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Lithium-ions uptake by MAX/graphene hybrid

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Abstract

Combining nanoparticles in well-designed architecture with complementary properties is an attractive strategy used for developing multi-functional, high-performance materials. Herein, to explore the mechanism of Li-ions uptake and storage potential of layered ternary carbides (MAX phases), we report on the Ti2SC and Ti3SiC2 with two-dimensional (2D)-reduced graphene oxide (rGO) that electrically connects MAX phase particles. The heterostructure formation was achieved through in-situ wet chemical processing. The method efficiently prevented restacking of rGO nanosheets, aggregation of MAX particles, and generated a porous heterostructure permeable for electrolyte. This facilitated the electrolyte transport and the access of ions to the electrode. In addition, there was a strong coupling effect between MAX phase compound and rGO in these hybrids. When tested as anodes for Li-ion batteries, the hybrids displayed high reversible capacity, very good rate performance, and excellent cycling stability. Specifically, the capacity of in-situ synthesized Ti2SC/rGO hybrid showed an increasing trend during cycling. After a few initial cycles, 576 mAh·g−1 was achieved after 500 charge/discharge cycles with a current of 400 mA·g−1. This work further demonstrates the Li-ion storage potential of MAX phases and suggests the need for further exploration of this large family of layered materials.

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Acknowledgements

J. Xu thanks the National Natural Science Foundation of China (No. 21671167), Starting fund for returned overseas Chinese scholars of Ministry of Education of China and the Joint Open Fund of Jiangsu Collaborative Innovation Center for Ecological Building Material and Environmental Protection Equipments and Key Laboratory for Advanced Technology in Environmental Protection of Jiangsu Province (No. JH201847). W. Yao thanks the National Natural Science Foundation of China (No. 51602277), the Natural Science Foundation of Jiangsu Province (No. BK20140473).

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  1. School of Materials Engineering, Yancheng Institute of Technology, 211 East Jianjun Road, Yancheng, 224051, Jiangsu, People’s Republic of China

    Jianguang Xu, Xiaoli Yao, Gan Sun, Yuchen Wang, Hong Yan & Wei Yao

  2. Key Laboratory for Advanced Technology in Environmental Protection of Jiangsu Province, Yancheng Institute of Technology, Yancheng, 224051, People’s Republic of China

    Jianguang Xu

  3. A.J. Drexel Nanomaterials Institute, and Materials Science and Engineering Department, Drexel University, 3141 Chestnut Street, Philadelphia, PA, 19104, USA

    Yury Gogotsi

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Xu, J., Yao, X., Sun, G. et al. Lithium-ions uptake by MAX/graphene hybrid. Graphene and 2D mater 7, 59–71 (2022). https://doi.org/10.1007/s41127-022-00048-w

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