 0.13 1.0<br />
0.70 MG/KG 0.12 1.0<br />
2.9 MG/KG 0.21 1.0<br />
172 NO/KO 3.3 1.0<br />
0.01 u MG/KG 0.01 1.0<br />
2680 MG/KG 2.2 1.0<br />
0.13 MG/KG 0.03 1.0<br />
691 MG/KG 0.92 1.0<br />
4.9 MG/KG 0.03 1.0<br />
0.28 u MG/KG 0.28 1.0<br />
1600 MG/KG 0.72 1.0<br />
0.23 u MG/KG 0.23 1.0<br />
10600 MG/KG 5.1 6.0<br />
0.33 MG/KG 0.30 1.0<br />
0.42 u MG/KG 0.42 1.0<br />
1.2 MG/KG 0.45 1.0<br />
54.5 MG/KG 2.1 1.0<br />
1.1 MG/KG 1.0 1.0<br />
17.6 MG/KG 0.01 1.0<br />
0.67 u MG/KG 0.67 1.0<br />
0.84 u MG/KG 0.84 1.0<br />
0.20 MG/KG 0.09 1.0<br />
78.3 MG/KG 0.15 1.0<br />
000000034
CLIENT: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITS ID ANALYTE<br />
-013 JIIL23 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boson, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercu ry , Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
St ro ntium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06108106<br />
LVL LOT #: 0604 1,904<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
0_07 u MO/KG 0.07 1.0<br />
53.9 MG/KG 2.2 1.0<br />
0.58 u MG/KG 0.58 1.0<br />
0.23 u MG/KG 0.23 1.0<br />
5.7 MG/KG 0.02 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
0.48 u MG/KG 0.48 1.0<br />
18400 MG/KG 1.5 1.0<br />
0.07 U MG/KG 0.07 1.0<br />
0.13 u MG/KG 0.13 1.0<br />
0.65 MG/KG 0.12 1.0<br />
2.7 MG/KG 0.21 1.0<br />
177 MG/KG 3.3 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
2900 MG/KG 2.1 1.0<br />
0.09 MG/KG 0.03 1.0<br />
656 MG/KG 0.91 1^0<br />
5.7 MG/KG 0.03 1.0<br />
0.27 u MG/KG 0.27 1.0<br />
1590 MG/KG 0.72 1.0<br />
0.29 MG/KG 0.23 1.0<br />
10<strong>300</strong> MG/KG 5.1 6.0<br />
0.61 MG/KG 0.29 1.0<br />
0.41 u MG/KG 0.41 1.0<br />
0.64 MG/KG 0.44 1.0<br />
67.5 MG/KG 2.1 1.0<br />
1.3 MG/KG 1.0 1.0<br />
12.7 MG/KG 0.009 1.0<br />
0.66 u MG/KG 0.66 1.0<br />
0.63 u MG/KG 0.83 1.0<br />
0.20 MG/KG 0.08 1.0<br />
67.1 MG/KG 0.15 1.0<br />
000000035
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06/08/06<br />
CLIENT: TNGHANFORD <strong>RC</strong>-<strong>047</strong> K0303 LVL LOT #: 0604L904<br />
WORK ORDER: 11343-606-001-9999-00<br />
REPORTING DILUTION<br />
SAMPLE SITE ID AMALYTB RESULT UNITS LIMIT FACTOR<br />
-014 JIIL26 Silver, Total 0.07 u MG/KG 0.07 .1 .0<br />
Aluminum, Total 28.5 MG/KG 2.2 1.0<br />
Arsenic, Total 0.58 u MG/KG 0.58 1.0<br />
Boron, Total 0.23 u MG/KG 0.23 1.0<br />
Barium, Total 2.7 MG/KG 0.02 1.0<br />
Beryllium, Total 0.02 u MG/KG 0.02 1.0<br />
Bismuth, Total 0.46 u MG/KG 0.48 1.0<br />
Calcium, Total 14<strong>300</strong> MG/KG 1.5 110<br />
Cadmium, Total 0.07 u MG/KG 0.07 1.0<br />
Cobalt, Total 0.13 u MG/KG 0.13 1.0<br />
Chromium, Total 0.65 MG/KG 0.12 1.0<br />
Copper, Total 3.3 MG/KG 0.21 1.0<br />
Iron, Total 117 MG/KG 3.3 1.0<br />
Mercury, Total 0.02 u MG/KG 0.02 1.0<br />
Potassium, Total 3110 MG/KG 2.1 1.0<br />
Lithium, Total 0.05 MG/KG 0.03 1.0<br />
Magnesium, Total 597 MG/KG 0.91 1.0<br />
Manganese, Total 5.6 MG/KG 0.03 1.0<br />
Molybdenum, Total 0.27 u MG/KG 0.27 1.0<br />
Sodium, Total 1610 MG/KG 0.72 1.D<br />
Nickel, Total 0.23 u MG/KG 0.23 1.0<br />
Phosphorus, Total 8060 MG/KG 0.65 1.0<br />
Lead, Total 1.2 MG/KG 0.29 1.0<br />
Antimony, Total 0.41 u MG/KG 0.41 1.0<br />
Selenium, Total 0.84 MG/KG 0.44 1.0<br />
Silicon, Total 42.2 MG/KG 2.1 1.0<br />
Tin, Total 1.2 MG/KG 1.0 3.0<br />
Strontium, Total 7.6 MG/KG 0.009 1.0<br />
Thallium, Total 0.66 u MG/KG 0.66 1.0<br />
Uranium, Total 0.83 u MG/KG 0.83 1.0<br />
Vanadium, Total 0.08 u MG/KG 0.08 1.0<br />
Zinc, Total 106 MO/KG 0.15 1.0<br />
000000036
CLIENT: T14URANFORD <strong>RC</strong>-<strong>047</strong> K0203<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID ANALYTE<br />
-015 7111,36 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Biemuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potaaaium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 06/08/06<br />
LVL LOT 8: 06041,904<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
0.07 u MG/KG 0.07 1.0<br />
30.1 MG/KG 2.2 1.0<br />
0.58 u MG/KG 0.58 1.0<br />
0.23 u MG/KG 0.23 1.0<br />
6.0 MG/KG 0.02 1.0<br />
0.02 u MG/KG 0.02 1..0<br />
0.49 u MG/KG 0.49 1.0<br />
11200 MG/KG 1.6 1.0<br />
0.07 u MG/KG 0.07 1.0<br />
0.13 u MG/KG 0.13 1.0<br />
0.48 MG/KG 0.12 1.0<br />
2.7 MG/KG 0.21 1.0<br />
114 MG/KG 3.3 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
2690 MG/KG 2.2 1.0<br />
0.08 MG/KG 0.03 1.0<br />
429 MG/KG 0.92 1.0<br />
3.5 MG/KG 0.03 1.0<br />
0.29 u MG/KG 0.28 1.0<br />
1490 MG/KG 0.72 1.0<br />
0.36 MG/KG 0.23 1-0<br />
6620 MG/KG 0.86 1.0<br />
0.30 u MG/KG 0.30 1.0<br />
0.42 u MG/KG 0.42 L.0<br />
0.97 MG/KG 0.45 1.0<br />
56.8 MG/KG 2.2 1.0<br />
1.5 MG/KG 1.0 1.0<br />
6.7 MG/KG 0.01 1.0<br />
0.67 u MG/KG 0.67 1.0<br />
0.84 u MG/KG 0.84 1.0<br />
0.18 MG/KG 0.09 110<br />
41.4 MG/KG 0.15 1.0<br />
000000037
Lionville Laboratory, T.C.<br />
INORGANICS METHOD BLANK DATA SUMMARY PAGE 06/06/06<br />
CLIENT: TNURANPORD <strong>RC</strong>-<strong>047</strong> X0303 LVL LOT k: 0604L904<br />
WORK ORDER: 11343-606-001-9999-00<br />
REPORTING DILUTION<br />
SAMPLE SITE ID ANALYTB RESULT UNITS LIMIT FACTOR<br />
SLANKL 06LO324-MB1 Silver, Total 0.07 u MG/KG 0.07 1.0<br />
Aluminum, Total 13.3 MG/KG 2.4 1.0<br />
Arsenic, Total 0.61 u MG/KG 0.61 1.0<br />
Boron, Total 0.27 MG/KG 0.24 1.0<br />
Barium, Total 0.03 MG/KG 0.02 1.0<br />
Beryllium, Total 0.02 u MG/XG 0.02 1.0<br />
Bismuth, Total 0.61 v MG/XG 0.51 1.0<br />
Calcium, Total 1.6 u MG/XG 1.6 1.0<br />
Cadmium, Total 0.07 u MG/KG 0.07 1.0<br />
Cobalt, Total 0.14 u MG/KG 0.14 1.0<br />
Chromium, Total 0.13 a MG/KG 0.13 1.0<br />
Copper, Total - 0.56 MG/KG 0.22 1.0<br />
Iron, Total 3.5 u MG/KG 3.5 1.0<br />
Potassium, Total 2.3 u MG/KG 2.3 1.0<br />
Lithium, Total 0.03 MG/KG 0.03 1.0<br />
Magnesium, Total 0.97 u MG/KG 0.97 1.0<br />
Manganese, Total 0.03 u MG/KG 0.03 1.0<br />
Molybdenum, Total 0.29 u MG/KG 0.29 1.0<br />
Sodium, Total 0.76 u MG/KG 0.76 1.0<br />
Nickel, Total 0.24 u MG/XG 0.24 1.0<br />
Phosphorus, Total 0.90 u MG/%G 0.90 1.0<br />
Lead, Total 0.31 u MG/KG 0.31 1.0<br />
Antimony, Total 0.44 u MG/KG 0.44 1.0<br />
Selenium, Total 0.47 u MG/KG 0.47 1.0<br />
Silicon, Total 2.3 u MG/KG 2.3 1.0<br />
Tin, Total 1.6 MG/KG 1.1 1.0<br />
Strontium, Total 0.03 MG/KG 0.01 1.0<br />
Thallium, Total 0.70 u MG/KG 0.70 1.0<br />
Uranium, Total 3.6 MG/KG 0.88 1-0<br />
Vanadium, Total 0.13 MG/KG 0.09 1.0<br />
_ Zino, Total 0.16 u MG/KG D.16 1.0<br />
BLANKS 0600086-MB1 Mercury, Total 0.02 u MG/KG 0.02 1.0<br />
000000038
CLIENT: TNUNANFORD <strong>RC</strong>-<strong>047</strong> K03O3<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITU ID ANALYTB<br />
-001 J11KK8 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Sari., Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS ACCURACY REPORT 06/08/06<br />
LVL LOT M: 06O4L904<br />
SPIKED INITIAL SPIKED DILUTION<br />
SAMPLE RESULT<br />
AMOUNT<br />
4R9COV FACTOR(SPK)<br />
.......<br />
4.4<br />
.......<br />
O.07u<br />
......<br />
4.8<br />
.......<br />
91.7<br />
..........<br />
1.0<br />
200 26.2 190 91.5 3.0<br />
179 O.58u 190 93.2 1.0<br />
90.6 0,45 95.2 94.7 1.0<br />
199 4.4 190 97.1 1.0<br />
4.2 O.02u 4.9 87.5 1.0<br />
454 O.49u 476 95.4 110<br />
900 9790 2380 677.1+ 1.0<br />
4.4 O.O7u 4.8 91.7 110<br />
43.7 O.13u 47.6 91.8 1.0<br />
16.6 0.41 19.0 95.8 1.0<br />
23.9 - 2.6 23.8 89.1 1.0<br />
252 94.3 95.2 165.1 1.0<br />
070 2680 2380 <strong>100</strong>.3 1.0<br />
106 0.1 95.2 111.2 1.0<br />
980 471 2380 105.4 1.0<br />
50.1 3.0 47.6 98.9 1,0<br />
87.5 0.28u 95.2 91.9 110<br />
850 1340 2380 105.2 1.0<br />
44.9 O.23u 47.6 94.1 1.0<br />
500 6060 476 1553 * 6.0<br />
44.7 O.3OU 47.6 93.9 1.0<br />
43.3 0.42u 47.6 91.0 1.0<br />
174 0.63 190 91.1 1.0<br />
177 42.9 95.2 140.4 1.0<br />
83.3 1.0 u 95.2 87.5 1.0<br />
LIS 10.9 95.2 112.2 1.0<br />
L74 0.67u 190 91.6 1.0<br />
lie 0.84u 238 91.7 1.0<br />
44.7 0.14 47.6 93.6 1.0<br />
LOS 46.6 47.6 131.5 1.0<br />
000000039
Lionville Laboratory, Inc.<br />
INORGANIC$ ACCURACY REPORT 06/06/06<br />
CLIENT: TNURANPORD <strong>RC</strong>-<strong>047</strong> KO3O3 LVL LOT tl: 06O41,9O4<br />
WORK ORDER: 11343-606-001-9999-00<br />
SPIKED INITIAL SPIKED DILUTION<br />
SAMPLE SITE ID ANALYTE SAMPLE RESULT AMOUNT 4RECOV PACTOR(SPK)<br />
-002 S11KLS Mercury, Total 0.16 O.02u 0.16 99.4 ' 1`0<br />
966696049
Lionville Laboratory, Inc.<br />
INORGANICS PRECISION REPORT 06/08/06<br />
CLIENT: TNUNANPORD <strong>RC</strong>-<strong>047</strong> K0303 LVL LOT M: 0604L904<br />
WORK ORDER: 11343-606-001-9999-00<br />
INITIAL DILUTION<br />
SAMPLE SITE ID ANALYTE RBS13LT REPLICATE RPD FACTOR(REP)<br />
-001REP JS11UC8 Silver, Total 0 . 07u 0 . 07u NC 1.0 ••<br />
Aluminum, Total 26.2 67.2 87.8 1.0<br />
Arsenic, Total 0.58u 0.58u NC 1.0<br />
Boron, Total 0.45 0.26 54.6 1.0<br />
Barium, Total 4.4 4.6 4.4 1.0<br />
Beryllium, Total 0.02u 0.02u NC 1.0<br />
Bismuth, Total 0.49u 0.49u NC 1.0<br />
Calcium, Total 9790 17500 56.6 1.0<br />
Cadmium, Total 0.07u 0.07u NC 1.0<br />
Cobalt, Total 0.13u 0.13u NC 1.0<br />
Chromium, Total 0.41 0.71 54.0 1.0<br />
Copper, Total 2.6 2.6 0.00 1.0<br />
Iron, Total 94.3 287 101.1 1.0<br />
Potassium, Total 2680 2740 2.1 1.0<br />
Lithium, Total 0.1 0.17 56.4 1.0<br />
Magnesium, Total 471 667 34.4 1.0<br />
Manganese, Total 3.0 5.4 57.1 1.0<br />
Molybdenum, Total 0.28u D.2RU NC 1.D<br />
Sodium, Total 1340 150D 11.0 p 1.0<br />
Nickel, Total 0.23u 0.29 -iC' l^ 1.0<br />
Phosphorus, Total 6060 9340 42.6 1.0<br />
Lead, Total 0.30u 0.42 JN.- 1.0<br />
Antimony, Total 0.42u 0.42u NC 110<br />
Selenium, Total 0.63 0.82 25.5 1.0<br />
Silicon, Total<br />
Tin, Total<br />
42.9<br />
1.0 u<br />
64.9<br />
1.1<br />
40.8<br />
,?1C<br />
Y^<br />
Tr<br />
1.0<br />
1.0<br />
Strontium, Total 10.9 13.3 19.6 1.0<br />
Thallium, Total 0.67u 0.67u NC 1.0<br />
Uranium, Total 0.84u 0.84u NC 1.0<br />
vanadium, Total 0.14 0.29 72.1 1.0<br />
Zinc, Total 46.6 69.2 39.0 110<br />
000000041
Lionville Laboratory, Inc.<br />
INORGANICS PRECISION REPORT O6/OSI06<br />
CLIENT: TNURANPORD <strong>RC</strong>-<strong>047</strong> K03O3 LVL LOT k: 06041,904<br />
WORK ORDER: 11343-606-001- 9999-00<br />
INITIAL DILUTION<br />
SAMPLE SITE ID ANALYTE RESULT REPLICATE RPD FACTOR (REP)<br />
-0O2REP J1lKL5 Mercury, Total O.O2u 0.O2u NC 1.0<br />
699690042
SAMPLE SITE ID<br />
LCS1 06L0324-LC1<br />
ANALYTB<br />
Silver, LCS<br />
Aluminum, LCS<br />
Arsenic, LCS<br />
Boron, LCS<br />
Barium, LCS<br />
Beryllium, LCS<br />
Bismuth, LCS<br />
Calcium, LCS<br />
Cadmium, LCS<br />
Cobalt, LCS<br />
Chromium, LCS<br />
Copper, LCS<br />
Iron, LCS<br />
Potassium, LCS<br />
Lithium, LCS<br />
Magnesium, LCS<br />
manganese, LCS<br />
Molybdenum, LCS<br />
Sodium, LCS<br />
Nickel, LCS<br />
Phosphorus, LCS<br />
Lead, LCS<br />
Antimony, LCS<br />
Selenium, LCS<br />
Silicon, LCS<br />
Tin, LCS<br />
Strontium, LCS<br />
Thallium, LCS<br />
Uranium, LCS<br />
Vanadium, LCS<br />
Zinc, LCS<br />
LCS1 0600086-LC1 Mercury, LCS<br />
Lionville Laboratory, Inc.<br />
INORGANICS LABORATORY CONTROL STANDARDS REPORT 06108106<br />
CLIENT: TNUHANPORD <strong>RC</strong>-<strong>047</strong> K0303 LVL LOT 4: 0604L904<br />
WORK ORDER: 11343-606-001-9999-00<br />
SPIKED SPIKED<br />
SAMPLE AMOUNT UNITS 4RECOV<br />
49.2 50.0 MG/KG 98.4<br />
446 500 MG/KO 89.3<br />
972 <strong>100</strong>0 MG/KG 97.2<br />
487 500 MG/KG 97.4<br />
493 500 MG/KG 98.6<br />
23.7 25.0 MG/KG 94.8<br />
487 500 MG/KG 97.4<br />
2530 2500 MG/KG 101.3<br />
24.9 25.0 MG/KG 99.6<br />
247 250 MG/KG 99.0<br />
50.3 50.0 MG/KG <strong>100</strong>.6<br />
114 125 MG/KG 91.4<br />
499 500 MG/KG 99.8<br />
2330 2500 MG/KG 93.2<br />
512 500 MG/KG 102.4<br />
2470 2500 MG/KG 99.0<br />
76.7 75.0 MG/KG 102.3<br />
508 500 MG/KG 101.5<br />
2360 2500 MG/KG 94.2<br />
200 200 MG/KG <strong>100</strong>.2<br />
445 500 MG/KG 89.1<br />
248 250 MG/KG 99.3<br />
294 <strong>300</strong> MG/KG 98.1<br />
92B <strong>100</strong>0 MG/KG 92.8<br />
342 500 MG/KG 69.6<br />
505 500 MG/KG 101.0<br />
492 500 MG/KG 99.5<br />
995 <strong>100</strong>0 MG/KG 99.5<br />
251 250 MG/KG <strong>100</strong>.4<br />
249 250 MG/KG 99.5<br />
98.1 <strong>100</strong> MG/KG 98.1<br />
6.5 6.2 MG/KG 104.6<br />
000000043
Lionville Laboratory Use Only<br />
Eat. Final Pr<strong>of</strong>. Sampl ing Date<br />
Project<br />
Project ContocWhone N<br />
Lionville Laboratory Project Manager<br />
`<br />
QC _ S^CG _ Del ^( a. -.._ TAT<br />
Date Rec'd<br />
LL<br />
U(, Dale Due<br />
u<br />
S/J b^: /^ b.'<br />
MATRIX<br />
CODES:<br />
S . SON<br />
SE - Sediment<br />
SO - Solid<br />
SL- Sludge<br />
W - Weber<br />
O . Oil<br />
A-<br />
Ale<br />
DS- Drum<br />
Sales<br />
DL. Drum<br />
Liquids<br />
L - E%lCLP<br />
Leaclrete<br />
Wl - Wipe<br />
x - O<strong>the</strong>r<br />
F - Fish<br />
Lab<br />
ID<br />
W<br />
J 11 KX8<br />
1w<br />
Custody Transfer Record/Lab Work Request Page 1 <strong>of</strong> a Vil VLI<br />
LC^^^ } FIELD PERSONNEL: COMPLETE ONLY SHADED AREAS<br />
C li<br />
ent IDIDescdpson<br />
a,-<br />
Special lm truetlow -Vt-CV.-I, ljF_,b.Ur^ -<br />
i`001<br />
^I jwo c'Ld^s^ a. ,bc", r A o<br />
nleduls, pus, 5 %/«<br />
-Suv-,^ 060 - 0015-Vil, 4JLLJ<br />
M e,A-oJf> PCB, P-ra+ r SOYL .<br />
ReNngWshed Remind<br />
by i by<br />
Dole TNrla<br />
Ki.t J (^/,<br />
Rel<br />
ReMgerelar X<br />
•/Type Container<br />
Volume<br />
Prese rvatives<br />
ANALYSES<br />
REQUESTED<br />
Liquid<br />
Sold<br />
Liquid<br />
Solid<br />
Malrlx<br />
OC<br />
Clen as<br />
V)<br />
Malrbr<br />
Date Time<br />
Collected Collect<br />
_wAha^^m<br />
sMM®N<br />
one<br />
DNS: ,/<br />
i.<br />
z.<br />
3.<br />
a.<br />
S.<br />
8.<br />
Recohrod<br />
Raw"wehad- Received<br />
Data Tunis<br />
Irl W<br />
by<br />
W AS TEN<br />
CveB S<strong>RC</strong> v<br />
i<br />
two Time<br />
m<br />
G<br />
ne<br />
ON<br />
M n
Lionville Laboratory Use On ly<br />
Custody Transfer Record /Lab Work Request Page moo► -;L<br />
FIELD PERSONNEL: COMPLETE ONLY SHADED REAS<br />
Client! J C<br />
Retrlgeraux #<br />
Eat Final Prol, Sampling Date<br />
Project #<br />
Proje<br />
aQ<br />
#/Type Container<br />
Liqu b<br />
sous<br />
U uia<br />
ct<br />
ContacttPtlone # Volume<br />
Lionville Laborato ry Prole<br />
OC Del<br />
ensger<br />
TAT<br />
Pretereellves<br />
Solid<br />
ORGANIC I NORG<br />
Date Recd Dale Due<br />
ANALYSES<br />
REQUESTED<br />
Is- Q<br />
p<br />
<<br />
to<br />
a P<br />
=<br />
1i<br />
- '^<br />
V<br />
MATRIX<br />
j Lbmllle Laboratory Use Only j<br />
CODES:<br />
a- soil<br />
Sediment<br />
SO • Solid oot<br />
SL- Sludge<br />
W .Water.<br />
0- ON<br />
Db<br />
Client ID/Description<br />
MsMs<br />
OC<br />
Chosen<br />
V1<br />
MS IMSD<br />
Mad"<br />
Date Time<br />
Colleeled Collected<br />
y^<br />
O<br />
o<br />
O U<br />
A. Air a<br />
l7s- Drum<br />
Solids<br />
DL- Drum<br />
oZ^<br />
^/<br />
.X<br />
^j J<br />
Liquids I J1 L a3 13^b .::.: - X X<br />
[L<br />
- x<br />
L - EP/TCLP<br />
LaMiats 5 a - X j^ . . X<br />
w,- YApe<br />
X. Mer 015 Jt1 S-2 v lom<br />
<strong>of</strong>S X xi X X<br />
F- Fish<br />
Special Instruc tions:<br />
DATE/REVISIONS:<br />
J7,(^ a.<br />
Re6nb bhsd Received<br />
Dais<br />
RNingalshed Received<br />
Time<br />
Dole Time<br />
Res shed Received<br />
by by by by by<br />
x a3<br />
2.<br />
4.<br />
6.<br />
6.<br />
Deb Time<br />
'Kan,<br />
a<br />
m
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong> 259 Pain -I <strong>of</strong> 1<br />
Collector<br />
TILLER, B. TR KLINCKMAN<br />
Company ContactTelenhone No,<br />
JOAN KESSNER 375-4688<br />
Protect Coordinator<br />
KESSNER, IH Price Code 9N Data Turna round<br />
Atr Qwlaty q<br />
45 Days m<br />
rolect DesianaHon Sanmlina Locat ion <strong>SAF</strong> No.<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA S ediment and Ti 600-132/600-190 OFFAL <strong>RC</strong>-<strong>047</strong> 9<br />
Ice Chat No. Field Loaboolc No. COA Method <strong>of</strong> Shioment m<br />
EL-159S BESRAS6520 FED EX m<br />
Shipp Offsik Proaeriv No. ?<br />
Bi<br />
®^J<br />
ll <strong>of</strong> Lad in stAir Bi ll No.<br />
QLAERLINE SERVICES LIONVILLE _ ^^^ SEE OSPC<br />
POSSIBLE SAMPLE RAZARDS/REMARJSS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-266<br />
Collector<br />
TILLER, B. rA KLIN<br />
lest Deslanation<br />
<strong>100</strong> k <strong>300</strong> Ana <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and T1<br />
Ice Chi N%yc p<br />
PirG C-Q2- Qr<br />
Comaanr Contact<br />
JOAN KESSNER<br />
Samolioa location<br />
JBB4H-24 OFFAL Ili O 7-112<br />
Fltl k No.<br />
EL- 1595<br />
Teleabone No.<br />
375.4688<br />
COA<br />
BESRAS6520<br />
Pags 1 <strong>of</strong> 1<br />
Protect Coordinator<br />
KESSNER, JH Price Code g]v Data Turnaround IT<br />
IT<br />
,a<br />
45 Days 6<br />
<strong>SAF</strong> No.<br />
Air Quality E] m<br />
<strong>RC</strong>-M7<br />
Method <strong>of</strong> Shipment<br />
FED EX<br />
Slijinago To Oaaile Prooertv No. q^6 D ^ d Bi ll <strong>of</strong> LdindAlr Bill No,<br />
EBER . IN ERVIC[Sy LIONVILLE<br />
/7 SEEOSPC<br />
POS E HAZARDSWMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-267 Pw 1 <strong>of</strong> I<br />
Collector Com pa ny Conta ct<br />
TILLER, B. TN KLINCKMAN JOAN KFESSNER<br />
Telephone No,<br />
375-4688<br />
Pro ieet Coordirulor<br />
KESSNER, IH Price Code 9N Data T7lrnarsund00<br />
It<br />
Protect factiona lism<br />
<strong>100</strong> & <strong>300</strong> Ara Compooeul <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Stmmline Locaflon<br />
110-N-3 OFFAL<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Air Quality q 45 Days m<br />
0<br />
Ice Chat No. Field Logbook No. COA Method <strong>of</strong> SWnmeat<br />
^i ^^-- ." -'IjOJT EL, 1595 BESRAS6520 FED EX m<br />
Shin Olraite Property No.<br />
/J /l<br />
<strong>of</strong> Lad hWAtr Bi ll • ERI.iNE SERVICES LIONVILLE O^v 6K13 6)<br />
No.<br />
SEE OSPC<br />
POSSIBLE SAMPLE AAZARDS(REMARKS<br />
POTENTIAL RADIOACTIVE k;'"I"<br />
Bill<br />
AG G/P G/P eG aG aG<br />
1<br />
I B a 0 0<br />
250g log 155 505 mg 50g<br />
Seek—Win Seeite-Ml- SeehenMi. PCB.- 31182 Pw& _ SmaFVOA-<br />
Spaiol Sp..:, Spnial 1011 9270A(7CLI<br />
humwkau Iwrrmum. me,sener, ,<br />
-.";_ _<br />
J71KL6 OTHER SOLID APR 01 <strong>100</strong>6 IVLCJ Al X x<br />
,.»+s `1:s` ,,, "f-`*"^'`^ a.t.:^'un 1`'' ,s, â4 _'^' ti':,' - ^` t'`3--"<br />
CHAIN OF POSSESSION Si6n/Prinl Names SPECIAL INSTRUC`nONS<br />
Matrix •<br />
8tquidcd By/Removed Tom rose NOTE: Rwrlfim- ^^<br />
vamo paWTIimr<br />
perfam Genera Spec Nee vaaship bottle to 1]otrville Labs, if p ossible maintain 4 C<br />
EAS LOCKED STOR GE •Y- °"<br />
Got++* cooling. n& LAWnille: pmferm secants, this is surykis available. Canon Joan<br />
s6seAnmt<br />
Kessler upon receipt. _ a^J<br />
' s A Aw Dawelriroe iwd By/Stored In<br />
V Flo<br />
d B lRenloved t Dame Remived B r/Slarxd<br />
N<br />
t*iA 04<br />
DoaelFnrtr<br />
tr<br />
D!<br />
me<br />
;<br />
(1)Gao nnSpec-(Full<br />
Us t) l Anrcm io241, Aveissmy-127, Be Beryllium-7, 7, Cesium- 134, Cesium 137.<br />
Cobak-60.Erro0uml52,EmoO 154, Ewapiw 155,Pa sim 40, RaAium226. Radium?g,<br />
- Ru1hmmmlo6, Uranium2i5. Urariwn2381<br />
l'-)SaaMm iu89,90--To<br />
msaw,<br />
0'a<br />
ta .—<br />
B<br />
b<br />
emgved Rpn I)aieTmr Reccived 5 din<br />
/,<br />
7 /i I^.UO F^l^<br />
b<br />
ime<br />
l Sr Isotopic lnon lThm m t2321: Isatlpit Utiure m l Urary um233f274,<br />
Unoin235. m L4 n 2381; Is otopic nonlinu<br />
Month<br />
Ma - 6010 (Full Lisa) I Aluminum num Antimony. A rsenic, Ba rium, Beryl<br />
os.d,..s,s,a.<br />
m.o,.eLws :<br />
T•T<br />
li<br />
X<br />
nonli<br />
(3) ICP<br />
um, Bistauk Boron<br />
Cadmi CadmiumCalcium Calcium Llnmium.<br />
Cobal4 Coypuron<br />
Manganese.<br />
. I I:ad, lithium Magnesiumq Mangaae.<br />
Molybdenum Nickel, Phosphorus. Pa sion Se lenium Silicon. Silver. So di she y/R Flop O+te/fitrc Received<br />
x 3<br />
Dote?inc<br />
um Strontium Thallium<br />
T^&Llmnium Vandium7iml:Mem y-7471-(CV)<br />
x"a<br />
Relirpuishe y/Renpved From Da¢Tnx ived By/Swr4i TA Dale/rine<br />
LABORATORY Received By Tide Date/rime<br />
SECTION<br />
FINALSAMPLE Disposal Method Disposed By Daterrine<br />
DISPOSiTiON<br />
BHI-EE-011 (08/2912005)
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-271 Pa9F 1 -I<br />
olledor Company Ca rrie d Telephone No. Prulact Coord in ator<br />
TILLER, B. TR KLINC JOAN KESSNER 375-4688 KESSNER, IH<br />
rolect Desienation Serenade Location <strong>SAF</strong> No.<br />
<strong>100</strong> & <strong>300</strong> Am <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and n 1607-D2:1 OFFAL <strong>RC</strong>-<strong>047</strong><br />
[ce Cheat Na. r e- DI '^ No.<br />
Fk EL-1595<br />
S<br />
Offshe Property No. ADG DJ rI[/<br />
BESRAS6520<br />
BN <strong>of</strong> Ladhie/Alr Bill No.<br />
ERIJNE SERVIC LIONVBLB JJ SEE OSPC<br />
POSSIBLE SAMPLE HAZARDS MEMARKS<br />
POTEMTIALRADIOACTIVE
WashlnRton Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>473 J PW 3 err 3<br />
Follecter<br />
TILLER, B. TA KLINCKNIAN<br />
Co mwr Contact<br />
JOAN KESSNER<br />
Telrobooe No.<br />
375-4688<br />
Pro kct Coordinator<br />
KESSNER. B-1<br />
rice Cods 9N<br />
Data Ttu-narotl Iect Dada nation<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ts<br />
Samullm Loca tion<br />
BORROW PH' 24 OFFAL<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Air Quality q 45 Daym<br />
IceChesiNo. p _ Field Loebook No.<br />
EL-1595<br />
COA<br />
BESRAS6520<br />
MetLadorShbm<br />
FED EX<br />
t<br />
m<br />
9<br />
Shi Odsite Prooertr No. BIB <strong>of</strong> Ladh»/Air BIB No.<br />
ERLME SERVK;ES LIONVILLE /-'^fDO 0 SEE OSPC<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
v<br />
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-274 J PAV 1 °f J<br />
Collector<br />
TILLER, B.<br />
Tfl KLINCKMAN<br />
Protect Dasimation<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>B RA Sediment and Ti<br />
Ice Chest No.<br />
- 4"e-O2<br />
Cmulpsuy Contact Telephone No.<br />
JOAN KBSSNER 375J688<br />
Sammlissa Location<br />
YAKIMA RIDGE II OFFAL<br />
Field Loabook No.<br />
EL, 1595<br />
COA<br />
BESRAS6520<br />
Protect Cootdinalor<br />
KESSN8R, 1H<br />
<strong>SAF</strong> Na<br />
<strong>RC</strong>-<strong>047</strong><br />
Price Code Data 9N TutnRrotuo-+<br />
In<br />
45 Da m<br />
Alr Quality El<br />
m<br />
Method <strong>of</strong> Shipment 0]<br />
FED ETC<br />
m<br />
Shi Oftalte Properly No. QO /D Big LLSt^dAlr Bill No.<br />
T<br />
RERLINE SERVICES LIONVIILE H<br />
POSSIBLE SAMPLE IIAZARDSIREMAIM<br />
0<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-275 J NF L <strong>of</strong> L<br />
TILLER, B. TR KIINCKAtAN<br />
C JOAN ESSNER<br />
T o<br />
375-4688 KESSNEA, Hlpator Price Code 9N Data TurnaroupdN<br />
roleet Ded imation Sampling Location <strong>SAF</strong> No. Air Quality E]<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> Compon ent <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti VERKITA UPRIVER ON SOUTH SIDE OFFAL <strong>RC</strong>-<strong>047</strong><br />
In<br />
45 Days (m<br />
Ice Cheat No. /^ /^ ^±^ Field Logbook No. COA<br />
m<br />
Metkod <strong>of</strong> Shipment<br />
4 T C' 612 ',7 a' `r FL- 1595 BESRAS6520 FED FX m<br />
9<br />
S OtTsite Proxrly No. Bie <strong>of</strong> LadhadAir Bill No.<br />
_ RERIAI@SERVICPS^ pNVIIAE ^Odo 33 o SEEOSPC<br />
POSSIBLE SAM I 7.A REMARKS<br />
POTEN7ALR4010ACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-276<br />
Collector<br />
TILLER, B. TR KUNCKMAN<br />
roieet Desho stlose<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> The <strong>RC</strong>BRA Sediment and Tie<br />
Ice Chest No.^A<br />
G — OZ -Sz s -<br />
S EBE L o S .R LIONVRJE<br />
POSSIBLE SAMPLE nAZARDS IR MARKS<br />
Company Contact Telephone No.<br />
LOAN KESSNER 375-4688<br />
Safrplloa Loca tion<br />
McOEE RANCH OFFAL<br />
Fi el d Logbook No.<br />
EL-1595<br />
OHsile Property No.<br />
POTENTIAL RADIOACTIVE<br />
_<br />
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTOIJIMAMPLE ANALYSIS REQUEST <strong>RC</strong>"<strong>047</strong>.277 I NP L <strong>of</strong> L<br />
Reclor _<br />
Comoaor Contact Telmhone No. Protect Coordinator<br />
9N<br />
Price<br />
Data Tutnarousut<br />
TILLER, B. 11 KUNCKMAM - JOAN KESSNER 775-4688 KESSNER, 7H<br />
In<br />
rolectDeslanation Sa urnslinaLoealim <strong>SAF</strong>No.<br />
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0<br />
Ice Chest No. o<br />
Field Loaboolc No. COA Melhad <strong>of</strong> SWm Sent<br />
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ShalooedTo - OBslle Property No. Bill Ladina/A ir Bi ll No.<br />
BE L.AIESERVIC LIONVILLE 1 406 b 3 3 D 1 EEOSPC<br />
POSSIBLE SAMPLE IIAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-322 Page L <strong>of</strong> I<br />
Collector<br />
TILLER, B. TN KLINCKMAN<br />
Company Contact<br />
JOAN KFSSNER<br />
Telephone No.<br />
375-4688<br />
Proiect Coordinator<br />
KESSNER, lH Pria Cow 9N Data 7•aswrou<br />
In<br />
Air Quality p 45 Days%<br />
Protect Designation Sampline Location <strong>SAF</strong> No.<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti 1(10-DO8:2 OFFAL <strong>RC</strong>-<strong>047</strong> m<br />
lee Chen( No. r Field Logbook No. COA Method <strong>of</strong> Shipment<br />
EL-1595 BEESSRAS6520 FED EX<br />
ShjRocdTo O(LSile Property No. 0 / ^<br />
E RLM LIONVILLE g O (/<br />
POSSIBLE SAMPLE H AZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-323 Pea 1 <strong>of</strong> I<br />
cotledcor<br />
TILLER, B. TR KLINCKMAN<br />
Prolect Dafenallo p<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> Cam ent <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
I" Chest No.<br />
.<br />
y^<br />
g j^C-01 '„rdf<br />
Company Canted Telephone No.<br />
JOAN KESSNER 375-4688<br />
SamolWa Loaaon<br />
<strong>100</strong>-D-492 OFFAL<br />
Prolect Coordinator<br />
KESSNER, )H<br />
<strong>SAF</strong>No.<br />
<strong>RC</strong>-<strong>047</strong><br />
FirW Loahaok No.<br />
COA<br />
Method <strong>of</strong> Shfomepl<br />
Shipp ed To<br />
EI. 1595<br />
ORsite Property No.yy^^ G<br />
/'>'Qlo6?.3<br />
BFSRAS6520<br />
FED EX<br />
Bi ll ER ESERVIC LIONVRtE<br />
<strong>of</strong> Ladipe/Air Bill No,<br />
EE OSPC<br />
POSSIBLE SAMPLE HAZARDS(REMARKS<br />
POTENTIALRADIOACTIVE
Washington Closure <strong>Hanford</strong> " CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-328 gR 1 <strong>of</strong> I<br />
Collector Company Contact Telephone No. Proled Coordinator<br />
Price Code 9N Data Turnamm<br />
TILLER, B. TR KLINCKMAN JOAN KESSNER 375-4688 - KESSNER, IH in<br />
Protect Designation Samoan Loca<br />
Air Quality q 45 Days%<br />
ti on <strong>SAF</strong> No.<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> Compon en t <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti 116-DR-I.DR-2/<strong>100</strong>-D-22 OFFAL <strong>RC</strong>-<strong>047</strong> m<br />
Ice Chest No.n Feld Logbook No. COA Method <strong>of</strong> Shiomeal m<br />
O/c C— 0.2 '4rQ.r El: 1595 - BFSRAS6520 FED EX m<br />
Shi 'o Offaite Properly No. ^D<br />
Bill <strong>of</strong> LadiaWAir Bill No.<br />
OERLINE SERVICES LIONVILLE SEE OSPC<br />
POSSIBLE SAMPLE HAZARDS/REMARES<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE -ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-330 [Ng-<br />
Collector<br />
TILLER, B.<br />
TB KLINCKMAN<br />
Protect Dealenadon<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Ice Cheat No . yy ^<br />
/Lxe e2 -„s175<br />
Sh'<br />
ComOauv Contact Telephone No,<br />
JOAN KESSNER 375.4688<br />
Saco olina L. scaflon<br />
BORROW PIT 23 OFFAL<br />
Field Loabs6ok No.<br />
EI.- is93<br />
Off lte Properly No.<br />
^<br />
COA<br />
BESRAS6520 -<br />
Protect Coordinator<br />
KPSSNER, III<br />
2 Big <strong>of</strong> LadilldAir Bill No.<br />
B FJ2LINESERVICPS LK)NVILLE<br />
4Os%s3t^ SEE OSPC<br />
1s SSIBLE SAMPLE IIAZARD.MU MARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>447-332 jPw I ar i<br />
Collector Company Contact Telephone No. Protect Coordinator<br />
TILLER, B. TR KLINCKMAN JOAN KESSNP,R 3754688 KESSNF.R, JH Prim Code 9N Data Turnaround;<br />
diem Desiapaaon Samptina Lorstim <strong>SAF</strong> No.<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> on <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Scdimml and Ti 600-131 OFFAL <strong>RC</strong>-<strong>047</strong><br />
Method<br />
lee Chest No. FiE 1595ookNo.<br />
aFjCC-0,2-tvs, BESRAS6520<br />
FED EX<br />
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ESERVI /LIONVILIE<br />
Ofbite Property No. ^/^n/ Q p<br />
/lf/Y/U33o<br />
Bill <strong>of</strong> Ladlae,/Alr Bill No.<br />
SEE OSPC<br />
POSSIBLE SAMPLE 11AZARDSMEMARKS<br />
POTEA77AL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-343 P 3 d 1<br />
Collector<br />
TILLER, B. TN KLINCKMAN<br />
Coolant, Contact<br />
JOAN KESSNER<br />
Telephone No.<br />
375.4688<br />
Protect Coordina tor<br />
KESSNER, IH<br />
Price Cade 9N Data Turparou11a9<br />
w<br />
Protect Designa tion<br />
<strong>100</strong> & <strong>300</strong> Ar a Co ent<strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sedim<br />
Samplingtion Loca <strong>SAF</strong> No.<br />
AIC Quality C]<br />
45 Days<br />
m<br />
e<br />
en t and Ti CENTRAL PLATEAU SHRUB STEPPE OFFAL <strong>RC</strong>-<strong>047</strong> m<br />
Ina Chest No.<br />
4ce e^"U 2-<br />
Field Logbook No. COA Method <strong>of</strong> Shipment mm<br />
—,D,% ELLI595 BESRAS6520 FED EX m<br />
Sh ORstle Property No<br />
Air BW No.<br />
_ BERLBdE SERVICE LIONVILE 14 0 6 033D<br />
B ll E OSPC<br />
POSSIBL PLEHAZARDSIREMARKS<br />
PO7'EA77AL RADIOACTIVE
Lionville Laboratory Incorporated<br />
SAMPLE RECEIPT CHECKLIST (S<strong>RC</strong>)<br />
CLIENT: __Tt U 1aRr^ c^ Date:<br />
e Order / Pmjact# 1<br />
<strong>SAF</strong>N / W# / Release #: <strong>RC</strong> ^^^<br />
v Batch #: r I n T I Sample Custodian:<br />
1. Samples Hand Delivered QLShipped<br />
2. Custody seals on coolers or shipping<br />
container intact, signed and dated?<br />
3. Outside <strong>of</strong> coolers or shipping containe rs are<br />
free from damage?<br />
4. All expected papetworkreceived (roc and<br />
o<strong>the</strong>r client specific information) sealed in<br />
plastic bag and easily accessible?<br />
5. Samples Mcciv4 cool r ambient? Z Q<br />
6. Custody seals on sample containe rs intact.<br />
signed and dated?<br />
7. coc signed and dated?<br />
S. Sample containers are intact?<br />
9. All samples on coc received? A ll samples<br />
received on coc?<br />
10. All sample label information matches coc?<br />
11. Samples properly preserved?<br />
12. Samples received within hold times?<br />
Short holds taken to wet lab?<br />
SR-001-11<br />
13. VOA, TOC, TOX free <strong>of</strong> headspaoe?<br />
14. QC stickers placed on bottles designated by<br />
client?<br />
15. Shipment meets LvLI Sample Acceptance<br />
Po licy? (Identify all bottles not within<br />
policy. See reverse side for po licy)<br />
16. Project Manager c=bwtedconcetactg<br />
discrepancies? namedate (or samples<br />
outside crite ria)<br />
vLI<br />
?4rs<br />
1/O<br />
7<br />
O No<br />
Yes O No<br />
Wes O No<br />
TTemp '7 3 °C<br />
¢(Yes O No O No Sells<br />
.r<br />
es 13 No<br />
0 Yes O No<br />
(L^Ya O No<br />
Yet q No<br />
)dYa<br />
O No<br />
Yes<br />
Jd O No<br />
0 Yu<br />
O Yes<br />
O Yes<br />
i7Yes<br />
q No ,ey NIA<br />
q No /C^4A<br />
O NO<br />
a7 a S 05 '7<br />
Airbill# 7 Cf<br />
O No Sells Comments<br />
Cooler# SAuDS—\b---3<br />
O No<br />
Dis r zodn<br />
000000061
Lionville Laboratory, Inc.<br />
BNA ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/28/06 LVL LOT # :0 E<br />
N<br />
r<br />
MME i<br />
3V` 24<br />
CLIENT ID LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
J11KKB 001 SO 06LE0457 04/05/06 06/02/06 06/29/06<br />
J11KKB 001 MS SO 06LE0457 04/05/06 06/02/06 06/29/06<br />
J11KK8 001 MSD SO 06LE0457 04/05/06 06/02/06 06/29/06<br />
J11KL5 002 SO 06LE0457 04/05/06 06/02/06 07/02/06<br />
JIIKL6 003 SO 06LE0457 04/03/06 06/02/06 06/30/06<br />
J11KMO 004 SO 06LE0457 04/05/06 06/02/06 06/30/06<br />
J11KM2 005 SO 06LE0457 04/03/06 06/02/06 06/30/06<br />
J11KM3 006 SO 06LE0457 04/03/06 06/02/06 06/30/06<br />
J11KM4 007 SO 06LE04S7 04/03/06 06/02/06 06/30/06<br />
J11KM5 008 SO 06LE0457 - 04/03/06 06/02/06 06/30/06<br />
J11KM6 009 SO 06LE0457 04/03/06 06/02/06 06/30/06<br />
J11KV1 010 SO 06LE0457 04/05/06 06/02/06 06/30/06<br />
J11KV2 011 SO 06LE0457 04/05/06 06/02/06 06/30/06<br />
J11L21 012 SO 06LE0457 04/03/06 06/02/06 06/30/06<br />
JllL23 013 SO 06LE0457 04/03/06 06/02/06 06/30/06<br />
0111,25 014 SO 06LE0457 04/05/06 06/02/06 06/30/06<br />
JIIL36 015 SO 06LE0457 04/03/06 06/02/06 06/30/06<br />
LAB QC:<br />
SBLKZH MB1 S 06LE0457 N/A 06/02/06 07/02/06<br />
SBLKZH MB1 BS S 06LE0457 N/A 06/02/06 07/02/06<br />
000000001
Case Narrative<br />
Client: TNU-HANFORD <strong>RC</strong>-<strong>047</strong> W.O. #: 11343-606-001-9999-00<br />
LVL #: 06041,904 Date Received: 04-28-2006<br />
SDG/<strong>SAF</strong> # K0303/<strong>RC</strong>-<strong>047</strong><br />
SEMIVOLATILE<br />
Fifteen (15) soil (mice) samples were collected on 04-03,05-2006.<br />
The samples and <strong>the</strong>ir associated QC samples were extracted according to Lionville Laboratory<br />
SOPs based on SW 846 method 3540C on 06-02-2006 and analyzed according to criteria set forth<br />
in Lionville Laboratory SOPS based on SW 846 Method 8270C for TCL Semivolatile target<br />
compounds on 06-29,30-2006 and 07-02-2006.<br />
The following is a summary <strong>of</strong> QC results accompanying <strong>the</strong> sample results. Lionville Laboratory<br />
Inc (LvLI) certifies that all test results meet <strong>the</strong> requirements <strong>of</strong> NELAC except as noted below:<br />
1. All results presented in this report are derived from samples that met LvLI's sample<br />
acceptance policy with <strong>the</strong> exception <strong>of</strong> some discrepancies, which were documented on <strong>the</strong><br />
Sample Receipt Checklist.<br />
2. All samples were stored in a refrigerator (ID# R003) that malfunctioned and failed to<br />
maintain <strong>the</strong> required sample storing temperature (4°C +/- 2°C) on 05-10-2006. A copy <strong>of</strong><br />
<strong>the</strong> Sample Discrepancy Report (SDR) has been enclosed.<br />
3. Samples were extracted outside required holding time. A copy <strong>of</strong> <strong>the</strong> Sample Discrepancy<br />
Report (SDR) has been enclosed.<br />
4. Due to <strong>the</strong> nature <strong>of</strong> <strong>the</strong> sample matrix, approximately 2g initial sample volume for <strong>the</strong><br />
extraction and reduced final volume was used for <strong>the</strong> analysis. A copy <strong>of</strong> <strong>the</strong> Sample<br />
Extraction Record has been enclosed for detail information.<br />
5. All sample results were reported on a wet-weight basis.<br />
6. Non-target compounds were detected in <strong>the</strong> samples.<br />
7. Seventy-seven (77) <strong>of</strong> one hundred fourteen (114) surrogate recoveries were outside<br />
acceptance criteria. A copy <strong>of</strong> <strong>the</strong> Sample Discrepancy Report (SDR) has been enclosed.<br />
The results presented in this report relate only to <strong>the</strong> analytical testing and conditions <strong>of</strong> <strong>the</strong> samples at receipt and during storage. All pages <strong>of</strong> this report are integral parts <strong>of</strong><br />
<strong>the</strong> analytical data. Therefore, this report should only be reproduced in its entirety <strong>of</strong> 5 3 pages.<br />
208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-<strong>300</strong>0 • Fax (610) 280-3041<br />
4(30.tVLi6(Cf4iL•
8. One hundred twenty-two (122) <strong>of</strong> one hundred twenty-eight (128) matrix spike recoveries<br />
were outside acceptance criteria. A copy <strong>of</strong> <strong>the</strong> Sample Discrepancy Report (SDR) has<br />
been enclosed.<br />
9. Sixty-three (63) <strong>of</strong> sixty-four (64) blank spike recoveries were outside acceptance criteria.<br />
A copy <strong>of</strong> <strong>the</strong> Sample Discrepancy Report (SDR) has been enclosed.<br />
10. The method blank contained <strong>the</strong> common laboratory contaminant Bis (2-Ethylhexyl)<br />
phthalate at a level less than <strong>the</strong> CRQL.<br />
11. Internal standard area criteria were not met for sample JllKK8 MSD. The analysis <strong>of</strong><br />
associated matrix spike sample fulfills <strong>the</strong> reanalysis requirement.<br />
12. Manual integrations are performed according to SOP QA-125 to produce quality data with<br />
<strong>the</strong> utmost integrity. All manual integrations are required to be technically valid and<br />
properly documented. Appropriate technical flags are defined in <strong>the</strong> Glossary ("Technical<br />
Flags For Manual Integration").<br />
13. LvLI is NELAP accredited by <strong>the</strong> state <strong>of</strong> Pennsylvania and holds over 20 additional state<br />
accreditations. For a complete listing <strong>of</strong> accrediting authorities and <strong>the</strong> corresponding<br />
analytes/methods, please contact your Project Manager.<br />
14. I certify, that this sample data package is in compliance with SOW requirements, both<br />
technically and for completeness, o<strong>the</strong>r than <strong>the</strong> conditions detailed above. Release <strong>of</strong> <strong>the</strong><br />
data, contained in this hard-copy data package, has been authorized, by <strong>the</strong> Laboratory<br />
Manager or a designee, as verified by <strong>the</strong> following signature.<br />
am<br />
`l<br />
Iai aniel<br />
La ratory Manager<br />
Lionville Laboratory Incorporated<br />
som\gomp\data\bna\mu-hanford\0604-904.doa<br />
208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-<strong>300</strong>0 • Fax (610) 280-3041<br />
ate<br />
V<br />
•raasuswxat4u
_WrrvurV r..duvrdtory -)ampie<br />
Initiator. Orlette Johnson Batch: ^<br />
Date: §117106 Samples:<br />
Client: dQt Method:<br />
<strong>RC</strong>oLi7<br />
1. Reason for SDR<br />
ncy Keport (ZwK) 111 - ' to o rr<br />
Parameter:<br />
Matrix: i] A<br />
Prep Batch:<br />
a. COC Disc repancy , Tech P r<strong>of</strong>ile Error Client Request Sampler Error on C-O-C<br />
Transc ri ption Error _ Wrong Test Code _ O<strong>the</strong>r<br />
b. General Discrepancy<br />
Missing Sample/Extract _ Container B roken Wrong Sample Pulled _ Label ID's Illegible<br />
Hold Time Exceeded Insufficient Sample Preserva ti on Wrong _ Received Past Hold<br />
_ Imp roper Bottle Type _ Not Amenable to Analysis X O<strong>the</strong>r<br />
Note`: Verified by (Logan] or [Prep Group] (circle) ... signaturelcI ta:<br />
c. Problem (Include all relevant spe cific results; attach data if necessa ry)<br />
On 5/10106 sample storage refrigerator ID# R003 malfunctioned and was not holding <strong>the</strong> required sample storage<br />
temperature <strong>of</strong> 4°C +/- 2°C<br />
2. Known or P robable Causes(s)<br />
B ro ken motor<br />
3-Discussion and Proposed Action O<strong>the</strong>r Desc ri ptions<br />
_ Re-log At <strong>the</strong> time <strong>of</strong> malfur ^tion R003 was used for storage <strong>of</strong> samples received<br />
_ En tire Batch for extractable organics, metals and wet chemist ry (except TOG) analyses.<br />
Following Samples: All samples we re removed from R003 to ano<strong>the</strong>r refrigerator on 5110/06.<br />
_ Re-leach R003 was tagged out on 5/10106, repaired on 5112/06, and we have<br />
_ Re-extractcertified fiat R003 is maintaining <strong>the</strong> required sample storage temperatu re.<br />
_ Re-digest<br />
Revise EDD<br />
_ Change Test Code to<br />
_ Place On/Take Off Hold (circle)<br />
4. Project Manager Instructions ... signaturerdate:<br />
Concur with Proposed Ac ti on<br />
ag ree with Proposed Action; See Instruc ti on<br />
nclude In Case Narrative<br />
Client Conta ^''<br />
Date/Person t3 G`40<br />
_ Add<br />
Cancel<br />
5. Final Action ... s4nature/dau O<strong>the</strong>r Explanation:<br />
_ VoRed rei4][leach][e ][digest][ n lysisJ clil<br />
eluded in Case Narrative<br />
_ Hard Copy COC Revised<br />
Elect ro nic COC Revised<br />
_ EDD Cor rections Completed<br />
When Final Action has been recorded, forward original to QA Specialist for distribution and filing.<br />
Route Distribu ti on <strong>of</strong> Completed SDR Route Distribution <strong>of</strong> Completed SDR<br />
X Ini ti ator_ Metals: Welsh<br />
X Lab Manager. I. Dan' _ _ Inorganic: Perrone<br />
X P roject Mgr. Ston ohnso GC/LC: Kiger<br />
_ Data Management MS: Schnsider/Beley C6t r0(C rL<br />
_ Sample P rep: Beegle/Kiger — _— Login: Per ry<br />
b,<br />
Admin:<br />
O <strong>the</strong>r.<br />
c `^r6^`'<br />
QA-105-A-0805<br />
13 00000004
Lionville Laborato ry Sample Discrepancy Report (SDR) SDR #: 06PM002<br />
Initiator: Orlette Johnson Batch: 06d6l,gM Parameter. G6 2S14<br />
Date: 6/21/06 Samples: Matrix: 'td<br />
...<br />
Client: 1W 4vii6d A Q2_ Method: cAm1cLPr Prep Batch:<br />
1. Reason for SDR<br />
a. COC Discrepancy _ Tech P r<strong>of</strong>ile Error Client Request Sampler Error on C-O-C<br />
Transcription Error _ Wrong Test Code _ O <strong>the</strong>r<br />
b. General Discrepancy .<br />
_ Missing Sample/Extract _ Container B roken _ Wrong Sample Pulled _ Label ID's Illegible<br />
X Hold Time Exceeded Insufficient Sample _ Preservation Wrong _ Received Past Hold<br />
_ Improper Bottle Type _ Not Amenable to Analysis<br />
Note: Vented by [Log4ril or (Prep Group) (drde)...algnatureddate:<br />
c. Problem (In clude all relevant specific results; attach data if necessa ry)<br />
Sample(s) waslwe re extracted 4^ days beyond <strong>the</strong> hold time<br />
Sa* rt o4d to 4 js kw/ku?'^V6 &J1t.1A6<br />
Z Known or P robable Causes(s) due to a temporary glassware shortage created by a malfunc tioning d rying kiln I.e,<br />
much <strong>of</strong> our glassware was lost when one <strong>of</strong> <strong>the</strong> kilns overheated. We made eve ry effort to replace glassware as soon as<br />
possible but our needs exceeded on-<strong>the</strong>-shelf vendor stocks <strong>of</strong> certain c ritical Items. This problem was exacerbated by an<br />
unusually high number <strong>of</strong> samples received du ring this period <strong>of</strong> time for organics extraction.<br />
3. Discussion and P roposed Action O<strong>the</strong>r Description:<br />
_ Re-log<br />
_ Entire Batch<br />
Following Samples: We have replenished glasswa re stocks to higher levels than those<br />
_ Re-leach in-house before <strong>the</strong> kiln malfunction. We have also replaced <strong>the</strong> kiln.<br />
_ Re-extract<br />
_ Re-digest<br />
_ Revise EDD<br />
Change Test Code to<br />
_ Place O rdTake Off Hold (circle)<br />
4. P roject Manager Instructions ... smnature/date:<br />
_ Concur with Proposed Action<br />
Disagree with P roposed Action; See Instruction<br />
X Include in Case Narra ti<br />
ve<br />
_ Client Contacted:<br />
Date/Person<br />
_ Add<br />
Cancel<br />
S. Final Action ... synatureidate: O<strong>the</strong>r Explana ti<br />
on:<br />
Ve rified re-[log][leach][ digest][analysr ] ( rcle)<br />
X Included in Case Narrative<br />
_ Hard Copy COC Revised<br />
Electronic COC Revised<br />
_ EDD Corrections Completed<br />
When Final Action has been recorded, forward original to OA Specialist for distribution and filing.<br />
Route Distribution <strong>of</strong> Completed SDR<br />
X Ini<br />
Route Distribution <strong>of</strong> Completed SDR<br />
ti<br />
ator<br />
X Lab Genera[ Man I. anrels<br />
X P roject Mgr. Ston o' son<br />
X Data Management<br />
_ Sample Prep: I(iger<br />
—<br />
_ Metals: Welsh<br />
_ _ Inorganic: Perrone<br />
GC/LC: Kiger<br />
'L `^ MS: Schne[de arclen<br />
_ _ Log-in: Per ry<br />
Admin:<br />
O<strong>the</strong>r.<br />
oA-ios-A-osos<br />
096000605
Lionville Laborato ry Sample Discrepancy Repo rt (SDR) SDR #: aarjrZZ?<br />
Initiator: Batch: L Parameter: 06WH<br />
Date: Samples: _ _ Matrix:<br />
Client: Method: wwi Prep Batch:<br />
1. Reason for SDR<br />
a. CDC Discrepancy _ Tech P r<strong>of</strong>ile Er ror Client RequestSampler Er ro r on C-0-C<br />
Transcription Er ro r _ Wrong Test Code _ O<strong>the</strong>r<br />
b. General Discrepancy<br />
_ Missing SampletExtract^ . _ Container B roken _ Wrong Sample Pulled _ Label ID's Illegible<br />
Hold Time Exceeded _ Insufficient Sample _ Preserva ti<br />
on Wrong _ Received Past Hold<br />
_ Improper Bo ttle Type _ Not Amenable to Analysis<br />
Note: Ve rified by [Log-Ini or [Prep Groupl (drde) ... aignatumWate:<br />
c. Problem (Include all relevant specific results; attach data If necessary)<br />
m<br />
4f 5-P6 IV FA" FCi^ntsV Gk l/hfrS<br />
2. Known or Probable Causes(s) ,,,, q, , ,^^ ^ _1 _ 4 _ ^,/^ eye `,<br />
Y"..'"'<br />
wl^uGc aMr^<br />
1&4) c*,,rp'<br />
3. Discussion and Proposed Action O<strong>the</strong>r Description,`^"^v<br />
_ Re-log<br />
_ En ti<br />
re Batch<br />
Following Samples:<br />
Re-leach<br />
Re-extract<br />
_ Re-digest<br />
_ Revise EDD<br />
Change Test Code to<br />
_ Place Onrrake Off Hold (circle)<br />
4. Pp6ject Manager Instructions ... signaturerd<br />
V Concur with P ro posed Action<br />
_ Disagree with P roposed Action; See Instruction<br />
_ Include in Case Narrative<br />
_ Client Contacted:<br />
DatelPerson<br />
_ Add<br />
Cancel<br />
5. Final Action ... signatu re/date:<br />
_WVenilled re-[bg](leach)[e digest][analysisj (<br />
O<strong>the</strong>r Explanation:<br />
ci<br />
"ncluded in Case Narrative<br />
_ Hard Copy CDC Revised<br />
Electronic COC Revised<br />
_ EDD Correc<br />
rcle)<br />
ti<br />
ons Completed<br />
When Final Action has been recorded, forward original to QA Specialist for dist ribution and filing.<br />
Route Distribution <strong>of</strong> Completed SDR<br />
X Initiator<br />
X Lab General Manager aylor<br />
X P roject Mgr. Ston ohnson<br />
_ Data Management:<br />
_ Sample Prep: BeeglelKger<br />
_<br />
Route Distribution <strong>of</strong> Completed SDR<br />
— Beegle<br />
_ _ Inorganic: Perrone<br />
GC/LC: Kiger<br />
f MS: Rychl aley<br />
_ Log-in: Perarr<br />
_ _Admin:<br />
O<strong>the</strong>r.<br />
oA- 1 05-A-pep5<br />
000000006
DATA QUALIFIERS<br />
GLOSSARY<br />
U = Compound was analyzed for but not detected. The associated numerical value is <strong>the</strong><br />
estimated sample quantitation limit which is included and corrected for dilution and percent<br />
moisture.<br />
J = Indicates an estimated value. This flag is used under <strong>the</strong> following circumstances: l) when<br />
estimating a concentration for tentatively identified compounds (TICS) where a l:I<br />
response is assumed; or 2) when <strong>the</strong> mass spectral data indicate <strong>the</strong> presence <strong>of</strong> acompound<br />
that meets <strong>the</strong> identification criteria but <strong>the</strong> result is less than <strong>the</strong> specified detection limit<br />
but greater than zero. For example, if <strong>the</strong> limit <strong>of</strong> detection is 10 ug/L and a concentration<br />
<strong>of</strong> 3 ug/L is calculated, it is reported as 3J.<br />
B = This flag is used when <strong>the</strong> analyte is found in <strong>the</strong> associated blank as well as in <strong>the</strong> sample.<br />
It indicates possible/probable blank contamination. This flag is also used for a TIC as well<br />
as for a positively identified TCL compound.<br />
E = Indicates that <strong>the</strong> compound was detected beyond <strong>the</strong> calibration range and was<br />
subsequently analyzed at a dilution.<br />
D = Identifies all compounds identified in an analysis at a secondary dilution factor.<br />
I = Interference.<br />
NQ = Result qualitatively confirmed but not able to quantify.<br />
N = Indicates presumptive evidence <strong>of</strong> a compound. This flag is only used for tentatively<br />
identified compounds (TICs), where <strong>the</strong> identification is based on a mass spectral library<br />
search. It is applied to all TIC results, For generic characterization <strong>of</strong> a TIC, such as<br />
chlorinated hydrocarbon, <strong>the</strong> N code is not used.<br />
X = This flag is used for a TIC compound which is quantified relative to a response factor<br />
generated from a daily calibration standard (ra<strong>the</strong>r than quantified relative to <strong>the</strong> closes<br />
internal standard).<br />
Y = Additional qualifiers used as required are explained in <strong>the</strong> case narrative.<br />
sb\10-01gloss.doc
ABBREVIATIONS<br />
GLOSSARY<br />
BS — Indicates blank spike in which reagent grade water is spiked with <strong>the</strong> CLP matrix spike<br />
solutions and carried through all <strong>the</strong> steps in <strong>the</strong> method. Spike recoveries are repo rted.<br />
BSD = Indicates blank spike duplicate.<br />
MS = Indicates matrix spike.<br />
MSD = Indicates matrix spike duplicate.<br />
DL Suffix added to sample number to indicate that results are from a diluted analysis.<br />
NA = Not Applicable.<br />
DF = Dilution Factor.<br />
NR Not Required.<br />
SP, Z = Indicates Spiked Compound.<br />
sb\I0-03\g1oss.dm<br />
r1<br />
L_^<br />
000000008
TECHNICAL FLAGS FOR MANUAL INTEGRATION<br />
Manual quan modifications or integrations are performed routinely to improve <strong>the</strong> data quality<br />
for a variety <strong>of</strong> technical reasons. Documentation <strong>of</strong> <strong>the</strong>se modifications should be clear and<br />
concise. The following `flags' are used to indicate <strong>the</strong> technical reasons for quan modifications:<br />
MP - Missed Peak: Manually added peak not found by automatic quan<br />
program.<br />
PA - Peak Assignment: Quan report was changed to reflect correct peak<br />
assignment.<br />
RI - Routine Integration: Routine integrations are performed for some<br />
analytes that are consistently integrated improperly by <strong>the</strong> automatic<br />
integration programs. Examples are <strong>the</strong> Dichlorobenzene isomers on <strong>the</strong><br />
VOA packed column and Benzo (b) fluoran<strong>the</strong>ne /Benzo (k) fluoran<strong>the</strong>ne<br />
which are poorly resolve on <strong>the</strong> BNA column.<br />
SP - Split Peak: The automatic integration improperly split <strong>the</strong> peak; a manual<br />
integration was performed to get <strong>the</strong> correct area.<br />
CB - Co-elution/ Background: Peak was manually integrated to eliminate<br />
contribution from co-eluting compounds, background signal, or o<strong>the</strong>r<br />
interference.<br />
PI - Proper Integration: A peak with poor or inconsistent integration (i.e.,<br />
excessive tail) was properly integrated manually.<br />
LV -21-21-035/AZM<br />
909099009
uivuviaio ueuaaa.n wa.]i, aau.<br />
Semivolatiles by GC/MS, HSL List Report Date: 07/13/06 13:42<br />
RFW Batch Number: 06041,904 Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303 Work Order: 11343606001 Pane, la<br />
Cust ID: JllKKS J11KK8 J11KK8 J11KL5 J11KL6 1T11KM0<br />
Sample RFW#: 001 001 MS 001 MSD 002 003 004<br />
Information Matrix: SOLID SOLID SOLID SOLID SOLID SOLID<br />
D.F.: 0.800 0.800 0.800 0.800 0.800 0.800<br />
Units: ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg<br />
Nitrobenzene-d5 0 * % 11 * t<br />
Surrogate 2-Fluorobiphenyl 6 * % 13 * t<br />
Recovery Terphenyl-d14 17 * % 16 * %<br />
Phenol-d5 2 * % 12 *<br />
2-Fluorophenol 1 * % 10 *<br />
2,4,6-Tribromophenol 15 * t 17 *<br />
Phenol 4000 U 14 * t<br />
bis(2-Chloroethyl)e<strong>the</strong>r 4000 U 12 *<br />
2-Chlorophenol 4000 U 13 * °s<br />
1,3-Dichlorobenzene 4000 U 11 * jr<br />
1,4-Dichlorobenzene 4000 U 11 * %<br />
1,2-Dichlorobenzene 4000 U 11 * t<br />
2-Methylphenol 4000 U 14 *<br />
2,2'-oxybis(1-Chloropropane) 4000 U 12 *<br />
4-Methylphenol 4000 U 15 * t<br />
N- Nitroso-di-n-propylamine 4000 U 15 * t<br />
Hexachloroethane 4000 U 10 * %<br />
Nitrobenzene 4000 U 12 * %<br />
Isophorone 4000 U 13 * t<br />
2-Nitrophenol 4000 U 13 * t<br />
2,4-Dimethylphenol 4000 U 15 * t<br />
bis(2-Chloroethoxy)methane 4000 U 13 * t<br />
2,4-Dichlorophenol 4000 U 14 *<br />
1,2,4-Trichlorobenzene 4000 U 12 * t<br />
Naphthalene 4000 U 12 * t<br />
4- Chloroaniline 4000 U 13 * %<br />
Hexachlorobutadiene 4000 U 14 *<br />
4- Chloro-3-methylphenol 4000 U 14 *<br />
2-Methylnaphthalene 4000 U 14 *<br />
Hexachlorocyclopentadiene 4000 U 7 * t<br />
2,4,6-Trichlorophenol 4000 U 15<br />
2,4,5-Trichlorophenol 9900 U 14 *<br />
*= Outside <strong>of</strong> EPA CLP QC limits.<br />
24 t 14 * 0 7 * % 17 * %<br />
30 % 25 * % 14 * t 21 * t<br />
37 % 31 1 22 % 31 %<br />
25 21 * 1 13 * % 21 * t<br />
21 * % 14 * t 7 * t 16.* %<br />
42 % 30 21 % 26 t<br />
29 * % 540 J 3700 U 640 J<br />
26 * % 3700 U 3700 U 3400 U<br />
28 * % 3700 U 3700 U 3400 U<br />
24 *s 3700 U 3700 U 3400 U<br />
24 * 3700 U 3700 U 3400 U<br />
25 * % 3700 U 3700 U 3400 U<br />
28 * t 3700 U 3700 U 3400 U<br />
25 * t 3700 U 3700 U 3400 U<br />
32 * t 230 J 3700 U 3400 U<br />
31 * % 3700 U 3700 U 3400 U<br />
22 * t 3700 U 3700 U 3400 U<br />
26 * t 3700 U 3700 U 3400 U<br />
29 * t 3700 U 3700 U 3400 U<br />
29 * % 3700 U 3700 U 3400 U<br />
31 * % 3700 U 3700 U 3400 U<br />
29 * t 3700 U 3700 U 3400 U<br />
30 * % 3700 U 3700 U 3400 U<br />
27 * % 3700 U 3700 U 3400 U<br />
27 * % 3700 U 3700 U 3400 U<br />
26 t 3700 U 3700 U 3400 U<br />
30 * t 3700 U 3700 U 3400 U<br />
28 * % 3700 U 3700 U 3400 U<br />
29 * % 3700 U 3700 U 3400 U<br />
24 t 3700 U 3700 U 3400 U<br />
32 t 3700 U 3700 U 3400 U<br />
30 * t 9200 U 9200 U 8600 U<br />
m<br />
m
RNW batcn NUmoer: u0U4L9u4 1.11C1LU: lAUu rVAW A^-Vzi nua-V. wUlx V1uCl: llJ%ODuOVV1 roue: lU<br />
Cust ID: J11KKS J11KK8 J11KK8 J11KL5 J11KL6 J11KM0<br />
RFW#: 001 001 MS 001 MSD 002 003 004<br />
2-Chloronaphthalene 4000 U 13 * % 30 * % 3700 U 3700 U 3400 U<br />
2-Nitroaniline 9900 U 14 * % 29 * % 9200 U 9200 U 8600 U<br />
Dimethylphthalate 4000 U 15 * % 34 * % 3700 U 3700 U 3400 U<br />
Acenaphthylene 4000 U 14 * % 30 * % 3700 U 3700 U 3400 U<br />
2,6-Dinitrotoluene 4000 U 14 * % 32 * % 3700 U 3700 U 3400 U<br />
3-Nitroaniline 9900 U 13 * % 25 * % 9200 U 9200 U 8600 U<br />
Acenaph<strong>the</strong>ne 4000 U 13 * % 30 * % 3700 U 3700 U 3400 U<br />
2,4-Dinitrophenol 9900 U 7 * % 25 9200 U 9200 U 8600 U<br />
4-Nitrophenol 9900 U 1 * %; 1 * °s 9200 U 9200 U 8600 U<br />
Dibenz<strong>of</strong>uran 4000 U 14 * % 30 * °s 3700 U 3700 U 3400 U<br />
2,4-Dinitrotoluene 4000 U 15 * % 29 * t 3700 U 3700 U 3400 U<br />
Diethylphthalate 4000 U 15 * % 33 * % 3700 U 3700 U 3400 U<br />
4-Chlorophenyl-phenyle<strong>the</strong>r 4000 U 14 * % 31 * % 3700 U 3700 U 3400 U<br />
Fluorene 4000 U 14 * % 30 * % 3700 U 3700 U 3400 U<br />
4-Nitroaniline 9900 U 14 * % 25 * % 9200 U 9200 U 8600 U<br />
4,6-Dinitro-2-methylphenol 9900 U 15 * % 38 * % 9200 U 9200 U 8600 U<br />
N-Nitrosodiphenylamine (1) 4000 U 13 * % 31 * % 3700 U 3700 U 3400 U<br />
4-Bromophenyl-phenyle<strong>the</strong>r 4000 U 15 * % 36 * % 3700 U 3700 U 3400 U<br />
Hexachlorobenzene 4000 U 18 * % 42 * % 3700 U 3700 U 3400 U<br />
Pentachlorophenol 9900 U 1 * % 32 % 9200 U 9200 U 8600 U<br />
Phenanthrene 4000 U 16 * % 43 * % 3700 U 3700 U 3400 U<br />
Anthracene 4000 U 15 * % 31 * % 3700 U 3700 U 3400 U<br />
Carbazole 4000 U 15 * % 36 * % 3700 U 3700 U 3400 U<br />
Di-n-butylphthalate 4000 U 15 * % 33 * % 3700 U 3700 U 3400 U<br />
Fluoran<strong>the</strong>ne 4000 U 15 * % 39 * % 3700 U 3700 U 3400 U<br />
Pyrene 4000 U 16 * % 36 * % 3700 U 3700 U 3400 U<br />
Butylbenzylphthalate 4000 U 16 * % 33 * % 3700 U 3700 U 3400 U<br />
3,3 1 -Dichlorobenzidine 4000 U 11 * % 21 %: 3700 U 3700 U 3400 U<br />
Benzo(a)anthracene 4000 U 15 * % 34 * % 3700 U 3700 U 3400 U<br />
Chrysene 4000 U 16 * % 32 * % 3700 U 3700 U 3400 U<br />
bis(2-Ethylhexyl)phthalate 230 JB 16 * % 30 * % 3700 U 3700 U 3400 U<br />
Di-n-octyl phthalate 4000 U 15 * % 26 * % 3700 U 3700 U 3400 U<br />
Benzo(b)fluoran<strong>the</strong>ne 4000 U 14 * % 33 * % 3700 U 3700 U 3400 U<br />
Benzo(k)fluoran<strong>the</strong>ne 4000 U 14 * % 27 * % 3700 U 3700 U 3400 U<br />
Benzo(a)pyrene 4000 U 14 * % 30 * % 3700 U 3700 U 3400 U<br />
Indeno(1,2,3-cd)pyrene 4000 U 16 * % 35 * It 3700 U 3700 U 3400 U<br />
Dibenz(a,h)anthracene 4000 U 16 * % 35 * % 3700 U 3700 U 3400 U<br />
Benzo(g,h,i)perylene 4000 U 16 * % 33 * % 3700 U 3700 U 3400 U<br />
(1) - Cannot be separated from Diphenylamine. *= Outside Of EPA CLP QC limits_<br />
m
--------- ----------- r-.--<br />
Semivolatiles by GC/MS, HSL List Report Date: 07/13/06 13:42<br />
RFW Batch Number: 0604L904 Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303 Work Order, 11343606001 Paae: 2a<br />
Cust ID: J11KM2 J11KM3 J11KM4 J11KM5 J11KM6 J11KV1<br />
Sample RFW#: 005 006 007 008 009 010<br />
Information Matrix: SOLID SOLID SOLID SOLID SOLID SOLID<br />
D.F.: 0.800 0.800 0.800 0.800 0.800 0.800<br />
Units: ug/Kg ug/Kg ug/Kg ug/Kg ug /Kg ug/Kg<br />
Nitrobenzene-d5 17 * % 17 * % 11 * % 28 0 19 * % 16 *<br />
Surrogate 2-Fluorobiphenyl 20 * % 19 * % 13 * % 33 % 21 * 19 *<br />
Recovery Terphenyl-d14 29 % 26 1 19 % 42 % 29 % 25<br />
Phenol-d5 19 * % 18 * % 12 * % 32 % 20 * % 15 *<br />
2-Fluorophenol 15 * % 15 * % 10 * 1 27 % 18 * % 13 * °s<br />
2,4,6-Tribromophenol 24 % 24 % 18 * % 39 % 27 % 20 %<br />
f1=====__===== f1===== __=====fl°==== __==== =f1<br />
Phenol 260 J 240 J 3200 U 660 J <strong>300</strong> J 540 J<br />
bis(2-Chloroethyl)e<strong>the</strong>r 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
2-Chlorophenol 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
1,3-Dichlorobenzene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
1,4-Dichlorobenzene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
1,2-Dichlorobenzene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
2-Methylphenol 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
2,2'-oxybis(1-Chloropropane) 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
4-Methylphenol 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
N-Nitroso-di-n-propylamine 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Hexachloroethane 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Nitrobenzene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Isophorone 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
2-Nitrophenol 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
2,4-Dimethylphenol 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
bis(2-Chloroethoxy)methane 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
2,4-Dichlorophenol 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
1,2,4-Trichlorobenzene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Naphthalene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
4-Chlorcaniline 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Hexachlorobutadiene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
4-Chloro-3-methylphenol 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
2-Methylnaphthalene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Hexachlorocyclopentadiene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
2,4,6-Trichlorophenol 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
2,4,5-Trichlorophenol 8<strong>300</strong> U 8400 U 8000 U 8<strong>100</strong> U 7400 U 9200 U<br />
*= Outside <strong>of</strong> EPA CLP QC limits.<br />
N<br />
.r<br />
m<br />
CD<br />
G<br />
W
0<br />
RFW BatCn Number- UbU4L5U4 Ellen ' 17xyn"ryj%y xl-"/ Ava w rvorx Uraer • IIJYJOVOUVI rave• zo<br />
Cust ID: J11KM2 J11KM3 J11KM4 J11KM5 J11KM6 J11KV1<br />
RFW#: 005 006 007 008 009 010<br />
2-Chloronaphthalene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
2-Nitroaniline 8<strong>300</strong> U 8400 U 8000 U 8<strong>100</strong> U 7400 U 9200 U<br />
Dimethylphthalate 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Acenaphthylene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
2,6-Dinitrotoluene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
3-Nitroaniline 8<strong>300</strong> U 8400 U 8000 U 8<strong>100</strong> U 7400 U 9200 U<br />
Acenaph<strong>the</strong>ne 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
2,4-Dinitrophenol 8<strong>300</strong> U 8400 U 8000 U 8<strong>100</strong> U 7400 U 9200 U<br />
4-Nitrophenol 8<strong>300</strong> U 8400 U 8000 U 8<strong>100</strong> U 7400 U 9200 U<br />
Dibenz<strong>of</strong>uran 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
2,4-Dinitrotoluene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Diethylphthalate 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
4-Chlorophenyl-phenyle<strong>the</strong>r 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Fluorene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
4-Nitroaniline 8<strong>300</strong> U 8400 U 8000 U 8<strong>100</strong> U 7400 U 9200 U<br />
4,6-Dinitro-2-methylphenol 8<strong>300</strong> U 8400 U 8000 U 8<strong>100</strong> U 7400 U 9200 U<br />
N- Nitrosodiphenylamine (1) 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
4-Bromophenyl-phenyle<strong>the</strong>r 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Hexachlorobenzene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Pentachlorophenol 8<strong>300</strong> U 8400 U 8000 U 8<strong>100</strong> U 7400 U 9200 U<br />
Phenanthrene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Anthracene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Carbazole 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Di-n-butylphthalate 3<strong>300</strong> U 3400 U 3200 U 2200 J <strong>300</strong>0 U 3700 U<br />
Fluoran<strong>the</strong>ne 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Pyrene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Butylbenzylphthalate 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
3,3 1 - Dichlorobenzidine 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Benzo(a)anthracene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Chrysene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
bis(2-Ethylhexyl)phthalate 3<strong>300</strong> U 250 JB 3200 U 3200 U 190 JB 3700 U<br />
Di-n-octyl phthalate 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Benzo(b)fluoran<strong>the</strong>ne 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Benzo(k)fluoran<strong>the</strong>ne 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Benzo(a)pyrene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Indeno(1,2,3-cd)pyrene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Dibenz(a,h)anthracene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
Benzo(g,h,i)perylene 3<strong>300</strong> U 3400 U 3200 U 3200 U <strong>300</strong>0 U 3700 U<br />
(1) - Cannot be separated from Diphenylamine. *= Outside <strong>of</strong> EPA CLP QC limits.<br />
M<br />
m
Semivolatiles by GC/MS, HSL List Report Date: 07/13/06 13:42<br />
RFW Batch Number: 06041,904 Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303 Work Order: 11343606001 Pape: 3a<br />
Cust ID: J11KV2 J111,21 JIIL23 JlIL25 J11L36 SHLKZH<br />
Sample RFW#: 011 012 013 014 015 06LE0457-MB1<br />
Information Matrix: SOLID SOLID SOLID SOLID SOLID SOIL<br />
D.F.: 0.800 0.800 0.800 0.800 0.800 0.800<br />
Units: ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg<br />
Nitrobenzene-d5 2 * % 13 * % 16 * % 20 * % 14 * % 26 a<br />
Surrogate 2-Fluorobiphenyl 8 * % 16 * % 20 * % 22 * % 16 * % 27 * %<br />
Recovery Terphenyl-d14 21 e 19 % 21 % 24 0 21 % 45 %<br />
Phenol-d5 6 * % 15 * % 17 * % 19 * % 14 * % 29 %<br />
2-Fluorophenol 3 * % 13 * °s 16 * % 20 * % 14 * % 26 %<br />
2,4,6-Tribromophenol 15 * % 12 * % 18 * % 20 % 14 * % 33<br />
----------------------------------------=====<br />
--------------------------- f1=====__===== f1=====__=====fl=====__===== fl=====__===== f1===== __=====fl<br />
Phenol 4000 U 280 J 160 J 220 J 260 J 270 U<br />
bis(2-Chloroethyl)e<strong>the</strong>r 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
2- Chlorcphenol 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
1,3-Dichlorobenzene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
1,4-Dichlorobenzene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
1,2-Dichlorobenzene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
2-Methylphenol 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
2,2'-oxybis(i-Chloropropane) 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
4-Methylphenol 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
N-Nitroso-di-n-propylamine 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Hexachloroethane 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Nitrobenzene<br />
Isophorone<br />
4000<br />
4000<br />
U<br />
U<br />
2900<br />
2900<br />
U<br />
U<br />
2800<br />
2800<br />
U<br />
U<br />
3200<br />
3200<br />
U<br />
U<br />
3700<br />
3700<br />
U<br />
U<br />
270<br />
270<br />
U<br />
U<br />
2-Nitrophenol 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
2,4-Dimethylphenol 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
bis(2-Chloroethoxy)methane<br />
2,4-Dichlorophenol<br />
1,2,4-Trichlorobenzene<br />
Naphthalene<br />
4-Chloroaniline<br />
Hexachlorobutadiene<br />
4-Chloro-3-methylphenol<br />
2-Methylnaphthalene<br />
Hexachlorocyclopentadiene<br />
2,4,6-Trichlorophenol<br />
2,4,5-Trichlorophenol<br />
*= Outside <strong>of</strong> EPA CLP QC limits.<br />
4000<br />
4000<br />
4000<br />
4000<br />
4000<br />
4000<br />
4000<br />
4000<br />
4000<br />
4000<br />
9900<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
2900<br />
2900<br />
2900<br />
2900<br />
2900<br />
2900<br />
2900<br />
2900<br />
2900<br />
2900<br />
7<strong>100</strong><br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
2800<br />
2800<br />
2800<br />
2800<br />
2800<br />
2800<br />
2800<br />
2800<br />
2800<br />
2800<br />
7<strong>100</strong><br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
3200<br />
3200<br />
3200<br />
3200<br />
3200<br />
3200.<br />
3200<br />
3200<br />
3200<br />
3200<br />
8<strong>100</strong><br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
3700<br />
3700<br />
3700<br />
3700<br />
3700<br />
3700<br />
3700<br />
3700<br />
3700<br />
3700<br />
9200<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
270<br />
270<br />
270<br />
270<br />
270<br />
270<br />
270<br />
270<br />
270<br />
270<br />
670<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
U<br />
a<br />
m
RFW Batcn Number: UOU4L `JU4 L11C11L: 11IV13 PVR3 n - v ^Vuo n4<br />
Cust ID: JllKV2 J11 1, 21 JllL23 JlIL25 JllL36 SBLKZH<br />
RFW#: Oil 012 013 014 015 06LE0457-MB1<br />
2-Chloronaphthalene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
2-Nitroaniline 9900 U 7<strong>100</strong> U 7<strong>100</strong> U B<strong>100</strong> U 9200 U 670 U<br />
Dimethylphthalate 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Acenaphthylene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
2,6-Dinitrotoluene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
3-Nitroaniline 9900 U 7<strong>100</strong> U 7<strong>100</strong> U 8<strong>100</strong> U 9200 U 670 U<br />
Acenaph<strong>the</strong>ne 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
2,4-Dinitrophenol 9900 U 7<strong>100</strong> U 7<strong>100</strong> U 8<strong>100</strong> U 9200 U 670 U<br />
4-Nitrophenol 9900 U 7<strong>100</strong> U 7<strong>100</strong> U 6<strong>100</strong> U 9200 U 670 U<br />
Dibenz<strong>of</strong>uran 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
2,4-Dinitrotoluene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Diethylphthalate 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
4-Chlorophenyl-phenyle<strong>the</strong>r 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Fluorene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
4-Nitroaniline 9900 U 7<strong>100</strong> U 7<strong>100</strong> U 8<strong>100</strong> U 9200 U 670 U<br />
4,6-Dinitro-2-methylphenol 9900 U 7<strong>100</strong> U 7<strong>100</strong> U 8<strong>100</strong> U 9200 U 670 U<br />
N-Nitrosodiphenylamine (1) 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
4-Bromophenyl-phenyle<strong>the</strong>r 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Hexachlorobenzene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Pentachlorophenol 9900 U 7<strong>100</strong> U 7<strong>100</strong> U 8<strong>100</strong> U 9200 U 670 U<br />
Phenanthrene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Anthracene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Carbazole 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Di-n-butylphthalate 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Fluoran<strong>the</strong>ne 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Pyrene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Butylbenzylphthalate 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
3,3 1 -Dichlorobenzidine 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Benzo(a)anthracene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Chrysene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
bis(2-Ethylhexyl)phthalate 4000 U 2900 U 2800 U 190 JB 2000 JB 18 J<br />
Di-n-octyl phthalate 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Benzo(b)fluoran<strong>the</strong>ne 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Benzo(k)fluoran<strong>the</strong>ne 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Benzc(a)pyrene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Indeno(1,2,3-cd)pyrene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Dibenz(a,h)anthracene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
Benzo(g,h,i)perylene 4000 U 2900 U 2800 U 3200 U 3700 U 270 U<br />
(1) - Cannot be separated from Diphenylamine. *= Outside <strong>of</strong> EPA CLP QC limits.<br />
N<br />
M<br />
m<br />
G<br />
m<br />
M<br />
CD<br />
m
RFW Batch Number: 0604L904<br />
Semivolatiles by GC/MS, HSL List Report Date: 07/13/06 13:42<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303 Work Order: 11343606001 Page: 4a<br />
Cust ID: SBLKZH BS - m mCD<br />
Sample<br />
Information<br />
RFW#:<br />
Matrix:<br />
D.F.:<br />
06LE0457-MB1<br />
SOIL<br />
0.800<br />
m<br />
Units: ug/Kg<br />
Nitrobenzene-d5 10 * %<br />
Surrogate 2-Fluorobiphenyl 11 * %<br />
Recovery Terphenyl-d14 16 *s<br />
Phenol-d5 9 * %<br />
2-Fluorophenol 9 * %<br />
2,4,6-Tribromophenol 14 *<br />
_____________________________________________ fl=====__===== fl=====__===== fl=====__=====f1=====__=====f1==°==__=====f1<br />
Phenol 10 * %<br />
bis(2-Chloroethyl)e<strong>the</strong>r 11<br />
2-Chlorophenol 11 * %<br />
1,3-Dichlorobenzene 10 * %<br />
1,4-Dichlorobenzene 9 * %<br />
1,2-Dichlorobenzene 10 * %<br />
2-Methylphenol 10 * %<br />
2,2'-oxybis(i-Chloropropane) 11 * %<br />
4-Methylphenol 10 * %<br />
N-Nitroso-di-n-propylamine 12 * %<br />
Hexachloroethane 10 *<br />
Nitrobenzene 10 *<br />
Isophorone 12 * %<br />
2-Nitrophenol 10 * %<br />
2,4-Dimethylphenol 7 * %<br />
bis(2-Chloroethoxy)methane 11 * t<br />
2,4-Dichlorophenol 10 * %<br />
1,2,4-Trichlorobenzene 11 * %<br />
Naphthalene 11 * %<br />
4-Chloroaniline 11 * %<br />
Hexachlorobutadiene 11 * %<br />
4-Chlaro-3-methylphenol 10 *<br />
2-Methylnaphthalene 12 *<br />
Hexachlorocyclopentadiene 7 * %<br />
2,4,6-Trichlorophenol 12 %<br />
2,4,5-Trichlorophenol 10 * %<br />
*= Outside <strong>of</strong> EPA CLP QC limits.<br />
ID
RFw batch Number , Ubu4L90 4 1:11enL: WilunAMOUnL n^ -ULl AU .3V3 WOrx uruer • 113434UbUU1 ease 40<br />
Cust ID: SBLRZH BS<br />
RFW#: 06LE0457-MB1<br />
2-Chloronaphthalene 11 * %<br />
2-Nitroaniline 11 * %<br />
Dimethylphthalate 13<br />
Acenaphthylene<br />
11<br />
2,6-Dinitrotoluene 11 * %<br />
3-Nitroaniline<br />
12<br />
Acenaph<strong>the</strong>ne 11 * %<br />
2,4-Dinitrophenol 0 * %<br />
4-Nitrophenol 0<br />
Dibenz<strong>of</strong>uran 12 * %<br />
2,4-Dinitrotoluene 12 * %<br />
Diethylphthalate 13 * %<br />
4-Chlorophenyl-phenyle<strong>the</strong>r 12 * %<br />
Fluorene<br />
12<br />
4-Nitroaniline 10<br />
4,6-Dinitro-2-methylphenol 10<br />
N-Nitrosodiphenylamine (1) 12 + %<br />
4-Bromophenyl-phenyle<strong>the</strong>r 12 *<br />
Hexachlorobenzene 15 *<br />
Pentachlorophenol 0 * %<br />
Phenanthrene 13 * %<br />
Anthracene 12 * %<br />
Carbazole 13 * %<br />
Di-n-butylphthalate 13 * %<br />
Fluoran<strong>the</strong>ne 13 * %<br />
Pyrene 17 * %<br />
Butylbenzylphthalate 16 * %<br />
3,3 1 -Dichlorobenzidine 11<br />
Benzo(a)anthracene 13<br />
Chrysene 14 * %<br />
bis(2-Ethylhexyl)phthalate 15 * %<br />
Di-n-octyl phthalate 17 * %<br />
Benzo(b)fluoran<strong>the</strong>ne 14 * %<br />
Benzo(k)fluoran<strong>the</strong>ne 15 * %<br />
Benzo(a)pyrene 14<br />
Indeno(1,2,3-cd)pyrene 14<br />
Dibenz(a,h)anthracene 11 * %<br />
Benzo(g,h,i)perylene 12 * %<br />
(1) - Cannot be separated from Diphenylamine. *= Outside <strong>of</strong> EPA CLP QC limits.<br />
h<br />
m<br />
m<br />
Q<br />
CD
IF CLiENT SAMPLE NO.<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS<br />
IJ11KKB<br />
Lab Name: Lionville Labs, Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
Matrix: (soil/water) SOLID Lab Sample ID: 06041,904-001<br />
Sample wt/vol: 2.02 (g/mL) Lab File ID: N062914<br />
Level: (low/med) LOW Date Received: 04/28/06<br />
%, Moisture: <strong>100</strong> decanted: (Y/N) _ Date Extracted: 06/02/06<br />
Concentrated Extract Volume: 500(uL) Date Analyzed: 06/29/06<br />
Injection Volume: 2_0(uL) Dilution Factor: 0.800<br />
GPC Cleanup: (Y/N) Y pH:<br />
Number TICS found: .5<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) ua/Kg<br />
1<br />
CAS NUMBER<br />
1<br />
COMPOUND<br />
1 1<br />
NAME RT EST.<br />
CONC.<br />
1<br />
1<br />
Q 1<br />
1. 110-82-7 1CYCLOHEXANE 1 3.539 1 70001 JNB 1<br />
2. JORGANIC ACID 1 21.6241 200001 J 1<br />
1 3. JUNKNOWN 1 22.7211 400001 J 1<br />
1 4. UNKNOWN 1 28.5681 <strong>300</strong>01 J 1<br />
1 5.<br />
1<br />
UNKNOWN 1 34.0861<br />
I I<br />
800001<br />
FORM 1 SV-TIC RFW (v3.3)<br />
I<br />
J 1<br />
000000018<br />
1
IF CLIENT SAMPLE NO.<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS<br />
J11KL5<br />
Lab Name: Lionville Labs, Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
Matrix: (soil/water) SOLID Lab Sample ID 0604L904-002<br />
Sample wt/vol: 2.18 (g/mL) G<br />
Level: (low/med) LOW<br />
g Moisture: <strong>100</strong> decanted: (Y/N) _,<br />
Concentrated Extract Volume: 5500(uL)<br />
Injection Volume: 22. (uL)<br />
GPC Cleanup: (Y/N) Y pH:<br />
Number TICS found: 5<br />
CAS NUMBER COMPOUND NAME<br />
1. 110-82-7 ^CYCLOHEXANE<br />
2. JORGANIC ACID<br />
3. JUNKNOWN<br />
4. JORGANIC ACID<br />
5. JUNKNOWN<br />
Lab File ID: N070111<br />
Date Received: 04/28/06<br />
Date Extracted: Q6/02/06<br />
Date Analyzed: 07/02/06<br />
Dilution Factor: 0.800<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) ua/Ka<br />
RT EST. CONC. Q<br />
3.419 1<br />
60001 JNB<br />
21.5471 600001 J<br />
22.6351 <strong>100</strong>0001 J<br />
1 22.7131 <strong>300</strong>001 J<br />
1 33.8201 5000001 J<br />
FORM 1 SV-TIC RFW (v3.3)<br />
000000019
1F<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS<br />
Lab Name: Lionville Labs Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
Matrix: (soil/water) SOLID<br />
Sample wt/vol: 2.17 (9/ML) -Q<br />
Level: (low/med) LOW<br />
& Moisture: <strong>100</strong> decanted: (Y/N)_<br />
Concentrated Extract Volume: 500 (uL)<br />
Injection Volume: 2_0(uL)<br />
GPC Cleanup: (YIN) Y pH:<br />
Number TICS found:<br />
Lab Sample ID:<br />
Lab File ID:<br />
Date Received:<br />
Date Extracted:<br />
Date Analyzed:<br />
Dilution Factor<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) ua/Kd<br />
CL1liIJ'r SAMPLE NO.<br />
I<br />
^J11KL6<br />
I<br />
0604 1, 904-003<br />
N06<strong>300</strong>6<br />
04/28/06<br />
06/02/06<br />
06/30/06<br />
0.800<br />
CAS NUMBER COMPOUND NAME RT EST. CONC. Q<br />
1. JUNKNOWN 1 5.804 1 80001 J<br />
1 2. JORGANIC ACID 1 21.5911 <strong>300</strong>001 J<br />
1 3. JUNKNOWN 1 22.6881 900001 J<br />
4. JORGANIC ACID 1 22.7661 200001 J<br />
5. UNKNOWN 1 33.9681 2000001 J<br />
FORM 1 SV-TIC RFW (v3.3)<br />
000000020
IF CLIENT SAMPLE NO.<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED .COMPOUNDS<br />
J11KMO<br />
Lab Name: Lionville Labs, Inc. Work Order: 11343606001<br />
i<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
Matrix: (soil/water) SOLID Lab Sample ID: 06041,904-004<br />
Sample wt/vol: 2.32 (g/ML) Lab File ID: N06<strong>300</strong>7<br />
Level: (low/med) LOW Date Received: 04/28/06<br />
Moisture: <strong>100</strong> decanted: (Y/N) _ Date Extracted: 06/02/06<br />
Concentrated Extract Volume: 500(uL) Date Analyzed: 06/30/06<br />
Injection Volume: 2.0(uL) Dilution Factor: 0.800<br />
GPC Cleanup: (YIN) Y pH:<br />
Number TICS found: 5<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) u K<br />
I<br />
CAS NUMBER<br />
1. 110-82-7 ICYCLOHEXANE<br />
1 2. JUNKNOWN<br />
1 3. JORGANIC ACID<br />
4. JUNKNOWN<br />
5. JUNKNOWN<br />
I<br />
COMPOUND NAME<br />
RT EST. CONC. Q<br />
3.471 1 <strong>100</strong>00 JNB<br />
5.829 1 80001 J<br />
1 21.5821 200001 J<br />
22.6701 <strong>300</strong>001 J<br />
1 33.9241 <strong>100</strong>000 J<br />
FORM 1 SV-TIC RFW (v3.3)<br />
000000021
1F CLIENT SP.MPLE NO.<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS<br />
I J11KM2<br />
Lab Name: Lionville Labs, Inc. Work Order.: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
Matrix: (soil/water) SOLID Lab Sample ID: 0604 1, 904-005<br />
Sample wt/vol: 2.42 (g/mL) G<br />
Level: (low/med) LOW<br />
°s Moisture: <strong>100</strong> decanted: (Y/N) _<br />
Concentrated Extract Volume: 500(uL)<br />
Injection Volume: 2_0(uL)<br />
GPC Cleanup: (Y/N) _y pH:<br />
Number TICS found: 5<br />
CAS NUMBER COMPOUND NAME<br />
1. 110-82-7 ICYCLOHEXANE<br />
2. (ORGANIC ACID<br />
1 3. (UNKNOWN<br />
1 4. JUNKNOWN<br />
5.<br />
UNKNOWN<br />
1<br />
I<br />
^<br />
Lab File ID: N06<strong>300</strong>8<br />
Date Received: 04/28/06<br />
Date Extracted: 06/02/06<br />
Date Analyzed: 06/30/06<br />
Dilution Factor: 0.800<br />
CONCENTRATION UNITS:<br />
(ug/L or u9/Kg) ua/Kq<br />
_I<br />
RT EST. CONC. Q<br />
1 3.471 1 <strong>100</strong>001 JNB I<br />
21.S901 400001 J<br />
22.6871 <strong>100</strong>0001 J<br />
28.4741 50001 J I<br />
33.9061 2000001 J<br />
FORM 1 SV-TIC RFW (v3.3)<br />
000000022<br />
I
1F CLIENT SAMPLE NO.<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS<br />
J I I KM3<br />
Lab Name: Lionville Labs, Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
Matrix: (soil/water) SOLID Lab Sample ID: 0604L904-006<br />
Sample wt/vol: 2.38 (g/mL) Lab File ID: N06<strong>300</strong>9<br />
Level: (low/med) LOW Date Received: 04/28/06<br />
g Moisture: <strong>100</strong> decanted: (YIN)_ Date Extracted: 06/02/06<br />
Concentrated Extract Volume: 500(uL) Date Analyzed: 06/30/06<br />
injection Volume: 2_0(uL) Dilution Factor: 0.800<br />
GPC Cleanup: (YIN) Y pH:<br />
CONCENTRATION UNITS:<br />
Number TICS found: 5 (ug/L or ug/Kg) u K<br />
CAS NUMBER COMPOUND NAME<br />
=-^-=a=asses======== ____:» ^a^:as==<br />
1.<br />
JUNKNOWN<br />
2. JORGANIC ACID<br />
1 3. JUNKNOWN<br />
1 4. JORGANIC ACID<br />
5.<br />
JUNKNOWN<br />
1<br />
11<br />
PT I EST. CONC. Q<br />
1 5.906 1 <strong>100</strong>001 J<br />
1 21.5591 600001 J 1<br />
22.7051 <strong>100</strong>0001 J 1<br />
22.7741 <strong>300</strong>001 J<br />
1 33.9841 4000001 J<br />
FORM 1 SV-TIC RFW (v3.3)<br />
000000023
Injection Volume: 2_0(uL)<br />
GPC Cleanup: (Y/N) Y<br />
Number TICS found: 5<br />
IF CLIENT SAMPLE NO.<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS I<br />
Lab Name: Lionville Labs, Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
1 1<br />
pH:<br />
Dilution Factor: 0.800<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) u cr /Ka<br />
^JllKM4<br />
Matrix: (soil/water) SOLID Lab Sample ID: 0604L904-007<br />
Sample wt/vol: 2.50 (g/mL) G Lab File ID: N063010<br />
Level: (low/med) LOW Date Received: 04/28/06<br />
% Moisture: <strong>100</strong> decanted: ( Y/N) _, Date Extracted: 06/02/06<br />
Concentrated Extract Volume: 500(uL) Date Analyzed: 06/30/06<br />
CAS NUMBER COMPOUND NAME RT EST. CONC. Q<br />
1. 110-82-7 I CYCLOHEXANE 1 3.473 1 <strong>100</strong>001 JNB<br />
1 2. JORGANIC ACID 1 21.6021 500001 J<br />
1 3. JUNKNOWN 1 22.6991 <strong>100</strong>0001 J<br />
4. JORGANIC ACID 122.7681 200001 J<br />
1 5. JUNKNOWN 1 33.9181 <strong>100</strong>0001 J<br />
FORM 1 SV-TIC RFW (v3.3)<br />
000000024
IF<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS<br />
Lab Name: Lionville Labs, Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
CLIENT SAMPLE NO.<br />
JJ11KM5<br />
Matrix: (soil/water) SOLID Lab Sample ID: 0604L904-008<br />
Sample wt/vol: 2.48 (g/mL) Q Lab File ID: N063011<br />
Level: (low/med) LOW Date Received: 04/28/06<br />
t Moisture: <strong>100</strong> decanted: (Y/N) _ Date Extracted: 06/02/06<br />
Concentrated Extract Volume: 500(UL) Date Analyzed: 06/30/06<br />
Injection Volume: ,2.0(UL) Dilution Factor: 0.800<br />
GPC Cleanup: (Y/N) Y pH:<br />
Number TICs found: 5<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) ug/Kg<br />
CAS NUMBER<br />
1<br />
COMPOUND<br />
I I 1<br />
NAME RT EST. CONC. Q<br />
1. 110-82-7 ICYCLOHEXANE 1 3.471 1 <strong>100</strong>001 JNB<br />
2. JUNKNOWN 1 5.603 1 80001 J<br />
1 3. JORGANIC ACID 1 21.6001 500001 J<br />
4. JUNKNOWN 1 22.6971 <strong>100</strong>0001 J<br />
S. JUNKNOWN 1 33.9671 <strong>300</strong>0001 J<br />
FORM 1 SV-TIC RFW (v3.3)<br />
I<br />
000000025
IF CLTENT SAMPLE NO.<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS 1<br />
I J11KM6<br />
Lab Name: Lionville Labs Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
Matrix: (soil/water) SOLID Lab Sample ID: 0604L904-009<br />
Sample wt/vol: 2,71 (g/mL) Lab File ID: N063012<br />
Level: (low/med) LOW_ Date Received: 04/28/06<br />
% Moisture: <strong>100</strong> decanted: (Y/N) _ Date Extracted: 06/02/06<br />
Concentrated Extract Volume: 500(uL) Date Analyzed: 06/30/06<br />
Injection Volume: 2_0(uL)<br />
GPC Cleanup: (Y/N) Y pH:<br />
Number TICS found: 5<br />
1 1<br />
1 CAS NUMBER 1 COMPOUND NAME<br />
1====_=..=.=====1========== a_<br />
1 1. 110-82-7 1CYCLOHEXANE<br />
1 2. (ORGANIC ACID<br />
3. (UNKNOWN<br />
1 4. JORGANIC ACID<br />
1 5. JUNKNOWN<br />
1 1-<br />
Dilution Factor: 0.800<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) ua/Kg<br />
RT<br />
1<br />
EST_ CONC.<br />
3.478 1 200001 JNB 1<br />
21.5891 <strong>300</strong>001 J<br />
22.6861 700001 J 1<br />
22.7641 200001 J 1<br />
33.9481 2000001 J<br />
FORM 1 SV-TIC RFW (v3.3)<br />
1<br />
Q<br />
1<br />
000000026
IF<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS<br />
Lab Name: Lionville Labs, Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
CLIENT SAMPLE NO.<br />
I<br />
^J11KV1<br />
Matrix: (soil/water) SOLI D Lab Sample ID: 0604 1, 904-010<br />
Sample wt/vol: 2.18 (g/mL) G<br />
Level: (low/med) LOW<br />
s Moisture:<strong>100</strong> decanted: (Y/N)<br />
Concentrated Extract Volume: 500(uL)<br />
Injection Volume: 2.0(uL)<br />
Lab File ID: N063013<br />
Date Received: 04/28/06<br />
Date Extracted: 06/02/06<br />
Date Analyzed: 06/30/06<br />
Dilution Factor: 0.800<br />
GPC Cleanup: (YIN) Y pH:<br />
Number TICS found: 5<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) u K<br />
CAS NUMBER COMPOUND NAME<br />
1. (UNKNOWN<br />
2. JORGANIC ACID<br />
3. JUNKNOWN<br />
1 4. JORGANIC ACID<br />
5. JUNKNOWN<br />
RT EST. CONC. Q<br />
5.862 200001 J<br />
21.5891 400001 J<br />
22.6B61 600001 J<br />
1 22.7641 200001 J<br />
1 33.957 <strong>300</strong>0001 J<br />
FORM 1 SV-TIC RFW (v3.3)<br />
000000027<br />
1
IF CLIENT SAMPLE NO.<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS I<br />
^J11KV2<br />
Lab Name: Lionville Labs, Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
Matrix: (soil/water) SOLID Lab Sample ID: 0604 1, 904-011<br />
Sample wt/vol: 2.02 (g/mL) G<br />
Level: (low/med) LOW<br />
% Moisture: <strong>100</strong> decanted: (YIN)—<br />
Concentrated Extract Volume: JU (uL)<br />
Injection Volume: 2.0(uL)<br />
GPC Cleanup: (YIN) Y pH:<br />
Number TICS found: 5<br />
Lab File ID: N063014<br />
Date - Received: 04/28/06<br />
Date Extracted: 06/02/06<br />
Date Analyzed: 06/30/06<br />
Dilution Factor: 0.800<br />
CONCENTRATION UNITS:<br />
( ug/L or ug / Kg) ua/Ka<br />
CAS NUMBER COMPOUND NAME RT EST. CONC. Q<br />
1. 110-82-7 I CYCLOHEXANE 1 3.469 1 60001 JNB<br />
2_ (ORGANIC ACID 1 21.5801 <strong>100</strong>001 J<br />
3. JUNKNOWN 1 22.6691 <strong>300</strong>00 1 J<br />
4: (UNKNOWN 1 29.1981 80001 J<br />
5. JUNKNOWN 1 33.9051 2000001 J<br />
FORM 1 SV-TIC RFW (v3.3)<br />
000000028
1F CLIENT SAMPLE NO.<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS<br />
IJ11L21<br />
Lab Name: Lionville Labs, Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
Matrix: (soil/water) SOLID Lab Sample ID: 00 4 1, 904-012<br />
Sample wt/vol: 2.80 (g/mL) Q<br />
Level: ( low/med) LOW<br />
°s Moisture: <strong>100</strong> decanted: (YIN)_<br />
Concentrated Extract Volume: 500(uL)<br />
Injection Volume: 2_0(uL)<br />
GPC Cleanup: (YIN) Y pH:<br />
Number TICS found: 5<br />
1 1<br />
Lab File ID: D06<strong>300</strong>6<br />
Date Received: 04/28/06<br />
Date Extracted: 06/02/06<br />
Date Analyzed: 06/30/06<br />
Dilution Factor: 0.800<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) ua/Kq<br />
CAS NUMBER COMPOUND NAME RT EST. CONC. Q<br />
______________<br />
1.<br />
JUNKNOWN<br />
----ewe-°===___^___ °___^_____________^_____^<br />
1 4.749 1<br />
50001 J<br />
2. (UNKNOWN 1 5.171 1 40001 J<br />
3. JUNKNOWN 1 8.523 1 60001 J<br />
1 4. JUNKNOWN 1 22.0231 50001 J<br />
5. JUNKNOWN 1 32.6541 2000001 J<br />
FORM 1 SV-TIC RFW (v3.3)<br />
000000029
IF<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS<br />
Lab Name: Lionville Labs, Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong> -<strong>047</strong> K0303<br />
CLIENT SAh]PLE NO.<br />
I<br />
IJIIL23<br />
I<br />
Matrix: (soil/water) SOLID Lab Sample ID: 0604L904-013<br />
Sample wt/vol: 2.83 (g/mL) G<br />
Level: (low/med) LOW<br />
%^ Moisture: <strong>100</strong> decanted: (Y/N) _<br />
Concentrated Extract Volume: 5_QQ(uL)<br />
Injection Volume: 2_0(uL)<br />
GPC Cleanup: (Y/N) Y pH:<br />
Number TICs found: 5<br />
CAS NUMBER COMPOUND NAME<br />
1. JUNKNOWN<br />
2. JORGANIC ACID<br />
3. JUNKNOWN<br />
4. JORGANIC ACID<br />
1 5. JUNKNOWN<br />
Lab File ID: D06<strong>300</strong>7<br />
Date Received: 04/28/06<br />
Date Extracted: 06/02/06<br />
Date Analyzed: 06/30/06<br />
Dilution Factor: 0.800<br />
'ONCENTRATION UNITS:<br />
(ug/L or ug/Kg) ua/Ka<br />
RT EST. CONC. Q<br />
4.782 1 90001 J<br />
1 20.9271 90001 J<br />
22.0291 200001 J<br />
1 22.1071 90001 J<br />
1 32.6611 <strong>300</strong>000 J<br />
_I<br />
FORM 1 SV-TIC RFW (v3.3)<br />
000000030<br />
I
1F<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS<br />
Lab Name: Lionville Labs. Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
CLIENT SAMPLE NO.<br />
JllL25<br />
I<br />
Matrix: (soil/water) SOLID Lab Sample ID: 0604L904-014<br />
Sample wt/vol: 2.47 (g/mL) G<br />
Level: (low/med) LOW<br />
Moisture: <strong>100</strong> decanted: (Y/N) _<br />
Concentrated Extract Volume: 500(uL)<br />
Injection Volume: 2_0(uL)<br />
GPC Cleanup: (Y/N) Y pH:<br />
Number TICs found: 5<br />
Lab File ID: D06<strong>300</strong>8<br />
Date Received: 04/28/06<br />
Date Extracted: 06/02/06<br />
Date Analyzed: 06/30/06<br />
Dilution Factor: 0.800<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) ua/Ka<br />
CAS NUMBER COMPOUND NAME RT EST. CONC. Q<br />
1. UNKNOWN 1 4.802 1 50001 J<br />
2. ORGANIC ACID 1 20.9381 <strong>300</strong>001 J<br />
3. JUNKNOWN 1 21.0421 50001 J 1<br />
4. JUNKNOWN 1 22.0411 <strong>100</strong>0001 J<br />
S. JUNKNOWN 1 32.6811 <strong>300</strong>0001 J<br />
FORM 1 SV-TIC RFW (v3.3)<br />
000000031
1F<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS<br />
Lab Name: Lionville Labs, Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
CLIENT SAMPLE NO.<br />
I<br />
IJIIL36<br />
Matrix: (soil/water) SOLID Lab Sample ID: 0604L904-015<br />
Sample wt/vol: 2.18 (9/ML) Q Lab File ID: D06<strong>300</strong>9<br />
Level: (low/med) Low Date Received: 04/28/06<br />
% Moisture: <strong>100</strong> decanted: (Y/N)_ Date Extracted: 06/02/06<br />
Concentrated Extract Volume: 500(uL) Date Analyzed: 06/30/06<br />
Injection Volume: 2_0(uL) Dilution Factor: 0.800<br />
GPC Cleanup: (Y/N) Y PH:<br />
Number TICS found:<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) u K<br />
CAS NUMBER COMPOUND NAME RT EST. CONC. Q<br />
1. JUNKNOWN 1<br />
13.2161 20001 J<br />
2. (UNKNOWN 1 21.0211 <strong>100</strong>01 J<br />
3. JUNKNOWN 1 21.2111 20001 J<br />
4. JUNKNOWN 1 24.3041 <strong>100</strong>01 J<br />
1 5.<br />
JUNKNOWN 1 32.6261 2000001 J<br />
1<br />
FORM 1 SV-TIC RFW (v3.3)<br />
000000032<br />
I
IF CLIENT SAMPLE NO.<br />
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET<br />
TENTATIVELY IDENTIFIED COMPOUNDS I<br />
ISBLKZH<br />
Lab Name: Lionville Labs, Inc. Work Order: 11343606001<br />
Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
Matrix: (soil/water) SOIL Lab Sample ID: 06LE0457-MB1<br />
Sample wt/vol: 30.0 (g/mL) G<br />
Level: (low/med) LOW<br />
Moisture: decanted: (YIN)<br />
Concentrated Extract Volume: 500(uL)<br />
Injection Volume: 2.0(uL)<br />
Lab File ID: N070108<br />
Date Received: 06/02/06<br />
Date Extracted: 06/02/06<br />
Date Analyzed: 07/02/06<br />
Dilution Factor: 0.800<br />
GPC Cleanup: (YIN) Y pH:<br />
Number TICS found: 5<br />
CONCENTRATION UNITS:<br />
(ug/L or ug/Kg) ua/Kq<br />
CAS NUMBER COMPOUND NAME RT EST. CONC. Q<br />
1 1. 110-82-7 ICYCLOHEXANE 1 3.421 1 <strong>100</strong>01 JN<br />
1 2. JUNKNOWN 1 29.0811 2001 J<br />
1 3. JUNKNOWN 1 30.6521 2001 J<br />
4. JUNKNOWN 1 32.5351 <strong>100</strong>1 J<br />
1 5. JUNKNOWN 1 37.8811 601 J<br />
FORM 1 SV-TIC RFW (v3.3)<br />
000000033
Lionville Lanoratory, inc.<br />
SAMPLE EXTRACTION RECORD<br />
Sheet no.: 1<br />
Extract. Date: 06/02/06 Extraction Batch No: 06LE0457 Analyst: MF Method: **** m mm<br />
Test: 0625 Cleanup Date: Analyst: Client: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303 mm mm<br />
LIMS Report Date: 07/13/06 Solvent: DCM Adsorbent:<br />
I<br />
Sample No:<br />
Client Name pH Initial Surr. Spike Final Final Split GPC It C/D I<br />
Client ID WT/VOL Mult. Mult. VOL VOL Mult. Y/N Solids FACTOR I<br />
0604L904- TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
001 H J11KK8 2.02 1.0 0.4 1.0 Y 0.00 198.0<br />
001 HS J11KKB 2.00 1.0 1.0 0.4 1.0 Y 0.00 200.0<br />
001 HT J11KK8 2.86 1.0 1.0 0.4 1.0 Y 0.00 139.9<br />
002 H J11KL5 2.18 1.0 0.4 1.0 Y 0.00 183.5<br />
003 H JllKL6 2.17 1.0 0.4 1.0 Y 0.00 184.3<br />
004 H J11KM0 2.32 1.0 0.4 1.0 Y 0.00 172.4<br />
005 H JllKM2 2.42 1.0 0.4 1.0 Y 0.00 165.3<br />
006 H J11KM3 2.38 1.0 0.4 1.0 Y 0.00 168.1<br />
007 H J11KM4 2.50 1.0 0.4 1.0 Y 0.00 160.0<br />
008 H J11KM5 2.48 1.0 0.4 1.0 Y 0.00 161.3<br />
009 H J11KM6 2.71 1.0 0.4 1.0 Y 0.00 147.6<br />
010 H J11KV1 2.18 1.0 0.4 1.0 Y 0.00 183.5<br />
011 H J11KV2 2.02 1.0 0.4 1.0 Y 0.00 198.0<br />
012 H J11 1, 21 2.80 1.0 0.4 1.0 Y 0.00 142.9<br />
013 H JlIL23 2.83 1.0 0.4 1.0 Y 0.00 141.3<br />
014 H JlIL25 2.47 1.0 0.4 1.0 Y 0.00 161.9<br />
015 H JllL36 2.18 1.0 0.4 1.0 Y 0.00 183.5<br />
06LE0457-MB1 H SBLKZH 30.0 1.0 0.4 1.0 Y <strong>100</strong>.00 13.33<br />
O6LE0457-MB1 HS SBLKZH 30.0 1.0 1.0 0.4 1.0 Y <strong>100</strong>.00 13.33<br />
Comments:<br />
Surrogate: 500 UL ESU BNA 89915405 @<strong>100</strong>-150 UG/ML<br />
Spike: 750 UL BNA LCS SPIKE 86951017E<br />
(Extracts Transferred Relinquished By Date Time ( Received By I Date Time I Reason for Transfer<br />
I I<br />
I I I I I I<br />
^ ^. I } 'I 3 Vb<br />
I I<br />
M
Extract. Date: 06/02/06<br />
ieSt: 3625<br />
LIMS Report Date: 06/29/06<br />
Sample No: Client ID<br />
SAMPLE EXTRACTION RECORD<br />
Sheet no.: t<br />
Extraction Batch No: 06LE0457 Analyst: MF Method: **** S ay'^S.^ J<br />
Cleanup Late: AL is iy'6t: Client: <strong>RC</strong>-547 K6363 m m<br />
Solvent: DCM Adsorbent: m m<br />
pH Initial Surr. Spike Final Final Split GPC t C/D<br />
WT/VOL Mult. Mult. VOL VOL Mult. Y/N Solids FACTOR<br />
.<br />
0604 1, 904- TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
001<br />
001<br />
001<br />
H<br />
HS<br />
HT<br />
J11KK8<br />
J11KK8<br />
J11KK8<br />
2.024W<br />
2.00 1.0 1.0<br />
2.86 1.0 1.0<br />
0.4<br />
0.4<br />
0.4<br />
0.5<br />
0.5<br />
0.5<br />
Y<br />
Y<br />
Y<br />
0.0<br />
0.0<br />
0.0<br />
99.01<br />
<strong>100</strong>.0<br />
69.93<br />
002 H J11KL5 2.18 1.0 0.4 0.5 Y 0.0 91.74<br />
003 H J11KL6 2.17 1.0 0.4 0.5 Y 0.0 92.17<br />
004 H J11 104 0 2.32 1.0 0.4 0.5 Y 0.0 86.21<br />
005 H J11KM2 2.42 1.0 0.4 0.5 Y 0.0 82.64<br />
006 H J11KM3 2.38 1.0 0.4 0.5 Y 0.0 84.03<br />
007 H J11KM4 2.50 1.0 0.4 0.5 Y 0.0 80.00<br />
008 H J11KM5 2.48 1.0 0.4 0.5 Y 0.0 80.65<br />
009<br />
01 0<br />
H<br />
H<br />
J11KM6<br />
311KV1<br />
2.71<br />
2.18<br />
1.0<br />
1.0<br />
0.4<br />
0.4<br />
0.5<br />
0.5<br />
Y<br />
Y<br />
0.0<br />
0.0<br />
73.80<br />
91.74<br />
011<br />
012<br />
H<br />
H<br />
J11KV2<br />
J111,21<br />
2.02<br />
2.80<br />
1.0<br />
1.0<br />
0.4<br />
0.4<br />
0.5<br />
0.5<br />
Y<br />
Y<br />
0.0<br />
0.0<br />
99.01<br />
71.43<br />
013<br />
014<br />
015<br />
06LE0457-MB1<br />
06LE0457-MB1<br />
H<br />
H<br />
H<br />
H<br />
HS<br />
711L23<br />
J11 1,25<br />
J11L36<br />
SBLKZH<br />
SBLKZH<br />
2.83<br />
2.47<br />
2.18<br />
30.0<br />
30.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0 1.0<br />
0.4<br />
0.4<br />
0.4<br />
0.4<br />
0.4<br />
0.5<br />
0.5<br />
0.5<br />
0.5<br />
0.5<br />
Y<br />
N<br />
N<br />
N<br />
N<br />
0.0<br />
0.0<br />
0.0<br />
<strong>100</strong>.00<br />
<strong>100</strong>.00<br />
70.67<br />
80.97<br />
91.74<br />
6.67<br />
6.67<br />
Comments:<br />
Surrogate: 500 UL ESU BNA 89915405 @<strong>100</strong>-150 UG/ML<br />
Spike: 750 UL BNA LCS SPIKE 86951017E<br />
Extracts Transterreo Relinquisned By Date Time Received By Date Time Reason for Transfer<br />
I I i<br />
__^/U^ I L 6 c^ j /^, l^rr<br />
N<br />
M<br />
m<br />
m
Lionville Laboratory Use On ly<br />
Client T14Lk % e%-CorP <strong>RC</strong>-<strong>047</strong><br />
Custody Transfer Record/Lab Work Request Page! <strong>of</strong> a IV=<br />
Es t. Final Pr<strong>of</strong>. Sampling Date #/Type Cemalner<br />
/./ ^}<br />
Project ^^^J^^1 ^4?1^G7' ^n^^-13—do -f 1<br />
Pro)ect CoMacUPhone A` Volume<br />
Lionville Laboratory Project 0<br />
^ Manager<br />
OC "" Del J! G(._. TAT l ti t G<br />
/.i<br />
Date Rec'd H'U^o Date Due S/J t''<br />
T'o^<br />
FIELD PERSONNEL. COMPLETE ONLY SHADED YEAS<br />
See S<strong>RC</strong> M<br />
m<br />
Rahgeretor• m<br />
p reservatives<br />
ANALYSES<br />
REQUESTED<br />
Liq uid<br />
Send<br />
U wid<br />
Sow<br />
ORGANIC INORG<br />
<<br />
O Zm a Q^ = CP M U<br />
j Llolwllle Laboratory Use only 1<br />
MATRIX<br />
CODES:<br />
Matrix<br />
SE - Soi<br />
Oc<br />
Time<br />
Lab<br />
Matrix<br />
CH<br />
sedenent ID<br />
ID/Deacrlpeon<br />
Chosen<br />
Colllected<br />
^l ^~<br />
so - Solid<br />
SL - Sludge<br />
J<br />
w- Water<br />
MS MSD<br />
V `^C<br />
O- Oil<br />
A- Air co, J ► S KKS y'S X<br />
DS- Drum<br />
solids<br />
DL - Drum<br />
Uquaa ow<br />
!<br />
q$-0te 14-20 X I X -<br />
L• EP/TCLP<br />
6 x X<br />
Leadate<br />
wl - wqm<br />
X • O<strong>the</strong>r<br />
F- fish<br />
cow<br />
oc<br />
3i 1<br />
C;)—<br />
S<br />
la<br />
10 3<br />
X<br />
X I X<br />
X I x<br />
X<br />
n<br />
X<br />
I X<br />
X<br />
OCA J 5 X X<br />
po° J l YY1<br />
J1 I KV I<br />
X X1<br />
Xi<br />
1X<br />
I<br />
X I-<br />
K Special Instructions: ruc ?--it -3-M" ttNlS:<br />
X<br />
,r , C<br />
ti<br />
^<br />
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^<br />
ewe ul.L1s^ 1x4.Da.^ ^W I^.-f'cs+, z.<br />
(Ylr ls, PC8,SJoL. s.<br />
Me-`V35 PCB, RrSA- S\10c<br />
Reanqulehed<br />
by<br />
Received<br />
by<br />
Dale Tlma<br />
^ea^,aA - rNcTRr ^ K-[ -rP'^r,^,<br />
4.<br />
MMrquasbad Rec eived Data<br />
RNlnqulaMd<br />
by Tirol<br />
by by ..<br />
Received<br />
W<br />
^c aYo ^!3 i,;Q POYIip<br />
WASTEe<br />
Data Three<br />
m<br />
m
Lionville Laborato ry Use Only Custody Transfer Record/Lab Work Request Page^ oj VaW O^ FIELD PERSONNEL: COMPLETE AREAS ONLY f SHADEDr<br />
M<br />
6<br />
Client 1 Z, C-<br />
Refrigerator #<br />
Est. Final Pro). Sampling Date orrype Container<br />
Project #<br />
G<br />
Project ContacVPhone # Volume<br />
Lion ville Laboratory Projectl4imager<br />
G<br />
Press. ral Ives<br />
OC Del TAT<br />
O NIC INORG<br />
Date Rec'd Date Due<br />
ANALYSES _^<br />
REQUESTED<br />
Q<br />
p<br />
¢<br />
Zm<br />
^a<br />
y<br />
a<br />
^<br />
= SJ<br />
MATRIX<br />
j /L Lionville<br />
L ionville Laboratory Use On ly j<br />
CODES:<br />
Marta<br />
S - Soil Lab<br />
OC Mahler<br />
Date<br />
lD/Descdpaon<br />
Chosen<br />
Coll<br />
SE.- S<br />
ID<br />
V)<br />
ec<br />
Time<br />
ted Collected<br />
>(1 C'O ^^<br />
SO •solid rd<br />
^ ^ ^--<br />
SL- Sludge<br />
W. Water O U v<br />
MS IMSO<br />
O • Oil<br />
A • Air<br />
N C;L<br />
DS • Drum<br />
.x:..<br />
Solids o I a X /1<br />
DL. Drum<br />
`<br />
1<br />
Liquids V, L a3<br />
a . _.<br />
1 ;:.. ^/<br />
X<br />
L, X<br />
EP/rCLP<br />
Lesahate 5 Q X^<br />
X-<br />
«her 016 J \^ o)s X )c X<br />
F - Fish<br />
Special Instruc ti<br />
ons:<br />
DATEtREYtS ONS:<br />
i1 r.:rJx r ^^^ ► .I SL, r< ^, f^i; t I, ^r? c, (% z.<br />
Re li<br />
r 9.<br />
nquished itacatvad<br />
Re<br />
Dale<br />
linquished Rece<br />
Time<br />
iv ed<br />
by by by by<br />
A-\m-ki 3<br />
1.<br />
5.<br />
8.<br />
Liquid<br />
Sold<br />
Liquid<br />
Solid<br />
Tbrna<br />
U<br />
Relinquished Received<br />
by<br />
by<br />
Date Tlma<br />
m
Washineton Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-259 Page l or i<br />
Collector<br />
TILLER, B. TR KLINCKMAN<br />
Conotnmv Contact<br />
JOAN KPSSNER<br />
Telephone No.<br />
375-4688<br />
Prolect Coordinator<br />
KESSNER, IH Pdce Code 9N Data Turnaround Co<br />
45 Days<br />
rolect DDesignation esi[<br />
Sampling Location SAY Na.<br />
Air Quality ^ Da y m <strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti 600-131/600-190 OFFAL <strong>RC</strong>-<strong>047</strong> 0<br />
9<br />
I ce Clsest Np.yp Field Lo[book No. COA Method <strong>of</strong> Shipment<br />
, rC e - a,2 ^fJ^ EL-1595 BESRAS6520 FED EX 0<br />
Ship ORsito Property No. a Bi ll <strong>of</strong> Lading/Air Bill No.<br />
RLINE SERViCEV LIONVILLE J L/ SEE OSPC<br />
POSSIBLE SAMPLE HAZARDSIREMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-266 Page 3 <strong>of</strong> I<br />
Collector Coamapv CORtaet Tdephouse No. Prolect Coordimtor<br />
TRJER, B. 111 KLINC JOAN KESSNER 375-4688 KESSNER, JH<br />
roiect Desiemtion Samplina Lismu n<br />
<strong>SAF</strong> No.<br />
<strong>100</strong> & <strong>300</strong> Ana <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti 3894H-3k OFFAL ^G 0 ] />^z<br />
<strong>RC</strong>-<strong>047</strong><br />
Ice ChestNo.y -<br />
t^iAOC —^2' D.r<br />
0 J11KL5 OTHER SOLID 1W6 Z,<br />
Fie E No. COA Method <strong>of</strong> Shisma l<br />
141oe Code 9th Data Turnreravuod m<br />
U,<br />
45 Days 9<br />
Air Quality q m_<br />
EL, 1595 BESRAS6520 FED EX m<br />
Sipmed To Offalte Property No. n^ 6 O y d BIB <strong>of</strong> LadiodAlr Bi ll No.<br />
EBERLM LIONVILLE /7 •7 SEE OSPC<br />
PO HAZARDSMEMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-267 j pxv 1. d I<br />
Collector<br />
TILLER, B. TH KLINCKMAN<br />
C[mmanv Cantact<br />
JOAN KESSNER<br />
Teletsbone No.<br />
375-4688<br />
Prolect Coordinator<br />
KESSNER, JH Price Code 9N<br />
Protect DesienaGon<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and n<br />
Ice Chest No.r<br />
y j^(J -- ^^<br />
Satnpbne Location<br />
1 I6-N-3 OFFAL<br />
Field Logbook No.<br />
FL-1595<br />
COA<br />
BESRAS6520<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Method <strong>of</strong> Shipment<br />
FED EX<br />
Air Quality<br />
Data Trrrnarourssm<br />
V<br />
45 Days m<br />
CD<br />
m—<br />
m<br />
m<br />
CD<br />
Ship<br />
L•RLINE SERVICES LIONVILLE _<br />
ORsile Pronety No. / p<br />
Q(/Q J^L/<br />
Bib <strong>of</strong> Ladlisit/A ir BIB No.<br />
SEEOSPC<br />
POSSIBLE SAMPLE HAZARD6/ItEMARKS<br />
POTENTIAL RADIOACTIVE eDOTUMITS<br />
Special Handling and/or Storage<br />
COOL 4C "MATRIX COMPOSED OF MICE"<br />
SAMPLE ANALYSIS<br />
S ^, 41<br />
Presevauon<br />
Type <strong>of</strong> Container<br />
No. <strong>of</strong> Contalaer(s)<br />
Volume<br />
Iw ® 3<br />
Sample No. Max Matrix •<br />
Sam Date Sample Time<br />
J11KL6 OTHER SOLID APR 0 3 2006 Wo k<br />
Coal Node Cu l 4C Goes 4C eu4C m Cu,d4C<br />
aG<br />
GIP G/P aG aG aG<br />
1 I 0 0 0 0<br />
25% log 158 30s 508 508<br />
Seeias(11n Seeinn(21in<br />
Speid Spew<br />
Seelam(3)in<br />
speew<br />
Porn-tion Peabides.<br />
anal<br />
SeriVOA-<br />
IMA (TCL)<br />
Ihharahfom Inamnbna I.urununa.<br />
_ r r<br />
k x<br />
r` £<br />
CHAIN OF POSSESSION Sign/Print Name SPECIAL INSTRUCTIONS<br />
Matrix'<br />
Re6nryished By/Remond From /K smc<br />
EAS LOCKED STOR ts^ ey'°,.^<br />
Dalefrime<br />
-<br />
NOTE: Ebalme. Perform Gaorna Spec *am baa+hp book I01Jomil le Labs, if possib le maintain 4 C<br />
Gong. <strong>of</strong>i L'omil le.Pulorm me ta Nk/V DalHnme<br />
NOW<br />
7h C)<br />
ell uis d B /Rmnuved F s Daemme<br />
aq<br />
Rttt^i ved By/5[aed In<br />
!<br />
r".<br />
Received B Y/Sward N<br />
Date/rime<br />
IeT^<br />
Z<br />
ls, FCBXEST,SVOC in order as simp le is avai lable. Contract Coact Joan<br />
Kessocr salon macipa. _<br />
(1) Gamma Spa-(Full lisp lAmencima:fl, Anrirraay-125. Be rylinm7, Cesitmn134-Cesium137,<br />
Cobalt-60. Europiuml52. Europium-154, Etaopiam155, P erassiu -40, Radium22 ( , Radlam226.<br />
•sa<br />
f^s E.s 4ma<br />
so-ASw<br />
sksh hs.<br />
W. W.<br />
OcO 1<br />
A.A.<br />
O/ RurlcniumlOO.Unoium235,Uracium23s) Relic 'hed e F DotNrmle<br />
X Yt^ ^! 6 OG ^G 17/7<br />
eGuquishe By/R Hued From Dame<br />
x<br />
4linqui 5hc y/Removedroom Daerfacc<br />
T*TA<br />
Received /S din<br />
D^—<br />
rived<br />
Received By/Stonfl 14<br />
_<br />
b<br />
)me<br />
DdeTme<br />
Durerring<br />
l^ (2) ShootinmB9.90--Tarsi Sr. lsaopk Tho ium(Tnaiwsr23?); Isotopic U ranium l Uranium-233834,<br />
Uranium235,Unomm238);lsouocPlalonium<br />
(3) ICP Meala-60101Fu11 IJsq lAlurhiaam Antieay.rse n Anic• Barium 8cryllium Bismank aca B.<br />
Cadmium Ca lcium, Chromium Cabal, Copper, bra, lead. IAtdum Magnesium Manganese,<br />
Molybdenum L ybdenum Nickel. Phosphdos, Po pnium Seleainm Silicon. Silver, Sodium Strontium Thallium<br />
Uranium. Vanadium Zinc ): Mercu ry - 7471 - (CV)<br />
uM<br />
sK.o, &"<br />
a.ne.,,ugy<br />
T.Ta..<br />
wr.w^l.<br />
'd<br />
z.alh.<br />
LAAORATORY Received By TitleDateTme<br />
`^+VS<br />
SECTION<br />
FINAL SAMPLE Disposal Method Disposed By D+INfime<br />
UISPOtiI'I'ION<br />
SHI-EE-011 (08/29/2005)
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-271 j Pw I <strong>of</strong> I<br />
Collector<br />
rnLLER, B. TR KLINC<br />
Compam Contact<br />
JOAN KESSNER<br />
Telephone No.<br />
375-4688<br />
Pro ject Coordinator<br />
KESSNER, Bit<br />
Price Code 9N Data TurOaro ..<br />
oiect Desianation<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Samdina Location<br />
1607-13 2:1 OFFAL<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Air Quality q<br />
Ice Chest No.///tea<br />
/y i[ (^- ^1 ^^<br />
Field Loabo rk No.<br />
EL-1595<br />
COA<br />
DESRAS6520<br />
Method <strong>of</strong> Shlomept<br />
FED EX<br />
(S)<br />
m<br />
Offxtle Pum1v No. ,y06D q?^ B<br />
Sh' ro<br />
BI <strong>of</strong> Ladmv/Air Bi ll No.<br />
ERLBVE SERVICE LIONVILLE •73 SEE OSPC<br />
POSSIBLE SAMPLE HAZARDSJREMARKS<br />
POTEN77ALRADIOAC77VE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-273 Nse t el 1<br />
011ecLE TILLER, TI B. TR KLINCKMAN<br />
CompanyContact<br />
T<br />
375-4689<br />
o<br />
KFSiSNER. III<br />
Price Code 9N Data Turtaarou^i<br />
Proled Designation<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>HRA Sediment and Ti -<br />
Samp ling Location<br />
BORROW PIT 74 OFFAL<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Air Quality q 45 Day%<br />
m<br />
Ice Cheat No.<br />
eree- e2 -/j Q r<br />
Field Loabook No. COA Method <strong>of</strong> Shipment h9<br />
_<br />
EL 1595 BESRAS6520 FED EX<br />
Shipp OBbite Property No. Bi ll<br />
<strong>of</strong> LadipdAir Bi ll<br />
No.<br />
HERLINESRVICES LIONVILLE SEE OSPC<br />
POSSIBLE SAMPLE IIAZA RDSfREMARKS<br />
POTENTIAL RADIOAC77VE eOOTLIMITS<br />
Special Handlingand/or Storage<br />
COOL 4C "MATRIX COMPOSED OF MICE"<br />
SAMPLE ANALYSIS<br />
S.^[. -afA<br />
Praeryatlon<br />
Type <strong>of</strong> Container<br />
No. <strong>of</strong> Contaicer(s)<br />
Volume<br />
^ 3 G1 ^<br />
Caa 4C none caul ac Caul 4C Cad 4C Qad 4C<br />
'Cs<br />
Gm GOP aG- aG aG<br />
I 1 0 0 0 0<br />
2508 log 15g SOB 509 50g<br />
Ses h.01n Scit.(2)a Seeionn P)ia PCns- M2 Paua _ Sbaivm.<br />
3P." S Pcdel Slaid tol l 8270A(7CL!<br />
lows+ Inu.iutm Invnlcl{pay<br />
Sample No. Matrix • Sample Date Samp le Tune c. may,,, =r .^.- -, w<br />
J1IHM2<br />
SOLID<br />
OTHER<br />
0 3 2570 /1( X x ^(<br />
CHAIN OF POSSESSION<br />
Re linquished ByliemovWPsom<br />
^/<br />
EAS L<br />
_qqu lRe rant,r:_jy<br />
IrLL<br />
Relinquished ey moved Fars<br />
Relingni B e ved Fran<br />
Relinquished By/Rerr oved Fran<br />
Y-/° -"`<br />
/ 3 e'<br />
Dale/Time<br />
/fp0<br />
Irate/time<br />
WidrMac<br />
DmcRi"n<br />
SigNPrint Names<br />
R i B din<br />
S<br />
Re caiv y/Staed to<br />
—ica<br />
4r—<br />
Hecehed By In<br />
H 8 In<br />
ived By S cd In<br />
SPECIAL INSTRUCTIONS<br />
DucTme<br />
NOTE: Bberire- perfpm Gardens Spec Men tranship bode to Lionville tabs, Possible smintain 4C<br />
cook IS. Lionvil le: pertinent net W. PCB.PBSTSVOC in this order as tample is availab le. Canaan Joan<br />
7p Kesster",etxipt.<br />
_<br />
DgaRme<br />
(I) Gammn Spec-(FAN tin) IAnerieiaawUl. Aninuny425, BeryIUum7,Caium134,Cesiam132,<br />
Cobek-60, Fnmpiuml5?, rwaopium154, Cvopiurth-155, PMassium40, Rahanm22ti, Radium?^8.<br />
Out _)(^<br />
,"^n/e<br />
Rulhnium106, Urnrium235, Undum23 11 I<br />
Z Vp V (2) Suaninm89.90 ._ Total Sr hoopic Thorium ITho ium2321: Isaapk Umnism iUmni m233/734.<br />
DatelTinac<br />
Unudhms235, Unnihms2381: Isaopic Plutonium<br />
(3) ICP Meta ls - 6010 (FUN List) IAkmdnum Asainmy, A rsenic, Ba rium Berylliu m Bismuth, Boron,<br />
'UL 0 ^ao Cadndum Gkium Chromium Cabe a. Copper, Imn, lead, Lithium Ma Magnesium Manganese,<br />
Da1c/lise Molybdenum Nickel, Phosphorus, Potassium Se lenium Silicon, Silver. Sodium Stradium T1ml lium,<br />
Trn, Umnium Vanadium Lncl: Mercury- 7471 - (CV)<br />
Matrix *'<br />
Ma<br />
aFiawae<br />
p.Sl<br />
`.w°tl<br />
n`al<br />
py us<br />
T•Twr•wxv<br />
n'^<br />
x.01-<br />
Relinquished By/Removed frown nafe/flne Received By/Srored in Date/fime<br />
S'4-A I(^j 3 C) 7)<br />
LABORATORY Received By Tide Date/1-mw<br />
SECTION<br />
FINAL SAMPLE Disposal Me thod Disposed By Dne?'me<br />
DISPOSITION<br />
BHI-EE-011 (08128!2005)
Washington Closu re <strong>Hanford</strong> CHAIN OF CUSTODYISAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-274 >,^ i w t<br />
Collector<br />
Company Contact Tekphone No. Pro tect Coordinator<br />
TILLER, B. TR KLINCKMAN<br />
JOAN KPSSNER 375-4688 KESSNER. JH<br />
^^ Code 9N Data 7Lrnerouda<br />
rrolect Desirnaaon - Sarnuline Lanaon <strong>SAF</strong>Ne.<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> Compon <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sedisnau and Ti YAKIPAA RIDGE IF OFFAL <strong>RC</strong>-<strong>047</strong> 0<br />
Ice Chest No. ! FIeELA 595ook No. Method^Shiproeot<br />
FSRAS6520<br />
Slri J<br />
ORsite Prow"v No. ^O^ O 2 ? Bill <strong>of</strong> Ladinv/Air Bill No.<br />
BERLfNESERVICFS LIONVR.LE<br />
JJ SEE OSPC<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-275 I pw J <strong>of</strong> 1<br />
Collect"<br />
TILLER, B. TR KLINCKMAN<br />
roiect Desienatioa<br />
<strong>100</strong> & <strong>300</strong> Arcs <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Tt<br />
Ice Chat No.p n<br />
/L TC " DZ -,dS<br />
Shi<br />
BERLINESERVICES ONVIL)E<br />
POSSIBLE SAM PUETFAZARDSJREMARILS<br />
POTENTIALRADIOAMV£
Washington Closu re <strong>Hanford</strong> CHAIN OF CUSTOIJIMAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-276 Page 2 <strong>of</strong> L<br />
Collector<br />
TILLER, B- TR KLINCKMAN<br />
Protect Destination<br />
<strong>100</strong> & <strong>300</strong> Arm <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
fee Chest No. p^<br />
plc C — Oz -5,D,57—<br />
Sh<br />
ERE LI ESER LIONVILLE<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE 3 D 3<br />
Prolect Coordinator<br />
KESSNER, JH price Code 9N Data Turnarounlll<br />
V<br />
SAP No.<br />
<strong>RC</strong>-<strong>047</strong><br />
43 Days m<br />
Air Quality El y m 0<br />
COA Method orShioment m<br />
ESRAS6520<br />
FED EX<br />
m<br />
2qBE<br />
Z2603 d0-<br />
<strong>of</strong><br />
BS E<br />
SO PC<br />
BRI No.<br />
Cue14C name Ceu14C C.1 4C C.1 4C I C-14C<br />
aG GIP GIP aG aG MG<br />
( 1 0 0 0 0<br />
1509 log 158 508 50g 508<br />
Sae imr(1)n Seeaann(2)ia Smkan Min iCB,.Wl P
Washin>;ton Closure <strong>Hanford</strong> CHAIN OF CUSTODYISAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-277 ^^ L or 5<br />
Ilect" _<br />
TILLER. B. R KLINCKMAII<br />
Comoanr Contact<br />
JOAN KESSNER<br />
Telephone No.<br />
375-4688<br />
Praiecl Coordinator<br />
ICESSNER, ]H Price code<br />
roiect Desirnndan<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Tt<br />
Sanoline Location<br />
SADDLE MOUNTAIN OFFAL<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-007<br />
9N<br />
Air Quality<br />
Data Turstarmumn<br />
a<br />
45 Da ^' sm m<br />
9<br />
Ice Chest No. y^^ _ Oz Field L.oebook No, COA Merlwd <strong>of</strong> Shimomt m<br />
C ^US<br />
Et, 1595 BESRAS6520 FED EX m<br />
Sld ed To - Offske Properly No. BID <strong>of</strong> Ah• BID No,<br />
BERLINE SFBVIC LIONVILLE ff J SEE OSPC<br />
POSSIBLE SAMPLE IIAZARDS /REMARKS<br />
POTEN77AL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REOUEST <strong>RC</strong>-<strong>047</strong>-322 J PW I <strong>of</strong> I<br />
Collector<br />
TILLER, B. TR KLINCKMAN<br />
Costwapy Contact Telephone No.<br />
JOAN KESSNER 375-4688<br />
Protect Coordinator<br />
KESSNER, JH<br />
Price Code 9N<br />
Data Tsrnarour^<br />
45 Days9<br />
'ralect 1)esienation Samalirs¢ Lo cation <strong>SAF</strong> No.<br />
Air Quality<br />
IM) & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and 71 <strong>100</strong>-DAS:2 OFFAL <strong>RC</strong>-<strong>047</strong> m<br />
Ice Chest No. r<br />
Field Loebook Na. COA Method <strong>of</strong> SWonant - m<br />
-JrO156-m<br />
C -Q.Z EL_ 1595 BFSRAS6520 FED EX<br />
MPO^SJBLF _= SAMPLE<br />
LIONVILLE<br />
HAZARDSIREMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS RE UEST <strong>RC</strong>-<strong>047</strong>-323 I Pate I Of I<br />
Collector<br />
TILLER, B. TN KLINCKMAN<br />
Protect Desknotion<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Company Contact<br />
JOAN KESSNER<br />
Samulina Loca ti on<br />
<strong>100</strong>-0.49:2 OFFAL<br />
Telephone No.<br />
375-4688<br />
Pro ieet Coordinator<br />
KESSNER, III<br />
SAP No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Price Code 9N<br />
Air Quality p<br />
pale Tururg0 naro<br />
m<br />
45 Day m<br />
(g<br />
m<br />
ICE Chest No. Field Logbook No.<br />
EL- 1595<br />
COA<br />
BESRAS6520<br />
Method <strong>of</strong> Shipmmtt<br />
FED EX<br />
m<br />
,^D,6oa33o<br />
S - ped'ra Olfsile Property No.<br />
Bill <strong>of</strong> Lading/Air Bill No.<br />
ER 04ESERVI 1LIONVILLE SEEOSPC<br />
POSSIBLE SAMPLE HAZARDWREMARKS<br />
POTENTIALRADIOACnVE
Washington Closure <strong>Hanford</strong> ' CHAIN OF CUSTODY/SAMPLE"ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-328 Paso 1 <strong>of</strong> 1<br />
Collector<br />
TILLER, B. TR KLINCKMAN -<br />
Company Contact<br />
JOAN KESSNER<br />
Telephone No.<br />
375-4688<br />
Proisd Coordinator<br />
KESSNER, JH Price Code 9N Date<br />
It u,<br />
roket Destenalion<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> Comp.mest <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Seditrseot and Ti<br />
Ice Chest No. y-N<br />
Pi le C' 0.2 - 3rO,S<br />
So sogna Locadat<br />
116-DR-I,DR-7JI00-D-22 OFFAL<br />
Field Lenbook No,<br />
Et.-1595<br />
COA<br />
BFSRAS6520<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Method <strong>of</strong> Shipment<br />
FED EX<br />
Air Quality Qy q<br />
5 Days%<br />
%m<br />
tD<br />
Ship<br />
D ERLINESERVICES LIONVILLE<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE.
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-330 [ P -P 1 « 1<br />
Collector<br />
TILLER, B.<br />
TR KLINCKMAN<br />
'rolat Designation<br />
<strong>100</strong> & <strong>300</strong> Atha <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
lee Chest No.pp<br />
2 see e.2 -,sly Jam'<br />
Company Contact Te lephone No.<br />
JOAN KESSNER 375-4688<br />
Samp ling Loca ti on<br />
BORROW PIT 23 OFFAL<br />
Field Losbook No.<br />
EL-1595<br />
A06033a<br />
COA<br />
BESRAS6520<br />
Sh OfEdtc Properly No.<br />
Bi ll <strong>of</strong> Ladins/Air Bill No.<br />
EBERLINESERVICES LIONVILLE SEE OSPC<br />
POSSIBLE SAMPLE HAZARDMU MARKS<br />
POTENTIAL RADIOACTIVE Tne ,04<br />
EM LOCJ(ED STORAG E<br />
R^li vep^ y ^^^<br />
s<br />
m b-4eH Dakrtirm<br />
/ ^(/aU<br />
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elirquis 8 eoved m Fmm Dak?nz<br />
SigulPrint Names<br />
fn :^^<br />
eceived BylStded In<br />
^(' ,d Cx<br />
Received B n<br />
SPECIAL INSTRUCTIONS<br />
Dn^me<br />
NOTE: aeffee-perform Gamma Spec 0sentranshipbottle toUm•ilk Labs, ifpossible rtsinaio4C<br />
caa ft limrilk: perform an PCB.PEST,SVOC in this 0 as sa yk is anilable. Cod t loan<br />
y0 (J<br />
R<br />
ICesnrr upm receipt.<br />
Datemme<br />
(1) Omani Spec - (Full Liso 1 Americium241, Andmany-13. Bnyllium7, Cesium134. Ceaium137.<br />
Cobdt-60, FLmpitn.152, Euopium154, BvWium155, Pomsiu1r1d0. Radii 226, Radior 228,<br />
'Dal ^'m 1^ Rudica u e, 106. Urmhm-235, Undom2381<br />
Relin sbedd c Fmm a Unt<br />
t1A 9,<br />
Received B In Iku<br />
(n<br />
me<br />
s/U (2) Stmndu n39.90- Toad Sr. holopie T hmium I Thork m2321:<br />
IsdWk Urtmsm l Uranimu233/r_34,<br />
Umniom235. Uamimt-2381: hdapie P lutonium<br />
Reli quisle y/Re ed From<br />
Relinquished BY/Remmed Fwn,<br />
De nse<br />
Datefftme<br />
Recei B<br />
Received BY<br />
InDndfine<br />
A ck 0730<br />
d In Outeflihm<br />
^G^ul (E^ 50-t.<br />
LABORATORY Received By Tit leDate?rte<br />
SECTION<br />
FINAL SAMPLE Dispmal Method Disposed By Dale/rim<br />
DISPOSITION<br />
13 HI-EE-011 (08/2912005)<br />
Matrix<br />
s .<br />
soaeta<br />
sasaw.<br />
W. W.<br />
°'O^<br />
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1a.a t.q. n<br />
T-Tiwe<br />
4LpuY<br />
v"vga°n.<br />
xon<br />
-
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>.332 Page I <strong>of</strong> L<br />
Collector<br />
TILLER, B.<br />
TH KLINCKMAN<br />
Conmur Contact<br />
JOAN KESSNER<br />
Telephone No,<br />
375-4688<br />
Protect Designation - Sampling Location <strong>SAF</strong> Na<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti 600.131 OFFAL <strong>RC</strong>-<strong>047</strong><br />
Protect Coord inator<br />
KESSNER, JH Price Code 9N Data Turnarour^<br />
Air Quality p<br />
45 Day ,'. 'n<br />
Ice Chat No.////^a Field Loahook No. COA Method <strong>of</strong> Shipment<br />
lee— m<br />
EL.- 1595 BESRAS6520 FED EX m<br />
Shinned To Offaile Property No. Atr Bill m<br />
^<br />
os^ Na<br />
- INESERV / LIONVILLE<br />
SEE<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-343 I NVe i <strong>of</strong> i<br />
collector - Company Contact Telephone No. Prolecl Coordinator<br />
TILLER, B. TR KLINCKIAAN JOAN KESSNER 375-4688 KESSNER,IH<br />
Price Code 9N<br />
Data Tnrstarousq^<br />
45 Daysm<br />
oiect Desiauation SampRne Location<br />
<strong>SAF</strong> No, Air Quality E]<br />
<strong>100</strong> & <strong>300</strong> Ar a <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sedimeat and Ts CF14TRAL PLATEAU SHRUB STEPPE OFFAL <strong>RC</strong>-<strong>047</strong> em_<br />
Ice Chest No. Fleld Na<br />
EL, 1595<br />
Slg C.<br />
OfrAle Property No<br />
HERLINE SERVIC LIONVILLE<br />
POSSIBLE XE HAZA RW/REMARKS<br />
POTEATIALRADIOAC71VE
^\<br />
CLIENT: —Y-VW<br />
Lionvi ll<br />
e Laboratory Incorporated<br />
SAMPLE RECEIPT CRECKLIST (S<strong>RC</strong>)<br />
(<br />
r<br />
Yurchs^e Order / Project# / C y<br />
/ W# / Release #: R<br />
n<br />
\iCiN-J- t3^ Date:<br />
Batch # : ?^ , 1 • Sample Custodian:<br />
1. Samples Hand De livered w Shipped<br />
2. Custody seals on coolers or shipping<br />
container intact, signed and dated?<br />
NOTE:<br />
3. Outside <strong>of</strong> coolers or shipping containe rs are<br />
free from damage?<br />
4. All expected paperwork received (coo and<br />
o<strong>the</strong>r c lient speci fic information) sealed in<br />
plastic bag and easily access ible?<br />
5. Samples receiv cool ambient? yQ<br />
6. Custody seals on sample containers intact<br />
signed and dated?<br />
7. coc signed and dated?<br />
8_ Sample containers are inta ct?<br />
9. All samples on coc received? A ll samples<br />
received on coc?<br />
10. Ali<br />
label information matches coc?<br />
11. Samples properly preserved?<br />
12. Samples received within hold times?<br />
Short holds taken to wet lab?<br />
SR-002-11<br />
13. VOA, TOC, TOX free <strong>of</strong> headspace?<br />
14. QC stickers placed on bottles designated by<br />
client?<br />
15. Shipment meets LvLI Sample Acceptance<br />
Policy? (Identify a ll bottles not within<br />
policy. See reverse side for policy)<br />
16. Project Manager contacted concerning<br />
discrepancies? nameldste (or samples<br />
outside criteria)<br />
vLl<br />
N ALL DISCREPk<br />
-e. so<br />
/<br />
l 4" O Ne<br />
P<br />
TT7<br />
Yes O No<br />
a O No<br />
emp —j-'J °C<br />
Yes O No<br />
ra<br />
Ya<br />
Y<br />
/ es<br />
I9(Yes<br />
)dyes<br />
Yes<br />
O Ya<br />
O Ycs<br />
O Yes<br />
6]"Yes<br />
O No<br />
ONO<br />
O No<br />
O No<br />
0 No<br />
O No<br />
ONO<br />
Airb ill# 701 27<br />
O No Seals Comments<br />
o15O'J 7<br />
Cooler# SANS-\^3<br />
O No Seals<br />
^N/A<br />
ONO n,(/A<br />
ONo<br />
44<br />
P.= 3<br />
0 N No<br />
Discrepancies<br />
000000053
w EBERLINE<br />
VSERVICES<br />
May 30, 2006<br />
Ms. Joan Kessner<br />
Washington Closure <strong>Hanford</strong><br />
3190 George Washington Way<br />
MSIN H9-02<br />
Richland, WA 99352<br />
Reference: P.O. #630<br />
Eberline Se rvices R6-04-093-7420, SDG K0303<br />
Dear Ms. Kessner:<br />
-12a<br />
\^,^OZ6l•8^<br />
Enclosed is <strong>the</strong> data report for sixteen solid (o<strong>the</strong>r solid) samples designated under <strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong>. The samples were received at Ebertine Se rvices on Ap ril 12, 2006. The samples were<br />
analyzed according to <strong>the</strong> accompanying chain-<strong>of</strong>-custody documents.<br />
Please call if you have any questions conce rn ing this report.<br />
Sincerely,<br />
Melissa C. Mannion<br />
Senior Program Manager<br />
MCM/njv<br />
Enclosure: Data Package<br />
,Zr<br />
Z<br />
w<br />
^^9^^^^'<br />
Analytical Services<br />
2030 Wright Avenue<br />
P.O. Box 4040<br />
Richmond, California 94804-0040<br />
(510) 235-2633 Fax (510) 235.0438<br />
Toll Free (800) 841-5487<br />
www.eberlineservices.com
Eberline Services Washington Closure <strong>Hanford</strong><br />
W.O. No. R6-04-093-7420 SDG K0303<br />
Case Narrative Page 1 <strong>of</strong> 1<br />
1.0 GENERAL<br />
Washington Closure <strong>Hanford</strong> (WCH) Sample Delivery Group K0303 was composed <strong>of</strong><br />
sixteen solid (o<strong>the</strong>r solid) samples designated under <strong>SAF</strong> No. <strong>RC</strong>-<strong>047</strong> with a Project<br />
Designation <strong>of</strong>: <strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti.<br />
The samples were received as stated on <strong>the</strong> Chain-<strong>of</strong>-Custody documents. Any<br />
discrepancies are noted on <strong>the</strong> Ebertine Services Sample Receipt Checklist. All results<br />
were transmitted to WCH via e-mail on May 25, 2006.<br />
2.0 ANALYSIS NOTES<br />
2.1 Total Strontium Analysis<br />
No problems were encountered during <strong>the</strong> course <strong>of</strong> <strong>the</strong> analyses.<br />
2.2 Isotopic Thorium Analysis<br />
No problems were encountered during <strong>the</strong> course <strong>of</strong> <strong>the</strong> analyses.<br />
2.3 Isotopic Uranium Analysis<br />
No problems were encountered during <strong>the</strong> course <strong>of</strong> <strong>the</strong> analyses.<br />
2.4 Isotopic Plutonium Analysis<br />
No problems were encountered during <strong>the</strong> course <strong>of</strong> <strong>the</strong> analyses.<br />
2.4 Gamma Spectroscopy<br />
No problems were encountered during <strong>the</strong> course <strong>of</strong> <strong>the</strong> analyses.<br />
Case Narrative Certification Statement<br />
"I certify that this data package is In compliance with <strong>the</strong> SOW, both technically<br />
and for completeness, for o<strong>the</strong>r than <strong>the</strong> conditions detailed above. Release <strong>of</strong> <strong>the</strong><br />
data obtained in this hard copy data package has been authorized by <strong>the</strong><br />
Laboratory Manager or a designee, as verified by <strong>the</strong> following signature."<br />
Melissa C. Mannion Date<br />
Senior Program Manager
E B E R L I N E S E R V I C E S/ R I C H M O N D<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion Contract No. 630<br />
Case no SDG K0303<br />
S U M M A R Y D A T A S E C T I O N<br />
T A B L E O F C O N T E N T S<br />
About this section 1<br />
Sample Summaries 3<br />
Prep Batch Summary 5<br />
Work Summary 6<br />
Method Blanks 10<br />
Lab Control Samples 12<br />
Duplicates 13<br />
Data Sheets 15<br />
Method Summaries 31<br />
Report Guides 41<br />
End <strong>of</strong> Section 55<br />
Lab id EBRLNE<br />
Prepared by Protocol <strong>Hanford</strong><br />
Version Ver 1.0<br />
Form DVD-TOC<br />
Version 3.06<br />
Reviewed by Report date 05/25/06
EBERLINE SERVI CES / RI CHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion R E P O R T G U I D E Contract No. 630<br />
Case no SDG K0303<br />
ABOUT THE DATA SUMMARY SECTION<br />
The Data Summary Section <strong>of</strong> a Data Package has all data, in several<br />
useful orders, necessary for first level, routine review <strong>of</strong> <strong>the</strong> data<br />
package for a Sample Delivery Group (SDG). This section follows <strong>the</strong><br />
Data Package Narrative, which has an overview <strong>of</strong> <strong>the</strong> data package and a<br />
discussion <strong>of</strong> special problems. It is followed by <strong>the</strong> Raw Data Section,<br />
which has full details.<br />
The Data Summary Section has several groups <strong>of</strong> reports:<br />
SAMPLE SUMMARIES<br />
The Sample and QC Summary Reports show all samples, including QC<br />
samples, reported in one SDG. These reports cross-reference client and<br />
lab sample identifiers.<br />
PREPARATION BATCH SUMMARY<br />
The Preparation Batch Summary Report shows all preparation batches<br />
(lab groupings reflecting how work was organized) relevant to <strong>the</strong><br />
reported SDG with information necessary to check <strong>the</strong> completeness and<br />
consistency <strong>of</strong> <strong>the</strong> SDG.<br />
WORK SUMMARY<br />
The Work Summary Report shows all samples and work done on <strong>the</strong>m<br />
relevant to <strong>the</strong> reported SDG.<br />
METHOD BLANKS<br />
The Method Blank Reports, one for each Method Blank relevant to <strong>the</strong><br />
SDG, show all results and primary supporting information for <strong>the</strong> blanks.<br />
LAB CONTROL SAMPLES<br />
The Lab Control Sample Reports, one for each Lab Control Sample relevant<br />
to <strong>the</strong> SDG, show all results, recoveries and primary supporting<br />
information for <strong>the</strong>se QC samples.<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 1 Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 1 Report date 05/25/06
E B ERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion G U I D E, C O n t Contract No. 630<br />
Case no SDG K0303<br />
DUPLICATES<br />
A BOUT T HE DATA SUMMARY SECTION<br />
The Duplicate Reports, one for each Duplicate and Original sample pair<br />
relevant to <strong>the</strong> SDG, show all results, differences and primary<br />
supporting information for <strong>the</strong>se QC samples.<br />
MATRIX SPIKES<br />
The Matrix Spike Reports, one for each Spiked and Original sample pair<br />
relevant to <strong>the</strong> SDG, show all results, recoveries and primary supporting<br />
information for <strong>the</strong>se QC samples.<br />
DATA SHEETS<br />
The Data Sheet Reports, one for each client sample in <strong>the</strong> SDG, show all<br />
results and primary supporting information for <strong>the</strong>se samples.<br />
METHOD SUMMARIES<br />
The Method Summary Reports, one for each test used in <strong>the</strong> SDG, show all<br />
results, QC and method performance data for one analyte on one or two<br />
pages. (A test is a short code for <strong>the</strong> method used to do certain work<br />
to <strong>the</strong> client's specification.)<br />
REPORT GUIDES<br />
The Report Guides, one for each <strong>of</strong> <strong>the</strong> above groups <strong>of</strong> reports, have<br />
documentation on how to read <strong>the</strong> associated reports.<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 2 Form DVD-RG<br />
SUbDIARY DATA SECTION Version 3.06<br />
Page 2 Report date 05/25/06
CLIENT SAMPLE ID<br />
J11KK8<br />
JllKL5<br />
JllKL6<br />
J11KM0<br />
JllKM2<br />
Jll KM3<br />
Jll KM4<br />
J11KM5<br />
JllKM6<br />
J11KT0<br />
J11KV1<br />
J11KV2<br />
JIIL21<br />
JIIL23<br />
JIIL25<br />
JllL36<br />
SIG 7420<br />
Contact Melissa C. Mannion<br />
Method Blank<br />
Lab Control Sample<br />
Duplicate (R604093-06)<br />
SAMPLE SUMMARY<br />
Page 1<br />
SUMMARY DATA SECTION<br />
Page 3<br />
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SAMPLE SUMMARY<br />
LAB CHAIN OF<br />
Client <strong>Hanford</strong><br />
Contract No. 630<br />
Case no SOO X0303<br />
LOCATION MATRIX LEVEL SAMPLE ID SAP NO CUSTODY COLLECTED<br />
600-132/600-190 OFFAL SOLID R604093-02 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-259 04/05/06 09:19<br />
1607-H2 OFFAL SOLID R604093-03 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-266 04/05/06 08:12<br />
116-N-3 OFFAL SOLID R604093-04 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-267 04/03/06 14:20<br />
1607-D2:1 OFFAL SOLID R604093-05 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-271 04/05/06 07:52<br />
BORROW PIT 24 OFFAL SOLID R604093-06 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-273 04/03/06 12:56<br />
YAKIMA RIDGE II OFFAL SOLID R604093-07 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-274 04/03/06 12:30<br />
VERNITA UPRV S.SIDE OFFL SOLID R604093-08 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-275 04/03/06 10:43<br />
MCGEE RANCH OFFAL SOLID R604093-09 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-276 04/03/06 09:45<br />
SADDLE MOUNTAIN OFFAL SOLID R604093-10 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-277 04/03/06 09:00<br />
116-N-3 INVERTEBRATES SOLID 8604093-01 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-311 04/D3/06 06:57<br />
<strong>100</strong>-D-48:2 OFFAL SOLID R604093-11 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-322 04/05/06 06:55<br />
<strong>100</strong>-D-49:2 OFFAL SOLID R604093-12 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-323 04/05/06 07:20<br />
116DR1,DR-2/<strong>100</strong>-D-22 OFL SOLID R604093-13 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-328 04/03/06 13:56<br />
BORROW PIT 23 OFFAL SOLID R6D4093-14 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-330 04/03/06 13:20<br />
600-131 OFFAL SOLID R604093-15 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-332 04/05/06 08:48<br />
CENT.PL.AT .SHRUB STEP.OFL SOLID R604093-16 <strong>RC</strong>-<strong>047</strong> <strong>RC</strong><strong>047</strong>-343 04/03/06 10:15<br />
SOLID 8604093-18 <strong>RC</strong>-<strong>047</strong><br />
SOLID R604093-17 <strong>RC</strong>-<strong>047</strong><br />
BORROW PIT 24 OFFAL SOLID R604093-19 <strong>RC</strong>-<strong>047</strong> 04/03/06 12:56<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
Version Ver 1.0<br />
Form DVD-CS<br />
Version 3.06<br />
Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
/^<br />
Contact Melissa C. Mannion<br />
4 C SUMMARY Contract No. 630<br />
Case no SDG K0303<br />
CHAIN OF t SAMPLE BASIS DAYS SINCE LAB DEPARTMENT<br />
QC BATCH CUSTODY CLIENT SAMPLE ID MATRIX SOLIDS AMOUNT AMOUNT RECEIVED COIL SAMPLE ID SAMPLE ID<br />
7420 <strong>RC</strong><strong>047</strong>-259 J11KK8 SOLID <strong>100</strong>.0 77.8 g 04/12/06 7 R604093-02 7420-002<br />
<strong>RC</strong><strong>047</strong>-266 JllKL5 SOLID <strong>100</strong>.0 69.6 g 04/12/06 7 R604093-03 7420-003<br />
<strong>RC</strong><strong>047</strong>-267 J11KL6 SOLID <strong>100</strong>.0 74.5 g 04/12/06 9 R604093-04 7420-004<br />
<strong>RC</strong><strong>047</strong>-271 JllKM0 SOLID <strong>100</strong>.0 86.8 g 04/12/ 06 7 R604093 -05 7420-005<br />
<strong>RC</strong><strong>047</strong>-273 J11KM2 SOLID <strong>100</strong>.0 88.7 g 04/12/06 9 R604093-06 7420-006<br />
<strong>RC</strong><strong>047</strong>-274 J11KM3 SOLID <strong>100</strong>.0 81.0 g 04/12/06 9 R604093-07 7420-007<br />
<strong>RC</strong><strong>047</strong>-275 J11KM4 SOLID <strong>100</strong>.0 91.5 g 04/12/06 9 R604093-08 7420-008<br />
<strong>RC</strong><strong>047</strong>-276 J11KM5 SOLID <strong>100</strong>.0 65.9 g 04/12/06 9 R604093-09 -7420-009<br />
<strong>RC</strong><strong>047</strong>-277 J11KM6 SOLID <strong>100</strong>.0 69.1 g 04/12/06 9 R604093-10 7420-010<br />
<strong>RC</strong><strong>047</strong>-311 JllKT0 SOLID <strong>100</strong>.0 2.21 g 04/12/06 9 R604093-01 7420-001<br />
<strong>RC</strong><strong>047</strong>-322 J11KV1 SOLID <strong>100</strong>.0 71.2 g 04/12/06 7 R604093-11 7420-011<br />
<strong>RC</strong><strong>047</strong>-323 JllKV2 SOLID <strong>100</strong>.0 67.6 g 04/12/06 7 R604093-12 7420-012<br />
<strong>RC</strong><strong>047</strong>-328 JIIL21 SOLID <strong>100</strong>.0 64.7 g 04/12/06 9 R604093-13 7420-013<br />
<strong>RC</strong><strong>047</strong>-330 JIIL23 SOLID <strong>100</strong>.0 71.4 g 04/12/06 9 R604093-14 7420-014<br />
<strong>RC</strong><strong>047</strong>-332 J11 1,25 SOLID <strong>100</strong>.0 80.8 g 04/12/06 7 R604093-15 7420-015<br />
<strong>RC</strong><strong>047</strong>-343 J11 1,36 SOLID <strong>100</strong>.0 71.5 g 04/12/06 9 R604093-16 7420-016<br />
Method Blank<br />
Lab Control Sample<br />
Duplicate (R604093-06)<br />
SOLID<br />
SOLID<br />
SOLID <strong>100</strong>.0 88.7 g 04/12/06 9<br />
R604093-18<br />
R604093-17<br />
R604093-19<br />
7420-018<br />
7420-017<br />
7420-019<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
QC SUMMARY Version Ver 1.0<br />
Page 1 Form DVD-OS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 4 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Manion PREP BATC:H SUMMARY Contract No. 630<br />
Case no SDG X0303<br />
PREPARATION ERROR PLANCHETS ANALYZED QUALI-<br />
TEST MATRIX METHOD BATCH 20 % CLIENT MORE RE BLANK LCS DUP/ORIG MS/ORIG PIERS<br />
Alpha Spectroscopy<br />
PU SOLID Plutonium, Isotopic in Solids 7161-066 5.0 15 1 1 1/1<br />
TH SOLID Thorium, Isotopic in Solids 7181-066 5.0 15 1 1 1/1<br />
U SOLID Uranium, Isotopic in Solids 7181-066 5.0 15 1 1 1/1<br />
Beta Counting<br />
SR SOLID Total Strontium in Solids 7181-066 10.0 16 1 1 1/1<br />
Gamma Spectroscopy<br />
GAM SOLID Gamma Scan 7181-066 15.0 15 1 1 1/1<br />
Duplicates and Matrix Spikes are those with original (Client) sample in this Sample Delivery Group.<br />
Blank and LCS planchets are those in <strong>the</strong> same preparation batch as some Client, Duplicate or Spike sample<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
PREP BATCH SUMMARY Version Ver 1.0<br />
Page 1 Form DVD-PBS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 5 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion WORK SUMMARY Contract No. 630<br />
CLIENT SAMPLE ID LAB SAMPLE ID<br />
LOCATION MATRIX COLLECTED SUF-<br />
CUSTODY <strong>SAF</strong> NO RECEIVED PLANCHET TEST FIX ANALYZED REVIEWED BY METHOD<br />
Case no BIG K0303<br />
J11KK8 R604093-02 7420-002 GAM 04/19/06 04/25/06 MWT Gamma Scan<br />
600-132/600-190 OFFAL SOLID 04/05/06 7420-002 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-259 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-002 SR 05/09/06 05/16/06 MWT Total Strontium in Solids<br />
7420-002 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-002 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
JllKL5 R604093-03 7420-003 GAM 04/19/06 04/25/06 MWT Gamma Scan<br />
1607-H2 OFFAL SOLID 04/05/06 7420-003 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-266 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-003 SR - 05/09/06 05/16/06 MWT Total Strontium in Solids<br />
7420-003 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-003 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
J11KL6 R604093-04 7420-004 GAM 04/20/06 04/25/06 MWT Gamma Scan<br />
116-N-3 OFFAL SOLID 04/03/06 7420-004 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-267 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-004 SR 05/09/06 05/16/06 MWT Total Strontium in Solids<br />
7420-004 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-004 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
JIlKM0 R604093-05 7420-005 GAM 04/21/06 04/25/06 MWT Gamma Scan<br />
1607-D2:1 OFFAL SOLID 04/05/06 7420-005 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-271 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-005 SR 05/09/06 05/16/06 MWT Total Strontium in Solids<br />
7420-005 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-005 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
JllKM2 R604093-06 7420-006 GAM 04/19/06 04/25/06 MWT Gamma Scan<br />
BORROW PIT 24 OFFAL SOLID 04/03/06 7420-006 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-273 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-006 SR 05/09/06 05/16/06 MWT Total Strontium in Solids<br />
7420-006 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-006 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
J11K43 R604093-07 7420-007 GAM 04/21/06 04/25/06 MWT Gamma Scan<br />
YAKIMA RIDGE II OFFAL SOLID 04/03/06 7420-007 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-274 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-007 SR 05/09/06 05/16/06 MWT Total Strontium in Solids<br />
7420-007 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-007 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
WORK SUMMARY Version Ver 1.0<br />
Page 1 Form DVD-CWS<br />
SUM4AARY DATA SECTION Version 3.06<br />
Page 6 Report date 05/25/06
ESERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion WORK SUMMARY, C oI1t. Contract No. 630<br />
CLIENT SAMPLE ID LAB SAMPLE ID<br />
LOCATION MATRIX COLLECTED SUP-<br />
CUSTODY <strong>SAF</strong> No RECEIVED PLANCRET TEST FIX ANALYZED REVIEWED BY METHOD<br />
Case no SDG X0303<br />
JllKM4 R604093-08 7420-008 GAM 04/21/06 04/25/06 MWT Gamma Scan<br />
VERNITA UPRV S.SIDE OFFL SOLID 04/03/06 7420-008 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-275 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-008 SR 05/09/06 05/16/06 MWT Total Strontium in Solids<br />
7420-008 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-008 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
JllXM5 R604093-09 7420-009 GAM 04/21/06 04/25/06 MWT Gamma Scan<br />
McGEE RANCH OFFAL SOLID 04/03/06 7420-009 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-276 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-009 SR 05/10/06 05/16/06 MWT Total Strontium in Solids<br />
7420-009 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-009 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
J11KM6 R604093-10 7420-010 GAM 04/21/06 04/25/06 MWT Gamma Scan<br />
SADDLE MOUNTAIN OFFAL SOLID 04/03/06 7420-010 PU 05/22/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-277 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-010 SR 05/10/06 05/16/06 MWT Total Strontium in Solids<br />
7420-010 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-010 D 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
J11KTO R604093-01 7420-001 SR 05/09/06 05/16/06 MWT Total Strontium in Solids<br />
116-N-3 INVERTEBRATES SOLID 04/03/06<br />
<strong>RC</strong><strong>047</strong>-311 <strong>RC</strong>-<strong>047</strong> 04/12/06<br />
J11KV1 R604093-11 7420-011 GAM 04/21/06 04/25/06 MWT Gamma Scan<br />
<strong>100</strong>-D-48:2 OFFAL SOLID 04/05/06 7420-011 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-322 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-011 SR 05/10/06 05/16/06 MWT Total Strontium in Solids<br />
7420-011 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-011 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
J11XV2 8604093-12 7420-012 GAM 04/22/06 04/25/06 MWT Gamma Scan<br />
<strong>100</strong>-D-49:2 OFFAL SOLID 04/05/06 7420-012 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-323 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-012- SR 05/10/06 05/16/06 MWT Total Strontium in Solids<br />
7420-012 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-012 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
J111,21 R604093-13 7420-013 GAM 04/22/06 04/25/06 MWT Gamma Scan<br />
116DR1,DR-2/<strong>100</strong>-D-22 OFL SOLID 04/03/06 7420-013 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-328 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-013 SR 05/10/06 05/16/06 MWT Total Strontium in Solids<br />
7420-013 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-013 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
Lab id REPINE<br />
Protocol <strong>Hanford</strong><br />
WORK SUMMARY Version Ver 1.0<br />
Page 2 Form DVD-CWS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 7 Report date 05/25/06
SDG 7420<br />
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
Client <strong>Hanford</strong><br />
Contact Melissa C. Mamion WORK SUMMARY, cont. Contract No. 630<br />
CLIENT SAMPLE ID LAB SAMPLE ID<br />
LOCATION MATRIX COLLECTED SUF-<br />
CUSTODY <strong>SAF</strong> No RECEIVED PLANCHET TEST FIX ANALYZED REVIEWED BY METHOD<br />
Case no SDG X0303<br />
J111,23 R604093-14 7420-014 GAM 04/22/06 04/25/06 MWT Gamma Scan<br />
BORROW PIT 23 OFFAL SOLID 04/03/06 7420-014 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-330 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-014 SR 05/10/06 05/16/06 MWT Total Strontium in Solids<br />
7420-014 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-014 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
J11L25 R604093-15 7420-015 GAM 04/22/06 04/25/06 MWT Gart Scan<br />
600-131 OFFAL SOLID 04/05/06 7420-015 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-332 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-015 SR 05/10/06 05/16/06 MWT Total Strontium in Solids<br />
7420-015 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-015 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
JIIL36 R604093-16 7420-016 GAM 04/22/06 04/25/06 MWT Gamma Scan<br />
CENT.PLAT.SHRUR STEP.OFL SOLID 04/03/06 7420-016 PO 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong><strong>047</strong>-343 <strong>RC</strong>-<strong>047</strong> 04/12/06 7420-016 SR 05/10/06 05/16/06 MWT Total Strontium in Solids<br />
7420-016 TH 05/13/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-016 q 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
Method Blank R604093-18 7420-018 GAM 04/20/06 04/25/06 MWT Gamma Scan<br />
SOLID 7420-018 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong>-<strong>047</strong> 7420-018 SR 05/09/06 05/16/06 MWT Total Strontium in Solids<br />
7420-018 TH 05/16/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-018 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
Lab Control Sample R604093-17 7420-017 GAM 04/20/06 04/25/06 MWT Gamma Scan<br />
SOLID 7420-017 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
<strong>RC</strong>-<strong>047</strong> 7420-017 SR 05/10/06 05/16/06 MWT Total Strontium in Solids<br />
7420-017 TH 05/16/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-017 U 05/16/06 05/22/06 MWT Uranium, Isotopic in Solids<br />
Duplicate (R604093-06) R604093-19 7420-019 GAM 04/21/06 04/25/06 MWT Gamma Scan<br />
BORROW PIT 24 OFFAL SOLID 04/03/06 7420-019 PU 05/17/06 05/23/06 MWT Plutonium, Isotopic in Solids<br />
WORK SUMMARY<br />
Page 3<br />
<strong>RC</strong>-<strong>047</strong> 04/12/06 7420-019 SR 05/09/06 05/16/06 MWT Total Strontium in Solids<br />
7420-019 TH 05/16/06 05/22/06 MWT Thorium, Isotopic in Solids<br />
7420-019 q 05/17/06 05/22/06 MET Uranium, Isotopic in Solids<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
Version Ver 1.0<br />
Form DVD-CWS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 8<br />
Report date 05/25/06
SDG 7420<br />
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
Contact Melissa C. Mannion WORK SUMMARY, cont.<br />
TEST SAP No<br />
METHOD<br />
COUNTS OF<br />
TESTS BY<br />
REFERENCE<br />
Client <strong>Hanford</strong><br />
Contract No. 630<br />
Case no SOO X0303<br />
SAMPLE TYPE<br />
CLIENT MORE RE BLANX ICE CUP SPIKE TOTAL<br />
GAM <strong>RC</strong>-<strong>047</strong> Gamma Scan GAFAtA_GS 15 1 1 1 18<br />
PU <strong>RC</strong>-<strong>047</strong> Plutonium, Isotopic in Solids PUISO_PLATE_AEA 15 1 1 1 18<br />
SR <strong>RC</strong>-<strong>047</strong> Total Strontium in Solids SRTOT_SEP_PRECIP_GPC 16 1 1 1 19<br />
TH <strong>RC</strong>-<strong>047</strong> Thorium, Isotopic in Solids THISO_IE_PLATE_AEA 15 1 1 1 18<br />
U <strong>RC</strong>-<strong>047</strong> Uranium, Isotopic in Solids UISO_PLATE_AEA 15 1 1 1 18<br />
TOTALS 76 5 5 5 91<br />
WORK SUMMARY<br />
Page 4<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
Version Ver 1.0<br />
Form DVD-CWS<br />
S^Y DATA SECTION Version 3.06<br />
Page 9 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
R604093-18 Method Blank<br />
METHOD BLANK<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
Lab sample id R604093-18<br />
Dept sample id 7420-018<br />
ANALYTE CAS NO<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id Method Blank<br />
Material/Matrix SOLID<br />
<strong>SAF</strong> No <strong>RC</strong>-<strong>047</strong><br />
RESULT<br />
PCi/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
RDL<br />
pci/g<br />
QUALI-<br />
PIERS TEST<br />
Total Strontium SR-RAD 0.023 0.18 0.32 1.0 U SR<br />
Thorium 228 14274-82-9 -0.087 0.35 0.84 1.0 U TH<br />
Thorium 230 14269-63-7 0.261 0.35 0.67 1.0 U TH<br />
Thorium 232 TH-232 0 0.17 0.67 1.0 U TH<br />
Uranium 233/234 U-233/234 0 0.052 0.20 1.0 U U<br />
Uranium 235 15117-96-1 0 0.063 0.24 1.0 U U<br />
Uranium 238 U-238 0 0.052 0.20 1.0 U U<br />
Plutonium 238 13981-16-3 0 0.071 0.27 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0 0.071 0.27 1.0 U PU<br />
Potassium 40 13966-00-2 U 3.1 U GAM<br />
Cobalt 60 10198-40-0 U 0.14 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.20 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.23 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.50 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.26 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.33 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.26 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.13 U GAM<br />
Thorium 232 TH-232 U 0.50 U GAM<br />
Uranium 235 15117-96-1 U 0.37 U GAM<br />
Uranium 238 U-238 U 13 U GAM<br />
Americium 241 14596-10-2 U 0.33 U GAM<br />
Beryllium 7 13966-02-4 U 0.68 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.84 U GAM<br />
Antimony 125 14234-35-6 U 0.23 U GAM<br />
Cesium 134 13967-70-9 U 0.14 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
METHOD BLANKS Version Ver 1.0<br />
Page 1 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 10 Report date 05/25/06
EBERLINE SERVICES / RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
R604093-18 Method Blank<br />
BLANK, con t.<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
Lab sample id R604093-18<br />
Dept sample id 7420-018<br />
QC-BLANK #56758<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id Method Blank<br />
Material/Matrix SOLID<br />
<strong>SAF</strong> No <strong>RC</strong>-<strong>047</strong><br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
METHOD BLANKS Version Ver 1.0<br />
Page 2 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 11 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
R604093-17 Lab Control Sample<br />
LAB CONTROL SAMPLE<br />
SIG 7420 Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contact Melissa C. Mannion Contract No. 630<br />
Lab sample id R604093-17 Client sample id Lab Control Sample<br />
Dept sample id 7420-017 Material/Matrix SOLID<br />
ANAL YTE<br />
RESULT<br />
pCi/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
RDL<br />
pCi/g<br />
QUALI-<br />
FIRM TEST<br />
<strong>SAF</strong> No <strong>RC</strong>-<strong>047</strong><br />
ADDED<br />
pCi/g<br />
2s ERR<br />
pCi/g<br />
REC<br />
g<br />
30 IMPS<br />
(TOTAL)<br />
PROTOCOL<br />
Total Strontium 10.9 0.52 0.18 1.0 SR 10.8 0.43 101 B2-118 80-120<br />
Thorium 230 38.6 5.0 0.43 1.0 TH 44.4 1.8 87 81-119 80-120<br />
Uranium 233/234 19.8 2.0 0.88 1.0 U 19.3 0.77 103 82-118 80-120<br />
Uranium 235 16.6 1.8 0.19 1.0 U 15.7 0.63 106 80-120 80-120<br />
Uranium 238 20.0 2.0 0.85 1.0 U 21.0 0.84 95 83-117 80-120<br />
Plutonium 238 24.7 2.4 0.20 1.0 PU 26.2 1.0 94 B4-116 80-120<br />
Plutonium 239/240 26.9 2.5 0.20 1.0 PU 29.0 1.2 93 84-116 80-120<br />
Cobalt 60 4.47 0.34 0.16 0.050 GAM 4.47 0.18 <strong>100</strong> 74-126 80-120<br />
Cesium 137 4.84 0.31 0.25 0.10 GAM 4.61 0.18 105 74-126 80-120<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>ERA Sediment&Ti<br />
QC-LCS #56757<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
LAB CONTROL SAMPLES Version Ver 1.0<br />
Page 1 Form DVD-LCS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 12 Report date 05/25/06<br />
LIMITS
SDG 7420<br />
Contact Melissa C. Mannion<br />
DUPLICATE<br />
Lab sample id R604093-19<br />
Dept sample id 7420-019<br />
ANALYTE<br />
6 solids <strong>100</strong>.0<br />
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
R604093-19 J11KM2<br />
DUPLICATE<br />
DUPLICATE<br />
pCi/g<br />
20 ERR<br />
(COUNT)<br />
ORIGINAL<br />
Lab sample id R604093-06<br />
Dept sample id 7420-006<br />
MDA<br />
pCi/g<br />
Received 04/12/06<br />
t solids <strong>100</strong>.0<br />
ML<br />
pCi/g<br />
QUALI-<br />
PIERS TEST<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id S11KM2<br />
Location/Matrix BORROW PIT 24 OFFAL SOLID<br />
Collected/Weight 04/03/06 12:56 8B.7 q<br />
Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-273 <strong>RC</strong>-<strong>047</strong><br />
ORIGINAL<br />
Total Strontium 0.386 0.15 0.22 1.0 SR 0.505 0.16 0.22 27 77 1.0<br />
Thorium 228 -0.053 0.11 0.41 1.0 U TH 0 0.10 0.39 U - 0.7<br />
Thorium 230 -0.158 0.11 0.40 1.0 U TH 0.051 0.31 0.49 U - 1.3<br />
Thorium 232 0 0.11 0.40 1.0 U TH -0.051 0.10 0.39 U - 0.7<br />
Uranium 233/234 0 0.054 0.21 1.0 U U 0.032 0.065 0.25 U - 0.8<br />
Uranium 235 0 0.065 0.25 1.0 U U 0 0.078 0.30 U - 0<br />
Uranium 238 0.054 0.054 0.21 1.0 U U 0 0.065 0.25 U - 1.3<br />
Plutonium 238 0 0.075 0.29 1.0 U PU 0 0.045 0.17 U - 0<br />
Plutonium 239/240 0 0.075 0.29 1.0 U PU 0 0.045 0.17 U - 0<br />
Potassium 40 2.65 0.99 0.60 GAM 3.28 1.0 0.55 21 78 0.8<br />
Cobalt 60 U 0.063 0.050 U GAM U 0.068 U - 0.1<br />
Cesium 137 U 0.064 0.10 U GAM U 0.066 U - 0<br />
Radium 226 U 0.11 0.10 U GAM U 0.12 U - 0.1<br />
Radium 228 U 0.25 0.20 U GAM U 0.30 U - 0.3<br />
Europium 152 U 0.15 0.10 U GAM U 0.15 U - 0<br />
Europium 154 U 0.21 0.10 U GAM U 0.21 U - 0<br />
Europium 155 U 0.14 0.10 U GAM U 0.15 U - 0.1<br />
Thorium 228 U 0.090 U GAM U 0.095 U - 0.1<br />
Thorium 232 U 0.25 U GAM U 0.30 U - 0.3<br />
Uranium 235 U 0.24 U GAM U 0.26 U - 0.1<br />
Uranium 238 U 8.2 U GAM U 9.7 U - 012<br />
Americium 241 U 0.25 U GAM U 0.28 U - 0.2<br />
Beryllium 7 U 0.53 U GAM U 0.58 U - 0.1<br />
Ru<strong>the</strong>nium 106 U 0.55 U GAM U 0.59 U - 0.1<br />
Antimony 125 U 0.15 U GAM U 0.16 U - 0.1<br />
Cesium 134 U 0.072 U GAM U 0.079 U - 0.1<br />
<strong>100</strong>6<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&T1<br />
pCi/g<br />
20 ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
QUALI-<br />
PIERS<br />
RPD<br />
t<br />
30<br />
TOT<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DUPLICATES Version Ver 1.0<br />
Page 1 Form DVD-DUP<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 13 Report date 05/25/06<br />
DER<br />
a
R604093-19<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
DUPLICATE<br />
Lab sample id R604093-19<br />
Dept sample id 7420-019<br />
4 solids <strong>100</strong>.0<br />
QC-OUP#6 56759<br />
DUPLICATES<br />
Page 2<br />
SUMMARY DATA SECTION<br />
Page 14<br />
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
DUPLICATE, cont.<br />
ORIGINAL<br />
Lab sample id R604093-06<br />
Dept sample id 7420-006<br />
Received 04/12/06<br />
t solids <strong>100</strong>.0<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id J11KM2<br />
Jll1<br />
Location/Matrix BORROW PIT 24 OFFAL SOLID<br />
Collected/Weight 04/03/06 12:56 88.7 a<br />
Custody/<strong>SAF</strong> NO <strong>RC</strong><strong>047</strong>-273 <strong>RC</strong>-<strong>047</strong><br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
Version Ver 1.0<br />
Form DVD-DUP<br />
Version 3.06<br />
Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
R604093-02 J11XK8<br />
DATA SHEET<br />
SDG 7420 Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contact Melissa C. Mannion Contract No. 630<br />
Lab sample id R604093-02 Client sample id JllKK8<br />
Dept sample id 7420-002 Location/Matrix 600-132/600-190 OFFAL SOLID<br />
Received 04/12/06 Collected/Weight 04/05/06 09:19 77.8 a<br />
% solids <strong>100</strong>.0 Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-259 <strong>RC</strong>-<strong>047</strong><br />
ANALYTE CAS NO<br />
RESULT<br />
pCi/g<br />
20 ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
ROL<br />
pCi/g<br />
QUALI-<br />
PIERS TEST<br />
Total Strontium SR-RAD 0.017 0.13 0.26 1.0 U SR<br />
Thorium 228 14274-82-9 0.069 0.14 0.53 1.0 U TH<br />
Thorium 230 14269-63-7 0.137 0.41 0.66 1.0 U TH<br />
Thorium 232 TH-232 0.069 0.14 0.53 1.0 U TH<br />
Uranium 233/234 U-233/234 0.423 0.20 0.19 1.0 U<br />
Uranium 235 15117-96-1 0 0.060 0.23 1.0 U U<br />
Uranium 238 U-238 0.597 0.25 0.19 1.0 U<br />
Plutonium 238 13981-16-3 0.031 0.13 0.24 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0.157 0.13 0.24 1.0 U PU<br />
Potassium 40 13966-00-2 U 3.5 U GAM<br />
Cobalt 60 10198-40-0 U 0.13 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.10 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.25 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.53 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.24 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.32 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.29 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.15 U GAM<br />
Thorium 232 TH-232 U 0.53 U GAM<br />
Uranium 235 15117-96-1 U 0.41 U GAM<br />
Uranium 238 U-238 U 13 U GAM<br />
Americium 241 14596-10-2 U 0.34 U GAM<br />
Beryllium 7 13966-02-4 U 0.81 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.84 U GAM<br />
Antimony 125 14234-35-6 U 0.22 U GAM<br />
Cesium 134 13967-70-9 U 0.12 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 1 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 15 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
R604093-03 J11KL5<br />
DATA SHEET<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
Lab sample id R604093-03<br />
Dept sample id 7420-003<br />
Received 04/12/06<br />
W solids <strong>100</strong>.0<br />
ANALYTH CAS NO<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id J11KL5<br />
Location/Matrix 1607-H2 OFFAL SOLID<br />
Collected/Weight 04/05/06 08:12 69.6 a<br />
Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-266 <strong>RC</strong>-<strong>047</strong><br />
RESULT<br />
pci/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
RDL<br />
pCi/g<br />
QUALI-<br />
PIERS TEST<br />
Total Strontium SR-RAD 0.035 0.14 0.27 1.0 U SR<br />
Thorium 228 14274-82-9 0 0.087 0.33 1.0 U TH<br />
Thorium 230 14269-63-7 0.044 0.26 0.42 1.0 U TH<br />
Thorium 232 TH-232 0 0.087 0.33 1.0 U TH<br />
Uranium 233/234 U-233/234 0.020 0.040 0.15 1.0 U U<br />
Uranium 235 15117-96-1 0 0.049 0.19 1.0 U U<br />
Uranium 238 U-238 0 0.040 0.15 1.0 U U<br />
Plutonium 238 13981-16-3 -0.053 0.053 0.25 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0 0.053 0.20 1.0 U PU<br />
Potassium 40 13966-00-2 U 3.0 U GAM<br />
Cobalt 60 10198-40-0 U 0.14 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.17 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.22 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.48 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.25 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.33 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.24 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.13 U GAM<br />
Thorium 232 TH-232 U 0.48 U GAM<br />
Uranium 235 15117-96-1 U 0.35 U GAM<br />
Uranium 238 U-238 U 12 U GAM<br />
Americium 241 14596-10-2 U 0.31 U GAM<br />
Beryllium 7 13966-02-4 U 0.77 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.78 U GAM<br />
Antimony 125 14234-35-6 U 0.21 U GAM<br />
Cesium 134 13967-70-9 U 0.14 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 2 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 16 Report date 05/25/06
EBERLINE SER V ICES / RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
R604093-04 J11KL6<br />
DATA SHEET<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
Lab sample id R604093-04<br />
Dept sample id 7420-004<br />
Received 04/12/06<br />
* solids <strong>100</strong>.0<br />
ANALYTE CAS NO<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id J11KL6<br />
Location/Matrix 116-N-3 OFFAL SOLID<br />
Collected/Weight 04/03/06 14:20 74.5 q<br />
Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-267 <strong>RC</strong>-<strong>047</strong><br />
RESULT<br />
PCi/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
RDL<br />
pCi/g<br />
QUALI-<br />
FIERS TEST<br />
Total Strontium SR-RAD 0.023 0.13 0.27 1.0 U SR<br />
Thorium 228 14274-82-9 0.162 0.33 0.62 1.0 U TH<br />
Thorium 230 14269-63-7 0.243 0.33 0.62 1.0 U TH<br />
Thorium 232 TH-232 0 0.16 0.62 1.0 U TH<br />
Uranium 233/234 U-233/234 0.024 0.048 0.18 1.0 U U<br />
Uranium 235 15117-96-1 0 0.058 0.22 1.0 U U<br />
Uranium 238 U-238 0.024 0.048 0.18 1.0 U U<br />
Plutonium 238 13981-16-3 0 0.052 0.20 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0 0.052 0.20 1.0 U PU<br />
Potassium 40 13966-00-2 U 3.4 U GAM<br />
Cobalt 60 10198-40-0 U 0.11 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.11 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.24 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.52 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.24 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.32 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.28 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.15 U GAM<br />
Thorium 232 TH-232 U 0.52 U GAM<br />
Uranium 235 15117-96-1 U 0.41 U GAM<br />
Uranium 238 U-238 U 13 U GAM<br />
Americium 241 14596-10-2 U 0.34 U GAM<br />
Beryllium 7 13966-02-4 U 0.80 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.85 U GAM<br />
Antimony 125 14234-35-6 U 0.22 U GAM<br />
Cesium 134 13967-70-9 U 0.12 U GAM<br />
<strong>100</strong>&30O<strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 3 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 17 Report date 05/25/06
EBER L INE SER V ICES / RICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
R604093-05 J11XM0<br />
DATA SHEET<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
Lab sample id R604093-05<br />
Dept sample id 7420-005<br />
Received 04/12/06<br />
* solids <strong>100</strong>.0<br />
ANALYTE CAS NO<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id JllKM0<br />
Location/Matrix 1607-D2:1 OFFAL SOLID<br />
Collected/Weight 04/05/06 07:52 86.8 a<br />
Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-271 <strong>RC</strong>-<strong>047</strong><br />
RESULT<br />
pCi/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
RDL<br />
pCi/g<br />
QUALI-<br />
PIERS TEST<br />
Total Strontium SR-RAD 0.073 0.13 0.26 1.0 U SR<br />
Thorium 228 14274-82-9 0 0.15 0.56 1.0 U TH<br />
Thorium 230 14269-63-7 0.147 0.30 0.56 1.0 U TH<br />
Thorium 232 TH-232 0 0.15 0.56 1.0 U TH<br />
Uranium 233/234 U-233/234 0 0.070 0.27 1.0 U U<br />
Uranium 235 15117-96-1 0 0.084 0.32 1.0 U U<br />
Uranium 238 U-238 0 0.070 0.27 1.0 U U<br />
Plutonium 238 13981-16-3 0 0.11 0.26 1.0 U PU<br />
Plutonium 239/240 PU-239/240 -0.027 0.055 0.21 1.0 U PU<br />
Potassium 40 13966-00-2 U 9.6 U GAM<br />
Cobalt 60 10198-40-0 U 0.10 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.092 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.21 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.46 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.20 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.31 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.25 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.13 U GAM<br />
Thorium 232 TH-232 U 0.46 U GAM<br />
Uranium 235 15117-96-1 U 0.36 U GAM<br />
Uranium 238 U-238 U 11 U GAM<br />
Americium 241 14596-10-2 U 0.30 U GAM<br />
Beryllium 7 13966-02-4 U 0.70 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.70 U GAM<br />
Antimony 125 14234-35-6 U 0.19 U GAM<br />
Cesium 134 13967-70-9 U 0.11 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 4 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 18 Report date 05/25/06
EBERLI N E SE RVIC ES /RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
R604093-06 J11KM2<br />
DATA SHEET<br />
SDG 7420 Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contact Melissa C. Mannion Contract No. 630<br />
Lab sample id R604093-06 Client sample id J11KM2<br />
Dept sample id 7420-006 Location/Matrix BORROW PIT 24 OFFAL SOLID<br />
Received 04/12/06 Collected/Weight 04/03/06 12:56 88.7 ca<br />
V solids <strong>100</strong>.0 Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-273 <strong>RC</strong>-<strong>047</strong><br />
ANALYTE CAS NO<br />
RESULT<br />
pCi/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
RDL<br />
pCi/g<br />
QUALI-<br />
FIERS TEST<br />
Total Strontium SR-RAD 0.505 0.16 0.22 1.0 SR<br />
Thorium 228 14274-82-9 0 0.10 0.39 1.0 U TH<br />
Thorium 230 14269-63-7 0.051 0.31 0.49 1.0 U TH<br />
Thorium 232 TH-232 -0.051 0.10 0.39 1.0 U TH<br />
Uranium 233/234 U-233/234 0.032 0.065 0.25 1.0 U U<br />
Uranium 235 15117-96-1 0 0.078 0.30 1.0 U U<br />
Uranium 238 U-238 0 0.065 0.25 1.0 U U<br />
Plutonium 238 13981-16-3 0 0.045 0.17 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0 0.045 0.17 1.0 U PU<br />
Potassium 40 13966-00-2 3.28 1.0 0.55 GAM<br />
Cobalt 60 10198-40-0 U 0.068 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.066 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.12 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.30 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.15 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.21 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.15 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.095 U GAM<br />
Thorium 232 TH-232 U 0.30 U GAM<br />
Uranium 235 15117-96-1 U 0.26 U GAM<br />
Uranium 238 U-238 U 9.7 U GAM<br />
Americium 241 14596-10-2 U 0.28 U GAM<br />
Beryllium 7 13966-02-4 U 0.58 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.59 U GAM<br />
Antimony 125 14234-35-6 U 0.16 U GAM<br />
Cesium 134 13967-70-9 U 0.079 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 5 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 19 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
R604093-07 JlIKM3<br />
DATA SHEET<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
Lab sample id R604093-07<br />
Dept sample id 7420-007<br />
Received 04/12/06<br />
t solids <strong>100</strong>.0<br />
ANALYTE CAS NO<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id J11KM3<br />
Location/Matrix YAKIMA RIDGE II OFFAL SOLID<br />
Collected/Weight 04/03/06 12:30 81.0 a<br />
Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-274 <strong>RC</strong>-<strong>047</strong><br />
RESULT<br />
pCi/g<br />
20 ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
ROL<br />
pCi/g<br />
QUALI-<br />
FIERS TEST<br />
Total Strontium SR-RAD 0.024 0.13 0.25 1.0 U SR<br />
Thorium 228 14274-82-9 0 0.12 0.46 1.0 U TH<br />
Thorium 230 14269-63-7 0.178 0.36 0.45 1.0 U TH<br />
Thorium 232 TH-232 0 0.12 0.45 1.0 U TH<br />
Uranium 233/234 U-233/234 0 0.056 0.22 1.0 U U<br />
Uranium 235 15117-96-1 0 0.068 0.26 1.0 U U<br />
Uranium 238 U-238 0 0.056 0.22 1.0 U U<br />
Plutonium 238 13981-16-3 0.036 0.036 0.14 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0 0.036 0.14 1.0 U PU<br />
Potassium 40 13966-00-2 U 2.5 U GAM<br />
Cobalt 60 10198-40-0 U 0.11 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.086 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.18 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.39 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.20 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.27 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.20 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.11 U GAM<br />
Thorium 232 TH-232 U 0.39 U GAM<br />
Uranium 235 15117-96-1 U 0.29 U GAM<br />
Uranium 238 U-238 U 9.9 U GAM<br />
Americium 241 14596-10-2 U 0.25 U GAM<br />
Beryllium 7 13966-02-4 U 0.67 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.67 U GAM<br />
Antimony 125 14234-35-6 U 0.17 U GAM<br />
Cesium 134 13967-70-9 U 0.096 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 6 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 20 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
R604093-08 J11XM4<br />
DATA SHEET<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
Lab sample id R604093-08<br />
Dept sample id 7420-008<br />
Received 04/12/06<br />
% solids <strong>100</strong>.0<br />
ANALYTE CAS NO<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id J11KM4<br />
Location/Matrix VERNITA UPRV S.SIDE OFFL SOLID<br />
Collected/Weight 04/03/06 10:43 91.5 a<br />
Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-275 <strong>RC</strong>-<strong>047</strong><br />
RESULT<br />
pCi/g<br />
20 ERR<br />
(COUNT)<br />
MDA<br />
pci/g<br />
RDL<br />
pci/g<br />
QUALI-<br />
PIERS TEST<br />
Total Strontium SR-RAD 0.139 0.15 0.27 1.0 U SR<br />
Thorium 228 14274-82-9 -0.112 0.11 0.54 1.0 U TH<br />
Thorium 230 14269-63-7 0.112 0.22 0.43 1.0 U TH<br />
Thorium 232 TH-232 0 0.11 0.43 1.0 U TH<br />
Uranium 233/234 U-233/234 0 0.048 0.18 1.0 U U<br />
Uranium 235 15117-96-1 0 0.056 0.22 1.0 U U<br />
Uranium 238 U-238 0.024 0.048 0.18 1.0 U U<br />
Plutonium 238 13981-16-3 0.032 0.13 0.25 1.0 U PU<br />
Plutonium 239/240 PU-239/240 -0.032 0.065 0.25 1.0 U PU<br />
Potassium 40 13966-00-2 2.74 0.77 0.46 GAM<br />
Cobalt 60 10198-40-0 U 0.060 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.054 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.11 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.25 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.12 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.15 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.12 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.071 U GAM<br />
Thorium 232 TH-232 U 0.25 U GAM<br />
Uranium 235 15117-96-1 U 0.17 U GAM<br />
Uranium 238 U-238 U 5.7 U GAM<br />
Americium 241 14596-10-2 U 0.12 U GAM<br />
Beryllium 7 13966-02-4 U 0.45 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.41 U GAM<br />
Antimony 125 14234-35-6 U 0.12 U GAM<br />
Cesium 134 13967-70-9 U 0.061 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 7 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 21 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
R604093-09 J11KM5<br />
DATA SHEET<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
Lab sample id R604093-09<br />
Dept sample id 7420-009<br />
Received 04/12/06<br />
% solids <strong>100</strong>.0<br />
ANALYTE CAS NO<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id J11KM5<br />
Location/Matrix McGEE RANCH OFFAL SOLID<br />
Collected/Weight 04/03/06 09:45 65.9 g<br />
Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-276 <strong>RC</strong>-<strong>047</strong><br />
RESULT<br />
PCi/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
RDL<br />
pCi/g<br />
QUALI-<br />
FIERS TEST<br />
Total Strontium SR-RAD 0.035 0.13 0.26 1.0 U SR<br />
Thorium 228 14274-82-9 0.064 0.26 0.49 1.0 U TH<br />
Thorium 230 14269-63-7 0.064 0.26 0.49 1.0 U TH<br />
Thorium 232 TH-232 0 0.13 0.49 1.0 U TH<br />
Uranium 233/234 U-233/234 0.024 0.048 0.18 1.0 U U<br />
Uranium 235 15117-96-1 0 0.058 0.22 1.0 U U<br />
Uranium 238 U-238 0 0.048 0.18 1.0 U U<br />
Plutonium 238 13981-16-3 -0.036 0.14 0.35 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0 0.072 0.28 1.0 U PU<br />
Potassium 40 13966-00-2 2.37 1.1 0.66 GAM<br />
Cobalt 60 10198-40-0 U 0.061 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.059 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.11 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.26 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.14 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.19 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.14 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.084 U GAM<br />
Thorium 232 TH-232 U 0.26 U GAM<br />
Uranium 235 15117-96-1 U 0.23 U GAM<br />
Uranium 238 U-238 U 6.8 U GAM<br />
Americium 241 14596-10-2 U 0.25 U GAM<br />
Beryllium 7 13966-02-4 U 0.49 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.55 U GAM<br />
Antimony 125 14234-35-6 U 0.13 U GAM<br />
Cesium 134 13967-70-9 U 0.071 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 8 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 22 Report date 05/25/06
EBERLINE SER V ICES / RICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
R604093-10 J11XM6<br />
DATA SHEET<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
Lab sample id R604093-10<br />
Dept sample id 7420-010<br />
Received 04/12/06<br />
W solids <strong>100</strong>.0<br />
ANALYTE CAS NO<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id J11KM6<br />
Location/Matrix SADDLE MOUNTAIN OFFAL SOLID<br />
Collected/Weight 04/03/06 09:00 69.1 q<br />
Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-277 <strong>RC</strong>-<strong>047</strong><br />
RESULT<br />
pCi/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
RDL<br />
pci/g<br />
QUALI-<br />
FIERS TEST<br />
Total Strontium SR-RAD -0.082 0.12 0.27 1.0 U SR<br />
Thorium 228 14274-82-9 0 0.14 0.53 1.0 U TH<br />
Thorium 230 14269-63-7 0.139 0.28 0.53 1.0 U TH<br />
Thorium 232 TH-232 0 0.14 0.53 1.0 U TH<br />
Uranium 233/234 U-233/234 0 0.053 0.20 1.0 U U<br />
Uranium 235 15117-96-1 0 0.065 0.25 1.0 U U<br />
Uranium 238 U-238 0 0.053 0.20 1.0 U U<br />
Plutonium 238 13981-16-3 0.051 0.10 0.39 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0 0.10 0.39 1.0 U PU<br />
Potassium 40 13966-00-2 U 2.5 U GAM<br />
Cobalt 60 10198-40-0 U 0.12 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.074 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.18 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.39 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.17 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.25 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.21 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.11 U GAM<br />
Thorium 232 TH-232 U 0.39 U GAM<br />
Uranium 235 15117-96-1 U 0.30 U GAM<br />
Uranium 238 U-238 U 9.2 U GAM<br />
Americium 241 14596-10-2 U 0.25 U GAM<br />
Beryllium 7 13966-02-4 U 0.62 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.61 U GAM<br />
Antimony 125 14234-35-6 U 0.16 U GAM<br />
Cesium 134 13967-70-9 U 0.20 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 9 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 23 Report date 05/25/06
EBER L INE S E R V I C E S / R I C H M O N D<br />
SAMPLE DELIVERY GROUP X0303<br />
R604093-01 J11KTO<br />
DATA SHEET<br />
SDG 7420 Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contact Melissa C. Mannion Contract No. 630<br />
Lab sample id R604093-01 Client sample id J11KTO<br />
Dept sample id 7420-001 Location/Matrix 116-N-3 INVERTEBRATES SOLID<br />
Received 04/12/06 Collected/Weight 04/03/06 06:57 2.21 a<br />
solids <strong>100</strong>.0 Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-311 <strong>RC</strong>-<strong>047</strong><br />
RESULT 20 ERR MDA RDL QUALI-<br />
ANALYTE CAS NO pCi/g (COUNT) pCi/g pci/g FIERS TEST<br />
Total Strontium SR-RAD -0.034 0.28 0.59 1.0 U SR<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 10 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 24 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
R604093-11 J11XV1<br />
DATA SHEET<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
Lab sample id R604093-11<br />
Dept sample id 7420-011<br />
Received 04/12/06<br />
W solids <strong>100</strong>.0<br />
ANALYTE CAS NO<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id J11KV1<br />
Location/Matrix <strong>100</strong>-D-48:2 OFFAL SOLID<br />
Collected/Weight 04/05/06 06:55 71.2 q<br />
Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-322 <strong>RC</strong>-<strong>047</strong><br />
RESULT<br />
pCi/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
RDL<br />
pCi/g<br />
QUALI-<br />
PIERS TEST<br />
Total Strontium SR-RAD 0.112 0.12 0.22 1.0 U SR<br />
Thorium 228 14274-82-9 0.110 0.33 0.68 1.0 U TH<br />
Thorium 230 14269-63-7 0.165 0.33 0.42 1.0 U TH<br />
Thorium 232 TH-232 0 0.11 0.42 1.0 U TH<br />
Uranium 233/234 U-233/234 0.040 0.080 0.30 1.0 U U<br />
Uranium 235 15117-96-1 0 0.096 0.37 1.0 U U<br />
Uranium 238 U-238 0 0.080 0.30 1.0 U U<br />
Plutonium 238 13981-16-3 -0.084 0.17 0.46 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0.042 0.084 0.32 1.0 U PU<br />
Potassium 40 13966-00-2 U 2.0 U GAM<br />
Cobalt 60 10198-40-0 U 0.087 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.068 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.14 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.32 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.16 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.21 0.10 U GAM<br />
Europium 155 ,14391-16-3 U 0.16 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.088 U GAM<br />
Thorium 232 TH-232 U 0.32 U GAM<br />
Uranium 235 15117-96-1 U 0.23 U GAM<br />
Uranium 238 U-238 U 8.4 U GAM<br />
Americium 241 14596-10-2 U 0.20 U GAM<br />
Beryllium 7 13966-02-4 U 0.52 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.54 U GAM<br />
Antimony 125 14234-35-6 U 0.14 U GAM<br />
Cesium 134 13967-70-9 U 0.087 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 11 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 25 Report date 05/25/06
EBE RL INE SERVICES /R ICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
R604093-12 J11KV2<br />
DATA SHEET<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
Lab sample id R604093-12<br />
Dept sample id 7420-012<br />
Received 04/12/06<br />
% solids <strong>100</strong>.0<br />
ANALYTE CAS NO<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id 711KV2<br />
Location/Matrix <strong>100</strong>-D-49:2 OFFAL SOLID<br />
Collected/Weight 04/05/06 07:20 67.6 a<br />
Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-323 <strong>RC</strong>-<strong>047</strong><br />
RESULT<br />
pCi/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
RDL<br />
pci/g<br />
QUALI-<br />
FIERS TEST<br />
Total Strontium SR-RAD -0.002 0.12 0.24 1.0 U SR<br />
Thorium 228 14274-82-9 0.282 0.38 0.63 1.0 U TH<br />
Thorium 230 14269-63-7 0.141 0.28 0.36, 1.0 U TH<br />
Thorium 232 TH-232 0 0.094 0.36 1.0 U TH<br />
Uranium 233/234 U-233/234 0 0.080 0.31 1.0 U U<br />
Uranium 235 15117-96-1 0.048 0.097 0.37 1.0 U U<br />
Uranium 238 U-238 0 0.080 0.31 1.0 U U<br />
Plutonium 238 13961-16-3 0.034 0.14 0.33 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0 0.069 0.26 1.0 U PU<br />
Potassium 40 13966-00-2 U 3.0 U GAM<br />
Cobalt 60 10198-40-0 U 0.21 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.12 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.22 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.50 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.26 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.32 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.26 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.14 U GAM<br />
Thorium 232 TH-232 U 0.50 U GAM<br />
Uranium 235 15117-96-1 U 0.35 U GAM<br />
Uranium 238 U-238 U 13 U GAM<br />
Americium 241 14596-10-2 U 0.32 U GAM<br />
Beryllium 7 13966-02-4 U 0.91 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.86 U GAM<br />
Antimony 125 14234-35-6 U 0.23 U GAM<br />
Cesium 134 13967-70-9 U 0.14 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 12 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 26 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
R604093-13 JIIL21<br />
DATA SHEET<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
Lab sample id R604093-13<br />
Dept sample id 7420-013<br />
Received 04/12/06<br />
W solids <strong>100</strong>.0<br />
ANALYTE CAS NO<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id J11L21<br />
Location/Matrix 116DR1,DR-2/<strong>100</strong>-D-22 OFL SOLID<br />
Collected/Weight 04/03/06 13:56 64.7 a<br />
Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-328 <strong>RC</strong>-<strong>047</strong><br />
RESULT<br />
pCi/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
RDL<br />
pCi/g<br />
QUALI-<br />
FIERS TEST<br />
Total Strontium SR-RAD 0.070 0.12 0.22 1.0 U SR<br />
Thorium 228 14274-82-9 0.060 0.24 0.46 1.0 U TH<br />
Thorium 230 14269-63-7 0.180 0.36 0.46 1.0 U TH<br />
Thorium 232 TH-232 0 0.12 0.46 1.0 U TH<br />
Uranium 233/234 U-233/234 0 0.055 0.21 1.0 U U<br />
Uranium 235 15117-96-1 0 0.066 0.25 1.0 U U<br />
Uranium 238 U-238 0 0.055 0.21 1.0 U U<br />
Plutonium 238 13981-16-3 0 0.12 0.29 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0 0.061 0.23 1.0 U PU<br />
Potassium 40 13966-00-2 3.02 1.4 1.0 GAM<br />
Cobalt 60 10198-40-0 U 0.099 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.097 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.20 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.52 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.23 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.34 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.23 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.20 U GAM<br />
Thorium 232 TH-232 U 0.52 U GAM<br />
Uranium 235 15117-96-1 U 0.36 U GAM<br />
Uranium 238 U-238 U 13 U GAM<br />
Americium 241 14596-10-2 U 0.25 U GAM<br />
Beryllium 7 13966-02-4 U 0.91 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.87 U GAM<br />
Antimony 125 14234-35-6 U 0.25 U GAM<br />
Cesium 134 13967-70-9 U 0.12 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 13 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 27 Report date 05/25/06
EBERLINE SERVICES/RICHMON D<br />
SAMPLE DELIVERY GROUP X0303<br />
R604093-14 J11L23<br />
D ATA SHEET<br />
SDG 7420 Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contact Melissa C. Mannion Contract No. 630<br />
Lab sample id R604093-14 Client sample id J11L23<br />
Dept sample id 7420-014 Location/Matrix BORROW PIT 23 OFFAL SOLID<br />
Received 04/12/06 Collected/Weight 04/03/06 13:20 71.4 a<br />
t solids <strong>100</strong>.0 Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-330 <strong>RC</strong>-<strong>047</strong><br />
ANALYTE CAS NO<br />
RESULT<br />
pCi/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pci/g<br />
RDL<br />
pCi/g<br />
QUALI-<br />
FIERS TEST<br />
Total Strontium SR-RAD 0.406 0.15 0.21 1.0 SR<br />
Thorium 228 14274-82-9 -0.038 0.15 0.42 1.0 U TH<br />
Thorium 230 14269-63-7 0 0.15 0.29 1.0 U TH<br />
Thorium 232 TH-232 -0.037 0.075 0.29 1.0 U TH<br />
Uranium 233/234 U-233/234 0.054 0.11 0.21 1.0 U U<br />
Uranium 235 15117-96-1 0 0.065 0.25 1.0 U U<br />
Uranium 238 U-238 0.081 0.11 0.21 1.0 U U<br />
Plutonium 238 13981-16-3 0.043 0.086 0.33 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0.043 0.086 0.33 1.0 U PU<br />
Potassium 40 13966-00-2 U 1.9 U GAM<br />
Cobalt 60 10198-40-0 U 0.062 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.077 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.13 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.34 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.19 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.24 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.18 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.11 U GAM<br />
Thorium 232 TH-232 U 0.34 U GAM<br />
Uranium 235 15117-96-1 U 0.30 U GAM<br />
Uranium 238 U-238 U 10 U GAM<br />
Americium 241 14596-10-2 U 0.28 U GAM<br />
Beryllium 7 13966-02-4 U 0.67 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.67 U GAM<br />
Antimony 125 14234-35-6 U 0.17 U GAM<br />
Cesium 134 13967-70-9 U 0.088 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 14 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 28 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
R604093-15 JllL25<br />
DATA SHEET<br />
SDG 7420 Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contact Melissa C. Mannion Contract No. 630<br />
Lab sample id R604093-15 Client sample id JllL25<br />
Dept sample id 7420-015 Location/Matrix 600-131 OFFAL SOLID<br />
Received 04/12/06 Collected/Weight 04/05/06 08:48 80.8 a<br />
% solids <strong>100</strong>.0 Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-332 <strong>RC</strong>-<strong>047</strong><br />
ANALYTE CAS NO<br />
RESULT<br />
pCi/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
RDL<br />
pCi/g<br />
QUALI-<br />
FIERS TEST<br />
Total Strontium SR-RAD -0.018 0.11 0.22 1.0 U SR<br />
Thorium 228 14274-82-9 -0.066 0.13 0.51 1.0 U TH<br />
Thorium 230 14269-63-7 -0.132 0.13 0.51 1.0 U TH<br />
Thorium 232 TH-232 0 0.13 0.51 1.0 U TH<br />
Uranium 233/234 U-233/234 0 0.071 0.27 1.0 U U<br />
Uranium 235 15117-96-1 0 0.086 0.33 1.0 U U<br />
Uranium 238 U-238 0.035 0.071 0.27 1.0 U U<br />
Plutonium 238 13981-16-3 -0.038 0.076 0.29 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0 0.076 0.29 1.0 U PU<br />
Potassium 40 13966-00-2 2.64 0.64 0.32 GAM<br />
Cobalt 60 10198-40-0 U 0.034 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.034 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.060 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.15 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.080 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.095 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.076 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.046 U GAM<br />
Thorium 232 TH-232 U 0.15 U GAM<br />
Uranium 235 15117-96-1 U 0.11 U GAM<br />
Uranium 238 U-238 U 3.9 U GAM<br />
Americium 241 14596-10-2 U 0.080 U GAM<br />
Beryllium 7 13966-02-4 U 0.29 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.26 U GAM<br />
Antimony 125 14234-35-6 U 0.079 U GAM<br />
Cesium 134 13967-70-9 U 0.039 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 15 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 29 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
R604093-16 JllL36<br />
DATA SHEET<br />
SDG 7420<br />
Contact Melissa C. Mannion<br />
Lab sample id R604093-16<br />
Dept sample id 7420-016<br />
Received 04/12/06<br />
% solids <strong>100</strong>.0<br />
ANALYTR CAS NO<br />
Client/Case no <strong>Hanford</strong> SDG K0303<br />
Contract No. 630<br />
Client sample id J11L36<br />
Location/Matrix CENT.PLAT.SHRUB STEP.OFL SOLID<br />
Collected/Weight 04/03/06 10:15 71.5 4<br />
Custody/<strong>SAF</strong> No <strong>RC</strong><strong>047</strong>-343 <strong>RC</strong>-<strong>047</strong><br />
RESULT<br />
pCi/g<br />
2a ERR<br />
(COUNT)<br />
MDA<br />
pCi/g<br />
RDL<br />
pCi/g<br />
QUALI-<br />
FIERS TEST<br />
Total Strontium SR-RAD -0.045 0.098 0.21 1.0 U SR<br />
Thorium 228 14274-82-9 0.<strong>100</strong> 0.20 0.48 1.0 U TH<br />
Thorium 230 14269-63-7 0.250 0.30 0.38 1.0 U TH<br />
Thorium 232 TH-232 0 0.10 0.38 1.0 U TH<br />
Uranium 233/234 U-233/234 0 0.054 0.21 1.0 U U<br />
Uranium 235 15117-96-1 0 0.065 0.25 1.0 U U<br />
Uranium 238 U-238 -0.027 0.054 0.21 1.0 U U<br />
Plutonium 238 13981-16-3 0 0.085 0.33 1.0 U PU<br />
Plutonium 239/240 PU-239/240 0.042 0.085 0.33 1.0 U PU<br />
Potassium 40 13966-00-2 2.95 0.78 0.34 GAM<br />
Cobalt 60 10198-40-0 U 0.032 0.050 U GAM<br />
Cesium 137 <strong>100</strong>45-97-3 U 0.031 0.10 U GAM<br />
Radium 226 13982-63-3 U 0.055 0.10 U GAM<br />
Radium 228 15262-20-1 U 0.13 0.20 U GAM<br />
Europium 152 14683-23-9 U 0.076 0.10 U GAM<br />
Europium 154 15585-10-1 U 0.092 0.10 U GAM<br />
Europium 155 14391-16-3 U 0.073 0.10 U GAM<br />
Thorium 228 14274-82-9 U 0.090 U GAM<br />
Thorium 232 TH-232 U 0.13 U GAM<br />
Uranium 235 15117-96-1 U 0.12 U GAM<br />
Uranium 238 U-238 U 3.6 U GAM<br />
Americium 241 14596-10-2 U 0.11 U GAM<br />
Beryllium 7 13966-02-4 U 0.27 U GAM<br />
Ru<strong>the</strong>nium 106 13967-48-1 U 0.28 U GAM<br />
Antimony 125 14234-35-6 U 0.071 U GAM<br />
Cesium 134 13967-70-9 U 0.034 U GAM<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
DATA SHEETS Version Ver 1.0<br />
Page 16 Form DVD-DS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 30 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
Test PU Matrix SOLID Client <strong>Hanford</strong><br />
SDG 7420 METHOD SUMMARY Contract No. 630<br />
Contact Melissa C. Mannion PLUTONIUM, ISOTOPIC IN SOLIDS Contract SDG K0303<br />
RESULTS<br />
ALPHA SPECTROSCOPY<br />
LAB RAW SUF- Plutonium Plutonium<br />
CLIENT SAMPLE ID SAMPLE ID TEST FIX PLANCHET 238 239/240<br />
Preparation batch 7181-066<br />
J11KK8 R604093-02 7420-002 U U<br />
J11KL5 R604093-03 7420-003 U U<br />
Jll KL6 R604093-04 7420-004 U U<br />
J11KM0 R604093-05 7420-005 U U<br />
JllKM2 R604093-06 7420-006 U U<br />
Jll KM3 R604093-07 7420-007 U U<br />
Jll KM4 R604093-OB 7420-008 U U<br />
J1lKM5 R604093-09 7420-009 U U<br />
J11KM6 R604093-10 7420-010 U U<br />
J11KV1 R604093-11 7420-011 U U<br />
J11KV2 R604093-12 7420-012 U U<br />
JIIL21 R604093-13 7420-013 U U<br />
JIIL23 R604093-14 7420-014 U U<br />
JlIL25 R604093-15 7420-015 U U<br />
JlIL36 R604093-16 7420-016 U U<br />
Method Blank R604093-18 7420-018 U U<br />
Lab Control Sample 8604093-17 7420-017 Ok Ok<br />
Duplicate (R604093-06) R604093-19 7420-019 - U - U<br />
Nominal values and limits from method RDLS (pCi/g) 1.0 1.0<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment6Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
METHOD SODAfARIES Version Ver 1.0<br />
Page 1 Form DVD-CMS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 31 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
Test PU Matrix SOLID Client <strong>Hanford</strong><br />
SDG 7420 METHOD SUMMARY Contract No. 630<br />
Contact Melissa C. Mannion PLUTONIUM, ISOTOPIC IN SOLIDS Contract SDO K0303<br />
METHOD PERFORMANCE<br />
ALPHA SPECTROSCOPY<br />
LAB RAW SUF- MAX MDA ALIQ PREP DILU- YIELD EFF COUNT FWHM DRIFT DAYS ANAL-<br />
CLIENT SAMPLE ID SAMPLE ID TEST FIX pci/g g PAC TION k % min keV KeV HELD PREPARED YZED DETECTOR<br />
Preparation batch 7181-066 2a prep error 5.0 % Reference Lab Notebook 7181 pg. 66<br />
J11KK8 R604093-02 0.24 0.500 49 172<br />
J11KL5 R604093-03 0.25 0.500 55 172<br />
J11KL6 R604093-04 0.20 0.500 58 173<br />
J11KMO R604093-05 0.26 0.500 56 173<br />
J11KM2 R604093-06 0.17 0.500 68 173<br />
J11KM3 R604093-07 0.14 0.500 82 173<br />
JIIKM4 R604093-08 0.25 0.500 49 173<br />
JllKM5 R604093-09 0.35 0.500 44 144<br />
J11KM6 R604093-10 0.39 0.500 '59 103<br />
J11KV1 R604093-11 0.46 0.500 37 144<br />
J11KV2 R604093-12 0.33 0.500 45 144<br />
J111,21 R604093-13 0.29 0.500 61 144<br />
J111,23 R604093-14 0.33 0.500 48 145<br />
J11L25 R604093-15 0.29 0.500 60 114<br />
JlIL36 R604093-16 0.33 0.500 55 114<br />
Method Blank R604093-18 0.27 0.500 68 114<br />
Lab Control Sample R604093-17 0.20 0.500 90 114<br />
Duplicate (R604093-06) R604093-19 0.29 0.500 69 113<br />
Nominal values and limits from method 1.0 0.500 20-105 <strong>100</strong> <strong>100</strong> 180<br />
PROCEDURES REFERENCE PUISO_PLATE_AEA<br />
CP-071 Soil Dissolution, > 1.Og Aliquot, rev 5<br />
CP-941 Plutonium in Water and Dissolved Samples by<br />
Extraction Chromatography, rev 3<br />
CP-008 Heavy Element Electroplating, rev 9<br />
42 05/17/06 05/17 SS-027<br />
42 05/17/06 05/17 SS-028<br />
44 05/17/06 05/17 SS-029<br />
42 05/17/06 05/17 SS-031<br />
44 05/17/06 05/17 SS-032<br />
44 05/17/06 05/17 SS-033<br />
44 05/17/06 05/17 SS-034<br />
44 05/17/06 05/17 SS-035<br />
49 05/17/06 05/22 SS-040<br />
42 05/17/06 05/17 SS-036<br />
42 05/17/06 05/17 SS-038<br />
44 05/17/06 05/17 SS-039<br />
44 05/17/06 05/17 SS-040<br />
42 05/17/06 05/17 SS-055<br />
44 05/17/06 05/17 SS-056<br />
05/17/06 05/17 SS-058<br />
05/17/06 05/17 SS-057<br />
44 05/17/06 05/17 SS-059<br />
AVERAGES t 2 SO M)A 0.28 3 0.16<br />
FOR 18 SAMPLES YIELD 58 ; 27<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
METHOD SUMMARIES Version Ver 1.0<br />
Page 2 Form DVD-CMS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 32 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
Test TH Matrix SOLID Client <strong>Hanford</strong><br />
SDG 7420 METHOD SUMMARY Contract No. 630<br />
Contact Melissa C. Manion THORIUM, ISOTOPIC IN SOLIDS Contract BIG K0303<br />
RESULTS<br />
LAB RAW SUF-<br />
ALPHA SPECTROSCOPY<br />
CLIENT SAMPLE ID SAMPLE ID TEST FIX PLANCHET Thorium 230<br />
Preparation batch 7181-066<br />
J11KKB R604093-02 7420-002 U<br />
J11KL5 R604093-03 7420-003 U<br />
J11KL6 R604093-04 7420-004 U<br />
J11KM0 R604093-05 7420-005 U<br />
JllKM2 R604093-06 7420-006 U<br />
J111043 R604093-07 7420-007 U<br />
Jll KM4 R604093-08 7420-008 U<br />
JIIKMS R604093-09 7420-009 U<br />
1T11KM6 R604093-10 7420-010 U<br />
JI1KV1 R604093-11 7420-011 U<br />
J11KV2 R604093-12 7420-012 U<br />
JIIL21 R604093-13 7420-013 U<br />
JIIL23 R604093-14 7420-014 U<br />
JIIL25 R604093-15 7420-015 U<br />
J111,36 R604093-16 7420-016 U<br />
Method Blank R604093-18 7420-018 U<br />
Lab Control Sample R604093-17 7420-017 ok<br />
Duplicate (R604093-06) R604093-19 7420-019 - U<br />
Nominal values and limits from method RDLS (pCi/g) 1.0<br />
<strong>100</strong>6<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
METHOD SUMMARIES Version Ver 1.0<br />
Page 3 Form DVD-CMS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 33 Report date 05/25/06
Test TH Matrix SOLID<br />
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY DROOP K0303<br />
SDG 7420 METHOD SUMMARY<br />
Contact Melissa C. Manion THORIUM, ISOTOPIC IN SOLIDS<br />
METHOD PERFORMANCE<br />
ALPHA SPECTROSCOPY<br />
Client <strong>Hanford</strong><br />
Contract No. 630<br />
Contract SDG K0303<br />
LAB RAW SUF- MAX MDA ALIQ PREP DILU-.YIELD EFF COUNT FWHM DRIFT DAYS ANAL-<br />
CLIENT SAMPLE ID SAMPLE ID TEST FIX pCi/g g PAC TION % It min keV XeV HELD PREPARED YZED DETECTOR<br />
Preparation batch 7181-066 2a prep error 5.0 } Reference Lab Notebook 7181 pg. 66<br />
J11KKB 8604093-02 0.66 0.250 50 160<br />
J11KL5 R604093-03 0.42 0.250 77 160<br />
J11KL6 R604093-04 0.62 0.250 42 160<br />
J11KM0 R604093-05 0.56 0.250 51 160<br />
J11XM2 R604093-06 0.49 0.250 66 160<br />
J11KM3 R604093-07 0.46 0.250 54 160<br />
J11KM4 R604093-08 0.54 0.250 56 160<br />
J1IKM5 R604093-09 0.49 0.250 51 160<br />
JIIKM6 R604093-10 0.53 0.250 47 161<br />
J11KV1 R604093-11 0.68 0.250 50 167<br />
J11XV2 R604093-12 0.63 0.250 57 168<br />
JIIL21 R604093-13 0.46 0.250 45 168<br />
JllL23 R604093-14 0.42 0.250 70 168<br />
JIIL25 R604093-15 0.51 0.250 55 169<br />
JIIL36 R604093-16 0.48 0.250 65 169<br />
Method Blank R604093-18 0.84 0.250 36 160<br />
Lab Control Sample R604093-17 0.43 0.250 59 159<br />
Duplicate (R604093-06) 8604093-19 0.41 0.250 62 160<br />
Nominal values and limits from method 1.0 0.250 20-105 150<br />
PROCEDURES REFERENCE THISO_IE_ PLATE _AEA<br />
SPP-073 Soil Leaching 10-200 g Aliquot, rev 0<br />
CP-900 Thorium in Water and Dissolved Solid Samples by<br />
Extraction Chromatography, rev 1<br />
CP-008 Heavy Element Electroplating, rev 9<br />
38 05/13/06 05/13 SS-060<br />
38 05/13/06 05/13 SS-061<br />
40 05/13/06 05/13 SS-062<br />
38 05/13/06 05/13 SS-063<br />
40 05/13/06 05/13 SS-064<br />
40 05/13/06 05/13 SS-027<br />
40 05/13/06 05/13 SS-028<br />
40 05/13/06 05/13 SS-029<br />
40 05/13/06 05/13 SS-031<br />
38 05/13/06 05/13 SS-035<br />
38 05/13/06 05/13 SS-036<br />
40 05/13/06 05/13 SS-037<br />
40 05/13/06 05/13 SS-038<br />
38 05/13/06 05/13 SS-040<br />
40 05/13/06 05/13 SS-042<br />
05/13/06 05116 SS-028<br />
05/13/06 05/16 SS-027<br />
43 05/13/06 05/16 SS-029<br />
180<br />
AVERAGES } 2 SD MDA 0.54 f 0.23<br />
POR 18 SAMPLES YIELD 55 3 20<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
METHOD SUMMARIES Version Ver 1.0<br />
Page 4 Form DVD-CMS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 34 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
Test U Matrix SOLID Client <strong>Hanford</strong><br />
SDG 7420 METHOD SUMMARY Contract No. 630<br />
Contact Melissa C. Mannion URANIUM, ISOTOPIC IN SOLIDS Contract SDG K0303<br />
RESULTS<br />
ALPHA SPECTROSCOPY<br />
LAB RAW SUP- 1: Uranium 2: Uranium 3: Uranium RESULT RATIOS M<br />
CLIENT SAMPLE ID SAMPLE ID TEST FIX PLANCRET 233/234 235 238 1a3 2s 2.3 20<br />
Preparation batch 7181-066<br />
JllKK8 R604093-02 7420-002 0.423 U 0.597 71 45 0 10<br />
JllKL5 R604093-03 7420-003 U U U<br />
J11KL6 R604093-04 7420-004 U U U<br />
J11KM0 R604093-05 7420-005 U U U<br />
J11KM2 R604093-06 7420-006 U U U<br />
J11KM3 R604093-07 7420-007 U U U<br />
J11KM4 R604093-08 7420-008 U U U<br />
J11KM5 R604093-09 7420-009 U U U<br />
J11KM6 R604093-10 '7420-010 U U U<br />
J11KV1 R604093-11 7420-011 U U U<br />
JllKV2 R604093-12 7420-012 U U U<br />
J111,21 R604093-13 7420-013 U U U<br />
J111,23 R604093-14 7420-014 U U U<br />
J11L25 R604093-15 7420-015 q U U<br />
J111,36 R604093-16 7420-016 U U U<br />
Method Blank R604093-18 7420-018 q U U<br />
Lab Control Sample R604093-17 7420-017 ok ok ok<br />
Duplicate (R604093-06) R604093-19 7420-019 - U - U - U<br />
Nominal Values and limits from method RDLS (pCi/g) 1.0 1.0 1.0 <strong>100</strong> 4<br />
<strong>100</strong>6<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA SedimentETi Averages 71 0<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
METHOD SUMMARIES Version Ver 1.0<br />
Page 5 Form DVD-CMS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 35 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
Test U Matrix SOLID Client <strong>Hanford</strong><br />
SDG 7420 METHOD SUMMARY Contract No. 630<br />
Contact Melissa C. Mannion URANIUM, ISOTOPIC IN SOLIDS Contract SDG K0303<br />
METHOD PERFORMANCE<br />
CLIENT SAMPLE ID<br />
LAB RAW SUF-<br />
SAMPLE ID TEST FIX<br />
MAX MDA<br />
pCi/g<br />
ALPHA SPECTROSCOPY<br />
ALIQ<br />
g<br />
PREP DILO- YIELD EFF<br />
FAC TION % t<br />
Preparation batch 7181-066 20 prep error 5.0 t Reference Lab Notebook 7181 pg. 66<br />
COUNT FWHM DRIFT DAYS<br />
min keV KeV HELD PREPARED<br />
ANAL-<br />
YZED DETECTOR<br />
J11KK8 R604093-02 0.23 0.500 63 145 41 05/15/06 05/16 SS-037<br />
J11KL5 R604093-03 0.19 0.500 76 145 41 05/15/06 05/16 SS-038<br />
JllKL6 R604093-04 0.22 0.500 76 145 43 05/15/06 05/16 SS-039<br />
JllKM0 8604093-05 0.32 0.500 59 146 41 05/15/06 05/16 SS-040<br />
J11KM2 8604093-06 0.30 0.500 56 146 43 05/15/06 05/16 SS-042<br />
J11KM3 R604093-07 0.26 0.500 66 138 43 05/15/06 05/16 SS-055<br />
J111044 R604093-08 0.22 0.500 81 138 43 05/15/06 05/16 SS-056<br />
J11KM5 R604093-09 0.22 0.500 79 139 43 05/15/06 05/16 SS-057<br />
J11KM6 R604093-10 0.25 0.500 74 139 43 05/15/06 05/16 SS-058<br />
J11KV1 R604093-11 0.37 0.500 54 136 41 05/15/06 05/16 SS-059<br />
J11KV2 R604093-12 0.37 0.500 52 137 41 05/15/06 05/16 SS-060<br />
JIIL21 R604093-13 0.25 0.500 73 137 43 05/15/06 05/16 SS-061<br />
JlIL23 R604093-14 0.25 0.500 72 137 43 05/15/06 05/16 SS-062<br />
JlIL25 R604093-15 0.33 0.500 65 137 41 05/15/06 05/16 SS-063<br />
Jll L36 R604093-16 0.25 0.500 72 137 43 05/15/06 05/16 SS-064<br />
Method Blank R604093-18 0.24 0.500 79 137 05/15/06 05/16 SS-066<br />
Lab Control Sample R604093-17 0.88 0.500 96 137 05/15/06 05/16 SS-065<br />
Duplicate (R604093-06) R604093-19 0.25 0.500 68 145 44 05/15/06 05/17 SS-042<br />
Nominal values and limits from method 1.0 0.500 20-105 <strong>100</strong> <strong>100</strong> 180<br />
PROCEDURES REFERENCE UISO_PLATE AEA<br />
CP-073 Soil Leaching, 10 - 200 g Aliquot, rev 3<br />
CP-921 Uranium in Water and Dissolved Samples by<br />
Extraction Chromatography, rev 1<br />
CP-008 Heavy Element Electroplating, rev 9<br />
AVERAGES ; 2 SO MDA 0.30 ; 0.31<br />
FOR 18 SAMPLES YIELD 70 3 22<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
METHOD SUMMARIES Version Ver 1.0<br />
Page 6 Form DVD-CMS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 36 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
Test SR Matrix SOLID Client <strong>Hanford</strong><br />
SDG 7420 METHOD SUMMARY Contract No. 630<br />
Contact Melissa C. Mannion TOTAL STRONTIUM IN SOLIDS Contract SOO K0303<br />
BETA COUNTING<br />
RESULTS<br />
LAB RAW SUF- Total<br />
CLIENT SAMPLE ID SAMPLE IO TEST FIX PLANCRET Strontium<br />
Preparation batch 1181-066<br />
JllKK8 R604093-02 7420-002 U<br />
J11KL5 R604093-03 7420-003 U<br />
1711KL6 8604093-04 7420-004 U<br />
J11KM0 R604093-05 7420-005 U<br />
J11KM2 R604093-06 7420-006 0.505<br />
J111043 R604093-07 7420-007 U<br />
J1IKM4 8604093-08 7420-008 U<br />
1711 RM5 R604093-09 7420-009 U<br />
J11KM6 R604093-10 7420-010 U<br />
J11KT0 R604093-01 7420-001 U<br />
JllKV1 R604093-11 7420-011 U<br />
J11KV2 R604093-12 7420-012 U<br />
JIIL21 R604093-13 7420-013 U<br />
JlIL23 R604093-14 7420-014 0.406<br />
JIIL25 R604093-15 7420-015 U<br />
JllL36 R604093-16 7420-016 U<br />
Method Blank 8604093-18 7420-018 U<br />
Lab Control Sample 8604093-17 7420-017 ok<br />
Duplicate (R604093-06) R604093-19 7420-019 ok<br />
Nominal values and limits from method RDLS (pCi/g) 1.0<br />
<strong>100</strong>&<strong>300</strong><strong>Area</strong> Compnt <strong>RC</strong>BRA Sediment&Ti<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
METHOD SUMMARIES Version Ver 1.0<br />
Page 7 Form DVD-CMS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 37 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
Test SR Matrix SOLID Client <strong>Hanford</strong><br />
SDG 7420 METHOD SUMMARY Contract No. 630<br />
Contact Melissa C. Mannion TOTAL STRONTIUM IN SOLIDS Contract SDG K0303<br />
METHOD PERFORMANCE<br />
BETA COUNTING<br />
LAB RAW SUP- MDA ALIQ PREP DILU- YIELD EFF COUNT FWHM DRIFT DAYS ANAL-<br />
CLIENT SAMPLE ID SAMPLE ID TEST FIX pCi/g g FAC TION % % in keV KeV HELD PREPARED Y2ED DETECTOR<br />
Preparation batch 7181-066 2s prep error 10.0 k Reference Lab Notebook 7181 pg. 66<br />
J11KK8 R604093-02 0.26 1.00 94 <strong>100</strong> 34 05/09/06 05/09 GRB-227<br />
J11KL5 R604093-03 0.27 1.00 94 <strong>100</strong> 34 05109106 05/09 GRB-229<br />
J11KL6 R604093-04 0.27 1.00 94 <strong>100</strong> 36 05/09/06 05/09 GRB-204<br />
J11KMO R604093-05 0.26 1.00 89 <strong>100</strong> 34 05/09/06 05/09 GRB-222<br />
J11KM2 R604093-06 0.22 1.00 94 <strong>100</strong> 36 05/09/06 05/09 GRB-227<br />
J11KM3 R604093-07 0.25 1.00 92 <strong>100</strong> 36 05/09/06 05/09 GRB-224<br />
J11KM4 R604093-08 0.27 1.00 95 <strong>100</strong> 36 05/09/06 05/09 GRB-225<br />
J11KM5 R604093-09 0.26 1.00 95 <strong>100</strong> 37 05/09/06 05/10 GRB-232<br />
J11XM6 8604093-10 0.27 1.00 93 <strong>100</strong> 37 05/09/06 05/10 GRB-231<br />
J11KTO R604093-01 0.59 0.500 95 <strong>100</strong> 36 05/09/06 05/09 GRB-222<br />
J11KV1 8604093-11 0.22 1.00 94 <strong>100</strong> 35 05/09/06 05/10 GRB-220<br />
J11KV2 R604093-12 0.24 1.00 90 <strong>100</strong> 35 05/09/06 05/10 GRB-221<br />
JIIL21 R604093-13 0.22 1.00 92 <strong>100</strong> 37 05/09/06 05/10 GRB-222<br />
JIIL23 R604093-14 0.21 1.00 94 <strong>100</strong> 37 05/09/06 05/10 GRB-231<br />
JIIL25 R604093-15 0.22 1.00 94 120 35 05/09/06 05/10 GRB-201<br />
JIIL36 R604093-16 0.21 1.00 90 120 37 05/09/06 05/10 GRB-202<br />
Method Blank R604093-18 0.32 1.00 94 <strong>100</strong> 05/09/06 05/09 GRB-226<br />
Lab Control Sample R604093-17 0.18 1.00 96 <strong>100</strong> 05/09/06 05/10 GRB-222<br />
Duplicate (R604093-06) R604093-19 0.22 1.00 95 <strong>100</strong> 36 05/09/06 05/09 GRB-219<br />
Nominal values and limits from method 1.0 1.00 30-105 <strong>100</strong> 180<br />
PROCEDURES REFERENCE SRTOT_SEP_PRECIP_GPC<br />
CP-071 Soil Dissolution, > 1.Og Aliquot, rev 5<br />
CP-383 Strontium in Dissolved Solid <strong>of</strong> < S.Og Aliquot,<br />
rev 1<br />
AVERAGES 3 2 SO MDA 0.26 S 0.17<br />
FOR 19 SAMPLES YIELD 93 3 4<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
METHOD SUMMARIES Version Ver 1.0<br />
Page 8 Form DVD-CMS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 38 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
Test GAM Matrix SOLID<br />
SOO 7420 METHOD SUMMARY<br />
Contact Melissa C. Manion GAMMA SCAN<br />
RESULTS<br />
LAB RAN SUF-<br />
GAMMA SPECTROSCOPY<br />
CLIENT SAMPLE ID SAMPLE ID TEST FIX PLANCEET Cobalt 60 Cesium 137<br />
Preparation batch 7181-066<br />
JllKK8 R604093-02<br />
JllKL5 R604093-03<br />
J11KL6 R604093-04<br />
JllKM0 R604093-05<br />
J11KM2 R604093-06<br />
Jll KM3 R604093-07<br />
Jll KM4 R604093-08<br />
J11KM5 R604093-09<br />
JllKM6 R604093-10<br />
J11KV1 R604093-11<br />
J11KV2 R604093-12<br />
JIIL21 R604093-13<br />
JlIL23 R604093-14<br />
J11L25 R604093-15<br />
JIIL36 R604093-16<br />
Method Blank R604093-18<br />
Lab Control Sample R604093-17<br />
Duplicate (R604093-06) R604093-19<br />
Nominal values and limits from method<br />
<strong>100</strong>E<strong>300</strong>Aiea Compnt <strong>RC</strong>BRA Sediment&Ti<br />
7420-002 U U<br />
7420-003 U U<br />
7420-004 U U<br />
7420-005 U U<br />
7420-006 U U<br />
7420-007 U U<br />
7420-GOB U U<br />
7420-009 U U<br />
7420-010 U U<br />
7420-011 U U<br />
7420-012 U U<br />
7420-013 U U<br />
7420-014 U U<br />
7420-015 U U<br />
7420-016 U U<br />
7420-018 U U<br />
7420-017 ok ok<br />
7420-019 - U -<br />
RDLS (PCi/g) 0.050 0.10<br />
U<br />
Client <strong>Hanford</strong><br />
Contract No. 630<br />
Contract SDG K0303<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
METHOD SUMMARIES Version Ver 1.0<br />
Page 9 Form DVD-CMS<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 39 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
Test GAM Matrix SOLID Client <strong>Hanford</strong><br />
SIG 7420 METHOD SUMMARY Contract No. 630<br />
Contact Melissa C. Manion GAMM SCAN Contract SIG K0303<br />
GAPM SPECTROSCOPY<br />
METHOD PERFORMANCE<br />
LAB RAW SUF- MDA ALIQ PREP DILU- YIELD EFF COUNT FWHM DRIFT DAYS ANAL-<br />
CLIENT SAMPLE ID SAMPLE ID TEST FIX pCi/g g PAC TION % } min keV KeV HELD PREPARED YZED DETECTOR<br />
Preparation batch 7181-066 2a prep error 15.0 t Reference Lab Notebook 7181 pg. 66<br />
J11KK8 R604093-02 24 77.8 354. 14 04/17/06 04/19 JR,02,00<br />
J11KL5 R604093-03 27 69.6 354 14 04/17/06 04/19 JR, 08, 00<br />
J11KL6 R604093-04 24 74.5 379 17 04/17/06 04/20 JR,02,00<br />
J11KM0 R604093-05 20 86.8 405 16 04/17/06 04/21 JR,02,00<br />
J11KM2 R604093-06 17 88.7 354 16 04/17/06 04/19 JR,05,00<br />
J11KM3 R604093-07 21 81.0 405 18 04/17/06 04/21 JR, 08, 00<br />
J11KM4 R604093-08 12 91.5 817 18 04/17/06 04/21 JR,03,00<br />
J11KM5 R604093-09 15 65.9 829 18 04/17/06 04/21 JR,05,00<br />
J11KM6 R604093-10 17 69.1 829 1S 04/17/06 04/21 JR, 02, 00<br />
J11KV1 8604093-11 17 71.2 829 16 04/17/06 04/21 JR,08,00<br />
J11KV2 R604093-12 27 67.6 425 17 04/17/06 04/22 JR,08,00<br />
J111,21 R604093-13 25 64.7 413 19 04/17/06 04/22 JR,03,00<br />
JIIL23 R604093-14 20 71.4 413 19 04/17/06 04/22 JR, 05, 00<br />
J11L25 R604093-15 8.1 80.8 2455 17 04/17/06 04/22 JR, 03, 00<br />
J111,36 R604093-16 7.8 71.5 2455 19 04/17/06 04/22 JR,05,00<br />
Method Blank R604093-18 29 64.0 379 04/17/06 04/20 JR,08,00<br />
Lab Control Sample 8604093-17 0.16 64.0 353 04/17/06 04/20 JR,03,00<br />
Duplicate (R604093-06) R604093-19 16 88.7 405 18 04/17/06 04/21 JR, 05, 00<br />
Nominal values and limits from method 0.050 64.0 <strong>100</strong> 180<br />
PROCEDURES REFERENCE GAMMA_GS<br />
SPP-<strong>100</strong> Ge(Li) Preparation for Commercial Samples, rev 7<br />
AVERAGES t 2 SO MDA 18 f 15<br />
FOR 18 SAMPLES YIELD f<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
METHOD SUM44ARIES Version Ver 1.0<br />
Page 10 Form DVD-CMS<br />
SUM2UZY DATA SECTION Version 3.06<br />
Page 40 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion R E P O R T G U I D E Contract No. 630<br />
Case no SDG K0303<br />
SAMPLE SUMMARY<br />
The Sample and QC Summary Reports show all samples, including QC<br />
samples, reported in one Sample Delivery Group (SDG).<br />
The Sample Summary Report fully identifies client samples and gives <strong>the</strong><br />
corresponding lab sample identification. The QC Summary Report shows at<br />
<strong>the</strong> sample level how <strong>the</strong> lab organized <strong>the</strong> samples into batches and<br />
generated QC samples. The Preparation Batch and Method Summary Reports<br />
show this at <strong>the</strong> analysis level.<br />
The following notes apply to <strong>the</strong>se reports:<br />
• LAB SAMPLE ID is <strong>the</strong> lab's primary identification for a sample.<br />
• DEPARTMENT SAMPLE ID is an alternate lab id, for example one<br />
assigned by a radiochemistry department in a lab.<br />
• CLIENT SAMPLE ID is <strong>the</strong> client's primary identification for a<br />
sample. It includes any sample preparation done by <strong>the</strong> client<br />
that is necessary to identify <strong>the</strong> sample.<br />
• QC BATCH is a lab assigned code that groups samples to be<br />
processed and QCed toge<strong>the</strong>r. These samples should have similar<br />
matrices.<br />
QC BATCH is not necessarily <strong>the</strong> same as SDG, which reflects<br />
samples received and reported toge<strong>the</strong>r.<br />
* All Lab Control Samples, Method Blanks, Duplicates and Matrix<br />
Spikes are shown that QC any <strong>of</strong> <strong>the</strong> samples. Due to possible<br />
reanalyses, not all results for all <strong>the</strong>se QC samples may be<br />
relevant to <strong>the</strong> SDG. The Lab Control Sample, Method Blank,<br />
Duplicate, Matrix Spike and Method Summary Reports detail <strong>the</strong>se<br />
relationships.<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 1 Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 41 Report date 05/25/06
EBER L INE SERVI CES / RI CHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion R E P O R T G U I D E Contract No. 630<br />
Case no SDG K0303<br />
PREPARATION BATCH SUMMARY<br />
The Preparation Batch Summary Report shows all preparation batches in<br />
one Sample Delivery Group (SDG) with information necessary to check <strong>the</strong><br />
completeness and consistency <strong>of</strong> <strong>the</strong> SDG.<br />
The following notes apply to this report:<br />
• The preparation batches are shown in <strong>the</strong> same order as <strong>the</strong><br />
Method Summary Reports are printed.<br />
• only analyses <strong>of</strong> planchets relevant to <strong>the</strong> SDG are included.<br />
• Each preparation batch should have at least one Method Blank<br />
and LCS in it to validate client sample results.<br />
* The QUALIFIERS shown are all qualifiers o<strong>the</strong>r than U, J, B, L<br />
and H that occur on any analysis in <strong>the</strong> preparation batch. The<br />
Method Summary Report has <strong>the</strong>se qualifiers on a per sample<br />
basis.<br />
These qualifiers should be reviewed as follows<br />
X Some data has been manually entered or modified.<br />
Transcription errors are possible.<br />
P One or more results are 'preliminary'. The data is not<br />
ready for final reporting.<br />
2 There were two or more results for one analyte on one<br />
planchet imported at one time. The results in DVD may<br />
not be <strong>the</strong> same as on <strong>the</strong> raw data sheets.<br />
O<strong>the</strong>r lab defined qualifiers may occur. In general, <strong>the</strong>se<br />
should be addressed in <strong>the</strong> SDG narrative.<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 2 Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 42 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion R E P O R T G U I D E Contract No. 630<br />
Case no SDG K0303<br />
WORK SUMMARY<br />
The Work Summary Report shows all samples, including QC samples, and all<br />
relevant analyses in one Sample Delivery Group (SDG). This report is<br />
<strong>of</strong>ten useful as supporting documentation for an invoice.<br />
The following notes apply to this report:<br />
* TEST is a code for <strong>the</strong> method used to measure associated<br />
analytes. Results and related information for each analyte<br />
are on <strong>the</strong> Data Sheet Report. In special cases, a test code<br />
used in <strong>the</strong> summary data section is not <strong>the</strong> same as in<br />
associated raw data. In this case, both codes are shown on <strong>the</strong><br />
Work Summary.<br />
* SUFFIX is <strong>the</strong> lab's code to distinguish multiple analyses<br />
(recounts, reworks, reanalyses) <strong>of</strong> a fraction <strong>of</strong> <strong>the</strong> sample.<br />
The suffix indicates which result is being reported. An empty<br />
suffix normally identifies <strong>the</strong> first attempt to analyze <strong>the</strong><br />
sample.<br />
* The LAB SAMPLE ID, TEST and SUFFIX uniquely identify all<br />
supporting data for a result. The Method Summary Report for<br />
each TEST has method performance data, such as yield, for each<br />
lab sample id and suffix and procedures used in <strong>the</strong> method.<br />
* PLANCHET is an alternate lab identifier for work done for one<br />
test. It, combined with <strong>the</strong> TEST and SUFFIX, may be <strong>the</strong> best<br />
link to raw data.<br />
* For QC samples, only analyses that directly QC some regular<br />
sample are shown. The Lab Control Sample, Method Blank,<br />
Duplicate, Matrix Spike and Method Summary Reports detail <strong>the</strong>se<br />
relationships.<br />
* The SAS (Special Analytical Services) Number is a client or lab<br />
assigned code that reflects special processing for samples, such<br />
as rapid turn around. Counts <strong>of</strong> tests done are lists by SAS<br />
number since it is likely to affect prices.<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 3 Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 43 Report date 05/25/06
EBERLINE SERVI CES / RI C HM O ND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion R E P O R T G U I D E Contract No. 630<br />
Case no SDG K0303<br />
DATA SHEET<br />
The Data Sheet Report shows all results and primary supporting<br />
information for one client sample or Method Blank. This report<br />
corresponds to both <strong>the</strong> CLP Inorganics and Organics Data Sheet.<br />
The following notes apply to this report:<br />
* TEST is a code for <strong>the</strong> method used to measure an analyte. If<br />
<strong>the</strong> TEST is empty, no data is available; <strong>the</strong> analyte was not<br />
analyzed for.<br />
* The LAB SAMPLE ID and TEST uniquely identify work within <strong>the</strong><br />
Summary Data Section <strong>of</strong> a Data Package. The Work Summary and<br />
Method Summary Reports fur<strong>the</strong>r identify raw data that underlies<br />
this work.<br />
The Method Summary Report for each TEST has method performance<br />
data, such as yield, for each Lab Sample ID and a list <strong>of</strong><br />
procedures used in <strong>the</strong> method.<br />
* ERRORs can be labeled TOTAL or COUNT. TOTAL implies a<br />
preparation (non-counting method) error has been added, as<br />
square root <strong>of</strong> sum <strong>of</strong> squares, to <strong>the</strong> counting error denoted by<br />
COUNT. The preparation errors, which may vary by preparation<br />
batch, are shown on <strong>the</strong> Method Summary Report.<br />
* A RESULT can be 'N.R.' (Not Reported). This means <strong>the</strong> lab did<br />
this work but chooses not to report it now, possibly because it<br />
was reported at ano<strong>the</strong>r time.<br />
* When reporting a Method Blank, a RESULT can be 'N.A.' (Not<br />
Applicable). This means <strong>the</strong>re is no reported client sample work<br />
in <strong>the</strong> same preparation batch as <strong>the</strong> Blank's result. This is<br />
likely to occur when <strong>the</strong> Method Blank is associated with<br />
reanalyses <strong>of</strong> selected work for a few samples in <strong>the</strong> SDG.<br />
The following qualifiers are defined by <strong>the</strong> DVD system:<br />
U The RESULT is less than <strong>the</strong> MDA (Minimum Detectable Activity).<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 4<br />
Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 44 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion G U I D E, C o n t Contract No. 630<br />
Case no SDG K0303<br />
DATA SHEET<br />
If <strong>the</strong> MDA is blank, <strong>the</strong> ERROR is used as <strong>the</strong> limit.<br />
J The RESULT is less than <strong>the</strong> RDL (Required Detection Limit) and<br />
no U qualifier is assigned.<br />
B A Method Blank associated with this sample had a result without<br />
a U flag and, after correcting for possibly different aliquots,<br />
that result is greater than or equal to <strong>the</strong> MDA for this sample.<br />
Normally, B is not assigned if U is. When method blank<br />
subtraction is shown on this report, B flags are assigned based<br />
on <strong>the</strong> unsubtracted values while U's are assigned based on <strong>the</strong><br />
subtracted ones. Both flags can be assigned in this case.<br />
For each sample result, all Method Blank results in <strong>the</strong> same<br />
preparation batch are compared. The Method Summary Report<br />
documents this and o<strong>the</strong>r QC relationships.<br />
L Some Lab Control Sample that QC's this sample had a low<br />
recovery. The lab can disable assignment <strong>of</strong> this qualifier.<br />
H Similar to 'L' except <strong>the</strong> recovery was high.<br />
P The RESULT is 'preliminary'.<br />
X Some data necessary to compute <strong>the</strong> RESULT, ERROR or MDA was<br />
manually entered or modified.<br />
2 There were two or more results available for this analyte. The<br />
reported result may not be <strong>the</strong> same as in <strong>the</strong> raw data.<br />
O<strong>the</strong>r qualifiers are lab defined. Definitions should be in <strong>the</strong><br />
SDG narrative.<br />
The following values are underlined to indicate possible problems:<br />
* An MDA is underlined if it is bigger than its RDL.<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 5 Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 45 Report date 05/25/06
EBE RLIN E SER V ICES / RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion G U I D E, C O n t Contract No. 630<br />
Case no SDG K0303<br />
DATA SHEET<br />
* An ERROR is underlined if <strong>the</strong> 1.645 sigma counting error is<br />
bigger than both <strong>the</strong> MDA and <strong>the</strong> RESULT, implying that <strong>the</strong> MDA<br />
may not be a good estimate <strong>of</strong> <strong>the</strong> 'real' minimum detectable<br />
activity.<br />
* A negative RESULT is underlined if it is less than <strong>the</strong> negative<br />
<strong>of</strong> its 2 sigma counting ERROR.<br />
* When reporting a Method Blank, a RESULT is underlined if<br />
greater than its MDA. If <strong>the</strong> MDA is blank, <strong>the</strong> 2 sigma counting<br />
error is used in <strong>the</strong> comparison.<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 6 Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 46 Report date 05/25/06
EBERLINE SERVI CES / RI CHMOND<br />
SANPLB DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion R E P O R T G U I D E Contract No. 630<br />
Case no SDG K0303<br />
LAB CONTROL SAMPLE<br />
The Lab Control Sample Report shows all results, recoveries and primary<br />
supporting information for one Lab Control Sample.<br />
The following notes apply to this report:<br />
• All fields in common with <strong>the</strong> Data Sheet Report have similar<br />
usage. Refer to its Report Guide for details.<br />
• An amount ADDED is <strong>the</strong> lab's value for <strong>the</strong> actual amount spiked<br />
into this sample with its ERROR an estimate <strong>of</strong> <strong>the</strong> error <strong>of</strong> this<br />
amount.<br />
An amount added is underlined if its ratio to <strong>the</strong> corresponding<br />
RDL is outside protocol specified limits.<br />
* REC (Recovery) is RESULT divided by ADDED expressed as a<br />
percent.<br />
* The first, computed limits for <strong>the</strong> recovery reflect:<br />
1. The error <strong>of</strong> RESULT, including that introduced by<br />
rounding <strong>the</strong> result prior to printing.<br />
If <strong>the</strong> limits are labeled (TOTAL), <strong>the</strong>y include<br />
preparation error in <strong>the</strong> result. If labeled (COUNT),<br />
<strong>the</strong>y do not.<br />
2. The error <strong>of</strong> ADDED.<br />
3. A lab specified, per analyte bias. The bias changes <strong>the</strong><br />
center <strong>of</strong> <strong>the</strong> computed limits.<br />
* The second limits are protocol defined upper and lower QC limits<br />
for <strong>the</strong> recovery.<br />
* The recovery is underlined if it is outside ei<strong>the</strong>r <strong>of</strong> <strong>the</strong>se<br />
ranges.<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 7 Form DVD-RG<br />
SUMKARY DATA SECTION Version 3.06<br />
Page 47 Report date 05/25/06
EBERLINE SERVI CES /RI CHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion R E P O R T G U I D E Contract No. 630<br />
Case no SDG K0303<br />
DUPLICATE<br />
The Duplicate Report shows all results, differences and primary<br />
supporting information for one Duplicate and associated Original sample.<br />
The following notes apply to this report:<br />
* All fields in common with <strong>the</strong> Data Sheet Report have similar<br />
usage. This applies both to <strong>the</strong> Duplicate and Original sample<br />
data. Refer to <strong>the</strong> Data Sheet Report Guide for details.<br />
If <strong>the</strong> Duplicate has data for a TEST and <strong>the</strong> lab did not do this<br />
test to <strong>the</strong> Original, <strong>the</strong> Original's RESULTS are underlined.<br />
* The RPD (Relative Percent Difference) is <strong>the</strong> absolute value <strong>of</strong><br />
<strong>the</strong> difference <strong>of</strong> <strong>the</strong> RESULTS divided by <strong>the</strong>ir average expressed<br />
as a percent.<br />
If both RESULTS are less than <strong>the</strong>ir MDAs, no RPD is computed and<br />
a '-' is printed.<br />
For an analyte, if <strong>the</strong> lab did work for both samples but has<br />
data for only one, <strong>the</strong> MDA from <strong>the</strong> sample with data is used as<br />
<strong>the</strong> o<strong>the</strong>r's result in <strong>the</strong> RPD.<br />
* The first, computed limit is <strong>the</strong> sum, as square root <strong>of</strong> sum <strong>of</strong><br />
squares, <strong>of</strong> <strong>the</strong> errors <strong>of</strong> <strong>the</strong> results divided by <strong>the</strong> average<br />
result as a percent, hence <strong>the</strong> relative error <strong>of</strong> <strong>the</strong> difference<br />
ra<strong>the</strong>r than <strong>the</strong> error <strong>of</strong> <strong>the</strong> relative difference. The errors<br />
include those introduced by rounding <strong>the</strong> RESULTS prior to<br />
printing.<br />
If this limit is labeled TOT, it includes <strong>the</strong> preparation error<br />
in <strong>the</strong> RESULTS. If labeled CNT, it does not.<br />
This value reported for this limit is at most 999.<br />
* The second limit for <strong>the</strong> RPD is <strong>the</strong> larger <strong>of</strong>:<br />
1. A fixed percentage specified in <strong>the</strong> protocol.<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 8 Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 48 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion G U I D E, C O n t Contract No. 630<br />
Case no SDG K0303<br />
DUPLICATE<br />
2. A protocol factor (typically 2) times <strong>the</strong> average MDA as<br />
a percent <strong>of</strong> <strong>the</strong> average result. This limit applies<br />
when <strong>the</strong> results are close to <strong>the</strong> MDAs.<br />
* The RPD is underlined if it is,greater than ei<strong>the</strong>r limit.<br />
* If specified by <strong>the</strong> lab, <strong>the</strong> second limit column is replaced by<br />
<strong>the</strong> Difference Error Ratio (DER), which is <strong>the</strong> absolute value<br />
<strong>of</strong> <strong>the</strong> difference <strong>of</strong> <strong>the</strong> results divided by <strong>the</strong> quadratic sum <strong>of</strong><br />
<strong>the</strong>ir one sigma errors, <strong>the</strong> same errors as used in <strong>the</strong> first<br />
limit.<br />
Except for differences due to rounding, <strong>the</strong> DER is <strong>the</strong><br />
same as <strong>the</strong> RPD divided by <strong>the</strong> first RPD limit with <strong>the</strong><br />
limit scaled to 1 sigma.<br />
* The DER is underlined if it is greater than <strong>the</strong> sigma factor,<br />
typically 2 or 3, shown in <strong>the</strong> header for <strong>the</strong> first RPD limit.<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 9 Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 49 Report date 05/25/06
EBER L INE SERVI CES / RI CHMOND<br />
SAMPLE DBLIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion R E P O R T G U I D E Contract No. 630<br />
Case no SDG K0303<br />
MATRIX SPIKE<br />
The Matrix Spike Report shows all results, recoveries and primary<br />
supporting information for one Matrix Spike and associated Original<br />
sample.<br />
The following notes apply to this report:<br />
* All fields in common with <strong>the</strong> Data Sheet Report have similar<br />
usage. This applies both to <strong>the</strong> Spiked and Original sample<br />
data. Refer to <strong>the</strong> Data Sheet Report Guide for details.<br />
If <strong>the</strong> Spike has data for a TEST and <strong>the</strong> lab did not do this<br />
test to <strong>the</strong> Original, <strong>the</strong> Original's RESULTS are underlined.<br />
* An amount ADDED is <strong>the</strong> lab's value for <strong>the</strong> actual amount spiked<br />
into <strong>the</strong> Spike sample with its ERROR an estimate <strong>of</strong> <strong>the</strong> error <strong>of</strong><br />
this amount.<br />
An amount is underlined if its ratio to <strong>the</strong> corresponding RDL is<br />
outside protocol specified limits.<br />
* REC (Recovery) is <strong>the</strong> Spike RESULT minus <strong>the</strong> original RESULT<br />
divided by ADDED expressed as a percent.<br />
* The first, computed limits for <strong>the</strong> recovery reflect:<br />
1. The errors <strong>of</strong> <strong>the</strong> two RESULTs, including those<br />
introduced by rounding <strong>the</strong>m prior to printing.<br />
If <strong>the</strong> limits are labeled (TOTAL), <strong>the</strong>y include<br />
preparation error in <strong>the</strong> result. If labeled (COUNT),<br />
<strong>the</strong>y do not.<br />
2. The error <strong>of</strong> ADDED.<br />
3. A lab specified, per analyte bias. The bias changes <strong>the</strong><br />
center <strong>of</strong> <strong>the</strong> computed limits.<br />
* The second limits are protocol defined upper and lower QC limits<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 10 Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 50 Report date 05/25/06
EBER L INE SER V ICES / RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion G U I D E, C O 11 t Contract No. 630<br />
Case no SDG K0303<br />
for <strong>the</strong> recovery.<br />
MATRIX SPIKE<br />
These limits are left blank if <strong>the</strong> Original RESULT is more than<br />
a protocol defined factor (typically 4) times ADDED. This is a<br />
way <strong>of</strong> accounting for that when <strong>the</strong> spike is small compared to<br />
<strong>the</strong> amount in <strong>the</strong> original sample, <strong>the</strong> recovery is unreliable.<br />
* The recovery is underlined (out <strong>of</strong> spec) if it is outside ei<strong>the</strong>r<br />
<strong>of</strong> <strong>the</strong>se ranges.<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 11 Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 51 Report date 05/25/06
EBERLINE SE RV I CES /RI CHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion R E P O R T G U I D E Contract No. 630<br />
Case no SDG K0303<br />
METHOD SUMMARY<br />
The Method Summary Report has two tables. One shows up to five results<br />
measured using one method. The o<strong>the</strong>r has performance data for <strong>the</strong><br />
method. There is one report for each TEST, as used on <strong>the</strong> Data Sheet<br />
Report.<br />
The following notes apply to this report:<br />
* Each table is subdivided into sections, one for each preparation<br />
batch. A preparation batch is a group <strong>of</strong> aliquots prepared at<br />
roughly <strong>the</strong> same time in one work area <strong>of</strong> <strong>the</strong> lab using <strong>the</strong> same<br />
method.<br />
There should be Lab Control Sample and Method Blank results in<br />
each preparation batch since this close correspondence makes <strong>the</strong><br />
QC meaningful. Depending on lab policy, Duplicates need not<br />
occur in each batch since <strong>the</strong>y QC sample dependencies such as<br />
matrix effects.<br />
* The RAW TEST column shows <strong>the</strong> test code used in <strong>the</strong> raw data to<br />
identify a particular analysis if it is different than <strong>the</strong> test<br />
code in <strong>the</strong> header <strong>of</strong> <strong>the</strong> report. This occurs in special cases<br />
due to method specific details about how <strong>the</strong> lab labels work.<br />
The Lab Sample or Planchet ID combined with <strong>the</strong> (Raw) Test Code<br />
and Suffix uniquely identify <strong>the</strong> raw data for each analysis.<br />
* If a result is less than both its MDA and RDL, it is replaced by<br />
just 'U' on this report. If it is greater than or equal to <strong>the</strong><br />
RDL but less than <strong>the</strong> MDA, <strong>the</strong> result is shown with a 'U' flag.<br />
The J and X flags are as on <strong>the</strong> data sheet.<br />
* Non-U results for Method Blanks are underlined to indicate<br />
possible contamination <strong>of</strong> o<strong>the</strong>r samples in <strong>the</strong> preparation<br />
batch. The Method Blank Report has supporting data.<br />
* Lab Control Sample and Matrix Spike results are shown as: ok, No<br />
data, LOW or HIGH, with <strong>the</strong> last two underlined. 'No data'<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 12 Form DVD-RG<br />
SU14K&RY DATA SECTION Version 3.06<br />
Page 52 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion G U I D E, C O n t Contract No. 630<br />
Case no SDG K0303<br />
METHOD SUMMARY<br />
means no amount ADDED was specified. 'LOW' and 'HIGH'<br />
correspond to when <strong>the</strong> recovery is underlined on <strong>the</strong> Lab Control<br />
Sample or Matrix .Spike Report. See <strong>the</strong>se reports for supporting<br />
data.<br />
* Duplicate sample results are shown as: ok, No data, or OUT, with<br />
<strong>the</strong> last two underlined. 'No data' means <strong>the</strong>re was no original<br />
sample data found for this duplicate. 'OUT' corresponds to when<br />
<strong>the</strong> RPD is underlined on <strong>the</strong> Duplicate Report. See this report<br />
for supporting data.<br />
* If <strong>the</strong> MDA column is labeled 'MAX MDA', <strong>the</strong>re was more than one<br />
result measured by <strong>the</strong> reported method and <strong>the</strong> MDA shown is <strong>the</strong><br />
largest MDA. If not all <strong>the</strong>se results have <strong>the</strong> same RDL, <strong>the</strong><br />
MAX MDA reflects only those results with RDL equal to <strong>the</strong><br />
smallest one.<br />
MDAs are underlined if greater than <strong>the</strong> printed RDL.<br />
* Aliquots are underlined if less than <strong>the</strong> nominal value specified<br />
for <strong>the</strong> method.<br />
* Prepareation factors are underlined if greater than <strong>the</strong> nominal<br />
value specified for <strong>the</strong> method.<br />
* Dilution factors are underlined if greater than <strong>the</strong> nominal<br />
value specified for <strong>the</strong> method.<br />
* Residues are underlined if outside <strong>the</strong> range specified for <strong>the</strong><br />
method. Residues are not printed if yields are.<br />
* Yields, which may be gravimetric, radiometric or some type <strong>of</strong><br />
recovery depending on <strong>the</strong> method, are underlined if outside <strong>the</strong><br />
range specified for <strong>the</strong> method.<br />
* Efficiencies are underlined if outside <strong>the</strong> range specified for<br />
<strong>the</strong> method. Efficiencies are detector and geometry dependent so<br />
this test is only approximate.<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 13 Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 53 Report date 05/25/06
EBERLINE SE RV ICES/RICHMOND<br />
SAMPLB DELIVERY GROUP K0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion G U I D E, c O n t Contract No. 630<br />
Case no SDG K0303<br />
METHOD SUMMARY<br />
• Count times are underlined if less than <strong>the</strong> nominal value<br />
specified for <strong>the</strong> method.<br />
• Resolutions (as FWHM; Full Width at Half Max) are underlined if<br />
greater than <strong>the</strong> method specified limit.<br />
• Tracer drifts are underlined if <strong>the</strong>ir absolute values are<br />
greater than <strong>the</strong> method specified limit. Tracer drifts are<br />
not printed if percent moistures are.<br />
• Days Held are underlined if greater than <strong>the</strong> holding time<br />
specified in <strong>the</strong> protocol.<br />
• Analysis dates are underlined if before <strong>the</strong>ir planchet's<br />
preparation date or, if a limit is specified, too far after<br />
it.<br />
For some methods, ratios as percentages and error estimates for <strong>the</strong>m are<br />
computed for pairs <strong>of</strong> results. A ratio column header like 1 1+3' means<br />
<strong>the</strong> ratio <strong>of</strong> <strong>the</strong> first result column and <strong>the</strong> third result column.<br />
Ratios are not computed for Lab Control Sample, Method Blank or<br />
Matrix Spike results since <strong>the</strong>ir matrices are not necessarily<br />
similar to client samples'.<br />
The error estimate for a ratio <strong>of</strong> results from one planchet reflects<br />
only counting errors since o<strong>the</strong>r errors should be correlated. For a<br />
ratio involving different planchets, if QC limits are computed based on<br />
total errors, <strong>the</strong> error for <strong>the</strong> ratio allows for <strong>the</strong> preparation errors<br />
for <strong>the</strong> planchets.<br />
The ratio is underlined (out <strong>of</strong> spec) if <strong>the</strong> absolute value <strong>of</strong> its<br />
difference from <strong>the</strong> nominal value is greater than its error estimate.<br />
If no nominal value is specified, this test is not done.<br />
For Gross Alpha or Gross Beta results, <strong>the</strong>re may be a column showing <strong>the</strong><br />
sum <strong>of</strong> o<strong>the</strong>r Alpha or Beta emitters. This sum includes all relevant<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES version Ver 1.0<br />
Page 14 Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 54 Report date 05/25/06
EBERLINE SERVICES/RICHMOND<br />
SAMPLE DELIVERY GROUP X0303<br />
SDG 7420 Client <strong>Hanford</strong><br />
Contact Melissa C. Mannion G U I D E, C o n t Contract No. 630<br />
Case no SDG K0303<br />
METHOD SUMMARY<br />
results in <strong>the</strong> DVD database, whe<strong>the</strong>r reported or not. Results in <strong>the</strong><br />
sum are weighted by a particles/decay value specified by <strong>the</strong> lab for<br />
each relevant analyte. Results less than <strong>the</strong>ir MDA are not included.<br />
No sums are computed for Lab Control, Method Blank or Matrix Spike<br />
samples since <strong>the</strong>ir various planchets may not be physically related.<br />
If a ratio <strong>of</strong> total isotopic to Gross Alpha or Beta is shown, <strong>the</strong> error<br />
for <strong>the</strong> ratio reflects both <strong>the</strong> error in <strong>the</strong> Gross result and <strong>the</strong> sum,<br />
as square root <strong>of</strong> sum <strong>of</strong> squares, <strong>of</strong> <strong>the</strong> errors in <strong>the</strong> isotopic results.<br />
For total elemental uranium or thorium results, <strong>the</strong>re may be a column<br />
showing <strong>the</strong> total weight computed from associated isotopic results.<br />
Ignoring results less than <strong>the</strong>ir MDAs, this is a weighted sum <strong>of</strong> <strong>the</strong><br />
isotopic results. The weights depend on <strong>the</strong> molecular weight and<br />
half-life <strong>of</strong> each isotope so as to convert activities (decays) to weight<br />
(atoms).<br />
If a ratio <strong>of</strong> total computed to measured elemental uranium or thorium is<br />
shown, <strong>the</strong> error for <strong>the</strong> ratio reflects <strong>the</strong> errors in all <strong>the</strong><br />
measurements.<br />
Lab id EBRLNE<br />
Protocol <strong>Hanford</strong><br />
REPORT GUIDES Version Ver 1.0<br />
Page 15 Form DVD-RG<br />
SUMMARY DATA SECTION Version 3.06<br />
Page 55 Report date 05/25/06
Washin0on Closure Hatiford CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-311 Page J <strong>of</strong> 1<br />
Collector<br />
Company Contact Telephone No.<br />
TN KLINCKN<br />
project Coordinator<br />
TILLER, B. JOAN KESSNER 375-4688 KESSNER, 1H Price Code 9N Data Turnaround<br />
oiect Destenation<br />
S=vline Loca<br />
<strong>100</strong><br />
ti on [^O D 9 /7^.y -\ <strong>SAF</strong> No.<br />
& <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti 116-N-3 INVERTEBRATES ) 3[I J / I0 <strong>RC</strong>-<strong>047</strong><br />
Ice Chest No. p<br />
Field Loebook No. COA Method <strong>of</strong> Shipment<br />
^P 6 -02 -SD5-<br />
EL-1595 BESRAS6520 FED EX<br />
Shin Offsite Proverty No. ^/ 7 Bi ll <strong>of</strong> LadbWAir Bi ll No.<br />
C BE INESERVIC LIONVILE 19*0330 SEE OSPC<br />
PO LE HAZARDS/REMARKS<br />
covi_ 4C<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-259 Page I <strong>of</strong> 1<br />
Collector<br />
Company Contact Telephone No Proiect Coordinator<br />
TILLER, B. TN KLINCKMAN<br />
JOAN KESSNER 375-4688 KESSNER, IH<br />
roiect Desdmnsdton<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Sampline Location<br />
600-1321600-190 OFFAL<br />
ff^ 2 /)1 2<br />
/' 3 v3<br />
7 LIw <strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Ice Chest No, _ OZ<br />
Field No.<br />
Method Shipment<br />
ELL 95^k<br />
BESRAS6520 FED<br />
^O,S<br />
(:Fj RUNE SERRVICES LIONVILLE<br />
POSSIBLE SAMPLE HAZARDSIREMARKS<br />
POTENTIALRADIOACTlVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-266 Page 1 <strong>of</strong> j<br />
Collector<br />
TILLER, B. TR KLINCK<br />
oiect Designation<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Ice Chest NoX C_ _ O r<br />
Ae Q 7<br />
Comnanv Contact Telephone No.<br />
JOAN KESSNER<br />
Saamline Loca tion<br />
.199-Fh94 OFFAL<br />
375-4688<br />
7 —/74.z /^030-3 (7 yin<br />
Ft gL-1595<br />
k No.<br />
BESRAS6520<br />
Proiect Coordinator<br />
KESSNER, JH price Code 9th Data Turnaround<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
EXShipmenl<br />
FED<br />
S ' To G<br />
Offsitc Proverty No. 2<br />
AO 6 O ^„7 O<br />
Bi La<br />
ll<br />
EBERLPIE LIONVBIR<br />
<strong>of</strong> diWA r B ill No.<br />
SEE OSPC<br />
POS E HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-267 Page I <strong>of</strong> I<br />
Collector<br />
TALLER, B. TR KLINCKMAN<br />
Protect Desiena tion<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Ice Chest No.<br />
r<br />
7^ieC ^' .^' t7 d 3^<br />
Companv Contact Telephone No.<br />
JOAN KESSNER 375-4688<br />
Sampling Loca tion<br />
l lti-N -3 OFFAL /%0,30,3(7^2.D<br />
Field Loabook No.<br />
EL-1595<br />
Ship o Offsite Property No,<br />
ERLINESERVICES LIONVILLE ('Jf/ J C/<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-271 Page 1 <strong>of</strong> 1<br />
Collector<br />
TR.LER, B. TR KLINCKMAN<br />
oiect Designation<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Ice Chest No. n^- D^<br />
Field<br />
EL-15955<br />
No.<br />
Sid<br />
BERLINE SERVVIC^ES LIONVI LE<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE 7, Cesium-134, Cesium137,<br />
Cobalt-60, Epium152, uro Etucpium154, Europi155, um Poassium-40, Radium226, Radi228, um<br />
RutMnium106, Umsuum235, Umruum2381<br />
(2) Strontium-89,90 -- Total Sr; Is ot opic Tho rium lThorium2321; Isotopic Uranium lUramum-233234,<br />
Unnium235, Umniom2381; Isotopic Plutonium<br />
(3) ICP Metals -6010 (Full List) lAlumnum Antimony, Arsenic, Ba rium Beryl lium BismuW, Boron,<br />
Cadmium Cakium Chromium Cobalt, Copper, I ron, Lead, Litbium Magnesium Manga ne Relinquished By/Removed Prom Dale,Time<br />
A LOCKED STORAGE<br />
&<br />
se,<br />
Molybdenum Nickel, Phosphorus. Poussium Se lenium Silicon, Silver, Sodium Strontium Thallium<br />
Tin, Uranium Vanadium Zi nc 1; Mercury - 7471 - (CV)<br />
n /^<br />
e^lyed ored In ,<br />
/ F<br />
Date/Ti.<br />
e- // 1840<br />
R.hi,iqme Received By/Stored In<br />
D tte/rinn<br />
^I OO -^- /SO O ^^^<br />
Relinquished B<br />
Relinquished B<br />
ved F om<br />
ermved From<br />
Date/I'irrc<br />
DateM.<br />
Received B /St<br />
emived B St<br />
U<br />
d In<br />
D<br />
1Da<br />
?ime<br />
0<br />
D ite/rime<br />
- 1<br />
^Y^<br />
Relinquished By/Rerroved From Date/Time Received By/Stoed In Datelrime<br />
Relinquished By/Removed From Date/Tir ne received By/Stored In Date/Time<br />
LABORATORY<br />
SECTION<br />
Received By Tine DateTnx<br />
FINAL SAMPLE Disposal Meth d Disposed By Date/I'ime<br />
DISPOSITION<br />
BHI-EE-011 (08/29/2005)<br />
Mat ri x<br />
s_ i<br />
^sy;<br />
ode<br />
si=amre<br />
o-o,WyQ<br />
ns=o,ma s+m<br />
nuDmm Liam:<br />
r=ruu<<br />
Vqa d<br />
[<br />
v=v,t,nn<br />
x=0m.,
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-273 Page 1 <strong>of</strong> I<br />
Company Contact Telephone No. Proiect Coordinator<br />
Collector<br />
TILLER, B. TR KLINCKMAN<br />
JOAN KESSNER 375-4688 KESSNER, III<br />
rotect Desienation Sampline Location /,[/ ? ^I<br />
0 Q<br />
<strong>SAF</strong> No.<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti BORROW PIT 24 OFFAL /' OJ<br />
7 —1 W <strong>RC</strong>-<strong>047</strong><br />
Ice Cheat No. Q_QC --,J<br />
rG e,?. Qs_<br />
Field Loe ll ook No. COA Method <strong>of</strong> Shipment<br />
EL-1595 BESRAS6520 FED EX<br />
Shipped To Offshe Property No. ,l / Bi ll<br />
<strong>of</strong> LadiwJAir Bi ll<br />
No.<br />
BERLINE SERVICES LIONVILLE ^vIOO ,?j0 SEE OSPC<br />
POSSIBLE SAMPLE HAZARDSIREMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-274 Page I <strong>of</strong> I<br />
Collector<br />
Comnanv Contact Telephone No. Proiect Coordinator<br />
TILLER, B. TR KLINCKMAN<br />
JOAN KFSSNER 33775-4688 KESSNER, JH Price Code 9N Data Turnaround<br />
roiect Desiena tion Stranding Location /a ? IR<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti YAKIMA RIDGE II OFFAL 03(ly /'<br />
lee Chest No.^^ FieELLo9book<br />
No.<br />
7/J^O<br />
S -^ZS^ BESRAS6520<br />
<strong>SAF</strong> No.<br />
FED EXShioment<br />
M<br />
Slq Offsite Propertv No. Bill <strong>of</strong> Air B il l No<br />
BER INE SERVICES LIONV B.LE /7 SEE OSPC<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-275 Page I <strong>of</strong> I<br />
Collector Comaanv Contact Telephone No. Proieel Coordinator<br />
TILLER, B. TR KLINCKMAN JOAN KESSNER 375-4688 KESSNER, IH pr Price Co de 9N Data Turnaround<br />
roiect Desih aa tiun Samulin r Loca tion ^L 7°/2J <strong>SAF</strong> No.<br />
<strong>100</strong> & <strong>300</strong> A rea <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti VERNrrA UPRIVER ON SOUTH S JD 6PFAL <strong>RC</strong>-<strong>047</strong><br />
Ice Chest No.^-7<br />
Field Loe llook No. COA Method <strong>of</strong> Stdoment<br />
4^C - QZ ",7 r' S EL-1595 BESRAS6520 FED EX<br />
S ' o Offsite Pronerty No. Bi ll <strong>of</strong> Ladine/Air B ill No.<br />
BERLINE SERVICES IONVILLE fro6o 33 o SEE OSPC<br />
POSSIBLE SAMMIMARDSIREMARKS<br />
POTENTIAL RADIOACTIVE <br />
Kessner upon receipt.<br />
sr=wummi<br />
s WW<br />
Datelrime Ri=-o cl By/Stored In DateTtne<br />
(1)Gamma Spec-(Fu1Ws0 l Amencium-341, Antimony-125, Beryllium-7. Cesium- 134, Cesiu137,<br />
stis lud,<br />
W=W,or<br />
Relinquished7eeaved From Date?ime e, ed By/S red I "<br />
tt<br />
Dotell'ime<br />
Cobalt-60, Europium152, Europium154, Europium-155, Potassium-40, Radium 226,Radium228,<br />
Ru<strong>the</strong>nium-106, Uranium235. Uraniurrf381<br />
(2) S trontium-89,90 -- To cel Sr; Iso topic Thonum I Thonum-2321; Is<br />
a-ei<br />
Ds=Dwm sa i m<br />
ot opic Umnium 1Umnium-233234, Dt_D—L,r.d:<br />
Relinquished B emoved From Date/Ti. eceive By/Stored In Datell'ime<br />
Uranium-235, U ranium-2381; Isotopic Plu tonium<br />
(3) ICP Metals - 6010 (Full List) IAluminum Anumony, Arsenic, Banton Beryllium Bismuth, Boron<br />
Cadmium Calcium Chromium, Cobal t. Copper, Iron, Lead, Lithium Magnesium Manganese,<br />
Molybdenum Nickel, Phosphorus, Potassium Selenium Silicon Silver, Sodium S<br />
v w ^<br />
tr on ti Re um Thallium<br />
V,e<br />
earn m<br />
xmmR<br />
li nquished By/Removed From Datelflme Received By/Stored In Date?ime<br />
Tin, Uranium Va nadium Zinc 1; Memory - 7471 - (CV)<br />
Relinquished By/Renroved From DateMnic Received By/Stored In Darellime<br />
LABORATORY<br />
SECTION<br />
Received By Title Daterrime<br />
FINAL SAMPLE Disposal Method Disposed By Da re/Time<br />
DISPOSITION<br />
SHI-EE-011 (08/29/2005)
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-276 Page 1 <strong>of</strong> 1<br />
Collector<br />
TILLER, B. TN KLINCKMAN<br />
oiect Designation<br />
<strong>100</strong> & <strong>300</strong> Arcs <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Ice Chest No. p^<br />
Pifc C'0<br />
S EBE LINE SERV LIONVI.L.E<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE . •sM ^at ^<br />
7 'e _ 7/-z) /_fva<br />
R et d / W In DativTime<br />
flN ra"<br />
^GV f<br />
Received By/Stotxd In<br />
DateTre s<br />
p rice Code<br />
9N<br />
Air Quality L]<br />
Data Turnaround<br />
45 Days<br />
11.7Mat<br />
rix<br />
NOTE: Eberine- perform Gamma Spec <strong>the</strong>n tranship bottle to Lionville Labs, if possible maintain 4 C<br />
cooling. Lionville: perform metals, PCB,PEST,SVOC in this order as sample is available. Contact loan<br />
Kess ner upon receipt.<br />
(1) Gamma Spec - (Full Ust) ( Amenaum- 24 1, Andmony-M, Be ryllium7, Cesium 134, Cesium 137,<br />
Cobalt-60, Europium 152, Europium 154, Europium 155, Potassium40, Radium?26, Radium228.<br />
RusheNum 106, Urarum235, Uanium238)<br />
(2) Svondum89,90 - - Total Sr; Isotopic Tho rium ITho rium2321; Isotopic U ra nium (Uanium2331134,<br />
Uaniom235, Unniu238); m Isotopic Plu tonium<br />
(3) ICP Metals -6010 (Full Lisp (Aluminum, Antimony, Arsemq Barium, Be ry l lium Bismuth, Boron ,<br />
Cadmium Calcium Chromium. Cobalt, Copper, Iron, Lead, Lithium Mag nesium Manganese.<br />
Molybdenum Nickel, Phospho rus, Potassium Selenium Si li Relinquished emoved Fro Date?ime<br />
^<br />
Received B St In Da<br />
6d 1 1<br />
'1r^e<br />
Vlo<br />
r „ ,2<br />
/(^o<br />
Relinquished y/Removed R6 Date/Time Received B Stored In Da /Time<br />
Relinquished By/Remrved From Dat con, Silver, Sodium S trontium ThalBum<br />
Tin, Uranium, Vanadium Zinc It Mercury - 7471 - (CV)<br />
efr'°e Received By/Stored In DateMme<br />
Relinquished By/Removed From Date/Time received By/Stored In DateMme<br />
LABORATORY<br />
SECTION<br />
Received By Title Date?true<br />
FINAL SAMPLE Disposal Method Disposed By Date/Lime<br />
DISPOSITION<br />
BHI-EE-011 (08/29/2005)<br />
s=s,.t<br />
srrswmmt<br />
so=sate<br />
st=sim^<br />
w=w"a<br />
0-0.1<br />
os=D,^m sd^m<br />
DL.=onm t ,d,<br />
T=T °'°<br />
M-..,<br />
mL,amd<br />
v=vsgnwnn<br />
x=aha
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-277 Page J <strong>of</strong> J<br />
ollector_<br />
TILLER, B. R KLINCKMAN<br />
Project Destination<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Company Contact<br />
JOAN KESSNER<br />
Telephone No.<br />
375-4688<br />
Samolina Location r/ y g<br />
SADDLE MOUNTA IN OFFAL /) xo,3 7w<br />
Project Coordinator<br />
KESSNER, JH price Code 9N Data Turnaround<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Ice Chest No. fin _ Oz<br />
Field No. Method SIdpment<br />
EL-1595 BESRAS6520 FED EX<br />
S ed To Fi h<br />
LINE SERVIC LIONVB.LE<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-322 Page I <strong>of</strong> I<br />
Collector<br />
TIII R, B. TR KLINCKMAN<br />
Companv Contact<br />
JOAN KESSNER<br />
Telephone No.<br />
375-4688<br />
Prolect Coordinator<br />
KESSNER,JH Rice Code 9th Data Turnaround<br />
oicet Dedenation<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
SamuliLocation<br />
<strong>100</strong>-D-48:2 OFFAL<br />
^,/<br />
/<br />
<strong>SAF</strong> No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Air Quality E] 45 Days<br />
o 303 7<br />
Ice Chest No. + nG _ —r0<br />
Field Logbook No. COA Method <strong>of</strong> Shipment<br />
Li F^ S EL-1595 RESRAS6520 FED EX<br />
SlijMwd,To Offsite Pronertv No.<br />
RO / E ERLINE RVI LIONVILLE O U (f^(^<br />
BIB <strong>of</strong> Lading/Air Bill No.<br />
SEE OSPC<br />
POSSIBLE SAMPLE RAZARDS/REMARES<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-323 jPw J <strong>of</strong> 1<br />
Collector<br />
TILLER, B. TR KLINCKMAN<br />
Protect Designation<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Ice Chest No.<br />
—IrlleC — z 1 '&-675—<br />
Shinned To<br />
B RLINE SERVICE ILIONVILLE<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTEIVTIALRADIOAC77VE
i<br />
Washington Closure <strong>Hanford</strong> ' CHAIN OF CUSTODY/SAMPLYNNALYSIS REQUEST I <strong>RC</strong>-<strong>047</strong>-328 Page J <strong>of</strong> I<br />
Collector Companv Contact Telephone No. Project Coordinator<br />
TILLER, B. TR KLINCKMAN JOAN KESSNER 375-4688 KESSNER, IH Price Code 9N Data Turnaround<br />
roiect Desienation Sampline Location 2Q<br />
<strong>SAF</strong> No<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti 116-DR-I,DR-21<strong>100</strong>-D-22 OFFAL 11 0303 ^^<br />
<strong>RC</strong>-<strong>047</strong><br />
Ice Chest No. yn Field Loehook No. COA Method <strong>of</strong> Shipment<br />
Ift C-02 'ro,- EL-1595 BESRAS6520 FED EX<br />
Ship o Offsite Property No. Bill <strong>of</strong> Bi ll<br />
BERLINE SERVICES LIONVILLE<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
/O<br />
f7 (O6)<br />
atAir<br />
SEE OSPC<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> ` 'CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-330 INge "<br />
1 <strong>of</strong><br />
Collector<br />
Company Contact Tele rthane No. Project Coordinator<br />
TILLER, B. TR KLINCKMAN<br />
JOAN KESSNER 375-4688 KESSNER, lH<br />
!^0 303 7`I<br />
Pro j ect Designa tion Samp ling Loca tion<br />
<strong>SAF</strong> No.<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti BURROW PIT 23 OFFAL 2D<br />
<strong>RC</strong>-<strong>047</strong><br />
Ice Chest No. .<br />
/Z^C e^'.2 '-5"D sj<br />
Field Loebook No. COA Method <strong>of</strong> Shipment<br />
EL-1595 BESRAS6520 FED EX<br />
Price Code 9N Data Ttt<br />
Air Quality q<br />
S Offsite Property No. Bill <strong>of</strong> Lactim Av BBI No.<br />
EBERLWESERVICES LIONVILLE /T SEE -<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
.<br />
pa<br />
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALI YSIS REQUEST <strong>RC</strong>-<strong>047</strong>-332 ge L <strong>of</strong> L<br />
Collector<br />
TILLER, B. TR KLINCKMAN<br />
Project Designation<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti<br />
Com oanv Contact Telephone No.<br />
JOAN KESSNER 375-4688<br />
Sampline Location `'<br />
600-131 OFFAL IrC 3 - D-3 71.zo<br />
Project Coordinator<br />
KESSNER, JH Price Code 9N Data Turnaround<br />
SAY No.<br />
<strong>RC</strong>-<strong>047</strong><br />
Ice Chest No. Ft dpment<br />
Method St<br />
0,2 r^ 0 OS<br />
EL- 1595<br />
No.<br />
BCESRAS6520<br />
Air Quality E]<br />
45 Days<br />
Shi ed To /L<br />
Of isite Property No. n / ^J 2 g<br />
Bill#JAir pp<br />
Bill No.<br />
'INE SERVIC /LIONVILLE // OIpV 3r7 v<br />
SEE OSPC<br />
_<br />
POSSIBLE SAMPLE HAZARDSIREMARKS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REOUEST <strong>RC</strong>-<strong>047</strong>-343 Page J <strong>of</strong> 1<br />
Collector Comi)anv Contact Telephone No. Proiecl Coordinator<br />
TILLER, B. iH KLINCKMAN JOAN KESSNER 375-4688 KESSNER, JH<br />
roiect Desienation SampBne Loca tion A030<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti CENTRAL PLATEAU SHRUB STEPPE OFFAL<br />
<strong>RC</strong>-<strong>047</strong><br />
Ice Chest No. Field Loebook No. COA Method <strong>of</strong> Shipment<br />
are, —aZ^,JO ,J EL-1595 BESRAS6520 FED EX<br />
Shi Offsite Properly No , ,l a<br />
EBERLP]E SERVICES LIONVR.LE<br />
POSSIBLE LE HAZARDS/REMARKS<br />
POTENTIAL RADIOACTIVE
iIL7<br />
I-lien-<br />
tC, Il ri t"T-u ^`y<br />
RicHM6NII. LA I-A'aaRA-ra RY<br />
SAMPLE RECEFT CHECKL:S7<br />
Gity I" 'CP ^^rv^ S3^ ""<br />
u e Sit 2, , "-7,271 Z73 -7 r 274 >--7S z76<br />
No ^'^^ / 277 , 3Zy r 313 1 hzB 1 33 a 1332<br />
GareTime received fLIO^°<br />
I(^^^^Gor<br />
Gorrainer 1. â . N g C ^^ Z ^"" !;epunsted79 (Days) P.O. Received Yes [ J No [<br />
1<br />
q<br />
^.<br />
E_<br />
7 .<br />
e<br />
g .<br />
1D.<br />
11.<br />
73.<br />
t3.<br />
14.<br />
15.<br />
INSP°_C I-ION<br />
CLlstony seals on shippin g container Inract' Yes NO( j N1 I'tj • )<br />
/ gstnty seats on srnoptno comarner rated & sinned" Y es j No j j IQ /F. j<br />
Gusmay seats on sample conramers rl4aCt? Yes<br />
/ j WO j j iv/,=.<br />
CUMDay seats on sample comamen; raced & stone d? Yes J No j j N//- j<br />
Packing matenal is -. r /Wet ( 1 Li ^ yj<br />
Number or samples in snipping ccmarner. Sample MET x qj* 1 n-- gOUD<br />
Number <strong>of</strong> comamers per sam ple (Or see Go--<br />
L-^—<br />
Samples are In correct cor Amer Yes jV j No j j<br />
Paperwork, agrees with samotes? Yes ^< j No ( j<br />
Samples nav e -. i ape j j Hazard tabets j-) Pad tabets j ) Approonate sample iaoeis'-'4' j<br />
Samptes are -. In 000d condition (A Leaking [ j BrOKen Gomamer j j Missing [ j<br />
Samptes are. Preserved j J Not p reserved j j pH Pr°SanratlVE<br />
Describe any anoma lies.<br />
Was P.M. notified <strong>of</strong> any anomattes^ Yes ( j No j J Data<br />
1 .<br />
tnspecred by Dare: Q ^Y 7rm:: 7 '<br />
Cusmmer I I<br />
Sample NO.<br />
Ism<br />
I I Lusromer Samoee I f I<br />
mRrm Wipe No. rpm f mRlnr mree<br />
I I I I I<br />
I I ^ I I I'<br />
I I I I<br />
I I I I I I<br />
I I I f I I<br />
i I i I I I I<br />
I<br />
ion Chamber Ser. No Calibaion dal<br />
Ainna McTer Ser. No. Calibnmon cal<br />
Bem/Gamma Mazer Ser, No. Cajibznnn raL.<br />
Form 5 P-01. , D1-_ Oz<br />
j<br />
I<br />
over55 yeas D; Duajjry nucjearsermces"<br />
t
Joan Kessner<br />
WC-<strong>Hanford</strong><br />
3190 Washington Way<br />
MSIN H9-03<br />
Richland, WA 99354<br />
Subject: Analytical Data Package<br />
Dear Ms. Kessner:<br />
Enclosed are <strong>the</strong> hard copy analytical repo rts for <strong>the</strong> batch number/fraction indicated<br />
(marked X) in <strong>the</strong> following table:<br />
LvLI Batch .f.. j 0604L750<br />
................ DG..# ...............................-.K0303_....<br />
Date ..... Received 1 4/12/06<br />
. . . . . ... . . . . . . . . . .... - . . -.<br />
.. .. ............. ..<br />
Samples.............................. .......... ....^.5...........<br />
.<br />
. . . . . . . . . . . . . . . . . . . . . . . . . . . Mat\nx . . . . .. . . . . . . . .. . . . _ . . . . . . . . . . . . . O<strong>the</strong>r Solid<br />
Volatiles .....................................................................<br />
Semivolatiles I<br />
PAH<br />
Herbicides<br />
........... . ... . . . . . . ... . . . . . . . ........... I. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .<br />
Metals i X<br />
The electronic data deliverable (EDD) will be emailed sho rtly. If you have any<br />
qqestions, please don't hesitate to contact me at (610) 280-3012.<br />
cerely,<br />
iville L Incorporated<br />
Orlette S. Johnson<br />
Project Manager<br />
r:\group\pm\orle tte\tnu-hanford\data\b_ltrs.doc<br />
208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-<strong>300</strong>0 • Fax (610) 280-3041
DATE RECEIVED: 04/12/06<br />
CLIENT ID LVL #<br />
J11KR2 Oil<br />
LAB QC:<br />
PBLKGG MBl<br />
PBLKGG MB1 BS<br />
^ G4<br />
ca ^^`' 2C<br />
Lionville Laboratory, Inc. e Nt.:<br />
PEST/PCB ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303 \4cx<br />
LVL LOT # :0 2 WVS6<br />
r ^<br />
MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
SO 06LE0112 04/03/06 04/23/06 05/07/06<br />
S 06LE0312 N/A 04/23/06 05/03/06<br />
S 06LE0312 N/A 04/23/06 05/03/06<br />
tll<br />
000000001<br />
N
Case Narrative<br />
Client: TNU-HANFORD <strong>RC</strong>-<strong>047</strong> W.O. #: 11343-606-001-9999-00<br />
LVL #: 0604L750 Date Received: 04-12-2006<br />
SDG/<strong>SAF</strong> # K0303/<strong>RC</strong>-<strong>047</strong><br />
CHLORINATED PESTICIDES<br />
One (1) solid samples was collected on 04-03-2006.<br />
The sample and it's associated QC samples were extracted on 04-23-2006 and analyzed according<br />
to Lionville Laboratory SOPS based on SW846, 3rd Edition procedures on 05-03,07-2006. The<br />
extraction procedure was based on method 3540C and <strong>the</strong> extracts were analyzed based on method<br />
8081. All soil samples are reported on a dry weight base unless requested by <strong>the</strong> client, required by<br />
<strong>the</strong> method or noted o<strong>the</strong>rwise.<br />
The following is a summary <strong>of</strong> QC results accompanying <strong>the</strong> sample results. Lionville Laboratory<br />
Inc (LvLI) certifies that all test results meet <strong>the</strong> requirements <strong>of</strong> NELAC except as noted below:<br />
1. The sample was analyzed within required holding time.<br />
2. The sample was extracted 20 days outside <strong>of</strong> recommended hold time. A copy <strong>of</strong> <strong>the</strong><br />
Sample Discrepancy Report has been enclosed.<br />
The sample and it's associated QC samples received Copper-Sulfur cleanups according to<br />
Lionville Laboratory SOPS based on SW846 methods 3660A respectively.<br />
4. The method blank was below <strong>the</strong> reporting limits for all target compounds.<br />
Two (2) <strong>of</strong> six (6) surrogate recoveries were outside acceptance criteria. A copy <strong>of</strong> <strong>the</strong><br />
Sample Discrepancy Report (SDR) has been enclosed.<br />
6. The blank spike recoveries were within acceptance criteria.<br />
7. Matrix spike analyses are associated with LvLi lot 0604L748.<br />
8. The results for soil samples were reported on a wet-weight basis.<br />
9. The sample 011 required a 4-fold instrument dilutions due to matrix. Reporting limits have<br />
been adjusted to reflect <strong>the</strong> necessary dilutions.<br />
10. The initial calibrations associated with this data set were within acceptance criteria.<br />
The results presented in this report relate only to <strong>the</strong> analytical testing and wnditiona <strong>of</strong> <strong>the</strong> samples at receipt mid dining storage. All pages <strong>of</strong> this report are integral pans <strong>of</strong><br />
<strong>the</strong> analytical data. Therefore, flus report should only be reproduced in its entirety <strong>of</strong> 42 7 pages.<br />
208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-<strong>300</strong>0 • Fax (610) 280-3041<br />
MGMG88Z
11. The continuing calibration standards analyzed prior to sample extracts were within<br />
acceptance criteria.<br />
12. LvLI is NELAP accredited by <strong>the</strong> state <strong>of</strong> Pennsylvania and holds over 20 additional state<br />
accreditations. For a complete listing <strong>of</strong> accrediting authorities and <strong>the</strong> corresponding<br />
analytes/methods, please contact your Project Manager.<br />
13. I certify that this sample data package is in compliance with SOW requirements, both<br />
technically and for completeness, o<strong>the</strong>r than <strong>the</strong> conditions detailed above. Release <strong>of</strong> <strong>the</strong><br />
data contained in this hard-copy data package has been authorized by <strong>the</strong> laboratory<br />
Manager or a designee, as verified by <strong>the</strong> following signature.<br />
Laboratory Manager<br />
Lionville Laboratory Incorporated<br />
Idmtr:\VoupWata\pest\mu ha,ifotd\0604-750.pst<br />
vLl<br />
,-511(10P<br />
Date
Lionville Laboratory Sample Discrepancy Repo rt (SDR) SDR#: 6YGC. 1447<br />
Initiator. Batch: arm. N-»^aParameter.<br />
Date: c Samples.. ^J Matrix:<br />
Client: gW Prep Batch:<br />
^^<br />
1. Reason for SDR<br />
a. CDC Discrepancy _ Tech Pr<strong>of</strong>ile Er ror Client RequestSampler E rror on C-O-C<br />
Transcription Error _ Wrong Test Code _ O<strong>the</strong>r<br />
b. General Discrepancy<br />
_ Missing Sample/Extract _ Container B roken — Wrong Sample Pulled _ Label ID's Illegible<br />
Hold Time Exceeded Insufficient Sample _ Preservation Wrong _ Received Past Hold<br />
_ Improper Bottle Type _ Not Amenable to Analysis<br />
Note": Vwffled by Rmg-ln] or [Prep Grout) (drde) ... slgnaturerdate:<br />
c. Problem (Include all relevant speci fic raspdata if necessary)<br />
2. Known or Probable Causes(s)<br />
^(4p<br />
3. Discussion and Proposed Action O<strong>the</strong>r Description:<br />
_ R<br />
_ En ti re Batch<br />
Following Samples:<br />
_ Re-leach<br />
_ Re-extract<br />
_ Re-digest<br />
_ Revise EDD<br />
Change Test Code to<br />
_ Place On/Take Off Hold (circle)<br />
4. Project Manager Instructions ... slpnatwddate:<br />
_ Concur with P roposed Ac tion<br />
_ Disagree wi th Proposed Action; See Instruc ti on<br />
_ In clude in Case Narrative<br />
_ Client Contacted:<br />
Date/Person<br />
_ Add<br />
Cancel<br />
cet.7 ^(s+-^- CY -fie 4--- F-N-r-..^o^^<br />
5. Final Action... algnaturardate: O<strong>the</strong>r Explanation:<br />
Verified re-[logJ[IeaehJ[extractJ[dig ysr5 (d te)<br />
7.X ad In Case Narrathre<br />
_ Hard Copy COC Revised<br />
Elect ro nic COC Revised<br />
_ EDD Corrections Completed<br />
When Final Ac ti on has been recorded, forward original to QA Specialist for distribution and filing.<br />
Route Distribution <strong>of</strong> Completed SDR Route Distribu ti on <strong>of</strong> Completed SDR<br />
X Initiator _ Metals: Beegle<br />
X Lab General Manager. M. Taylor _ Inorganic: Perrone<br />
X P roject Mgr: Stone/Johnson _ _ _ GC/LC: IGger<br />
Data Management: Stilwell _ MS: Rychlak/Daley<br />
_ Sample P rep: Beeglel4ger _ _ Log-in: Per ry<br />
_ _Admin:<br />
O<strong>the</strong>r.<br />
OA-1 05-A-0805<br />
A
VLY=LM=1W<br />
DATA OUALIF'IERS<br />
GLOSSARY OF DATA<br />
U = Indicates that <strong>the</strong> compound was analyzed for but not detected. The minimum detection limit for <strong>the</strong><br />
sample (not <strong>the</strong> method detection ]unit) is reported with <strong>the</strong> U (e.g., I Op.<br />
J = Indicates an estimated value. This flag is used in cases where a target analyte is detected at a level<br />
less than <strong>the</strong> lower quantification level.. If <strong>the</strong> limit <strong>of</strong> quantification is 10 ug/L and a concentration<br />
<strong>of</strong> 3 ug/L is calculated, it is reported as 33.<br />
B = This flag is used when <strong>the</strong> analyte is found in <strong>the</strong> associated blank as well as in <strong>the</strong> sample. It<br />
indicates possible/probable blank comemination.<br />
E<br />
I = Interference.<br />
Indicates that <strong>the</strong> compound was detected beyond <strong>the</strong> calibration range and was subsequently<br />
analyzed at a dilution.<br />
1 = Indicates an interference on one analytical column only. Result is reported from remaining analytical<br />
column.<br />
ABBREVIATIONS<br />
BS = Indicates blank sprite in which reagent grade water is spiked with <strong>the</strong> CLP matrix spiking solutions<br />
and carried through all <strong>the</strong> steps in <strong>the</strong> method. Spike recoveries are reported.<br />
BSD = Indicates blank spike duplicate.<br />
MS = Indicates matrix spike.<br />
MSD =<br />
Indicates matrix spike duplicate.<br />
DL = indicates that recoveries wen not obtained because <strong>the</strong> extract had to be diluted for analysis.<br />
NA = Not Applicable.<br />
DF<br />
Dilution Factor.<br />
NR Not Required.<br />
NS = Not Spiked.<br />
SP Indicates Spiked Compound.<br />
P = This flag is used for an PESTTCIDE/PCB target analyte when <strong>the</strong>re is greater than 25%<br />
difference for detected concentrations between <strong>the</strong> two GC columns (see Form X). The<br />
Iowa <strong>of</strong> <strong>the</strong> two values is reported on Form I and flagged with a'P'.<br />
D Ibis flag identifies all compounds identified in an analysis at a secondary dilution factor.<br />
C This flag applies to a compound that has been confirmed by GOMS.<br />
NPM = No patient match for mull-component target analytes.<br />
000000005
.....,.. +i.a ua Vlaw+:y, XK&C.<br />
Pesticide/PCBs by GC, CLP List Report Date: 05/11/06 13:19<br />
RFW Batch Number: 0604L750 Client, TNUHANPORD <strong>RC</strong>-<strong>047</strong> K0303 Work Order: 11343606001 Page: 1<br />
Cust ID: J11KR2 PBLKGG PBLKGG BS<br />
Sample RFW#: 011 06LE0312 -NB1 06LE0312-NB1<br />
Information Matrix: SOLID SOIL SOIL<br />
D.F.: 4.00 1.00 1.00<br />
Units: UG/KG UG/KG UG/KG<br />
Surrogate: Tetrachloro-m-xylene 177 * t 106 t 117<br />
Decachlorobiphenyl 173 * t 88 % 96 t<br />
____'________________________________________ fl=====__=====f1=====__===== f1=====__=====f1=====__=====f1=====___====£1<br />
Alpha-BHC 40 U 0.33 U <strong>100</strong><br />
gamma-BHC (Lindane) 40 U 0.33 U 97 t<br />
Beta-BHC 40 U 0.33 U <strong>100</strong> t<br />
Heptachlor 40 U 0.33 U 92 t<br />
Delta-BHC 40 U 0.33 U 89 t<br />
Aldrin 40 U 0.33 U 78 %<br />
Heptachlor epoxide 40 U 0.33 U 90<br />
gamma-Chlordane 40 U 0.33 U 90 %<br />
Endosulfan I 40 U 0.33 U 90 %<br />
alpha-Chlordane 220 .I 0.33 U 89 t<br />
4,4'-DDE 40 U 0.33 U 92 %<br />
Dieldrin 40 U 0.33 U 92 %<br />
Endrin 40 U 0.33 U 96 %<br />
4,4'-DDD 40 U 0.33 U 96 t<br />
Endosulfan II 40 U 0.33 U 89 %<br />
4,4'-DDT 40 U 0.33 U 87 %<br />
Endrin aldehyde 40 U 0.33 U 85 %<br />
Endosulfan sulfate 40 U 0.33 U 86 %<br />
Methoxychlor 40 U 0.33 U 90 t<br />
Endrin ketone 40 U 0.33 U 87 %<br />
Toxaphene 400 U 3.3 U 3.3 U<br />
U= Analyzed, not detected. J= Present below detection limit. B= Present in blank. NR= Not reported. NS= Not spiked.<br />
%= Percent recovery. D= Diluted out. I= Interference. NA= Not Applicable. *= Outside <strong>of</strong> EPA CLP QC<br />
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<strong>100</strong>& 30D <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti McGEE RANCH INVERTEBRA TES<br />
<strong>RC</strong>-<strong>047</strong><br />
G<br />
ice C6eet No Field Lpakook No. COA Method <strong>of</strong> Shimncot<br />
m<br />
07 EL- 1595 BESRAS6520 FED EX m<br />
Shipped To Ofbik Properly No. /1O6 Q 2s-/ Bill <strong>of</strong> LadindAir Bill No-<br />
EBERLESERVIC IN<br />
LIONVILIE ' .7 ^" SEE OSPC<br />
POSSIBLE SAMPLE IiA RSS -- .-- --- ---<br />
PO7ENTIALRADJOACJ7VE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REOUFST <strong>RC</strong>-<strong>047</strong>-321<br />
° TR KLIflf:KMAN Company Contact Telephone No. Proiect Courduwtelr<br />
TILLER, B. JOAN KE.SSNER' 375.4688 KESSNER, Ili Ptice Code 9N<br />
Oatu'1'un::n-mtudp.<br />
Proleet Dedamillon Samodua Location <strong>SAF</strong> No.<br />
Air Qttality q YJ Days<br />
<strong>100</strong> & <strong>300</strong> Am Compoment <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti SADDLE MOUNTA<br />
0 '<br />
IN INVERTEBRATES <strong>RC</strong>-<strong>047</strong> m<br />
Ice Cheat No, Field Loahuok No. COA Method <strong>of</strong> Shipment<br />
0 7 EI. 1595 BESRAS6520 FED EX<br />
Shipped To,<br />
EBERLINESERVIC ONVRIE<br />
Othite Property No.<br />
Ao60 3tS<br />
Bi ll <strong>of</strong> Ladine/Air Bill No.<br />
SEE OSPC<br />
POSSIBLE SAMPLE HAZARDS/REMARKS<br />
POTENTJAL RAD/OAC77VE
Washinoton Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-31 a 1'a e<br />
olleetar . CommarContact<br />
T eleohone<br />
TR KLINCKMAN<br />
No. Proiect Coordinator<br />
TILLER, B. ^<br />
JOAN KESSNER 375-4668 KESSNER, JH Yricc Code t DaL•r 7lornaruuud<br />
00<br />
. rolectIlleslumitton SamoBne LOUfdoB 160;9jf^^ <strong>SAF</strong> No.<br />
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m<br />
<strong>RC</strong>-<strong>047</strong> 19<br />
)N<br />
Air Quality 0 4 5 Days<br />
let Chest No.<br />
Fld No, COA Method <strong>of</strong> Shioneat W<br />
, ! Re e2 ` ff'O 7 EL- 1595 BESRAS6520 FED EX m<br />
S Eyed To SERVICES ONVBllr<br />
Offsite Ptnoerts No. NO^ ^^ O<br />
f1<br />
BiB <strong>of</strong> Ladioa/Air Bill No.<br />
SEEOSPC<br />
m<br />
POSSIBLE SAMPLE HAZARD.S/AEMAR ICS<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-303 ?-1e'c = n(<br />
Collector - Comoany Contact Teleohone No. Protect Coordinator<br />
TRIER, B. XM Xi wrKMAN JOAN KESSNER 375-4688 KESSNER, JH Price Code 9N Win Turnaround<br />
olecl Desfanaaon Saaaoli=Lo ti= <strong>SAF</strong> No. Alr Quality 45 Days m<br />
<strong>100</strong> & <strong>300</strong> Am <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti 6M132/WD-190 INVERTEBRATES <strong>RC</strong>-(M7<br />
O<br />
0<br />
Ice Chat No. n Field Loahook No. COA Method <strong>of</strong> SI»ometst m<br />
7 641595 BESRAS6520 FED EX m<br />
Shinned To<br />
EBERLINESERVICPS uONVn.in<br />
POSSIBLE SAMPLE HAZARWRF.MARKS<br />
I<br />
Offaite Pronerp No '/<br />
603^^<br />
BID <strong>of</strong> Ladin2/Air BRI No.<br />
SEE OSPC<br />
POTEWML RADIOACTIVE
-i<br />
Washington C osure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-345 1•:,g,. w<br />
Collector<br />
TILLER, B. TR KLIKKKAN<br />
Commany Contact Telephone No.<br />
JOAN KFSSNER 375-4688<br />
Proiecl Coordinator<br />
KESSNER, JH Price Code 9N Data Turnaround<br />
m<br />
Air Quality I,_f 4^ B2<br />
y'<br />
i (V<br />
9<br />
Protect Deshmation Sampling Lo cation <strong>SAF</strong> No.<br />
LBO & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sedim cat and Ti CENTRAL PLATEAU SHRUB STEPPE INVERTEBRATES <strong>RC</strong>-<strong>047</strong> 6<br />
Ice Chtat No. // -+.<br />
y07<br />
Fleld Logbook No. COA Method FEDEXSItioment<br />
EL- 1595 BESRAS6520<br />
Shipped To<br />
EBERLINE SERVICESONVUlE<br />
ORgite ProDWO No.<br />
060<br />
Bill <strong>of</strong> Ladinp/Air Bi ll No.<br />
SEE OSPC<br />
POSSIBLE SAMPLE HAZARDS/REMARKS ------ - _. --. - - - -<br />
POTENTIALRADIOACTJVE
s -<br />
Washington Closure <strong>Hanford</strong> CHAIN OF CUST01Y/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-342 ,'ng i n<br />
ector<br />
Coany mp Cemtact Telephone No.<br />
Proiect Coordinator<br />
TR KLINCKMAN<br />
JOAN<br />
MCC Cade 9N a)ata'1'unm ruwuh<br />
TILLER, B. KESSNER 375-4688 KESSNER, JH<br />
T^ N<br />
ieel Deslenalion Sampling Location <strong>SAF</strong> No.<br />
45 D"-Ys<br />
Air Quality<br />
m '.<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> Compm cut <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and n 600-131 INVERTEBRATES <strong>RC</strong>-<strong>047</strong> q<br />
m<br />
Ice Chest No. p<br />
/y .QC-Ol 0<br />
Field Loebook No. COA Method <strong>of</strong> Sldument<br />
-7 EL-1595 BESRAS6520 FED EX m<br />
m<br />
Shioced To Onsite Property No. ^y Bill <strong>of</strong> Ladiae/Air Bi ll No.<br />
EBERLINE SERVICES VB1E SEE OSPC<br />
POSSIBLE SAMPLE HAMAIJ) /REMARES -- --<br />
POTENTIAL RADIOACTIVE
Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>.340 l'agc ! ar !<br />
Collector<br />
TR KUNCKMAN<br />
Company Contact Telephone No. Proicet Coordinator<br />
TILLER, B. - JOAN KPSSNER 375-4688 Price Code yN Data Turrarotuw,N<br />
KESSNER, IH<br />
a<br />
Protect et IJel[mtlon<br />
SampWU lg Load" tl<br />
<strong>SAF</strong> No.<br />
Days<br />
Ail• Quality ^_l`'3"m<br />
<strong>100</strong> A <strong>300</strong> Arm Coripaoenl <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti BORROW PIT 23 INVERTEBRATES <strong>RC</strong>-<strong>047</strong> m<br />
Ice Chat No.<br />
ArieG ^Q,7 - O'<br />
Field Loeb" No.<br />
1141595<br />
COA Method <strong>of</strong> Shipment m<br />
BESRAS6520 FED EX<br />
m—<br />
m<br />
Shipped To Offaita Property No. .2 q Bill <strong>of</strong> Ladine/Air Bill No.<br />
EBERLINE SERVICESell SEEOSPC<br />
POSSIBLE SAMPLE HAZA RKS<br />
POTENTIALRADIOACTIVE
Washington Closu re <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>.335 ;Ace ! u<br />
Collector<br />
- Comanv Contact Telephone No. Proiect Coordinator<br />
T11.1-11R, B. AR JOAN KESSNER 375-4688 KESSNER, JH Price Code 9N llxta -furn:u•owsd<br />
M<br />
Protect Desienat)on Sanmllne Location <strong>SAF</strong> No.<br />
45 D<br />
Air Quality q<br />
a V S N<br />
9<br />
<strong>100</strong> A <strong>300</strong> Ara Compoteot <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sedisneat and Ti 116-DR-i, DR-Tl1lK1-0.22 INVP.RTEBRATES <strong>RC</strong>-<strong>047</strong> m<br />
Ice Chat No. Xwe —<br />
Fi el d Umbook No. COA Method <strong>of</strong> Shioment m<br />
EI- 1395 BESRAS6520 FED EX m<br />
Shipped To O/fdhe Property No. nom/ Bill <strong>of</strong> Ladine/Air Bi ll No. m<br />
EBERLINE SERVICES llONVn 7F " C23^ SEE OSPC<br />
POSSIBLE SAMPLE HAZA RKS<br />
POTEN77ALRADIOAC77VE
1_ Samples Hand Delivered orhippe<br />
Lionville Laboratory Incorporated<br />
SAMTLE RECEIPT CHECKLIST (S<strong>RC</strong>)<br />
CLIENT:-T ISU VA4r-,Coe- P Date: 4- la• d-<br />
P chase Order/ Project# / R C.O+-4'7<br />
CAF#' SOW#/Release#:<br />
LvLI Batch 9 : h ` 1 —7 ^ Sample Custodian:<br />
2. Custody seals on coole rs or shipping<br />
container intact, signed and dated?<br />
l 1 t n f Y^L I GJIJ<br />
NOTE: EXPLAIN ALL DISCREPANCIES /<br />
3. Outside <strong>of</strong> coolers or shipping containers are<br />
free from damage?<br />
4. All expected paperwork received (coc and<br />
o<strong>the</strong>r client specific information) sealed in<br />
plastic bag and easily accessible?<br />
5. Samples receiver ambient?<br />
6. Custody seals on sample containers intact,<br />
signed and dated?<br />
7. coc signed and dated?<br />
3. Sample containers are intact?<br />
9. All samples on coc received? AL samples<br />
received on coc?<br />
10. All sample label information matches coc?<br />
11. Samples properly preserved?<br />
12. Samples received within bold times?<br />
Short holds taken to wet lab?<br />
a-M-B<br />
13. VOA, TOC, TOX free <strong>of</strong> headspace?<br />
14. QC stickers placed on bottles designated by<br />
client?<br />
13. Shipment meets LvLI Sample Acceptance<br />
Po licy? (Identify all bottles cot within<br />
policy. See reverse side for policy)<br />
16. Project Manager contacted concerning<br />
discrepancies? nameldate (or samples<br />
outside criteria)<br />
^Lr<br />
Airbili# —IgD3 169-11 -)- 1-q<br />
G(Yes ONO O No Seals Comments<br />
VYes ONO<br />
IXYes O No<br />
Temp ^.8 OC Cooler # F—K4 'Oa • 4
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
1234ss)<br />
^ N ti^ N<br />
^Pyw<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L ^Ol 816<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
J11KV5<br />
SILVER, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SILVER, TOTAL 001 REP SO 06L0284 04 /03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
ALUMINUM, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ARSENIC, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 001 REP SO 06L0284 04 /03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL REP 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL _ 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 001 REP SO 06L0264 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 001 SO 0600080 04/03/06 04/27/06 04/27/06<br />
ME<strong>RC</strong>URY, TOTAL 001 REP SO 0600080 04 /03/06 04/27/06 04/27/06<br />
ME<strong>RC</strong>URY, TOTAL 001 MS SO 0600080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
POTASSIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 001 SO 06L0284 04/03/06 05/09/06 .05/09/06<br />
LITHIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
000000001
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
MANGANESE,.TOTAL 001 SO 06LO284 04/03/06 05/09/06 - 05/09/06<br />
MANGANESE, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06<br />
PHOSPHORUS, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
PHOSPHORUS, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
LEAD, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 001 REP SO 06-LO284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 001 REP SO 06LO284 04/03/06 05/09/06 05/09/06.<br />
URANIUM, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 001 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 001 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 001 REP SO 06L0284 04/03/06 05/09/06 05/12/06<br />
J11KV6<br />
SILVER, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SILVER, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
000000002
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
ALUMINUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 002 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ARSENIC, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 002 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 002 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 002 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 002 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL SPIKE 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 002 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 002 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 002 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 002 SO 0600080 04/03/06 04/27/06 04-/27/06<br />
POTASSIUM, TOTAL 002 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
POTASSIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 002 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 002 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 002 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL. 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
000000003
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
PHOSPHORUS, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
PHOSPHORUS, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
LEAD, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 002 MS SO 06L0264 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 002 MS SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 002 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 002 MS SO 06L0284 04/03/06 05/09/06 05/12/06<br />
J11KT0<br />
SILVER, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 003 S0 06LO284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
000000004
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :06041,750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
COPPER, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 003 SO 0600080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
PHOSPHORUS, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 003 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 003 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
J11KT4<br />
SILVER, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 004 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 004 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 004 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 004 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 004 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 004 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 004 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
000000005
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :06041,750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
ME<strong>RC</strong>URY, TOTAL 004 SO 0600080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 004 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 004 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 004 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 004 SO 06LO284 04/03/06 05/09/06 0,5/09/06<br />
PHOSPHORUS, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 004 SO 06L0264 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 004 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 004 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 004 SO 061,02B4 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 004 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
J11KT6<br />
SILVER, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 005 $O 06L0284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 005 SO 0600080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
000000006
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
LITHIUM, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
PHOSPHORUS, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 005 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 005 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
J11KT7<br />
SILVER, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 006 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 006 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 006 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 006 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 006 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL, 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 006 50 0600080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 006 SO 06L02B4 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 006 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 006 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
000000007
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
MANGANESE, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
PHOSPHORUS, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 006 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 006 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 006 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 006 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 006 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
J11KT8<br />
SILVER, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 007 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 007 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 007 SO 0600080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
000000008
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE.FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
SODIUM, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 007 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
PHOSPHORUS, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 007 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 007 SO 06L0284 - 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 007 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 007 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 007 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 007 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 007 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 007 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 007 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 007 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
J11KT9<br />
SILVER, TOTAL 008 SO 06L0284 . 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 008 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 008 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 008 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 008 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 008 SO 0610284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 008 SO 0600080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
000000009
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
PHOSPHORUS, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 008 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 008 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 008 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 008 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 008 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
J11KVO<br />
SILVER, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL - 009 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 009 SO 0600080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
PHOSPHORUS, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
000000010
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
ANTIMONY, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 009 SO 06L0264 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 009 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 009 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
J11KR9<br />
SILVER, TOTAL 010 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 010 SO 0600080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
PHOSPHORUS, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
000000011
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
SILICON, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 010 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
J11KR2<br />
SILVER, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL O11 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL O11 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL O11 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL O11 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL O11 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL O11 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 011 SO 0600080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
PHOSPHORUS, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL Oil SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL Oil SO 06L0284 04/03/06 05/09/06 05/09/06<br />
000000012
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :06041,750<br />
CLIENT ID /ANALYSIS LVL # MIX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
STRONTIUM, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 011 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 011 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 011 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
JllL38<br />
SILVER, TOTAL 012 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 012 SO 06LO264 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 012 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 012 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 012 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 012 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 012 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 012 SO 06CO080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 012 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 012 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
PHOSPHORUS, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
000000013
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
URANIUM, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 012 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 012 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 012 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
JlIL35<br />
SILVER, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 013 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 013 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 013 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 013 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 013 $O 06L0284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 013 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 013 SO 0600080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
PHOSPHORUS, TOTAL 013 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 013 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 013 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 013 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
000000014
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
ZINC, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 013 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
JIIL33<br />
SILVER, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 014 SO 0600080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
PHOSPHORUS, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 014 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 014 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
000000015
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :06041,750<br />
CLIENT ID /ANALYSIS LVL # MIX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
J11L31<br />
SILVER, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ALUMINUM, TOTAL 015 SO 06LO284 04/03/06 05/09/06 05/12/06<br />
ARSENIC, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BORON, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BARIUM, TOTAL 015 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
BISMUTH, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
CALCIUM, TOTAL 015 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CADMIUM, TOTAL 015 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
COBALT, TOTAL 015 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
CHROMIUM, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
COPPER, TOTAL 015 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
IRON, TOTAL 015 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY, TOTAL 015 SO 0600080 04/03/06 04/27/06 04/27/06<br />
POTASSIUM, TOTAL 015 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
LITHIUM, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
MANGANESE, TOTAL 015 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL 015 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SODIUM, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
NICKEL, TOTAL 015 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
PHOSPHORUS, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
LEAD, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ANTIMONY, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
SELENIUM, TOTAL 015 SO 06LO284 04/03/06 05/09/06 05/09/06<br />
SILICON, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
TIN, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
STRONTIUM, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
THALLIUM, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
URANIUM, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
VANADIUM, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZINC, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL 015 SO 06L0284 04/03/06 05/09/06 05/12/06<br />
LAB QC:<br />
SILVER LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06<br />
000000016
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS<br />
SILVER, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
ALUMINUM LABORTORY LC1 BE S 06LO284 N/A 05/09/06 05/12/06<br />
ALUMINUM, TOTAL MB1 S 06L0284 N/A 05/09/06 05/12/06<br />
ARSENIC LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06<br />
ARSENIC, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
BORON LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06<br />
BORON, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
BARIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06. 05/09/06<br />
BARIUM, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
BERYLLIUM LABORATORY LC1 BE S 06L0284 N/A 05/09/06 05/09/06<br />
BERYLLIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
BISMUTH, LCS LC1 BE S 06L0284 N/A 05/09/06 05/09/06<br />
BISMUTH, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
CALCIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06<br />
CALCIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
CADMIUM LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06<br />
CADMIUM, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
COBALT LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06<br />
COBALT, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
CHROMIUM LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06<br />
CHROMIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
COPPER LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06<br />
COPPER, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
IRON LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06<br />
IRON, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
ME<strong>RC</strong>URY LABORATORY LC1 BS S 0600080 N/A 04/27/06 04/27/06<br />
ME<strong>RC</strong>URY, TOTAL MB1 S 06C0080 N/A 04/27/06 04/27/06<br />
POTASSIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06<br />
POTASSIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
LITHIUM LABORATORY LC1 BE S 06LO284 N/A 05/09/06 05/09/06<br />
LITHIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
MAGNESIUM LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06<br />
MAGNESIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
MANGANESE LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06<br />
MANGANESE, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
MOLYBDENUM LABORATOR LC1 BS S 06L0284 N/A 05/09/06 05/09/06<br />
MOLYBDENUM, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
SODIUM LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06<br />
000000017
Lionville Laboratory, Inc.<br />
INORGANIC ANALYTICAL DATA PACKAGE FOR<br />
TNUHANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
DATE RECEIVED: 04/12/06 LVL LOT # :0604L750<br />
CLIENT ID /ANALYSIS LVL # MTX PREP #1 COLLECTION EXTR/PREP ANALYSIS<br />
SODIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
NICKEL LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06<br />
NICKEL, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
PHOSPHORUS LCS LC1 BS S 06L0284 N/A 05/09/06 05/12/06<br />
PHOSPHORUS, TOTAL MB1 S 06L0284 N/A 05/09/06 05/12/06<br />
LEAD LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06<br />
LEAD, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
ANTIMONY LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06<br />
ANTIMONY, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
SELENIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06<br />
SELENIUM, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
SILICON LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06<br />
SILICON, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
TIN LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06<br />
TIN, TOTAL MB1 S 06L0284 N/A 05/09/06 05/09/06<br />
STRONTIUM LCS STANDA LC1 BS S 06L0284 N/A 05/09/06 05/09/06<br />
STRONTIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
THALLIUM LABORATORY LC1 BS S 06L0284 N/A 05/09/06 05/09/06<br />
THALLIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
URANIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06<br />
URANIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
VANADIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06<br />
VANADIUM, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
ZINC LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/09/06<br />
ZINC, TOTAL MB1 S 06LO284 N/A 05/09/06 05/09/06<br />
ZI<strong>RC</strong>ONIUM LABORATORY LC1 BS S 06LO284 N/A 05/09/06 05/12/06<br />
ZI<strong>RC</strong>ONIUM, TOTAL MB1 S 06L0284 N/A 05/09/06 05/12/06<br />
000000018
Client: TNU-HANFORD <strong>RC</strong>-<strong>047</strong> W.O.#: 11343-606-001-9999-00<br />
LVL#: 0604L750 Date Received: 04-12-06<br />
SDG/<strong>SAF</strong>#: K1428/<strong>RC</strong>-<strong>047</strong><br />
METALS CASE NARRATIVE<br />
The following is a summary <strong>of</strong> <strong>the</strong> QC results accompanying <strong>the</strong> sample results. Lionville<br />
Laboratory (LvLI) certifies that all test results meet <strong>the</strong> requirements <strong>of</strong> NELAC except as noted<br />
below.<br />
All soil samples are reported on a dry weight basis unless requested by <strong>the</strong> client, required by <strong>the</strong><br />
method, or noted o<strong>the</strong>rwise.<br />
1. This narrative covers <strong>the</strong> analyses <strong>of</strong> 15 solid samples.<br />
2. The samples were prepared and analyzed in accordance with methods checked on <strong>the</strong> attached<br />
glossary. The samples are reported on a wet weight, ` as received' b asis.<br />
In file HG042701 for Mercury, sample J11KT6 read 2.07 µg2 in <strong>the</strong> digestate, followed by<br />
sample J11KT7, which read -0.728 µg/L in <strong>the</strong> digestate. These 2 samples were rerun in file<br />
HG050401 (3 days p ast hold) to confirm <strong>the</strong> results. Initially, J11KT6 read 4.48 µg/L, and<br />
J11KT7 read -2.73 µg/L. The CCB following <strong>the</strong>se samples dropped to -0.226 gg/L. The<br />
instrument was recalibrated, and <strong>the</strong>se 2 samples rerun once again, with 5-fold dilutions, and<br />
each followed by a blank. In this file, HG050402, both read between -0.1 and 0.1 µg/L.<br />
Results from HG042701 were reported, which were within <strong>the</strong> hold time for Mercu ry .<br />
3. All analyses were performed within <strong>the</strong> required holding times.<br />
4. All Initial and Continuing Calibration Verifications (ICV/CCVs) were within <strong>the</strong> 90-110%<br />
control limits (80-120% for Mercury).<br />
5. All Initial and Continuing Calibration Blanks (ICB/CCBs) were within control limits (less<br />
than <strong>the</strong> PQL).<br />
6. All preparation/method blanks (MB) were within method crite ria {less than <strong>the</strong> Practical<br />
Quantitation Limit (3X <strong>the</strong> IDL), or samples greater than 20X MB value). Refer to <strong>the</strong><br />
Inorganics Method Blank Data Summary .<br />
7. All ICP Interference Check Standards were within control limits.<br />
The re su lt<br />
s presented in this report relate only to <strong>the</strong> analy tical testing and conditions <strong>of</strong><strong>the</strong> samples at receipt and during storage. All pages <strong>of</strong>this report are<br />
integral parts <strong>of</strong> <strong>the</strong> analytical data The refo re , this re port should only be reproduced in its entirety <strong>of</strong> (pO pages.<br />
208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-<strong>300</strong>0 • Fax (610) 280-3041<br />
44?R€'ir'!^#41 t?f
8. All laboratory control samples (LCS) were within <strong>the</strong> 80-120% control limits with <strong>the</strong><br />
exception <strong>of</strong> Silicon at 31.2%. Refer to <strong>the</strong> Inorganics Laboratory Control Standards Report.<br />
Associated sample results may be biased low.<br />
9. The matrix spike (MS) recoveries for 4 analytes were outside <strong>the</strong> 75-125% control limits.<br />
Refer to <strong>the</strong> Inorganics Accuracy Report.<br />
10. For analytes where <strong>the</strong> ICP MS is out-<strong>of</strong>-control, a post-digestion MS (PDS) and serial<br />
dilution are performed. A PDS was not performed for Zinc. A PDS was prepared at<br />
meaningful concentration level for <strong>the</strong> following analytes:<br />
PDS PDS<br />
Sample ID Element Concentration (onb) % Recovery<br />
J11KV6 Iron 22,000 101.9<br />
Phosphorous 4,000 110.5<br />
Zirconium 200 <strong>100</strong>.4<br />
11. The duplicate analyses for 8 analytes were outside <strong>the</strong> 201/6 Relative Percent Difference<br />
(RPD) control limits. Refer to <strong>the</strong> Inorganics Precision Report.<br />
12. For <strong>the</strong> purposes <strong>of</strong> this report, <strong>the</strong> data has been reported to <strong>the</strong> Instrument Detection Limit<br />
(IDL). Values between <strong>the</strong> IDL and <strong>the</strong> Practical Quantitation Limit (PQL) are acquired in a<br />
region <strong>of</strong> less-certain quantification.<br />
13. LvLI is NELAP accredited by <strong>the</strong> state <strong>of</strong> Pennsylvania and holds over 20 additional state<br />
accreditations. For a complete listing <strong>of</strong> accrediting authorities and <strong>the</strong> corresponding<br />
analytes/methods, please contact your Project Manager.<br />
14. I certify that this sample data package is in compliance with SOW requirements, both<br />
technically and for completeness, o<strong>the</strong>r than <strong>the</strong> conditions detailed above. Release <strong>of</strong> <strong>the</strong> data<br />
contained in this hard-copy data package has been authorized by <strong>the</strong> Laboratory Manager or a<br />
designee, as verified by <strong>the</strong> following signature.<br />
aniel<br />
rrrr Laboratory Manager<br />
Lionville Laboratory Incorporated<br />
jjw/m<strong>047</strong>50<br />
vLl<br />
4u<br />
Date
METALS METHOD GLOSSAR Y<br />
The following methods are used as'reference for <strong>the</strong> digestion and analysis <strong>of</strong> samples contained within f<br />
Lot#: pbo y L^5-v s<br />
Leaching Procedure: _1310 _1311 _1312 _O<strong>the</strong>r:<br />
CLP Metals _Digestion and _ Analysis Methods:<br />
"03.0 _ILMO4.0<br />
Metals Digestion Methods: _<strong>300</strong>5A _3010A _3015 _3020A Zo3050B _3051 _200.7 _SS17<br />
O<strong>the</strong>r.<br />
Aluminum<br />
Antimony<br />
Arsenic<br />
Ba<br />
SW846<br />
-)C 601 OR<br />
)c601 0B _7041'<br />
^C 601 OR `7060A<br />
ri Metals Analysis Methods<br />
EPA<br />
um<br />
Beryllium<br />
Bismuth<br />
Boron<br />
Cadmium<br />
Calcium<br />
Chromium<br />
Cobalt<br />
Copper<br />
Iron<br />
Lead<br />
Lithium<br />
Magnesium<br />
Manganese<br />
Mercury<br />
Molybdenum<br />
Nickel<br />
Potassium<br />
Rare Earths<br />
Selenium<br />
Silicon<br />
Silica<br />
Silver<br />
Sodium<br />
Stron tium<br />
Thallium<br />
Tin<br />
Titanium<br />
Uranium<br />
Vanadium<br />
Zinc<br />
Zirconium<br />
EPA STD MTD<br />
_200.7<br />
_200.7 204.2<br />
200.7 206.2 311313<br />
-f- 601 OR _200.7<br />
*C6010B _200.7<br />
Y-6010B' _200.7'<br />
6010B _200.7<br />
16010B _7131A' _200.7 _213.2<br />
7r-6010B _200,9<br />
^C6010B _7191' 200.7 218.2<br />
--ewlw _200.7<br />
r 6010 _7211' _200.7 _220.2<br />
r6010B<br />
200.7<br />
35601013 _7421' _200.7 _239.2 3113B<br />
^J6010B _7430' 200;7<br />
Zc6OIOB<br />
200.7<br />
-f-6010B<br />
::200.7<br />
7470A'r-7471 245.1 '_245.5 2<br />
-jC 6010B _200.7<br />
f- 601<br />
_200.7<br />
^EWJOB _7610' _200.7 _258.1'<br />
_601013 '<br />
200.7 1<br />
6010B _7740' 200.7 270.2 3113B<br />
1601 OR<br />
200.7<br />
_6010B _200.7<br />
601013 _7761 _200.7 _272.2<br />
601013 _7770' _200.7 273.14<br />
^601 OR<br />
200.7<br />
•,f6010B _7841' 200.7!279.2_200.9<br />
JG60IOB _200.7<br />
_601 OR _200.7<br />
5&OlOB'<br />
200.7'<br />
6010B -200,7<br />
601013<br />
200.7<br />
^6010B' 200,7'<br />
OSWR<br />
_1620<br />
_1620<br />
_1620<br />
_1620<br />
_1620<br />
_1620<br />
_1620<br />
USATHAMA<br />
99<br />
_99<br />
99<br />
99<br />
99<br />
_SS17<br />
_99<br />
_99<br />
_99<br />
_99<br />
_99<br />
-^•<br />
_99<br />
_99<br />
99<br />
99<br />
_99<br />
99<br />
99<br />
99<br />
99<br />
99<br />
99<br />
99<br />
99<br />
-^<br />
99<br />
99<br />
99<br />
99<br />
O<strong>the</strong>r: p Method• 4moQ 4m, .<br />
000000021
METHOD REFERENCES AND DATA QUALIFIERS<br />
U = Indicates that <strong>the</strong> parameter was not detected at or above <strong>the</strong> reported limit. The<br />
associated numerical value is <strong>the</strong> sample detection limit.<br />
+ = Indicates that <strong>the</strong> original sample result is greater than 4x <strong>the</strong> spike amount added.<br />
MB = Method or Preparation Blank.<br />
MS = Matrix-Spike.<br />
MSD = Matrix Spike Duplicate.<br />
REP - Sample Replicate<br />
LCS = Laboratory Control Sample..<br />
NC — Not calculated.<br />
1. Not included in <strong>the</strong> method element list.<br />
2. Modified Hg: Hgl and Hg2 require less total volume <strong>of</strong> digestate due to <strong>the</strong><br />
autosampler analysis. Sample volumes and reagents for mercury determinations<br />
in water and soil have been proportionately scaled down to adapt to this semiautomated<br />
technique. The sample volume used for water analysis is 33 mL. For<br />
soils, approximately 0.3 grams <strong>of</strong> sample is taken to a final volume <strong>of</strong> 50 ml,<br />
(including all reagents).<br />
3. Flame AA.<br />
4. Graphite Furnace AA.<br />
L-WI-033/N-04/98<br />
000000022
CLIENT: TNURANPORD <strong>RC</strong>-<strong>047</strong> X0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID ANALYTB<br />
-001 011KV5 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
I., Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnavium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Zirconium, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 05/25/06<br />
LVL LOT #: 0604L750<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
0.1 MG/KG 0.07 1.0<br />
30.2 MG/KG 2.3 1.0<br />
0.95 MG/KG 0.59 1.0<br />
619 MG/KG 0.23 1.0<br />
2.1 MO/KG 0.02 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
0.50 u MG/KG 0.50 1.0<br />
511 MG/KG 1.6 1.0<br />
0.07 MG/KG 0.07 1.0<br />
0.14 u MG/KG 0.14 1.0<br />
0.42 MG/KG 0.13 1.0<br />
6.5 MG/KG 0.12 1.0<br />
94.8 MG/KG 3.4 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
2600 MG/KG 2.2 1.0<br />
0.08 MG/KG 0.03 1.0<br />
826 MG/KG 0.94 1.0<br />
7.5 MG/KG 0.03 1.0<br />
0.53 MG/KG 0.28 1.0<br />
446 MG/KG 0.74 1.0<br />
0.23 u MG/KG 0.23 1.0<br />
2840 MG/KG 0.87 1.0<br />
0.30 u MG/KG 0.30 1.0<br />
D.43 u MG/KG 0.43 1.0<br />
D.56 MO/ICG 0.46 1.0<br />
47.2 MG/KG 2.2 1.0<br />
1.0 a MG/KG 1.0 1.0<br />
6.3 MG/KG 0.01 1.0<br />
0.68 u MG/KG 0.68 1.0<br />
0.85 u MG/KG 0.65 110<br />
D.15 MG/KG 0.09 1.D<br />
6015 MG/KG 0.16 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
000000023
CLIENT: TNUHANFORD <strong>RC</strong>-<strong>047</strong> X0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID ANALYTB<br />
-002 311KV6 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnsaium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Zirconium, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 05/25/06<br />
LVL LOT #: 06041,750<br />
RRPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
........ ......<br />
........<br />
0.07<br />
MG/KG<br />
..........<br />
0.07<br />
110<br />
$2.3 MG/KG 2.3 1.0<br />
0.85 MG/KG 0.59 1.0<br />
S.9 MG/KG 0.23 1.0<br />
2.1 MG/KG 0.02 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
0.49 u MG/KG 0.49 1.0<br />
346 MG/RG 1.6 1.0<br />
0.07 u MG/1(G 0.07 1.0<br />
0.13 u MG/KG 0.13 1.0<br />
0.31 MG/KG 0.12 1.0<br />
6.5 MG/KG 0.12 1.0<br />
211 MG/KG 3.4 1.0<br />
0.01 U MG/KG 0.01 1.0<br />
2540 MG/KG 2.2 1.0<br />
0.11 MG/KG 0.03 1.0<br />
828 MG/KG '0.93 1.0<br />
9.2 MG/KG 0.03 1.0<br />
0.54 MG/KG 0.28 1.0<br />
491 MG/KG 0.73 1.0<br />
0.35 MG/KG 0.23 110<br />
2590 MG/KC 0.86 1.0<br />
0.30 u MG/KG 0.30 1.0<br />
0.42 U MG/KG 0.42 1.0<br />
0.45 u MG/KG 0.45 1.0<br />
57.1 MG/KG 2.2 1.0<br />
1.0 U MG/KG 1.0 1.0<br />
5.5 MG/KG 0.01 1.0<br />
0.67 u MG/KG 0.67 1.0<br />
0.6S u MG/KG 0.65 1.0<br />
0.46 MG/KG 0.09 1.0<br />
51.9 MG/KG 0.15 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
000000024
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 05/25/06<br />
CLIENT: TNUAANPORD <strong>RC</strong>-<strong>047</strong> X0303 LVL LOT 4: 0604L75O<br />
WORK ORDER: 11343-606-001-9999-00<br />
REPORTING DILUTION<br />
SAMPLE SITS ID ANALYTB RESULT UNITS LIMIT FACTOR<br />
....... ........ ........<br />
-003 1T11KT0 Silver, Total 0.07 U MG/KG 0.07 1.0<br />
Aluminum, Total 19.5 MG/KG 2.2 1.0<br />
Arsenic, Total 1.4 MG/KG 0.50 1.0<br />
Boron, Total 3.9 MG/KG 0.21 1.0<br />
Barium, Total 1.6 MG/KG 0.02 1.0<br />
Beryllium, Total 0.02 U MG/KG 0.02 1.0<br />
Bismuth, Total 0.49 u MG/KG D.49 1.0<br />
Calcium, Total 639 MG/KG 1.6 1.0<br />
Cadmium, Total 0.09 MG/KG 0.07 1.0<br />
Cobalt. Total 0.14 MG/KG 0.13 1.0<br />
Chromium, Total 3.7 MG/KG 0.12 1.0<br />
Copper, Total 5.1 MG/KG 0.11 1.0<br />
Iron, Total 84.3 MG/KG 3.3 1.0<br />
Mercury, Total 0.01 U MG/KG 0.01 1.0<br />
Potasoium, Total 2560 MG/KG 2.2 1.0<br />
Lithium, Total 0.08 MG/KG 0.03 1.0<br />
Magnaaium, Total 613 MG/KG 0.92 1.0<br />
Manganese, Total 7.2 MG/KG 0.03 1.0<br />
Molybdenum, Total 0.79 MG/KG 0.20 1.0<br />
Sodium, Total 399 MG/KG 0.72 1.0<br />
Nickel, Total 1.9 MG/KG 0.23 1.0<br />
Phosphorus, Total 2280 MG/KG 0.86 1.0<br />
Lead, Total 0.30 u MG/KG 0.30 1.0<br />
Antimony, Total 0.42 u MG/KG 0.42 1.0<br />
Selenium, Total 0.55 MG/KG 0.45 1.0<br />
Silicon, Total 41.5 MG/KG 2.2 1.0<br />
Tin, Total 1.0 u MG/KG 1.0 1.0<br />
Strontium, Total 5.2 MG/KG 0-01 1.0<br />
Thallium, Total 0.67 u MG/KO 0.67 1.0<br />
Uranium, Total 0.84 u MO/KG 0.04 1.0<br />
Vanadium, Total 0.16 MG/KG 0.09 1.0<br />
Zinc, Total 33.4 MG/KG 0.15 1.0<br />
Zirconium, Total 1.0 U MG/KG 1.0 1.0<br />
000000025
CLIENT: TNUHANPORD <strong>RC</strong>-<strong>047</strong> K0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID ANALYTE<br />
-004 J11KT4 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Zirconium, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 05/25/06<br />
LVL LOT M: D604L750<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
0.07 u MG/KG 0.07 110<br />
34.3 MG/KG 2.3 1.0<br />
0.85 MG/KG 0.60 1.0<br />
3.7 MG/KG 0.24 1.0<br />
1.3 MG/KG 0.02 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
0.50 u MG/KG 0.50 1.0<br />
414 MG/KG 1.6 1.0<br />
0.07 u MG/KG 0.07 1.0<br />
0.14 MG/KG 0.14 1.0<br />
0.22 MG/KG 0.13 1.0<br />
6.6 MG/1CG 0.12 1.0<br />
120 MG/KG 3.4 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
2670 MG/KG 2.2 1.0<br />
0.10 MG/KG 0.03 1.0<br />
678 MG/KG 0.95 1.0<br />
7.2 MG/KG 0.03 1.0<br />
0.62 MG/KG 0.28 1.0<br />
461 MG/KG 0.74 1.0<br />
0.24 u MG/KG 0.24 1.0<br />
2520 MG/KG 0.88 1.0<br />
0.30 u MG/KG 0.30 1.0<br />
0.43 u MG/KG 0.43 1.0<br />
0.64 MG/KG 0.46 1.0<br />
48.3 MG/KG 2.2 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
4.2 MG/KG 0.01 1.0<br />
0.69 u MG/KG 0.69 1.0<br />
0.86 u MG/KG 0.86 1.0<br />
0.15 MG/KG 0.09 1.0<br />
45.1 MG/KG 0.16 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
000000026
CLIENT: TNUHANFORD <strong>RC</strong>-<strong>047</strong> K03D3<br />
NORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID<br />
005 JIIKT6<br />
ANALYTE<br />
Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Zirconium, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 05/25/06<br />
LVL LOT p: 0604L750<br />
REPORTING<br />
RESULT UNITS LIMIT<br />
0.12 MG/KG 0.08<br />
19.2 MG/KG 2.6<br />
0.81 MG/KG 0.68<br />
4.0 MG/KG 0.27<br />
3.3 MG/KG 0.02<br />
0.02 a MG/KG 0.02<br />
0.57 u MG/KG 0.57<br />
327 MG/KG 1.8<br />
0.08 u MG/KG 0.08<br />
0.16 u MG/KG 0.16<br />
0.20 MG/KG 0.14<br />
6.4 MG/KG 0.13<br />
76.3 MG/KG 3.9<br />
0.36 MG/KG 0.02<br />
2530 MG/KG 2.5<br />
0.05 MG/KG 0.03<br />
697 MG/KG 1.1<br />
5.0 MG/KG 0.03<br />
0.57 MG/KG 0.32<br />
542 MG/KG 0.84<br />
0.27 u MG/KG 0.27<br />
2500 MG/KG 1.0<br />
0.34 u MG/KG 0.34<br />
0.49 u MG/KG 0.49<br />
0.53 MG/KG 0.52<br />
45.6 MG/KG 2.5<br />
1.2 u MG/KG 1.2<br />
3.3 MG/KG 0.01<br />
0.78 u MG/KG 0.78<br />
0.98 u NG/KG 0.98<br />
0.1 u MG/RG 0.1<br />
36.8 MG/KO 0.19<br />
1.2 u MG/KG 1.2<br />
DILUTION<br />
FACTOR<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
1.0<br />
990069027
CLIENT: TNUHAN17ORD <strong>RC</strong>-<strong>047</strong> K0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID ANALYTE<br />
-006 aI1KT7 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Zirconium, Total<br />
Lion Ville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 05/25/06<br />
LVL LOT #: 06041,750<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
0.07 MG/KG 0.07 1.0<br />
29.9 MG/KG 2.3 1.0<br />
0.86 MG/KG O.S9 1.0<br />
3.2 MG/KG 0.23 1.0<br />
1.8 MG/KG 0.02 1.0<br />
0.02 a MG/KG 0.02 1.0<br />
0.50 u MG/KG O.SO 1.0<br />
714, MG/KG 1.6 1.0<br />
0.07 MG/KG 0.07 1.0<br />
0.16 MG/KG 0.14 1.0<br />
0.13 u MG/KG 0.11 1.0<br />
611 MG/KG 0.12 1.0<br />
81.9 MG/KG 3.4 1.0<br />
0.01 u MG/KG 0.01 1.0<br />
2370 MG/KG 2.2 1.0<br />
0.06 MG/KG 0.03 1.0<br />
496 MG/KG 0.94 1.0<br />
8.4 MG/KG 0.03 1.0<br />
0.48 MG/KG 0.28 1.0<br />
432 MG/KG 0.74 1.0<br />
0.23 u MG/KG 0.23 1.0<br />
2040 MG/KG 0.87 1.0<br />
0.30 u MG/KG 0.30 1.0<br />
0.43 u MG/KG 0.43 1.0<br />
0.46 u MG/KG 0.46 1.0<br />
39.6 MG/KG 2.2 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
6.2 MG/KG 0.01 1.0<br />
0.68 u MG/KG 0.68 1.0<br />
D.85 u MG/KG 0.85 1.0<br />
0.19 MG/KG 0.09 1.0<br />
30.5 MG/KG 0.16 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
999090028
CLIENT: TNUNANPORD <strong>RC</strong>-<strong>047</strong> X0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID ANALYTR<br />
-007 J11KTS Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Zirconium, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 05/25/06<br />
LVL LOT A: O6041,750<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
.....: .. ......<br />
........<br />
0.07 u<br />
MG/KG<br />
..........<br />
0.07<br />
1.0<br />
11.6 MG/KG 2.2 1.0<br />
0.59 MG/KG 0.58 1.0<br />
2.1 MG/KG 0.23 1.0<br />
1.2 MG/KG 0.02 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
0.46 u MG/KG 0.48 1.0<br />
222 MG/XG 1.5 1.0<br />
0.07 u MG/KG 0.07 1.0<br />
-0.13 u MG/KG 0.13 1.0<br />
0.16 MG/KG 0.12 1.0<br />
4.6 MG/KG D_11 1.0<br />
61.0 MG/KG 3.3 1.0<br />
0.01 u MG/KG 0.01 1.0<br />
2310 MG/KG 2.1 1.0<br />
0.03 MG/KG 0.03 1.0<br />
700 MG/KG 0.91 1.0<br />
3.7 MG/KG 0.03 1.0<br />
0.48 MG/KG 0.27 1.0<br />
389 MG/KG 0.72 1.0<br />
0.23 u MG/KG 0.23 1.0<br />
7340 MG/KG 0.85 1.0<br />
0.29 u MG/KG 0.29 1.0<br />
0.41 u MG/KG 0.41 1.0<br />
0.44 u MG/KG 0.44 1.0<br />
31.3 MG/KG 2.1 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
2.5 MG/KG 0.009 1.0<br />
0.66 u MG/KG 0.66 1.0<br />
0.83 u MG/KG 0.83 1.0<br />
0.08 u MG/KG 0.06 1.0<br />
29.1 MG/KG 0.15 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
000000029
Lionville Laboratory. Inc.<br />
INORGANICS DATA SUMMARY REPORT O5/25/D6<br />
CLIENT: TNUHAUPORD <strong>RC</strong>-<strong>047</strong> K03O3 LVL LOT #: 06041,750<br />
ifORK ORDER: 11343-606-001-9999-00<br />
REPORTING DILUTION<br />
SAMPLE SITE ID ANALYTS RESULT UNITS LIMIT FACTOR<br />
..c o ee .................... -....................<br />
-0c8 J13KT9 Silver, Total 0.07 u MG/KG 0.07 1.0<br />
Aluminum, Total 25.3 MG/KG 2.3 1.0<br />
Arsenic, Total 0.75 MG/KG 0.59 1.0<br />
Boron, Total 1.6 MG/KG 0.23 1.0<br />
Barium, Total 1.0 MG/KG 0.02 1.0<br />
Beryllium, Total 0.02 u MG/KG 0.02 1.0<br />
Bismuth, Total 0.49 u MG/KG 0.49 1.0<br />
Calcium, Total 520 MG/KG 1.6 1.0<br />
Cadmium, Total 0.07 u MG/KG 0.07 1.0<br />
Cobalt, Total 0.17 MG/KG 0.13 1.0<br />
Chromium, Total 0.12 u MG/KG 0.12 1.0<br />
Copper, Total 5.8 MG/KG 0.12 1.0<br />
Iron, Total 88.5 MG/KG 3.4 1.0<br />
Mercury, Total 0.01 u MG/KG 0.01 1.0<br />
Potassium, Total 2290 MG/KG 2.2 1.0<br />
Lithium, Total 0.05 MG/KG 0.03 1.0<br />
Magnesium, Total 522 MG/KG 0.93 - 1.0<br />
- Manganese, Total 5.5 MG/KG 0.03 1.0<br />
Molybdenum, Total 0.51 MG/KG 0.28 1.0<br />
Sodium, Total 480 MG/KG 0.73 1.0<br />
Nickel, Total 0.23 u MG/KG 0.23 1.0<br />
Phosphorus, Total 2170 MG/KG 0.66 1.0<br />
Lead, Total 0.30 u MG/KG 0.30 1.0<br />
Antimony, Total 0.42 u MG/KG 0.42 1.0<br />
Selenium, Total 0.45 u MG/KG 0.45 1.0<br />
Silicon, Total 50.0 MG/KG 2.2 1.0<br />
Tin, Total 1.0 u MG/KG 1.0 1.0<br />
Strontium, Total 2.9 MG/KG 0.01 1.0<br />
Thallium, Total 0.67 u MG/KG 0.67 1.0<br />
Uranium, Total 0.85 u MG/KG 0.65 1.0<br />
Vanadium, Total 0.10 MG/KG 0.09 1.0<br />
Zinc, Total 35.2 MG/KG 0.15 1.0<br />
Zirconium, Total 1.0 u MG/KG 1-0 1.0<br />
000000030
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 05/25/06<br />
CLIENT: TNUNANFORD <strong>RC</strong>-<strong>047</strong> X0303 LVL LOT #: O604L750<br />
WORK ORDER: 11343-606-001-9999-00<br />
REPORTING DILUTION<br />
SAMPLE SITS ID ANALYTE RESULT UNITS LIMIT FACTOR<br />
-009 331KV0 Silver, Total 0.07 U MG/KG 0.07 1.0<br />
Aluminum, Total 21.4 MG/KG 2.3 1.0<br />
Arsenic, Total 0.86 MG/KG 0.59 1.0<br />
Boron, Total 1.3 MG/KG 0.23 1.0<br />
Barium, Total 2.3 MG/KG 0.02 1.0<br />
Beryllium, Total 0.02 u MG/KG 0.02 1.0<br />
Bismuth, Total 0.49 u MG/KG 0.49 1.0<br />
Calcium, Total 223 MG/KG 1,6 1.0<br />
Cadmium, Total 0.07 u MG/KG 0.07 1.0<br />
Cobalt, Total 0.13 u MG/KG 0.13 1.0<br />
Chromium, Total 0.16 MG/KG 0.12 110<br />
Copper, Total 5.9 MG/KG 0.12 1.0<br />
Iron, Total 63.9 MG/KG 3.4 1.0<br />
Mercury, Total 0.01 u MG/KG 0.01 1.0<br />
Potassium, Total 2360 MG/KG 2.2 1.0<br />
Lithium, Total 0.04 MG/KG 0.03 1.0<br />
Magnesium. Total 760 MG/KG 0.93 1.0<br />
Manganese, Total 7.1 MG/KG 0.03 1.0<br />
Molybdenum, Total 0.46 MG/XG 0.28 110<br />
Sodium, Total 377 MG/KG 0.73 1.0<br />
Nickel, Total 0.23 u MG/XG 0.23 1.0<br />
Phosphorus, Total 2460 MG/KG 0.86 1.0<br />
Lead, Total 0.30 u MG/KG 0.30 1.0<br />
Antimony, Total 0.42 V MG/KG 0.42 1.0<br />
Selenium, Total 0.45 u MG/KG 0.45 1.0<br />
Silicon, Total 44.1 MG/KG 2.2 1.0<br />
Tin, Total 1.0 u MG/KG 1.0 1.0<br />
Strontium, Total 2.0 MG/KG 0.01 110<br />
Thallium, Total 0.67 u MG/KG 0.67 1.0<br />
Uranium, Total 0.85 u MG/KG 0.95 1.0<br />
Vanadium, Total 0.09 u MG/KG 0.09 1.0<br />
Zinc, Total 27.4 MG/KG 0.15 1.0<br />
Zirconium, Total 1.0 u MG/KG 1.0 1.0<br />
000000031
CLIENT: TNURANPORD <strong>RC</strong>-<strong>047</strong> K0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID ANALYTE<br />
....... .................... ...<br />
-010 J11KI9 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Zirconium, Total<br />
Lionville Laboratory, Inc.<br />
IMORGANICS DATA SUMMARY REPORT 05/25/06<br />
LVL LOT #: O6O4L75O<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
0.07 u MG/KG- 0.07 1.0<br />
36.0 MG/KG 2.3 1.0<br />
1.5 MG/KG 0.59 1.0<br />
5.4 MG/KG 0.23 1.0<br />
1.4 MG/KG 0.02 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
0.50 u MG/KG 0.50 1.0<br />
264 MG/KG 1.6 1.0<br />
0.07 u MG/KG 0.07 1.0<br />
0.14 u MG/KG 0.14 1.D<br />
0.16 MG/KG 0.13 1.0<br />
6.0 MG/KG 0.12 1.0<br />
110 MG/KG 3.4 1.0<br />
0.01 u MG/KG D.01 1.0<br />
2370 MG/KG 2.2 1.0<br />
0.05 MG/KG 0.03 1.0<br />
710 MG/KG 0.94 3.0<br />
4.8 MG/KG - 0.03 1.0<br />
0.74 MG/KG 0.25 1.0<br />
446 MG/KG 0.74 1.0<br />
0.33 u MG/KG 0.23 1.0<br />
2640 MG/KG 0.87 1.0<br />
0.30 u MG/KG 0.30 1.0<br />
0.43 u MG/KG 0.43 1.0<br />
0.46 u MG/KG 0.46 1.0<br />
54.5 MG/KG 2-2 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
3.6 MG/KG 0.03 1.0<br />
0.68 u MO/KG 0.69 1.0<br />
0.85 u MG/KG 0.85 1.0<br />
0.14 MG/KG 0.09 1.0<br />
36.1 MG/KG 0.16 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
000000032
CLIENT; TNURANFORD <strong>RC</strong>-<strong>047</strong> X0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID ANALYT6<br />
-011 J11XR2 Silver, Total<br />
Aluminum, Total<br />
Arsenic. Total<br />
Moron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Biemuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Pataesium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Zirconium, Total<br />
Lionville Laboratory, Inc-<br />
INORGANICS DATA SUMMARY REPORT 05/25/06<br />
LVL LOOT #! 0604L750<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
........ ......<br />
........<br />
0.07 u<br />
MG/KG<br />
..........<br />
0.07<br />
1.0<br />
38.1 MG/KG 2.3 1.0<br />
0.59 u MO/KG 0.59 1.0<br />
2.6 MG/KG 0.23 1.0<br />
1.3 MG/KG 0.02 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
0.50 U MG/XG 0.50 1.0<br />
511 MG/KG 1.6 1.0<br />
0.07 u MG/KG 0.07 1.0<br />
0.14 U MG/KG 0.14 1.0<br />
0.57 MG/KG 0.13 1.0<br />
7.8 MG/KG 0.12 1.0<br />
121 MG/KG 3.4 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
2640 MG/KG 2.2 1.D<br />
0.06 MG/KO 0.03 1.0<br />
739 MG/KG 0.94 1.0<br />
6.6 MG/KG 0.03 1.0<br />
0.52 MG/KG D.28 1.0<br />
524 MG/KG 0.74 1.0<br />
0.30 MG/KG 0.23 1.0<br />
2710 MG/KG 0.87 1.0<br />
0.30 u MG/KG 0.30 1.0<br />
0.43 u MG/KG 0.43 1.0<br />
0.46 u MG/KG 0.46 1.0<br />
53.5 MG/KG 2.2 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
3.4 MG/KG 0.01 1.0<br />
0.68 u MG/RG 0.68 1.0<br />
D.85 u MG/KO 0.85 1.0<br />
0.15 MG/KG 0.09 1.0<br />
38.7 MG/KG 0.16 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
000000033
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 05/25/06<br />
CLIENT: TNUKANFORD <strong>RC</strong>-<strong>047</strong> K0303 LVL LOT 1!: 06041,750<br />
WORK ORDER: 11341-606-001-9999-00<br />
REPORTING DILUTION<br />
SAMPLE SITE ID ANALYTE RESULT UNITS LIMIT FACTOR<br />
....................<br />
------'<br />
-012 J31L38 Silvar, Total 0.07 u MG/KG 0.07 1.0<br />
Aluminum, Total 2S.2 MG/KG 2.3 1.0<br />
Arsenic, Total 0.94 MG/KG 0.59 1.0<br />
Boron, Total 5.6 MG/KG 0.23 1.0<br />
Barium, Total 1.1 MG/KG 0.02 1.0<br />
Beryllium, Total 0.02 u MG/KG 0.02 1.0<br />
Biamuth, Total 0.49 u MG/KG 0.49 1.0<br />
Calcium, Total 318 MG/KG 1.6 1.0<br />
Cadmium, Total 0.07 u MG/KG 0.07 1.0<br />
Cobalt, Total 0.13 u MG/XG 0.13 1.0<br />
Chromium, Total 0.23 MG/KG 0.12 1.0<br />
Copper, Total 5.0 MG/KG 0.12 1.0<br />
Iron, Total 108 MG/KG 3.4 1.0<br />
Mercury, Total 0.01 u MO/KG 0.01 1.0<br />
Potassium, Total 2240 MG/KG 2.2 1.0<br />
Lithium, Total 0.05 MG/KG 0.03 1.0<br />
Magnesium, Total 927 MG/1(G 0.93 1.0<br />
Manganese, Total 7.0 MG/KG 0.03 1.0<br />
Molybdenum, Total 0.79 MG/KG 0.29 1.0<br />
Sodium, Total 456 MG/KG 0.73 1.0<br />
Nickel, Total 0.26 MG/KG 0.23 1.0<br />
Phosphoruo, Total 2400 MG/KG 0.86 1.0<br />
Lead, Total 0.30 u MG/KG 0.30 1.0<br />
Antimony, Total 0.42 u MG/KG 0.42 1.0<br />
Selenium, Total - 0.48 MG/KG 0.45 1.0<br />
Silicon, Total 4S.4 MG/KG 2.2 1.0<br />
Tin, Total 1.0 u MG/KG 1.0 - 1.0<br />
Strontium, Total 4.8 MG/KG 0.01 1.0<br />
Thallium, Total 0.67 u MG/KG 0.67 1.0<br />
uranium, Total 0.65 u MG/KG 0.95 1.0<br />
Vanadium, Total 0.09 u MG/KG 0.09 1.0<br />
Zinc, Total 49.9 MG/KG 0.15 1.0<br />
Zirconium, Total 1.0 u MG/KG 1.0 1.0<br />
000000034
CLIENT: TNUNANFORD <strong>RC</strong>-<strong>047</strong> KD302<br />
MORIC ORDER: 11343-606-001-9999-00<br />
SAMPLE SITS ID ANALYTE<br />
-013 Tl2L35 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total.<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin. Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Zirconium, Total<br />
Lionville Laboratory, Inc.<br />
INDRGAMICS DATA SUMMARY REPORT 05/25/06<br />
LVL LOT k: 06041,750<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
........ ......<br />
........<br />
0.07 u<br />
MG/KG<br />
..........<br />
0.07<br />
1.0<br />
23.7 MG/KG 2.2 1.0<br />
0.93 MG/KG 0.58 1.0<br />
2.5 MO/KG 0.23 1.0<br />
0.97 MG/KG 0.02 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
0.49 u MG/KG 0.49 1.0<br />
392 MG/KG 1.6 1.0<br />
0.07 u MG/KG 0.07 110<br />
0.13 u MG/KG 0.13 3.0<br />
0.17 MG/KG 0.12 1.0<br />
7.3 MG/KG 0.11 110<br />
66.9 MG/KG 3.3 1.0<br />
0.02 V MG/KG 0.02 1.0<br />
2240 MG/KG 2.2 1.0<br />
0.03 MG/KG 0.03 1.0<br />
579 MG/KG 0.92 1.0<br />
5.1 MG/KG 0.03 1.0<br />
0.45 MG/KG 0.28 1.0<br />
499 MG/KG 0.72 1.0<br />
0.27 MG/KG 0.23 1.0<br />
2110 MG/KG - 0.86 1.0<br />
0.30 u MG/KG 0.30 1.0<br />
0.42 u MG/KG 0.42 1.0<br />
0.45 u MG/KG 0.45 1.0<br />
44.6 MG/KG 2.2 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
3.1 MG/KG 0.01 1.0<br />
0.67 u MG/KG 0.67 1.0<br />
0.64 u MG/KG 0.64 1.0<br />
0.1 MG/KG 0.09 1.0<br />
30.1 MG/KG 0.15 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
000000035
CLIENT: TNVNANFORD <strong>RC</strong>-<strong>047</strong> X0303<br />
WORK ORDER: 11343-606-DO1-9999-00<br />
SAMPLE SITS ID ANALYTE<br />
-014 JIIL33 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Baryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Load, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Zirconium, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 05/25/06<br />
LVL LOT #: 06041,750<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
0.07 MG/KG 0.07 1.0<br />
24.6 MG/KG 2.2 1.0<br />
0.58 u MG/KG 0.56 1.0<br />
311 MG/KG 0.23 1.0<br />
1.6 MG/KG 0.02 1.0<br />
0.02 u MG/XG 0.02 1.0<br />
0.49 u MG/KG 0.49 1.0<br />
354 MG/KG 1.6 1.0<br />
0107 MG/KG 0.07 1.0<br />
0.13 u MG/XG 0.13 1.0<br />
0.21 MG/KG 0.12 1.0<br />
5.1 MG/XG 0.11 1.0<br />
76.2 MG/KG 3.3 110<br />
0.01 u MG/KG 0.01 1.0<br />
2600 MG/KG 2.2 1.0<br />
0.03 MG/KG 0.03 1.0<br />
690 MG/KG 0.92 1.0<br />
5.9 MG/KG 0.03 1.0<br />
0.49 MG/KG 0.28 1.0<br />
432 MG/KG 0.72 1.0<br />
0.23 U MG/KG 0.23 1.D<br />
2560 MG/KG 0.86 1.0<br />
0.30 U MG/KG 0.30 1.0<br />
0.42 u MG/KG 0.42 1.0<br />
0.45 u MG/KG 0.45 1.0<br />
50.1 MG/KG 2.2 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
3.9 MG/KG 0.01 1.0<br />
0.67 u MG/KG 0.67 1.0<br />
0.84 u MG/KG 0.84 1.0<br />
0.14 MG/KG 0.09 1.0<br />
30.9 MG/KG 0.15 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
000000036
CLIENT: TNOMANFORD <strong>RC</strong>-<strong>047</strong> K0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID ANALYTE<br />
....... .................... .............<br />
-015 JLIL31 Silver, Total<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Mercury, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
vanadium. Total<br />
Zinc, Total<br />
Zirconium, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS DATA SUMMARY REPORT 05/25/06<br />
LVL LOT S: 0604LISO<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
0.07 U MG/KG 0.07 1.0<br />
57.0 MG/KG 2.3 1.0<br />
0.59 u MG/KG 0.59 1.0<br />
3.5 MG/KG 0.23 1.0<br />
2.4 MG/KG 0.02 1.0<br />
0.02 U MG/KG 0.02 110<br />
0.49 u MG/KG 0.49 1.0<br />
580 MG/KG 1.6 1.0<br />
0.09 MG/KG 0.07 1.0<br />
0.18 MG/1(G 0.13 1.0<br />
0.22 MG/KG 0.12 1.0<br />
6.1 MG/KG 0.12 1.0<br />
188 MG/KG 3.4 1.0<br />
0.01 u MG/KG 0.01 1.0<br />
2360 MG/KG 2.2 1.0<br />
0.10 MG/KG 0.03 1.0<br />
740 MG/KG 0.93 1.0<br />
7.7 MG/KG 0.03 1.0<br />
0.61 MG/KG 0.26 1.0<br />
386 MG/KG 0.73 1.0<br />
0.23 u MG/KG 0.23 1.0<br />
2470 MG/KG 0.86 1.0<br />
0.30 u MG/KG 0.30 1.0<br />
0.42 u MG/KG 0.42 110<br />
0.45 u MG/KG 0.45 110<br />
63.5 MO/KG 2.2 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
4.2 MG/KG 0.01 1.0<br />
0.67 u MG/KG 0.67 1.0<br />
0.85 u MG/KG 0.85 1.0<br />
0.29 MG/KG 0.09 1.0<br />
32.6 MG/KG 0115 1.0<br />
1.0 u MG/KG 1.0 1.0<br />
000000037
CLIENT: TNUKANPORD <strong>RC</strong>-<strong>047</strong> X0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
SAMPLE SITE ID ANALYTE<br />
BLANKS 04LO284-MB1 Silver, Total<br />
Lionville Laboratory, Inc.<br />
INORGANICS METHOD BLANK DATA SUMMARY PASS 05/25/06<br />
Aluminum, Total<br />
Arsenic, Total<br />
Boron, Total<br />
Barium, Total<br />
Beryllium, Total<br />
Bismuth, Total<br />
Calcium, Total<br />
Cadmium, Total<br />
Cobalt, Total<br />
Chromium, Total<br />
Copper, Total<br />
Iron, Total<br />
Potassium, Total<br />
Lithium, Total<br />
Magnesium, Total<br />
Manganese, Total<br />
Molybdenum, Total<br />
Sodium, Total<br />
Nickel, Total<br />
Phosphorus, Total<br />
Lead, Total<br />
Antimony, Total<br />
Selenium, Total<br />
Silicon, Total<br />
Tin, Total<br />
Strontium, Total<br />
Thallium, Total<br />
Uranium, Total<br />
Vanadium, Total<br />
Zinc, Total<br />
Zirconium, Total<br />
BLANKI 0600080-MB1 Mercury, Total<br />
LVL LOT #: 06O4L750<br />
REPORTING DILUTION<br />
RESULT UNITS LIMIT FACTOR<br />
........ ......<br />
--------<br />
0.07 u<br />
MG/KG<br />
..........<br />
0.07<br />
1.0<br />
2.4 u MG/KG 2.4 1.0<br />
0.61 u MG/KG 0.61 1.0<br />
0.24 u MG/KG 0.24 1.0<br />
0.02 u MG/KG 0.02 1.0<br />
0.02 U MG/KG 0.02 1.0<br />
0.51 u MG/KG 0.51 1.0<br />
2.0 MG/KG 1.6 1.0<br />
0.07 u MG/KG 0.07 1.0<br />
0.14 u MG/KG 0.14 1.0<br />
0.13 u MG/KG 0.13 1.0<br />
0.12 u MG/KG 0.12 1.0<br />
3.5 u MG/KG 3.5 1.0<br />
2.3 U MG/KG 2.3 1.0<br />
0.03 u MG/KG 0.03 1.0<br />
0.97 u MG/KG 0.97 1.0<br />
0.03 u MG/KG 0.03 1.0<br />
0.29 u MG/KG D.29 1.0<br />
0.76 u MG/KG 0.76 110<br />
0.24 u MG/KG 0.24 110<br />
0.90 u MG/KG 0.90 1.0<br />
0.31 u MG/KG 0.31 1.0<br />
.0.44 u MG/KG 0.44 1.0<br />
0.47 u MG/KG 0.47 1.0<br />
2.) u MG/KG 2.3 110<br />
1.1 u MG/KG 1.1 1.0<br />
0.01 MG/KG 0.01 1.0<br />
0.70 U MG/KG 0.70 1.0<br />
0.68 u MG/KG 0.88 1.0<br />
0.09 u MG/KG 0.09 1.0<br />
0.16 u MG/KG 0.16 1.0<br />
1.1 u MG/KG 1.1 1.0<br />
0.02 u MG/KG 0.02 3.0<br />
000000038
Lionville Laboratory, Inc.<br />
INORGANICS ACCURACY REPORT 05/35/06<br />
CLIENT: TNUNANPORD <strong>RC</strong>-<strong>047</strong> K0303 LVL LOT M: 06041,750<br />
WORK ORDER: 11343-606 -OD1- 9999-00<br />
SPIKED INITIAL SPIKED<br />
SAMPLE SITE ID ANALYTE SAMPLE RESULT AMOUNT TREODV<br />
-001 011KV5 Mercury, Total 0.14 0.02u 0.15 96.6<br />
DILUTION<br />
FACTORS PK)<br />
1.0<br />
000000039
Lionville Laboratory, Inc.<br />
INORGANICS ACCURACY REPORT 05/25/06<br />
CLIENT: TNVRANPORD <strong>RC</strong>-<strong>047</strong> X0303 LVL LOT p: 06041,750<br />
WORK ORDER: 11343-606-001-9999-00<br />
SPIKED INITIAL SPIKED DILUTION<br />
SAMPLE<br />
.......<br />
SITE ID<br />
....................<br />
ANALYTE<br />
......................<br />
SAMPLE<br />
.......<br />
RESULT<br />
.......<br />
AMOUNT<br />
......<br />
tRSOOV<br />
.......<br />
PACTOR(SPK)<br />
..........<br />
-002 JI1KV6<br />
Silver, Total<br />
4.5<br />
0.07<br />
4.8<br />
92.3<br />
Aluminum, Total 202 52.3 192 77.9 1.0<br />
Arsenic, Total 162 0.85 192 84.1 1.0<br />
Boron, Total 69.3 5.9 96.1 86.8 1.0<br />
Barium, Total 173 2.1 192 88.8 1.0<br />
Beryllium, Total 4.3 0.O2u 4.8 89.6 1.0<br />
Bismuth, Total 418 O.49u 480 87.0 1.0<br />
Calcium, Total 2640 346 2400 95.3 1.0<br />
Cadmium, Total 4.3 O.O7u 4.8 89.6 1.0<br />
Cobalt, Total 43.6 O.13u 48.0 90.8 1.0<br />
Chromium, Total 17.8 0.31 19.2 91.1 1.0<br />
Copper, Total 27.5 6.5 24.0 87.5 1.0<br />
Iron, Total 224 211 96.1 13.6 1.0<br />
Potassium, Total 4420 2540 2400 78.4 1.0<br />
Lithium, Total 94.2 0.11 96.1 97.9 1.0<br />
Magnesium, Total 3030 828 2400 91.7 1.0<br />
Manganese, Total 52.3 9.2 48.0 89.8 1.0<br />
Molybdenum, Total 86.5 0.54 96.1 89.4 1.0<br />
Sodium, Total 2660 491 2400 90.3 1.0<br />
Nickel, Total 42.9 0.35 48.0 88.7 1.0<br />
Phosphorus, Total 2930 2590 480 48.5- 1. 0,<br />
Lead, Total 42.2 0.30u 48.0 87.9 1.0<br />
Antimony, Total 39.5 0.42u 48.0 82.3 1.0<br />
Selenium, Total 156 0.45u 192 82.5 1.0<br />
Silicon, Total 174 57.1 96.1 121.3 1.0<br />
Tin, Total 80.9 1.0 u 96.1 84.2 - 1.0<br />
Strontium, Total 90.7 515 96.1 88.7 1.0<br />
Thallium, Total 168 O.67u 192 87.4 1.0<br />
Uranium, Total ,213 O.85u 240 89.9 1.0<br />
Vanadium, Total 44.9 0.46 48.0 92.6 1.0<br />
Zinc, Total 134 51.9 48.0 172.1<br />
Zirconium, Total 320 1.0 u 4S0 66.6 1.0<br />
1.0<br />
000000040
Lionville Laboratory, Inc.<br />
INORGANICS PRECISION REPORT 05/25/06<br />
CLIENT! TNUKANFORD <strong>RC</strong>-<strong>047</strong> K0303 LVL LOT 8: 0604L750<br />
WORK ORDER: 11343-606-001-9999-00<br />
INITIAL DILUTION<br />
SAMPLE SITE ID ANALYTR RESULT REPLICATE RFD FACTOR(REP)<br />
....: .. ...........................:a.........:.... ........ ...».... ._.:..: -----------<br />
-001REP S11KV5 Silver, Total 0.1 0. 07u -No. 1.0<br />
Aluminum, Total 30 . 2 43.3 35.6 1.0<br />
Arsenic, Total 0.95 1.1 14.4 1.0<br />
Boron, Total 6.9 6.1 12.3 1.0<br />
Barium, Total 2.1 2.3 9.1 1.0<br />
Beryllium, Total 0 . 02u 0 . 02u NC 1.0<br />
Bismuth, Total O.SOu 0.49u NC 1.0<br />
Calcium, Total 511 506 0.88 1.0<br />
Cadmium, Total 0.07 0.07u .IiC 1.0<br />
Cobalt, Total 0.14u 0.13u NC 1.0<br />
Chromium, Total 0.42 0.28 38.2 1.0<br />
Copper, Total 6.5 6.7 3.0 1.0<br />
Iron, Total 94,8 159 50.6 1.0<br />
Mercury , Total 0.02u 0.02U NC 1.0<br />
Potassium, Total 260D 2420 7.1 1.0<br />
Lithium, Total 0.08 0.09 4.9 1.0<br />
Magnesium, Total 826 874 5 .7 1.0<br />
Manganese, Total 7.5 8.6 13.7 1.0<br />
Molybdenum, Total 0.53 0.48 10 1.0<br />
Sodium, Total 446 413 7.8 1.0<br />
Nickel, Total 0.23u 0.27 -?w 1.0<br />
Phosphorus, Total 2840 2710 4.7 1.0<br />
Lead, Total 0.3Du 0.30u NC 1.0<br />
Antimony, Total<br />
Selenium, Total<br />
0.43U<br />
0.56<br />
0.42U<br />
0.45u<br />
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Tin, Total 1.0 v 1.0 u NC 1.0<br />
St ro ntium, Total 6.3 5.8 9.3 1.0'<br />
Thallium, Total 0,68u 0.67u NC 1.0<br />
Uranium, Total 0.66u O.BSu NC 1.0<br />
Vanadium, Total 0.15 0.26 54.9 1 1 0'<br />
Zinc, Total 60.5 62.7 3.6 1.0<br />
Zirconium, Total 1.0 u 1.0 u NC 1.0<br />
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000009041
CLIENT: TNUHA14PORD <strong>RC</strong>-<strong>047</strong> K0303<br />
WORK ORDER: 11343-606-001-9999-00<br />
Lionville Laboratory, Inc.<br />
INORGANICS LABORATORY CONTROL STANDARDS REPORT 05/25/06<br />
SPIKED SPIKED<br />
LVL LOT $: 0604050<br />
SAMPLE SITE ID ANALYTE SAMPLE AMOUNT UNITS LRECOV<br />
LC81 06L0284- LC1$6`ii : Silver, LCS 47.8 50.0 MG/KG 95.6<br />
Aluminum, Les 458 500 MG/KG 91.6<br />
Arsenic, LCS 895 <strong>100</strong>0 MG/KG 89.5<br />
Boron, LCS 454 500 MG/KG 90.8<br />
Barium, LCS 468 500 MG/KG 93.5<br />
Beryllium, LCS 22.9 25.0 MG/KG 91.6<br />
Bismuth, LCS 455 500 MG/KG 91.1<br />
Calcium, LCS 2370 2500 MG/KG 94.8<br />
Cadmium, LCS 2219 25.0 MG/KG 91.6<br />
Cobalt, LCS 232 250 MG/KG 92.9<br />
Chromium, LCS 46.7 50,0 MG/KG 93.4<br />
Copper, LCS 117 125 MG/KG 93.4<br />
Iron, LCS 477 500 MG/KG 95.5<br />
Potassium, LCS 2260 2500 NG/KG 91.1<br />
Lithium, LCS 491 500 MG/KG 98.3<br />
Magnesium, LCS 2350 2500 MG/KG 94.1<br />
Manganese, LCS 72.2 75.0 MG/KG 96.3<br />
Molybdenum, LCS 478 500 MG/KG 95.7<br />
Sodium, LCS 2310 2500 MG/KG 92.5<br />
Nickel, LCS 184 200 MG/KG 92.0<br />
Phosphorus, LCS 466 500 MG/KG 93.5<br />
Lead, LCS 226 250 MG/KG 91.0<br />
Antimony, LCS 273 <strong>300</strong> MG/KG 91.0<br />
Selenium, LCS 873 <strong>100</strong>0 MG/KG 87.3<br />
Silicon, LCS 156 500 MG/KG 31.2<br />
Tin, LCS 473 500 WKG 94.6<br />
Strontium, LCS 476 500 MG/KG 95.2<br />
Thallium, LCS 924 <strong>100</strong>0 MG/KG 92.4<br />
Uranium, LCS 235 250 MG/KG 93.9<br />
Vanadium, LCS 239 250 MG/KG 95.8<br />
Zinc, LCS 90,6 <strong>100</strong> MG/KG 90.6<br />
Zirconium, LCS 478 500 MG/KG 95.6<br />
LCS1 06C0000-LC1 Mercury, LCS 6.6 6.2 MG/KG 106.4<br />
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Washington Closure <strong>Hanford</strong> CHAIN OF CUSTO USAWLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>.342 Pa; 1 v !<br />
Bedor<br />
Company<br />
Tfl KUNCKMAN<br />
Contact Telephone No. Protect Coordinator<br />
MIER B JOAN KESSNER 375-4688 KESSNER, JH Price Code 9^r a<br />
roiecl Dedanation Santana Location <strong>SAF</strong> No.<br />
<strong>100</strong> & <strong>300</strong> <strong>Area</strong> <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti 600-131 INVERTEBRATES <strong>RC</strong>-<strong>047</strong><br />
Ice Cheat No.<br />
IF -'ee - p22- 0'<br />
Field Leabook No. COA Method <strong>of</strong> Shipment<br />
EIA595 BESRAS6520 FED EX<br />
Air Quality q<br />
nnh: ratan,-uurd<br />
45 Days<br />
Shipped To Offsite P ro perty No. ^J Bi ll<br />
EBERLINE SERVICES ONVBLE /TO^pO S<br />
<strong>of</strong> Lading/Air Bill No.<br />
SEE OSPC<br />
POSSIBLE SAMPLE HAZARDS/REMARKS -<br />
i-<br />
POTENTIALRADIOACTIVE
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Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong>-340 1'av I nl<br />
Collector<br />
TN KLINCKMAN Connonr Contact Tdeohone Ne. Project Coordinator<br />
TILLER, B. JOAN KESSNER 375.4688 KESSNER, JH<br />
roieet DalEnation SamoBata Loca ti on <strong>SAF</strong> No.<br />
<strong>100</strong> R <strong>300</strong> <strong>Area</strong> Complmrnt <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti BORROW Pfl' 23 INVBRTEDRA7FS <strong>RC</strong>-<strong>047</strong><br />
Im Chat No.p<br />
g lee, -Q? - O 7<br />
Field Logbook No. COA Method or Shioment<br />
EIr1595 BFSRAS6520 FED EX<br />
Price Code 9\ Dp'1'uroorocnd<br />
[a<br />
Air Quality []<br />
Shinned To Offshe Proper" No. ^r Diu or LadinE/Air Bill No.<br />
EBERLWE SERVICESONVILLE SEE OSPC<br />
POSSIBLE SAMPLE RAZARDWOUSURKS ^^<br />
POTFJMAL JZADIOAC77VF.
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Washington Closure <strong>Hanford</strong> CHAIN OF CUSTODY/SAMPLE ANALYSIS REQUEST <strong>RC</strong>-<strong>047</strong> -333<br />
Collector Comuaas ContactTelephone No. - Project Coordinator<br />
TILLER, B. NCKMAN JOAN KESSNER 375-4688 KESSNER, JH Price Code 9th<br />
Data Tnrnasrol:nrt<br />
,,tt<br />
lecl Destenation Sampling Location <strong>SAF</strong> No.<br />
Air Quality [^ `t1 Days<br />
160 & <strong>300</strong> Ana <strong>Component</strong> <strong>of</strong> <strong>the</strong> <strong>RC</strong>BRA Sediment and Ti 116-DR-i. DR-2/ <strong>100</strong>-D-22 INVERTEBRATES <strong>RC</strong>-<strong>047</strong><br />
Ice Chest No. Field Loalaoolt No. COA Method <strong>of</strong> Shiomcut<br />
"e-e — OZ -- 7 EL- 1595 BESRAS6520 PFD EX<br />
Shinned To - Offsite Prooetty No. ^J ` Bill <strong>of</strong> Ladine/Air Bill No.<br />
EBERLINE SERVICES UONVn rF {y(/(/D,73 SEE OSPC<br />
POSSIBLE SAMPLE HAZA ARKS ---<br />
POTENTIAL RADIOACTIVE
A<br />
Lionville Laboratory Incorporated<br />
SAlVIP]C E RECEIPT CHECKLIST (SRQ<br />
CL NT:^" t1 t f VA 0.c-rCo P Date:<br />
P)^rcbase Order / Project# / R C-CA7<br />
L* SOW'S/Release#r:<br />
C(Yes ONO q No Seals Comments<br />
i<br />
CVYes a No<br />
yes q No<br />
[3 Cs ONO allo Seals<br />
1 Yes 17 No<br />
Yes ONO<br />
Cf 9. All samples on coc received? A Yes ONO<br />
ll<br />
samples<br />
Yes ONO<br />
rYa q No<br />
Yes q No<br />
a Yes a No 94A<br />
a Yes ONO 94A<br />
Yes 13 No<br />
t^^ Ola<br />
LvLT Batch # : Sample Custodian:<br />
0(-0 lSO<br />
NOTE: EXPLA IN ALL DISCREPANCITS<br />
1. Samples Hand De livered<br />
2. Custody seals on coolers or shipping<br />
container intact, signed and dated?<br />
3. Outside <strong>of</strong> coolers or shipping containers are<br />
free from damage?<br />
4. All expected paperwork received (coc and<br />
o<strong>the</strong>r client specific information) sealed in<br />
plastic bag and easily accessible?<br />
5. Samples receivoled r ambient?<br />
MR.<br />
6. Custody seals on sample containers intact,<br />
signed and dated?<br />
7. coc signed and dated?<br />
8. Sample containers are intact?<br />
received on coc?<br />
10. All sample label information matches coc?<br />
11. Samples properly preserved?<br />
12. Samples received within hold t imes?<br />
Short holds taken to wet lab?<br />
13. VOA, TOC, TOX free <strong>of</strong> hesdspaee?<br />
14. QC stickers placed on bottles.designated by<br />
client?<br />
15. Shipment meets LvLI Sample Acceptance<br />
Policy? (Identify all bottles not with in<br />
policy. See reverse side for po licy)<br />
16. Proje ct Manager contacted concerning<br />
discrepancies? aame/date (or samples<br />
outside criteria)<br />
SR-0o2•B<br />
V^<br />
eX<br />
a Yes ONO ,p No<br />
/ Discrepaeties<br />
Airbill# ' 1 ge3 b'1-1 I ")-k<br />
Temp 1. 8 °C Cooler # EK4 - 63 • 41^17<br />
ee0eeoo66